Crystallography Open Database

Information card for entry 7702934

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Coordinates	7702934.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H23 Cl2 O P Ru
Calculated formula	C14 H23 Cl2 O P Ru
Title of publication	Half-sandwich ruthenium(ii) complexes with tethered arene-phosphinite ligands: synthesis, structure and application in catalytic cross dehydrogenative coupling reactions of silanes and alcohols.
Authors of publication	González-Fernández, Rebeca; Crochet, Pascale; Cadierno, Victorio
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2020
Journal volume	49
Journal issue	1
Pages of publication	210 - 222
a	8.8108 ± 0.0001 Å
b	13.2483 ± 0.0002 Å
c	27.2268 ± 0.0004 Å
α	90°
β	90°
γ	90°
Cell volume	3178.13 ± 0.08 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0294
Residual factor for significantly intense reflections	0.0262
Weighted residual factors for significantly intense reflections	0.0648
Weighted residual factors for all reflections included in the refinement	0.0673
Goodness-of-fit parameter for all reflections included in the refinement	1.044
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
247699 (current)	2020-02-04	cif/ Updating files of 7702933, 7702934, 7702935, 7702936 Original log message: Adding full bibliography for 7702933--7702936.cif.	7702934.cif
244872	2019-12-03	cif/ Adding structures of 7702933, 7702934, 7702935, 7702936 via cif-deposit CGI script.	7702934.cif