#------------------------------------------------------------------------------ #$Date: 2021-07-05 20:44:41 +0300 (Mon, 05 Jul 2021) $ #$Revision: 267197 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/73/7707364.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707364 loop_ _publ_author_name 'Masaryk, Luk\'a\ 2\s(I)' _cod_data_source_file d1dt00466b2.cif _cod_data_source_block IrOH _cod_depositor_comments 'Adding full bibliography for 7707364--7707367.cif.' _cod_original_cell_volume 1248.63(4) _cod_database_code 7707364 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL lm_2020_03_a.res in P-1 CELL 1.54184 8.0751 11.6201 14.4540 103.800 92.704 107.122 ZERR 2.00 0.0002 0.0002 0.0002 0.002 0.002 0.002 LATT 1 SFAC C H N O F P CL IR UNIT 44 54 4 4 12 2 2 2 MERG 2 MORE -1 FMAP 2 PLAN 2 ACTA BOND BOND $H CONF LIST 4 L.S. 22 WGHT 0.042700 0.684700 FVAR 0.48984 C9 1 0.453150 0.463382 0.745041 11.00000 0.06279 0.04956 = 0.05334 0.01745 0.02494 0.02442 AFIX 43 H9 2 0.369239 0.453683 0.786940 11.00000 -1.20000 AFIX 0 C10 1 0.532619 0.372126 0.719397 11.00000 0.06963 0.04201 = 0.06033 0.01888 0.01568 0.02296 AFIX 43 H10 2 0.503904 0.303208 0.744557 11.00000 -1.20000 AFIX 0 C11 1 0.654852 0.384516 0.656126 11.00000 0.05222 0.04248 = 0.04402 0.00387 0.00042 0.02237 C12 1 0.753710 0.291451 0.625025 11.00000 0.07088 0.05051 = 0.07487 0.01698 0.00810 0.03483 AFIX 23 H12A 2 0.752777 0.272800 0.555879 11.00000 -1.20000 H12B 2 0.874385 0.329142 0.654182 11.00000 -1.20000 AFIX 0 C13 1 0.692147 0.487223 0.619231 11.00000 0.04619 0.04440 = 0.04433 0.01132 0.01141 0.02537 AFIX 43 H13 2 0.773407 0.497159 0.575896 11.00000 -1.20000 AFIX 0 C14 1 0.607445 0.575495 0.647312 11.00000 0.03594 0.03916 = 0.03195 0.00439 0.00665 0.01546 C15 1 0.632864 0.684139 0.608442 11.00000 0.03560 0.03705 = 0.03468 0.00319 0.00737 0.01457 C16 1 0.742575 0.710144 0.540249 11.00000 0.04060 0.04590 = 0.04008 0.00797 0.01413 0.01717 AFIX 43 H16 2 0.811194 0.659750 0.519121 11.00000 -1.20000 AFIX 0 C17 1 0.750523 0.810700 0.503450 11.00000 0.05378 0.04929 = 0.03386 0.00965 0.01272 0.01468 C18 1 0.873916 0.838669 0.430582 11.00000 0.07429 0.06101 = 0.05285 0.01943 0.03178 0.02001 AFIX 23 H18A 2 0.993545 0.867724 0.461366 11.00000 -1.20000 H18B 2 0.858333 0.762963 0.380179 11.00000 -1.20000 AFIX 0 C19 1 0.648321 0.883906 0.537274 11.00000 0.08144 0.05057 = 0.05144 0.02227 0.02695 0.02988 AFIX 43 H19 2 0.650763 0.952416 0.514103 11.00000 -1.20000 AFIX 0 C20 1 0.542797 0.854654 0.605566 11.00000 0.06944 0.05279 = 0.05254 0.02022 0.02508 0.03806 AFIX 43 H20 2 0.473144 0.904132 0.627022 11.00000 -1.20000 AFIX 0 C21 1 0.394826 0.892585 0.836751 11.00000 0.05904 0.03362 = 0.04604 -0.00097 0.01705 0.01171 C22 1 0.217102 0.815528 0.815898 11.00000 0.04887 0.04848 = 0.04653 0.00064 0.02018 0.02036 C23 1 0.200916 0.710220 0.855006 11.00000 0.04610 0.04807 = 0.04035 -0.00415 0.02138 0.00825 C24 1 0.366582 0.724047 0.901126 11.00000 0.06179 0.05308 = 0.03032 0.00785 0.01332 0.01823 C25 1 0.491058 0.833241 0.886317 11.00000 0.04494 0.05622 = 0.03505 -0.00345 0.00872 0.00923 C26 1 0.680999 0.887332 0.925763 11.00000 0.05852 0.08054 = 0.05913 0.00133 0.00422 0.00680 AFIX 137 H26A 2 0.724495 0.821898 0.935118 11.00000 -1.50000 H26B 2 0.694859 0.948074 0.986085 11.00000 -1.50000 H26C 2 0.745163 0.926630 0.881323 11.00000 -1.50000 AFIX 0 C27 1 0.408789 0.641221 0.958113 11.00000 0.10685 0.07391 = 0.03921 0.02027 0.00990 0.02442 AFIX 137 H27A 2 0.320287 0.561020 0.939865 11.00000 -1.50000 H27B 2 0.412879 0.678530 1.025371 11.00000 -1.50000 H27C 2 0.520120 0.631287 0.945447 11.00000 -1.50000 AFIX 0 C28 1 0.032242 0.609097 0.853251 11.00000 0.05576 0.06602 = 0.06193 0.00376 0.02798 -0.00007 AFIX 137 H28A 2 -0.026522 0.575628 0.788776 11.00000 -1.50000 H28B 2 -0.041126 0.643549 0.894221 11.00000 -1.50000 H28C 2 0.057057 0.543778 0.875639 11.00000 -1.50000 AFIX 0 C29 1 0.069653 0.839890 0.766376 11.00000 0.06379 0.08942 = 0.08540 0.01227 0.01023 0.04851 AFIX 137 H29A 2 0.111769 0.882414 0.718646 11.00000 -1.50000 H29B 2 0.021176 0.890883 0.812503 11.00000 -1.50000 H29C 2 -0.018885 0.762052 0.736106 11.00000 -1.50000 AFIX 0 C30 1 0.470508 1.016790 0.815937 11.00000 0.09148 0.04644 = 0.07177 0.00771 0.02932 0.01884 AFIX 137 H30A 2 0.589635 1.028078 0.804407 11.00000 -1.50000 H30B 2 0.466243 1.082095 0.869937 11.00000 -1.50000 H30C 2 0.404061 1.019650 0.760153 11.00000 -1.50000 AFIX 0 N2 3 0.492274 0.565524 0.711864 11.00000 0.04950 0.03671 = 0.04133 0.01017 0.01449 0.02101 N1 3 0.535117 0.758308 0.642891 11.00000 0.04489 0.04754 = 0.03681 0.00968 0.01333 0.02339 O1 4 0.842574 0.930317 0.390284 11.00000 0.12957 0.08952 = 0.06829 0.04192 0.04860 0.04907 AFIX 147 H1 2 0.853105 0.913252 0.332910 11.00000 -1.50000 AFIX 0 O2 4 0.681814 0.179961 0.650796 11.00000 0.10021 0.05663 = 0.10447 0.02026 0.00001 0.03893 AFIX 147 H2 2 0.740518 0.180428 0.698829 11.00000 -1.50000 AFIX 0 F10 5 1.005161 0.142176 0.932234 11.00000 0.18511 0.11786 = 0.10707 0.07318 -0.02872 -0.03081 F11 5 1.206168 0.187906 0.835049 11.00000 0.08315 0.14093 = 0.16399 0.00490 0.00914 0.06116 F12 5 0.925186 0.106921 0.776032 11.00000 0.09494 0.07722 = 0.07469 0.00003 -0.00462 0.01688 F13 5 1.072193 0.305090 0.786198 11.00000 0.12711 0.09861 = 0.08036 0.04516 0.01583 0.02016 F14 5 0.871045 0.259050 0.881975 11.00000 0.08296 0.15161 = 0.15043 -0.00547 0.03904 0.05170 F15 5 1.152593 0.339816 0.943028 11.00000 0.11015 0.08869 = 0.07200 0.00234 0.00331 -0.00767 P4 6 1.038496 0.223769 0.861750 11.00000 0.05549 0.05604 = 0.04676 0.01354 0.00953 0.01436 CL1 7 0.158513 0.580459 0.614261 11.00000 0.04870 0.08439 = 0.04390 -0.00779 0.00451 0.02028 IR1 8 0.376533 0.707364 0.747318 11.00000 0.03861 0.03932 = 0.03342 0.00586 0.01179 0.01652 HKLF 4 REM lm_2020_03_a.res in P-1 REM R1 = 0.0312 for 4275 Fo > 4sig(Fo) and 0.0328 for all 4538 data REM 323 parameters refined using 0 restraints END WGHT 0.0426 0.6852 REM Highest difference peak 0.761, deepest hole -1.784, 1-sigma level 0.105 Q1 1 0.4680 0.7022 0.6926 11.00000 0.05 0.76 Q2 1 0.2898 0.7114 0.8024 11.00000 0.05 0.73 ; _shelx_res_checksum 35165 _shelx_hkl_file ; -9 -1 1 44.33 7.75 -9 -1 2 69.59 10.64 -9 -1 3 78.00 11.35 -9 -1 4 81.84 10.44 -9 0 0 149.65 14.54 -9 0 1 81.23 11.64 -9 0 1 74.10 7.50 -9 0 2 75.06 11.74 -9 0 2 76.77 7.64 -9 0 3 46.33 8.87 -9 0 4 90.23 11.22 -9 1 -2 92.15 9.05 -9 1 -1 242.07 18.37 -9 1 -1 226.33 15.33 -9 1 0 3.54 3.27 -9 1 0 5.21 2.65 -9 1 1 127.43 15.27 -9 1 1 127.83 10.89 -9 1 2 16.28 5.88 -9 1 3 159.35 16.34 -9 1 4 46.86 7.90 -9 2 -4 118.86 10.77 -9 2 -3 11.12 3.49 -9 2 -2 370.80 21.82 -9 2 -1 3.24 3.20 -9 2 -1 2.97 2.20 -9 2 0 266.17 21.44 -9 2 0 223.59 15.97 -9 2 1 3.94 3.37 -9 2 1 3.72 2.34 -9 2 2 105.45 13.57 -9 2 3 31.67 6.99 -9 2 4 317.49 21.60 -9 3 -5 171.12 13.50 -9 3 -4 3.25 2.55 -9 3 -3 286.63 19.34 -9 3 -2 13.23 3.99 -9 3 -1 114.41 13.21 -9 3 -1 117.94 11.49 -9 3 0 21.13 6.13 -9 3 0 16.90 4.42 -9 3 1 55.52 9.96 -9 3 1 73.89 8.89 -9 3 2 5.97 3.76 -9 3 3 336.96 23.02 -9 3 3 282.95 19.16 -9 3 4 -0.83 1.93 -9 3 5 319.58 20.97 -9 3 6 6.26 3.11 -9 3 7 79.20 9.39 -9 4 -5 0.83 1.94 -9 4 -4 152.70 13.80 -9 4 -3 27.03 5.65 -9 4 -2 146.74 13.36 -9 4 -1 12.90 4.05 -9 4 0 175.72 14.26 -9 4 0 151.75 13.66 -9 4 1 2.48 2.59 -9 4 1 4.23 2.94 -9 4 2 265.42 17.92 -9 4 2 238.91 17.70 -9 4 3 26.34 5.73 -9 4 4 245.90 18.16 -9 4 5 67.91 9.21 -9 4 6 116.54 12.01 -9 4 7 18.42 4.56 -9 5 -5 175.04 14.75 -9 5 -4 40.34 7.01 -9 5 -3 135.41 13.36 -9 5 -2 65.82 8.89 -9 5 -1 107.11 11.36 -9 5 -1 103.55 11.41 -9 5 0 60.63 8.30 -9 5 0 63.89 8.78 -9 5 1 174.99 14.91 -9 5 2 165.71 14.50 -9 5 3 268.83 19.15 -9 5 4 177.68 14.92 -9 5 5 128.38 12.41 -9 5 6 23.62 5.01 -9 6 -5 76.75 9.33 -9 6 -4 36.39 6.13 -9 6 -4 33.40 6.69 -9 6 -3 95.72 10.22 -9 6 -2 114.98 11.22 -9 6 -1 139.51 13.55 -9 6 0 162.22 14.52 -9 6 1 148.80 13.64 -9 6 2 87.84 10.17 -9 6 3 174.27 14.52 -9 6 4 25.07 5.22 -9 6 5 96.70 9.81 -9 7 -4 90.85 9.90 -9 7 -3 59.83 8.18 -9 7 -2 184.93 14.85 -9 7 0 206.73 16.38 -9 7 1 12.75 4.10 -9 7 2 249.21 17.48 -9 7 3 20.76 4.58 -9 7 4 203.52 14.34 -9 8 -4 6.35 2.89 -9 8 -3 192.52 15.12 -9 8 -2 19.37 4.67 -9 8 -1 363.90 21.82 -9 8 0 1.45 1.86 -9 8 1 193.24 14.02 -9 8 1 207.90 15.31 -8 -4 2 82.85 10.18 -8 -4 3 99.40 12.08 -8 -4 4 44.37 8.15 -8 -3 -2 47.43 6.83 -8 -3 0 123.92 12.45 -8 -3 1 90.60 11.95 -8 -3 2 63.87 11.42 -8 -3 3 58.89 11.53 -8 -3 4 16.32 6.04 -8 -3 5 87.07 11.58 -8 -2 -4 51.47 6.80 -8 -2 -3 26.33 5.66 -8 -2 -2 62.37 9.63 -8 -2 0 205.14 19.14 -8 -2 1 22.27 7.48 -8 -2 2 173.96 20.81 -8 -2 3 47.11 10.92 -8 -2 4 149.68 17.98 -8 -2 5 106.60 13.42 -8 -1 -5 50.17 6.97 -8 -1 -4 6.46 3.06 -8 -1 -3 155.45 15.69 -8 -1 -2 35.58 8.19 -8 -1 -1 364.16 26.11 -8 -1 0 28.76 8.14 -8 -1 1 233.87 23.91 -8 -1 2 11.51 6.37 -8 -1 3 185.07 21.38 -8 -1 4 13.89 5.62 -8 -1 5 298.61 23.49 -8 0 -5 10.15 3.76 -8 0 -4 152.98 15.25 -8 0 -3 13.08 4.96 -8 0 -2 251.34 22.49 -8 0 -1 4.26 4.21 -8 0 -1 1.72 2.21 -8 0 0 322.79 27.54 -8 0 1 46.60 10.73 -8 0 2 162.53 19.68 -8 0 3 6.67 4.94 -8 0 4 337.05 26.43 -8 0 5 6.07 3.82 -8 1 -5 153.06 14.95 -8 1 -4 17.92 4.88 -8 1 -4 23.51 6.51 -8 1 -3 376.07 23.89 -8 1 -3 378.84 27.73 -8 1 -2 44.57 9.38 -8 1 -2 45.38 7.54 -8 1 -2 36.98 8.54 -8 1 -1 394.77 29.59 -8 1 -1 390.33 24.47 -8 1 0 28.46 8.09 -8 1 1 250.15 24.28 -8 1 2 22.02 7.76 -8 1 3 232.49 22.32 -8 1 4 59.40 10.32 -8 2 -6 142.91 13.80 -8 2 -5 31.95 6.74 -8 2 -4 288.94 21.16 -8 2 -3 69.78 9.80 -8 2 -3 61.10 10.58 -8 2 -2 176.34 18.80 -8 2 -2 197.05 16.59 -8 2 -1 87.10 13.82 -8 2 -1 96.03 11.39 -8 2 0 237.00 23.23 -8 2 1 213.53 22.09 -8 2 2 153.60 18.09 -8 2 3 209.35 20.54 -8 2 4 250.93 21.71 -8 3 -8 58.11 7.50 -8 3 -7 47.73 7.84 -8 3 -6 60.00 9.43 -8 3 -5 110.56 13.04 -8 3 -4 233.50 19.35 -8 3 -3 184.10 16.70 -8 3 -2 295.01 25.17 -8 3 -2 328.01 22.69 -8 3 -1 143.41 17.63 -8 3 -1 162.37 15.15 -8 3 0 208.55 21.42 -8 3 0 185.67 16.70 -8 3 1 79.88 13.11 -8 3 1 68.48 10.11 -8 3 2 322.31 26.60 -8 3 2 293.30 22.08 -8 3 3 25.99 7.46 -8 3 4 274.98 22.65 -8 3 10 196.13 12.92 -8 4 -8 40.74 6.85 -8 4 -7 179.42 16.36 -8 4 -6 134.74 14.93 -8 4 -5 342.30 24.76 -8 4 -4 33.23 7.33 -8 4 -3 211.31 18.41 -8 4 -3 234.33 20.97 -8 4 -3 216.69 18.97 -8 4 -2 39.00 7.56 -8 4 -2 27.01 7.29 -8 4 -2 37.00 7.74 -8 4 -1 170.70 15.70 -8 4 -1 163.70 18.29 -8 4 -1 139.65 14.79 -8 4 0 105.44 15.12 -8 4 0 90.64 11.92 -8 4 1 280.88 24.96 -8 4 1 303.47 22.60 -8 4 2 62.83 11.06 -8 4 2 34.32 7.57 -8 4 3 519.70 33.94 -8 4 9 361.51 20.48 -8 5 -9 28.96 5.20 -8 5 -8 112.28 11.93 -8 5 -7 25.12 6.49 -8 5 -6 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64.63 0 2 -10 1466.07 63.07 0 2 -10 1473.42 62.56 0 2 -10 1500.59 63.29 0 2 -10 1540.93 63.19 0 2 -9 776.33 39.39 0 2 -9 658.01 34.88 0 2 -9 635.41 33.20 0 2 -9 709.60 34.06 0 2 -9 716.76 34.15 0 2 -9 699.43 33.61 0 2 -9 716.31 33.75 0 2 -8 2609.32 98.83 0 2 -8 2683.69 101.56 0 2 -8 2450.47 97.52 0 2 -7 702.18 33.25 0 2 -7 682.85 33.84 0 2 -7 661.22 31.39 0 2 -6 1006.74 43.63 0 2 -6 1074.77 44.03 0 2 -6 977.48 39.99 0 2 -6 970.02 40.94 0 2 -5 5.16 1.78 0 2 -5 7.01 2.53 0 2 -5 5.45 2.55 0 2 -5 10.02 2.32 0 2 -4 901.07 35.67 0 2 -4 928.19 35.91 0 2 -4 926.04 37.34 0 2 -4 964.84 39.22 0 2 -4 919.47 35.69 0 2 -3 1132.34 44.45 0 2 -3 1089.32 42.19 0 2 -3 1116.52 41.76 0 2 -3 1132.22 44.61 0 2 -3 1112.72 40.28 0 2 -3 1232.60 43.92 0 2 -2 3215.82 112.03 0 2 -2 3634.28 120.09 0 2 -2 3276.37 112.39 0 2 -2 3194.37 113.93 0 2 -2 3170.29 112.54 0 2 -2 3423.44 119.94 0 2 -1 4364.87 149.99 0 2 -1 4252.17 141.14 0 2 -1 4079.13 140.78 0 2 -1 4106.33 140.90 0 2 -1 4043.59 141.41 0 2 -1 4013.87 150.61 0 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0 3 -6 1309.67 53.44 0 3 -6 1408.61 57.35 0 3 -5 2565.66 94.46 0 3 -5 2606.74 96.69 0 3 -5 2521.30 92.89 0 3 -4 1690.78 61.92 0 3 -4 1600.29 63.88 0 3 -4 1572.00 63.65 0 3 -4 1643.39 61.46 0 3 -4 1736.15 63.69 0 3 -3 4826.65 164.85 0 3 -3 4686.29 167.01 0 3 -3 4778.73 165.69 0 3 -3 4791.81 172.09 0 3 -2 785.68 29.48 0 3 -2 723.92 28.95 0 3 -2 729.16 30.06 0 3 -1 345.16 15.47 0 3 -1 360.38 15.38 0 3 -1 359.94 15.67 0 3 -1 382.02 16.32 0 3 -1 400.67 24.35 0 3 0 589.14 24.16 0 3 0 622.93 31.52 0 3 0 549.36 22.28 0 3 1 1154.17 46.26 0 3 1 1296.67 51.71 0 3 2 1857.08 70.89 0 3 2 1899.99 71.73 0 3 3 1827.84 70.50 0 3 4 2170.77 83.37 0 3 5 2009.93 79.10 0 3 6 955.27 43.91 0 3 7 506.85 28.44 0 4 -17 77.76 8.12 0 4 -16 199.31 15.58 0 4 -16 194.45 15.16 0 4 -15 130.73 13.44 0 4 -15 148.20 14.14 0 4 -14 177.35 16.39 0 4 -14 155.47 15.67 0 4 -14 148.11 14.99 0 4 -13 284.03 21.74 0 4 -13 285.36 24.23 0 4 -13 293.52 21.90 0 4 -13 290.85 21.95 0 4 -13 270.06 22.98 0 4 -12 225.23 19.12 0 4 -12 250.02 20.13 0 4 -12 235.72 19.31 0 4 -12 283.51 22.51 0 4 -12 308.82 24.45 0 4 -11 1057.43 50.38 0 4 -11 1109.04 51.56 0 4 -11 1181.89 54.78 0 4 -11 1070.91 50.72 0 4 -11 1091.39 54.78 0 4 -11 993.08 56.29 0 4 -10 286.78 21.89 0 4 -10 259.77 18.50 0 4 -10 253.73 22.29 0 4 -10 252.77 18.33 0 4 -10 262.78 18.78 0 4 -10 233.41 19.37 0 4 -10 199.19 18.76 0 4 -9 1843.18 76.24 0 4 -9 1702.68 74.65 0 4 -9 1723.95 71.36 0 4 -9 1734.71 71.83 0 4 -9 1893.84 75.64 0 4 -9 1827.26 78.06 0 4 -9 1757.61 75.78 0 4 -8 1341.27 60.51 0 4 -8 1370.73 60.34 0 4 -7 285.59 19.35 0 4 -7 291.89 20.33 0 4 -7 293.81 18.19 0 4 -6 1436.96 60.29 0 4 -6 1412.19 57.24 0 4 -5 1474.21 57.55 0 4 -5 1325.72 57.13 0 4 -5 1399.34 55.38 0 4 -4 333.90 19.62 0 4 -4 325.77 18.10 0 4 -4 277.94 19.11 0 4 -3 2986.73 106.55 0 4 -3 2812.66 98.94 0 4 -3 2609.58 99.69 0 4 -3 2760.37 107.81 0 4 -2 483.70 20.99 0 4 -2 455.02 20.49 0 4 -2 515.47 29.89 0 4 -2 494.83 21.49 0 4 -1 1105.00 43.10 0 4 -1 1196.08 54.06 0 4 -1 1172.91 44.84 0 4 0 58.08 5.21 0 4 0 68.95 9.45 0 4 0 62.40 6.25 0 4 1 1229.40 52.86 0 4 1 1207.72 48.98 0 4 2 1510.63 60.43 0 4 3 794.39 37.03 0 4 4 152.02 13.04 0 4 5 1588.11 66.81 0 4 6 60.95 8.73 0 4 7 1087.25 51.45 0 5 -17 33.79 5.19 0 5 -16 165.68 13.91 0 5 -15 25.32 6.46 0 5 -15 17.78 4.89 0 5 -15 20.26 5.56 0 5 -15 13.57 4.46 0 5 -15 13.94 4.46 0 5 -14 482.41 30.08 0 5 -14 531.09 30.94 0 5 -14 505.99 32.32 0 5 -14 482.28 30.14 0 5 -14 511.72 33.68 0 5 -13 2.35 3.25 0 5 -13 11.03 5.21 0 5 -13 1.15 2.09 0 5 -13 5.86 3.88 0 5 -13 1.53 3.59 0 5 -12 254.04 20.36 0 5 -12 233.33 19.69 0 5 -12 292.40 23.44 0 5 -12 300.74 24.67 0 5 -12 264.58 20.72 0 5 -11 276.99 23.82 0 5 -11 294.38 22.76 0 5 -11 317.71 22.30 0 5 -11 291.09 21.65 0 5 -11 371.95 26.32 0 5 -11 326.53 24.66 0 5 -11 320.65 22.64 0 5 -10 438.46 29.66 0 5 -10 428.27 26.46 0 5 -10 458.59 28.58 0 5 -10 499.49 31.18 0 5 -10 466.41 27.23 0 5 -10 497.08 30.32 0 5 -10 437.19 26.84 0 5 -10 411.22 29.59 0 5 -10 447.12 26.06 0 5 -9 11.09 3.80 0 5 -9 7.62 4.00 0 5 -9 14.70 5.29 0 5 -9 1.06 2.50 0 5 -9 10.98 3.76 0 5 -9 11.03 3.61 0 5 -9 10.29 4.15 0 5 -9 14.73 4.94 0 5 -8 1516.37 62.30 0 5 -8 1572.40 65.60 0 5 -8 1545.69 62.58 0 5 -8 1503.06 66.42 0 5 -8 1522.76 67.88 0 5 -8 1464.07 61.32 0 5 -7 7.31 3.46 0 5 -6 3789.63 141.76 0 5 -5 134.63 11.76 0 5 -5 113.52 11.58 0 5 -4 1276.26 53.37 0 5 -4 1351.18 57.76 0 5 -3 53.97 9.01 0 5 -3 76.12 10.03 0 5 -3 84.07 7.16 0 5 -2 700.64 39.26 0 5 -2 670.31 29.82 0 5 -1 142.30 10.65 0 5 -1 121.58 13.80 0 5 -1 152.51 14.80 0 5 0 2409.02 90.95 0 5 0 2105.12 83.58 0 5 1 165.41 14.18 0 5 1 141.63 11.89 0 5 2 2762.95 105.17 0 5 3 110.75 11.44 0 5 4 3512.82 133.70 0 5 5 112.30 12.70 0 5 6 1572.05 69.95 0 5 7 12.51 4.37 0 5 12 401.95 24.29 0 6 -16 9.25 3.43 0 6 -15 173.18 15.10 0 6 -15 156.11 15.55 0 6 -15 182.97 17.26 0 6 -15 173.62 15.11 0 6 -14 4.34 3.01 0 6 -14 7.12 4.22 0 6 -14 5.12 3.79 0 6 -14 6.50 3.59 0 6 -14 3.29 2.81 0 6 -13 578.04 33.99 0 6 -13 543.92 33.36 0 6 -13 590.54 36.31 0 6 -13 636.96 38.73 0 6 -13 570.04 33.83 0 6 -12 3.49 2.99 0 6 -12 7.01 4.64 0 6 -12 1.16 2.44 0 6 -12 1.54 2.80 0 6 -12 3.48 3.22 0 6 -12 3.02 4.47 0 6 -12 2.65 3.92 0 6 -11 523.59 31.56 0 6 -11 505.14 31.21 0 6 -11 602.80 36.97 0 6 -11 541.30 34.16 0 6 -11 500.60 29.85 0 6 -11 581.86 35.77 0 6 -11 528.10 31.72 0 6 -11 536.19 33.50 0 6 -10 61.02 9.17 0 6 -10 74.18 10.91 0 6 -10 56.92 10.48 0 6 -10 63.35 9.34 0 6 -10 71.73 9.30 0 6 -10 62.63 10.67 0 6 -10 66.23 10.28 0 6 -9 1242.88 56.08 0 6 -9 1230.53 56.13 0 6 -9 1352.75 63.07 0 6 -9 1351.76 60.02 0 6 -9 1228.35 55.06 0 6 -9 1240.98 62.24 0 6 -9 1299.31 60.75 0 6 -9 1333.63 60.63 0 6 -8 369.09 24.95 0 6 -8 395.73 26.80 0 6 -8 409.83 26.92 0 6 -8 395.52 25.51 0 6 -8 425.45 24.12 0 6 -8 396.81 28.24 0 6 -8 416.19 24.15 0 6 -8 402.68 28.03 0 6 -8 378.87 22.81 0 6 -7 814.29 40.34 0 6 -7 792.09 41.02 0 6 -7 858.69 44.61 0 6 -7 833.04 38.30 0 6 -7 804.52 39.93 0 6 -7 803.67 42.72 0 6 -7 808.58 37.59 0 6 -7 820.08 37.31 0 6 -7 872.70 42.64 0 6 -6 150.00 14.16 0 6 -5 652.33 36.02 0 6 -5 648.73 33.11 0 6 -4 142.08 14.79 0 6 -3 883.98 46.00 0 6 -2 52.59 9.25 0 6 -1 2383.37 95.47 0 6 -1 2206.65 87.10 0 6 0 1.12 3.11 0 6 0 1.60 1.87 0 6 1 2915.29 111.75 0 6 2 3.96 2.74 0 6 2 3.33 3.02 0 6 3 910.19 43.69 0 6 3 1022.87 48.36 0 6 3 1009.58 46.06 0 6 4 180.26 16.99 0 6 4 174.92 15.40 0 6 5 752.10 41.71 0 6 5 752.12 38.57 0 6 6 198.47 19.04 0 6 7 762.41 43.45 0 6 10 24.20 6.15 0 6 11 377.84 23.85 0 6 12 10.84 3.40 0 7 -16 144.93 11.77 0 7 -15 -1.13 3.12 0 7 -15 -1.01 2.80 0 7 -15 5.26 3.18 0 7 -14 386.56 27.96 0 7 -14 388.13 27.04 0 7 -14 406.57 28.49 0 7 -14 383.29 26.47 0 7 -14 436.53 26.48 0 7 -13 16.19 5.99 0 7 -13 13.14 5.17 0 7 -13 9.35 4.67 0 7 -13 26.18 7.58 0 7 -13 21.59 5.73 0 7 -12 376.94 25.44 0 7 -12 351.77 27.58 0 7 -12 392.42 29.85 0 7 -12 321.24 25.95 0 7 -12 364.80 24.11 0 7 -12 389.30 27.92 0 7 -12 341.89 24.67 0 7 -11 42.67 8.08 0 7 -11 43.77 9.04 0 7 -11 39.55 9.38 0 7 -11 34.87 7.28 0 7 -11 44.36 7.60 0 7 -11 23.63 7.20 0 7 -11 50.71 9.53 0 7 -10 323.45 22.47 0 7 -10 298.95 25.89 0 7 -10 294.14 23.52 0 7 -10 296.81 21.29 0 7 -10 313.17 25.08 0 7 -10 357.69 26.17 0 7 -9 27.41 6.67 0 7 -9 27.73 7.79 0 7 -9 22.84 6.81 0 7 -9 41.74 8.51 0 7 -9 24.48 6.48 0 7 -9 32.82 6.51 0 7 -8 770.38 41.39 0 7 -8 825.02 45.78 0 7 -8 800.01 41.27 0 7 -8 851.87 44.18 0 7 -8 689.94 40.71 0 7 -8 808.44 38.80 0 7 -7 216.59 18.02 0 7 -7 207.90 19.70 0 7 -7 178.39 15.91 0 7 -7 216.99 18.52 0 7 -7 190.10 17.79 0 7 -7 190.42 14.70 0 7 -6 2315.51 90.47 0 7 -6 2233.28 86.32 0 7 -6 2127.41 89.54 0 7 -6 2228.61 94.68 0 7 -6 2228.10 92.97 0 7 -5 119.11 10.84 0 7 -5 134.31 15.44 0 7 -5 133.93 12.58 0 7 -5 102.35 11.16 0 7 -5 112.43 13.23 0 7 -4 1293.86 51.69 0 7 -4 1228.12 52.98 0 7 -4 1382.35 62.83 0 7 -4 1273.90 57.43 0 7 -3 150.54 12.80 0 7 -3 162.33 14.91 0 7 -3 200.70 19.49 0 7 -3 153.04 13.15 0 7 -2 1112.63 49.34 0 7 -2 1055.59 48.74 0 7 -2 1188.72 57.81 0 7 -1 5.17 2.86 0 7 -1 1.39 2.92 0 7 -1 0.85 1.53 0 7 0 1962.50 78.06 0 7 0 1740.25 77.42 0 7 0 2069.70 84.07 0 7 0 1863.34 77.10 0 7 1 223.99 17.62 0 7 1 208.69 17.70 0 7 1 196.25 16.43 0 7 2 1263.41 61.19 0 7 2 1260.43 58.77 0 7 2 1426.74 60.83 0 7 2 1413.81 59.74 0 7 3 263.84 22.09 0 7 3 246.30 19.39 0 7 3 312.12 21.88 0 7 3 308.50 21.59 0 7 4 707.82 40.82 0 7 4 639.47 35.82 0 7 4 684.09 37.59 0 7 4 763.92 39.16 0 7 5 66.71 10.39 0 7 5 55.27 9.20 0 7 5 52.68 9.88 0 7 6 579.69 34.87 0 7 7 77.79 11.28 0 7 8 451.94 29.36 0 7 9 58.51 9.22 0 7 10 215.67 16.97 0 7 11 53.80 7.22 0 8 -16 1.13 1.44 0 8 -15 162.91 13.31 0 8 -15 157.44 14.61 0 8 -14 32.69 7.46 0 8 -14 27.42 5.86 0 8 -13 238.41 21.40 0 8 -13 264.54 23.35 0 8 -13 223.22 19.93 0 8 -13 249.52 19.42 0 8 -13 250.87 21.16 0 8 -12 105.31 14.31 0 8 -12 104.16 15.11 0 8 -12 107.69 13.79 0 8 -12 107.00 14.04 0 8 -12 103.50 12.41 0 8 -11 216.45 21.17 0 8 -11 237.82 23.28 0 8 -11 199.02 19.33 0 8 -11 265.97 23.00 0 8 -10 21.61 6.22 0 8 -10 20.90 6.86 0 8 -10 29.55 7.03 0 8 -10 23.86 7.82 0 8 -9 869.32 48.50 0 8 -9 854.32 46.58 0 8 -9 973.77 50.96 0 8 -9 953.18 48.96 0 8 -8 109.08 13.46 0 8 -8 80.22 10.10 0 8 -8 136.10 15.63 0 8 -8 101.96 13.57 0 8 -8 117.23 15.39 0 8 -8 103.11 12.40 0 8 -7 1066.71 51.14 0 8 -7 955.93 45.56 0 8 -7 1030.73 52.73 0 8 -7 969.39 49.70 0 8 -6 98.97 12.15 0 8 -6 80.37 9.48 0 8 -6 60.40 10.81 0 8 -6 98.09 14.38 0 8 -5 386.50 25.03 0 8 -5 365.88 22.56 0 8 -5 367.07 27.01 0 8 -5 389.17 30.55 0 8 -4 279.86 20.39 0 8 -4 304.38 23.26 0 8 -4 309.88 19.78 0 8 -4 327.06 27.68 0 8 -3 718.28 44.40 0 8 -3 670.85 36.42 0 8 -2 457.55 34.05 0 8 -2 466.04 28.76 0 8 -2 492.15 28.73 0 8 -1 1785.78 81.26 0 8 -1 1632.51 73.31 0 8 -1 1776.66 74.14 0 8 0 413.06 27.26 0 8 0 417.75 27.07 0 8 1 825.67 42.96 0 8 1 793.67 42.25 0 8 2 181.71 16.91 0 8 2 136.22 15.94 0 8 2 176.83 16.69 0 8 3 295.80 22.00 0 8 3 282.10 21.66 0 8 3 257.70 22.93 0 8 3 273.03 21.70 0 8 4 196.65 17.31 0 8 4 172.16 16.77 0 8 4 165.18 16.68 0 8 5 353.33 25.68 0 8 5 391.12 26.38 0 8 6 257.85 20.80 0 8 7 514.73 31.07 0 8 8 231.44 18.46 0 8 9 199.49 15.85 0 8 10 35.53 5.77 0 9 -15 61.60 7.18 0 9 -14 155.57 13.49 0 9 -14 174.87 15.46 0 9 -13 42.94 7.34 0 9 -13 41.39 8.05 0 9 -12 203.47 20.94 0 9 -12 220.23 18.11 0 9 -12 244.79 20.73 0 9 -11 118.43 16.02 0 9 -11 102.99 14.05 0 9 -10 306.00 26.37 0 9 -10 285.59 24.15 0 9 -10 312.75 25.92 0 9 -10 250.95 22.37 0 9 -9 261.21 24.10 0 9 -9 252.71 23.61 0 9 -9 196.66 20.31 0 9 -9 267.32 22.71 0 9 -8 475.86 33.11 0 9 -8 472.41 27.97 0 9 -7 334.77 26.81 0 9 -7 336.91 22.41 0 9 -6 512.80 35.13 0 9 -6 554.19 39.40 0 9 -6 559.35 30.68 0 9 -5 371.64 27.75 0 9 -5 375.53 23.59 0 9 -5 373.74 31.92 0 9 -4 313.45 20.91 0 9 -4 288.23 28.19 0 9 -3 205.80 18.04 0 9 -3 218.20 19.26 0 9 -3 252.85 25.82 0 9 -2 288.77 21.62 0 9 -2 262.70 21.60 0 9 -2 230.41 24.63 0 9 -1 385.85 26.71 0 9 -1 379.27 27.09 0 9 -1 413.88 32.19 0 9 0 286.96 23.05 0 9 0 265.98 21.88 0 9 1 747.01 42.21 0 9 1 765.66 42.08 0 9 2 172.41 17.38 0 9 2 170.83 17.46 0 9 3 317.12 24.39 0 9 3 353.00 25.53 0 9 4 173.10 16.80 0 9 4 194.29 17.92 0 9 4 184.09 17.15 0 9 5 235.22 19.50 0 9 5 222.84 18.87 0 9 6 103.65 12.11 0 9 7 185.25 15.58 0 9 8 49.71 7.19 0 9 9 87.45 8.51 0 10 -14 60.25 7.21 0 10 -13 29.53 5.57 0 10 -12 142.19 13.39 0 10 -11 127.10 15.39 0 10 -11 109.56 13.95 0 10 -10 343.55 26.97 0 10 -10 306.22 25.55 0 10 -10 316.79 24.29 0 10 -9 109.91 15.19 0 10 -9 110.90 14.56 0 10 -8 344.47 27.43 0 10 -7 83.73 10.31 0 10 -7 55.73 10.76 0 10 -6 89.73 10.72 0 10 -6 70.80 11.80 0 10 -5 87.68 10.64 0 10 -5 81.86 12.43 0 10 -4 384.91 24.39 0 10 -3 48.08 7.82 0 10 -3 53.10 9.81 0 10 -3 40.43 8.03 0 10 -2 1274.93 56.17 0 10 -2 1283.70 61.29 0 10 -2 1211.88 59.02 0 10 -1 79.33 12.25 0 10 -1 95.35 12.61 0 10 0 582.52 36.04 0 10 0 533.13 33.67 0 10 1 27.01 7.53 0 10 1 24.26 6.74 0 10 2 56.46 10.16 0 10 2 61.03 9.87 0 10 3 173.36 16.80 0 10 3 174.01 16.76 0 10 4 125.45 13.70 0 10 4 171.89 15.69 0 10 5 78.48 9.79 0 10 6 229.62 16.49 0 10 7 13.97 3.49 0 11 -13 63.58 7.17 0 11 -12 35.55 5.81 0 11 -11 131.36 14.03 0 11 -11 148.37 12.93 0 11 -10 20.31 6.27 0 11 -9 198.75 19.60 0 11 -8 18.24 6.78 0 11 -7 180.68 18.23 0 11 -7 222.12 21.86 0 11 -7 184.01 15.48 0 11 -6 50.13 9.38 0 11 -6 71.00 9.22 0 11 -5 283.64 19.81 0 11 -4 62.98 8.70 0 11 -3 224.42 20.05 0 11 -3 253.33 18.34 0 11 -3 253.50 20.07 0 11 -2 4.66 3.23 0 11 -2 -1.27 3.25 0 11 -1 201.14 18.28 0 11 -1 249.46 20.86 0 11 0 11.59 4.86 0 11 0 7.45 4.51 0 11 1 119.42 13.52 0 11 1 142.09 14.98 0 11 2 45.65 8.06 0 11 2 45.97 8.06 0 11 3 136.99 13.27 0 11 3 137.58 13.58 0 11 4 72.85 8.76 0 11 4 49.70 7.36 0 11 5 282.69 17.26 0 12 -11 5.59 2.90 0 12 -11 5.34 2.41 0 12 -10 165.45 15.02 0 12 -9 7.64 3.97 0 12 -8 167.23 16.55 0 12 -7 3.79 2.96 0 12 -6 138.19 15.56 0 12 -6 145.18 12.33 0 12 -5 6.37 3.78 0 12 -5 3.71 2.33 0 12 -2 281.06 20.87 0 12 -2 301.91 20.74 0 12 -1 1.98 2.93 0 12 -1 2.80 2.77 0 12 0 202.48 16.71 0 12 0 199.86 15.85 0 12 1 3.38 2.51 0 12 1 2.45 2.09 0 12 2 115.89 11.16 0 12 2 133.48 11.44 0 12 3 0.58 1.73 0 12 3 -0.59 1.75 0 13 -8 17.09 4.34 0 13 -7 131.84 12.14 1 -13 2 22.63 5.25 1 -13 3 207.95 17.00 1 -13 4 31.81 6.71 1 -12 1 177.00 16.80 1 -11 -6 83.26 8.13 1 -10 -8 34.63 4.98 1 -10 -7 238.37 16.17 1 -9 -9 13.36 3.42 1 -9 -8 413.77 24.11 1 -8 -11 202.58 12.86 1 -8 -10 1.39 1.78 1 -8 -9 386.36 23.63 1 -8 -9 412.07 24.35 1 -8 -8 25.42 5.99 1 -7 -12 182.04 12.25 1 -7 -11 16.69 4.20 1 -7 -10 435.75 25.99 1 -7 -10 472.88 26.59 1 -7 -9 114.09 12.56 1 -7 -9 120.22 13.88 1 -6 -13 224.58 14.00 1 -6 -12 44.48 6.56 1 -6 -11 443.36 26.43 1 -6 -11 481.13 26.88 1 -6 -10 251.57 18.98 1 -6 -10 225.60 18.19 1 -6 -10 230.63 19.96 1 -6 -9 316.63 22.26 1 -6 -9 278.11 22.55 1 -6 -8 454.04 29.47 1 -6 -7 160.66 19.50 1 -6 -7 228.00 18.40 1 -6 -4 690.61 38.42 1 -6 -3 1602.05 70.34 1 -6 -2 1544.67 67.78 1 -5 -14 167.31 11.49 1 -5 -13 147.81 12.19 1 -5 -12 353.56 22.46 1 -5 -12 367.36 22.53 1 -5 -11 604.32 33.11 1 -5 -11 616.99 33.22 1 -5 -11 572.48 34.90 1 -5 -10 228.20 18.31 1 -5 -10 223.17 18.33 1 -5 -10 225.22 20.16 1 -5 -9 639.10 36.30 1 -5 -9 577.84 33.53 1 -5 -8 447.24 28.88 1 -5 -8 483.33 34.60 1 -5 -7 275.49 20.68 1 -5 -6 1029.60 48.31 1 -5 -5 379.05 22.64 1 -5 -4 1098.27 51.83 1 -5 -3 3144.52 121.38 1 -5 -2 651.88 34.65 1 -5 -1 1426.91 61.66 1 -4 -14 198.26 14.14 1 -4 -13 217.31 16.24 1 -4 -13 225.65 16.66 1 -4 -12 841.91 41.44 1 -4 -12 881.19 41.64 1 -4 -12 743.83 42.14 1 -4 -11 70.60 9.66 1 -4 -11 58.79 8.98 1 -4 -11 60.01 9.85 1 -4 -10 508.10 30.10 1 -4 -10 514.76 30.36 1 -4 -10 506.95 31.90 1 -4 -9 94.00 12.00 1 -4 -9 78.96 10.24 1 -4 -8 851.88 42.61 1 -4 -8 799.22 40.02 1 -4 -8 822.85 46.74 1 -4 -7 264.52 19.33 1 -4 -7 350.26 22.50 1 -4 -6 3105.53 116.67 1 -4 -5 554.48 27.80 1 -4 -4 3774.42 140.82 1 -4 -3 5.04 2.64 1 -4 -2 1813.02 73.36 1 -4 -1 225.97 15.95 1 -4 0 1593.85 63.20 1 -3 -15 209.53 14.04 1 -3 -14 36.93 6.16 1 -3 -14 37.71 6.46 1 -3 -13 375.38 24.18 1 -3 -13 405.41 24.75 1 -3 -12 1.03 1.88 1 -3 -12 -1.04 2.17 1 -3 -12 -1.21 3.09 1 -3 -11 821.21 41.67 1 -3 -11 811.39 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655.20 31.89 1 3 2 1637.48 67.48 1 3 6 2495.08 98.78 1 3 7 2.10 2.69 1 3 8 954.33 47.76 1 4 -17 130.94 10.67 1 4 -16 7.77 3.06 1 4 -16 9.04 3.92 1 4 -16 13.22 4.07 1 4 -15 287.05 20.73 1 4 -15 300.16 21.39 1 4 -15 320.65 23.04 1 4 -14 17.06 6.16 1 4 -14 17.82 5.37 1 4 -14 18.02 6.05 1 4 -14 16.85 5.42 1 4 -14 12.76 4.62 1 4 -13 1192.42 54.77 1 4 -13 1217.31 57.14 1 4 -13 1007.06 51.66 1 4 -13 1121.33 53.63 1 4 -13 1086.07 57.20 1 4 -12 18.25 5.44 1 4 -12 24.98 7.09 1 4 -12 24.85 7.02 1 4 -12 15.91 5.24 1 4 -12 31.41 6.89 1 4 -11 515.41 30.68 1 4 -11 538.15 31.28 1 4 -11 571.71 33.73 1 4 -11 553.08 30.90 1 4 -11 505.29 33.58 1 4 -10 78.38 9.83 1 4 -10 76.57 9.76 1 4 -10 79.64 9.69 1 4 -10 83.09 10.72 1 4 -10 77.32 11.59 1 4 -9 913.83 41.80 1 4 -9 894.24 45.09 1 4 -9 873.59 41.28 1 4 -9 935.54 41.60 1 4 -9 842.99 42.34 1 4 -9 841.79 43.48 1 4 -9 863.81 45.79 1 4 -8 494.17 26.13 1 4 -8 495.86 27.67 1 4 -8 463.67 28.82 1 4 -8 535.08 31.86 1 4 -7 4374.08 158.70 1 4 -6 47.40 6.51 1 4 -5 5174.68 189.97 1 4 -5 5048.30 180.83 1 4 -4 147.71 13.44 1 4 -4 159.74 11.09 1 4 -4 139.50 15.53 1 4 -4 155.33 11.33 1 4 -3 2066.80 85.09 1 4 -3 2095.88 76.96 1 4 -3 1994.28 88.18 1 4 -3 2046.58 77.45 1 4 -2 106.87 12.88 1 4 -2 127.07 9.17 1 4 -2 124.11 14.79 1 4 -1 1760.05 80.52 1 4 -1 1960.52 71.09 1 4 -1 1861.65 82.14 1 4 0 5.94 3.95 1 4 0 7.75 4.35 1 4 0 12.42 3.17 1 4 1 3739.13 146.87 1 4 1 3916.21 139.99 1 4 1 3919.32 145.08 1 4 2 220.86 15.42 1 4 3 4206.46 154.17 1 4 4 115.74 11.89 1 4 5 713.03 35.48 1 4 5 750.29 38.26 1 4 6 36.55 7.25 1 4 7 351.30 25.11 1 4 8 44.81 8.50 1 5 -17 0.61 1.92 1 5 -16 226.41 16.48 1 5 -16 216.73 15.42 1 5 -16 199.25 16.25 1 5 -15 14.61 4.46 1 5 -15 10.92 3.95 1 5 -15 11.20 4.41 1 5 -15 14.80 4.75 1 5 -14 507.88 31.33 1 5 -14 538.80 31.44 1 5 -14 583.20 33.19 1 5 -14 573.77 34.47 1 5 -14 549.69 35.41 1 5 -13 292.16 22.27 1 5 -13 291.85 22.71 1 5 -13 335.19 25.13 1 5 -13 296.65 21.86 1 5 -13 289.39 24.94 1 5 -12 564.06 33.36 1 5 -12 621.75 37.84 1 5 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1880.27 74.70 1 5 1 227.87 19.74 1 5 1 243.18 16.72 1 5 2 690.60 35.05 1 5 3 265.52 18.12 1 5 3 242.43 18.62 1 5 4 157.21 13.65 1 5 4 125.24 13.53 1 5 5 784.63 38.57 1 5 5 709.60 39.83 1 5 6 1196.32 54.30 1 5 6 1172.90 57.18 1 5 7 397.55 28.26 1 5 12 87.57 9.99 1 5 13 37.05 5.46 1 6 -16 61.53 8.24 1 6 -15 199.34 17.12 1 6 -15 187.63 15.65 1 6 -14 220.55 18.58 1 6 -14 227.81 18.02 1 6 -14 233.78 20.12 1 6 -14 215.25 20.34 1 6 -14 253.69 19.55 1 6 -13 300.87 24.68 1 6 -13 267.54 21.40 1 6 -13 237.36 19.52 1 6 -13 286.31 23.08 1 6 -13 242.28 22.37 1 6 -13 277.16 21.29 1 6 -12 227.51 21.69 1 6 -12 188.95 17.43 1 6 -12 181.99 18.18 1 6 -12 193.05 16.69 1 6 -12 174.23 18.75 1 6 -12 180.82 16.93 1 6 -12 149.50 16.85 1 6 -11 35.74 7.13 1 6 -11 37.94 8.18 1 6 -11 40.51 9.36 1 6 -11 29.70 6.95 1 6 -11 25.87 6.43 1 6 -11 32.70 7.86 1 6 -11 29.03 7.46 1 6 -10 13.06 5.70 1 6 -10 18.15 5.68 1 6 -10 12.77 4.14 1 6 -10 13.38 4.95 1 6 -10 9.52 4.17 1 6 -9 598.80 32.72 1 6 -9 582.91 31.84 1 6 -9 629.53 34.56 1 6 -9 552.21 35.88 1 6 -9 590.75 36.93 1 6 -9 627.47 37.52 1 6 -8 1242.27 60.66 1 6 -8 1114.66 57.40 1 6 -8 1526.88 64.22 1 6 -8 1103.89 57.45 1 6 -8 1349.03 56.07 1 6 -8 1319.87 57.28 1 6 -7 1548.74 69.08 1 6 -7 1590.39 68.93 1 6 -7 1632.48 64.12 1 6 -7 1547.49 69.75 1 6 -7 1599.69 65.23 1 6 -7 1493.91 69.45 1 6 -7 1507.89 65.38 1 6 -6 828.71 41.30 1 6 -6 779.61 40.31 1 6 -6 813.82 36.57 1 6 -6 752.77 37.76 1 6 -6 755.51 40.03 1 6 -6 840.35 43.77 1 6 -5 433.10 30.71 1 6 -5 368.87 27.01 1 6 -5 397.65 24.24 1 6 -5 379.24 22.78 1 6 -5 377.35 27.15 1 6 -4 180.01 19.54 1 6 -4 163.51 17.83 1 6 -3 272.20 24.32 1 6 -3 211.55 21.31 1 6 -2 272.57 24.47 1 6 -2 259.50 23.74 1 6 -1 1058.69 55.76 1 6 -1 1031.50 54.90 1 6 0 1294.56 62.16 1 6 0 1196.96 59.75 1 6 1 1427.87 58.37 1 6 1 1388.48 59.08 1 6 2 1715.06 68.93 1 6 2 1498.72 68.06 1 6 2 1644.97 69.97 1 6 3 742.85 38.11 1 6 3 740.03 39.95 1 6 4 159.39 15.06 1 6 4 176.20 16.97 1 6 5 407.89 26.03 1 6 5 354.82 26.65 1 6 6 309.96 22.35 1 6 6 306.11 24.53 1 6 11 58.75 8.13 1 6 12 66.64 7.52 1 7 -16 57.40 7.51 1 7 -15 82.07 10.33 1 7 -15 95.01 10.27 1 7 -14 100.89 13.03 1 7 -14 87.80 11.65 1 7 -14 95.85 12.59 1 7 -14 97.60 11.34 1 7 -13 222.82 20.86 1 7 -13 183.38 17.99 1 7 -13 161.54 17.80 1 7 -13 178.32 16.48 1 7 -12 216.25 21.49 1 7 -12 174.51 17.76 1 7 -12 164.39 18.40 1 7 -12 165.40 17.75 1 7 -12 181.57 16.96 1 7 -11 408.64 30.36 1 7 -11 339.16 25.50 1 7 -11 317.54 26.22 1 7 -11 311.16 25.64 1 7 -11 336.64 24.20 1 7 -10 144.99 17.59 1 7 -10 107.00 13.53 1 7 -10 133.36 16.44 1 7 -10 126.17 15.72 1 7 -10 118.47 15.14 1 7 -9 178.91 19.52 1 7 -9 175.60 18.45 1 7 -9 153.58 17.74 1 7 -9 153.87 16.45 1 7 -8 605.34 36.99 1 7 -8 663.21 39.26 1 7 -8 549.90 35.45 1 7 -7 495.12 29.39 1 7 -7 474.71 30.90 1 7 -7 504.80 27.47 1 7 -7 476.87 32.22 1 7 -6 227.00 21.28 1 7 -6 293.91 18.53 1 7 -6 240.57 18.97 1 7 -5 614.28 33.39 1 7 -5 641.96 38.00 1 7 -4 200.56 18.43 1 7 -4 220.33 22.31 1 7 -4 194.98 15.92 1 7 -4 204.56 17.02 1 7 -3 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9.11 1 8 -9 40.55 9.10 1 8 -8 1077.74 55.37 1 8 -8 880.24 50.77 1 8 -8 1085.80 55.10 1 8 -8 946.51 51.08 1 8 -7 161.96 17.70 1 8 -7 129.52 12.67 1 8 -6 569.38 34.44 1 8 -6 648.94 39.12 1 8 -6 634.07 32.52 1 8 -5 381.87 28.03 1 8 -5 381.37 25.67 1 8 -4 259.07 20.80 1 8 -4 242.00 20.80 1 8 -4 276.23 20.44 1 8 -3 90.50 11.19 1 8 -3 107.53 13.02 1 8 -2 602.31 35.36 1 8 -1 27.67 6.65 1 8 -1 23.80 6.48 1 8 0 992.67 48.00 1 8 0 913.96 49.26 1 8 1 4.65 3.85 1 8 1 7.96 4.61 1 8 2 964.67 47.32 1 8 2 840.50 46.95 1 8 3 41.11 8.27 1 8 3 26.28 6.64 1 8 4 581.21 34.53 1 8 5 7.84 3.53 1 8 5 12.70 4.53 1 8 6 567.12 32.28 1 8 6 526.91 31.34 1 8 7 5.86 3.54 1 8 7 3.80 2.64 1 8 8 248.47 17.71 1 8 9 1.40 1.79 1 9 -15 73.65 7.45 1 9 -14 3.67 2.31 1 9 -13 213.88 16.51 1 9 -13 208.29 18.80 1 9 -12 9.87 4.02 1 9 -12 15.39 5.87 1 9 -11 335.12 27.04 1 9 -11 391.35 25.21 1 9 -11 405.34 29.51 1 9 -10 1.55 3.25 1 9 -10 1.57 3.67 1 9 -9 424.88 30.65 1 9 -9 372.10 29.73 1 9 -8 44.90 10.12 1 9 -7 527.19 29.96 1 9 -7 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408.95 26.65 2 -6 -10 448.64 28.88 2 -6 -9 50.14 9.34 2 -6 -8 461.38 30.29 2 -6 -7 119.41 13.46 2 -6 -7 92.85 14.57 2 -6 -6 754.27 39.71 2 -6 -6 746.32 45.88 2 -6 -5 5.04 3.94 2 -6 -4 1467.74 72.53 2 -6 -3 1.67 3.02 2 -5 -14 1.10 1.41 2 -5 -13 192.11 14.63 2 -5 -12 49.33 7.71 2 -5 -12 43.69 7.96 2 -5 -11 598.18 35.27 2 -5 -11 636.63 34.59 2 -5 -10 1.13 2.89 2 -5 -10 1.24 2.60 2 -5 -9 884.59 46.62 2 -5 -8 43.62 7.95 2 -5 -8 54.81 11.02 2 -5 -7 1949.88 82.90 2 -5 -7 2082.46 82.79 2 -5 -7 1954.64 90.15 2 -5 -6 97.34 11.26 2 -5 -6 99.75 14.50 2 -5 -6 106.49 11.38 2 -5 -5 1632.95 76.39 2 -5 -4 19.11 6.38 2 -5 -3 1730.62 78.86 2 -5 -2 12.18 4.97 2 -5 -2 19.71 4.98 2 -5 -1 3203.10 122.36 2 -5 4 159.64 14.47 2 -4 -14 339.91 20.22 2 -4 -13 34.73 6.44 2 -4 -13 39.61 7.51 2 -4 -12 655.29 37.03 2 -4 -12 700.57 36.66 2 -4 -11 27.53 6.39 2 -4 -11 29.97 6.94 2 -4 -10 884.42 44.36 2 -4 -10 910.60 46.42 2 -4 -10 813.00 43.25 2 -4 -9 10.36 4.01 2 -4 -9 6.07 3.36 2 -4 -9 8.79 4.37 2 -4 -9 6.65 4.61 2 -4 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0 2 3926.14 138.44 2 0 4 3.60 2.53 2 0 5 4060.16 146.45 2 0 6 153.40 12.56 2 0 7 1837.97 74.60 2 0 8 -0.92 1.37 2 1 -17 9.04 2.69 2 1 -16 334.17 20.57 2 1 -15 1.89 2.80 2 1 -15 0.98 2.52 2 1 -14 425.05 26.32 2 1 -14 348.26 23.53 2 1 -13 51.61 8.68 2 1 -13 47.79 8.36 2 1 -13 37.37 7.25 2 1 -12 791.08 40.42 2 1 -12 707.62 38.47 2 1 -12 761.19 39.80 2 1 -11 21.56 5.64 2 1 -11 25.32 6.00 2 1 -11 22.00 6.56 2 1 -11 30.60 6.68 2 1 -11 24.53 5.81 2 1 -11 16.09 5.11 2 1 -10 1198.48 53.22 2 1 -10 1160.05 53.79 2 1 -10 1181.02 53.55 2 1 -10 1160.19 53.07 2 1 -10 1154.64 52.63 2 1 -10 1140.43 54.29 2 1 -9 12.06 3.69 2 1 -9 7.34 3.06 2 1 -9 13.49 4.49 2 1 -9 12.58 3.70 2 1 -9 12.17 3.82 2 1 -9 13.43 4.14 2 1 -8 999.89 44.94 2 1 -7 79.48 8.26 2 1 -7 67.56 9.01 2 1 -6 4177.50 150.39 2 1 -6 4286.52 154.41 2 1 -5 315.50 16.85 2 1 -5 361.46 19.32 2 1 -4 3756.90 131.66 2 1 -4 3862.87 133.86 2 1 -4 3678.72 132.32 2 1 -3 182.89 9.33 2 1 -3 172.22 10.16 2 1 -3 174.32 10.41 2 1 -2 1186.79 48.36 2 1 -2 1271.27 47.24 2 1 -1 350.74 18.16 2 1 0 2991.25 103.44 2 1 0 2753.78 99.94 2 1 1 99.04 8.16 2 1 1 83.04 6.70 2 1 2 6075.13 211.75 2 1 2 6010.62 209.68 2 1 3 357.01 20.64 2 1 3 416.79 20.42 2 1 4 4144.46 149.07 2 1 5 2089.73 81.32 2 1 6 204.21 15.63 2 1 7 241.48 18.09 2 1 8 536.57 30.78 2 2 -17 125.79 10.16 2 2 -16 15.77 4.29 2 2 -16 16.60 4.26 2 2 -15 277.45 20.37 2 2 -15 307.71 21.94 2 2 -14 72.59 10.12 2 2 -13 823.93 42.65 2 2 -12 123.52 13.46 2 2 -12 106.03 12.26 2 2 -12 95.05 11.89 2 2 -11 1108.56 50.98 2 2 -11 1077.45 50.42 2 2 -11 1119.43 50.78 2 2 -11 1103.84 55.69 2 2 -10 88.04 12.11 2 2 -10 67.18 10.40 2 2 -10 66.85 9.03 2 2 -10 47.61 7.81 2 2 -10 67.33 8.89 2 2 -9 753.62 42.97 2 2 -9 841.16 40.06 2 2 -9 845.73 39.88 2 2 -9 813.60 39.11 2 2 -9 940.21 45.44 2 2 -8 2.34 2.00 2 2 -7 866.94 40.02 2 2 -7 1000.05 44.03 2 2 -6 303.59 17.15 2 2 -6 326.40 19.87 2 2 -5 3743.93 134.95 2 2 -5 3830.42 136.92 2 2 -4 2251.97 82.92 2 2 -3 443.10 20.87 2 2 -3 422.62 22.04 2 2 -2 1308.03 52.01 2 2 -2 1271.68 49.82 2 2 -2 1263.21 48.35 2 2 -1 667.36 31.98 2 2 -1 744.36 29.04 2 2 0 963.04 38.04 2 2 0 940.87 41.30 2 2 1 2407.89 88.40 2 2 2 518.07 24.89 2 2 3 1214.01 50.38 2 2 4 4966.47 178.27 2 2 5 769.06 37.24 2 2 6 447.85 26.52 2 3 -17 24.58 4.39 2 3 -17 29.31 4.67 2 3 -16 260.91 17.89 2 3 -16 241.75 17.81 2 3 -15 81.77 10.30 2 3 -15 91.91 11.48 2 3 -14 308.15 22.76 2 3 -14 373.67 25.73 2 3 -13 115.65 13.37 2 3 -13 117.62 13.46 2 3 -12 481.99 29.08 2 3 -12 444.69 28.11 2 3 -12 413.07 30.21 2 3 -12 437.81 28.14 2 3 -11 207.87 17.02 2 3 -11 191.27 16.66 2 3 -11 205.35 17.12 2 3 -10 241.96 21.78 2 3 -10 240.72 18.41 2 3 -10 243.70 18.46 2 3 -10 250.55 18.55 2 3 -10 254.38 19.69 2 3 -9 617.75 38.97 2 3 -9 639.63 33.47 2 3 -9 640.64 33.58 2 3 -9 668.54 33.29 2 3 -9 662.36 34.88 2 3 -9 671.11 38.31 2 3 -8 1335.58 63.65 2 3 -8 1213.52 53.38 2 3 -8 1223.06 54.69 2 3 -8 1268.63 60.52 2 3 -8 1264.09 52.74 2 3 -8 1268.79 53.36 2 3 -8 1260.67 60.81 2 3 -7 920.28 42.23 2 3 -6 1898.71 74.36 2 3 -5 883.82 39.19 2 3 -5 933.43 39.37 2 3 -4 1234.77 51.90 2 3 -4 1234.96 49.66 2 3 -4 1241.16 50.22 2 3 -3 1128.06 45.30 2 3 -3 1156.33 48.69 2 3 -3 1113.20 46.24 2 3 -2 1578.86 56.91 2 3 -2 1449.08 60.45 2 3 -2 1378.59 57.33 2 3 -1 984.19 44.33 2 3 -1 993.23 41.56 2 3 1 2078.98 78.71 2 3 2 2064.90 79.36 2 3 3 587.12 29.62 2 3 5 130.82 11.93 2 3 6 68.85 8.90 2 3 7 230.82 17.55 2 3 7 215.43 18.97 2 3 8 266.13 22.05 2 4 -17 107.72 9.62 2 4 -16 45.52 7.34 2 4 -16 50.26 7.15 2 4 -15 168.03 15.06 2 4 -15 169.79 16.15 2 4 -14 316.02 22.93 2 4 -14 343.04 24.90 2 4 -14 339.86 23.49 2 4 -13 230.48 19.49 2 4 -13 254.45 21.26 2 4 -13 222.21 19.08 2 4 -12 295.48 22.27 2 4 -12 309.81 24.14 2 4 -12 304.29 22.30 2 4 -12 291.15 24.88 2 4 -12 329.66 23.32 2 4 -11 414.41 30.61 2 4 -11 412.70 26.80 2 4 -11 417.14 27.22 2 4 -11 472.23 28.19 2 4 -11 428.07 28.71 2 4 -10 143.48 17.18 2 4 -10 157.51 14.70 2 4 -10 156.95 14.82 2 4 -10 152.14 16.66 2 4 -10 185.81 15.66 2 4 -10 148.73 15.31 2 4 -10 166.96 17.02 2 4 -9 768.59 44.50 2 4 -9 688.27 35.80 2 4 -9 718.59 36.29 2 4 -9 636.51 40.46 2 4 -9 716.89 35.60 2 4 -9 652.72 36.97 2 4 -9 751.21 41.71 2 4 -8 744.61 36.73 2 4 -8 771.64 40.73 2 4 -8 680.17 43.89 2 4 -8 719.52 43.73 2 4 -8 790.48 36.31 2 4 -8 751.04 38.31 2 4 -8 784.77 43.40 2 4 -7 380.12 28.73 2 4 -7 378.25 25.11 2 4 -7 387.53 22.53 2 4 -7 382.87 23.49 2 4 -7 444.73 29.46 2 4 -6 2332.28 90.64 2 4 -5 520.58 35.84 2 4 -5 525.08 27.02 2 4 -5 517.37 26.79 2 4 -4 1118.34 50.25 2 4 -4 1075.97 46.91 2 4 -4 1171.46 47.81 2 4 -3 250.57 15.33 2 4 -3 235.95 17.47 2 4 -3 227.35 15.20 2 4 -2 956.95 45.16 2 4 -2 958.51 41.60 2 4 -1 410.42 25.86 2 4 -1 420.96 22.45 2 4 0 2384.59 90.60 2 4 1 349.25 27.82 2 4 1 390.35 21.99 2 4 2 1635.95 67.43 2 4 3 5.48 2.88 2 4 4 1700.16 70.33 2 4 4 1725.73 72.70 2 4 5 490.64 27.75 2 4 5 455.42 29.03 2 4 6 1043.30 48.85 2 4 6 1038.99 51.60 2 4 7 471.86 27.79 2 4 7 405.94 28.82 2 5 -16 57.80 7.92 2 5 -15 255.06 18.59 2 5 -15 245.22 19.39 2 5 -15 253.98 18.46 2 5 -14 160.60 15.38 2 5 -14 179.64 17.35 2 5 -14 163.91 15.49 2 5 -13 466.58 32.10 2 5 -13 474.75 30.10 2 5 -13 471.95 31.46 2 5 -13 551.45 31.69 2 5 -12 200.19 18.01 2 5 -12 256.48 21.30 2 5 -12 209.47 20.91 2 5 -12 213.85 18.71 2 5 -11 712.14 45.29 2 5 -11 873.58 43.04 2 5 -11 842.75 43.27 2 5 -11 814.18 42.48 2 5 -11 912.13 45.80 2 5 -11 782.16 44.00 2 5 -10 24.60 7.51 2 5 -10 32.20 7.21 2 5 -10 36.82 7.21 2 5 -10 34.18 8.58 2 5 -10 32.90 7.14 2 5 -10 21.36 5.53 2 5 -10 41.02 7.65 2 5 -9 1545.89 64.54 2 5 -9 1434.75 70.99 2 5 -9 1487.27 63.17 2 5 -9 1429.83 63.37 2 5 -9 1417.22 71.46 2 5 -9 1429.80 68.62 2 5 -9 1420.23 65.99 2 5 -9 1558.77 70.11 2 5 -8 210.32 19.38 2 5 -8 192.15 16.05 2 5 -8 212.87 21.42 2 5 -8 222.41 18.37 2 5 -8 252.57 21.63 2 5 -8 219.82 21.50 2 5 -7 1980.60 79.53 2 5 -7 2065.97 85.58 2 5 -7 1954.72 78.66 2 5 -7 1917.24 81.16 2 5 -7 1809.93 85.36 2 5 -6 355.28 25.25 2 5 -6 355.89 21.64 2 5 -6 357.77 26.61 2 5 -6 394.76 23.70 2 5 -6 352.23 24.91 2 5 -5 715.26 34.73 2 5 -5 799.34 36.43 2 5 -5 788.91 48.55 2 5 -5 758.80 36.21 2 5 -4 238.39 17.02 2 5 -4 305.61 28.06 2 5 -3 1549.15 63.03 2 5 -3 1516.72 67.41 2 5 -3 1545.25 78.09 2 5 -2 76.23 10.45 2 5 -2 77.43 8.58 2 5 -2 89.99 15.23 2 5 -1 2101.28 90.57 2 5 -1 2209.86 99.46 2 5 0 12.60 6.27 2 5 1 2733.36 105.12 2 5 1 2834.58 118.76 2 5 2 252.47 18.16 2 5 2 264.35 19.24 2 5 3 737.44 36.88 2 5 3 694.52 37.65 2 5 4 391.03 24.77 2 5 4 368.59 25.66 2 5 5 253.34 19.54 2 5 5 248.38 20.76 2 5 6 26.55 6.33 2 5 6 18.62 5.62 2 5 7 670.17 36.62 2 5 8 -1.06 2.93 2 5 12 15.76 3.97 2 6 -16 188.28 14.41 2 6 -15 0.84 2.48 2 6 -15 2.88 2.84 2 6 -14 418.08 26.24 2 6 -14 424.84 28.40 2 6 -14 434.67 28.02 2 6 -13 15.03 5.58 2 6 -13 12.93 5.23 2 6 -13 10.15 4.28 2 6 -12 425.67 31.54 2 6 -12 585.44 36.55 2 6 -12 478.95 29.88 2 6 -12 535.90 32.62 2 6 -12 428.12 29.04 2 6 -11 14.45 4.71 2 6 -11 27.17 6.70 2 6 -11 24.22 6.84 2 6 -11 25.53 6.30 2 6 -11 26.66 7.74 2 6 -10 431.73 27.66 2 6 -10 445.69 30.06 2 6 -10 387.08 30.53 2 6 -10 456.37 32.41 2 6 -10 419.27 27.24 2 6 -9 9.67 4.81 2 6 -9 12.26 5.57 2 6 -9 7.27 3.62 2 6 -8 315.11 22.17 2 6 -8 352.01 27.06 2 6 -8 357.65 26.60 2 6 -8 344.58 22.79 2 6 -7 5.62 3.11 2 6 -7 11.21 5.29 2 6 -7 2.67 3.43 2 6 -7 5.64 2.79 2 6 -6 1291.15 61.65 2 6 -6 1191.31 54.42 2 6 -5 15.98 6.28 2 6 -5 7.08 3.61 2 6 -5 10.26 6.80 2 6 -4 1742.97 84.24 2 6 -4 1622.07 66.85 2 6 -4 1646.43 66.85 2 6 -4 1446.16 67.16 2 6 -3 19.16 8.35 2 6 -3 10.67 4.56 2 6 -3 14.27 5.45 2 6 -3 15.14 4.16 2 6 -2 1438.77 59.15 2 6 -2 1268.77 60.09 2 6 -2 1319.58 64.80 2 6 -1 8.39 4.40 2 6 -1 13.85 6.04 2 6 -1 9.97 6.61 2 6 0 422.17 28.62 2 6 0 497.32 27.43 2 6 0 485.84 36.09 2 6 1 14.91 4.38 2 6 1 8.68 4.32 2 6 2 574.63 32.22 2 6 3 2.42 3.11 2 6 3 5.24 3.81 2 6 4 774.96 43.23 2 6 4 842.06 42.48 2 6 5 4.45 3.49 2 6 6 984.61 48.43 2 6 7 12.92 4.80 2 6 8 415.96 26.07 2 6 10 97.45 10.45 2 6 11 18.74 4.00 2 7 -15 222.68 15.71 2 7 -15 221.27 17.12 2 7 -15 214.47 16.25 2 7 -14 5.42 3.00 2 7 -14 5.01 3.16 2 7 -14 5.86 3.68 2 7 -13 197.27 17.14 2 7 -13 199.26 18.13 2 7 -12 1.54 3.22 2 7 -12 1.13 2.05 2 7 -11 387.81 28.98 2 7 -11 343.52 23.70 2 7 -11 281.87 24.18 2 7 -11 252.17 20.51 2 7 -11 273.81 25.13 2 7 -10 72.90 10.18 2 7 -10 73.90 12.76 2 7 -9 370.46 27.14 2 7 -9 401.16 30.28 2 7 -9 375.89 25.20 2 7 -8 20.22 5.39 2 7 -8 15.73 6.20 2 7 -8 19.60 5.85 2 7 -8 29.65 6.54 2 7 -7 1048.75 49.66 2 7 -7 993.37 54.78 2 7 -7 1042.47 49.88 2 7 -6 14.27 5.99 2 7 -6 5.26 3.12 2 7 -5 714.50 44.76 2 7 -5 725.52 38.60 2 7 -5 846.91 51.58 2 7 -4 8.52 5.06 2 7 -4 5.97 3.47 2 7 -4 10.75 6.38 2 7 -4 14.62 4.72 2 7 -3 629.02 33.78 2 7 -3 682.00 45.80 2 7 -3 576.60 34.65 2 7 -2 104.58 16.78 2 7 -2 117.64 15.62 2 7 -2 108.46 11.79 2 7 -2 99.93 12.76 2 7 -1 775.90 43.56 2 7 -1 770.37 48.45 2 7 0 147.56 16.38 2 7 0 153.27 19.37 2 7 0 145.50 19.45 2 7 0 198.23 16.50 2 7 1 742.25 38.09 2 7 1 680.56 46.86 2 7 1 614.95 38.91 2 7 2 4.50 3.33 2 7 2 4.29 3.89 2 7 2 -1.36 2.47 2 7 3 627.24 35.76 2 7 4 75.31 10.60 2 7 5 471.07 29.48 2 7 6 146.54 14.62 2 7 7 328.14 22.00 2 7 7 291.59 21.05 2 7 8 66.55 8.73 2 7 8 69.07 8.88 2 7 9 151.95 12.60 2 7 10 28.54 4.65 2 8 -15 22.50 4.94 2 8 -15 24.10 4.32 2 8 -14 172.25 15.67 2 8 -14 176.01 13.76 2 8 -13 8.12 3.42 2 8 -13 11.24 5.07 2 8 -12 418.86 29.51 2 8 -12 384.26 25.09 2 8 -11 28.78 7.66 2 8 -11 26.19 7.45 2 8 -10 413.61 30.39 2 8 -10 387.55 25.47 2 8 -10 357.61 29.25 2 8 -9 216.92 21.57 2 8 -9 225.86 18.52 2 8 -9 205.85 21.24 2 8 -8 175.58 16.33 2 8 -8 178.93 19.51 2 8 -7 21.25 5.85 2 8 -7 30.01 8.22 2 8 -7 19.03 5.55 2 8 -6 824.48 43.19 2 8 -6 812.02 48.57 2 8 -5 147.67 15.07 2 8 -5 150.63 18.74 2 8 -4 1029.00 50.05 2 8 -3 78.76 11.89 2 8 -3 110.77 12.53 2 8 -2 624.03 36.91 2 8 -2 561.16 40.46 2 8 -1 39.38 8.68 2 8 -1 38.31 9.99 2 8 0 87.01 13.15 2 8 0 114.83 13.15 2 8 1 56.09 10.40 2 8 1 61.05 9.64 2 8 2 287.50 24.12 2 8 2 351.73 24.53 2 8 3 242.64 20.06 2 8 4 391.60 26.24 2 8 5 311.59 22.15 2 8 6 253.26 18.70 2 8 7 39.57 6.57 2 8 8 83.26 8.52 2 9 -14 14.01 4.16 2 9 -13 105.30 12.07 2 9 -12 56.09 9.29 2 9 -11 183.75 18.55 2 9 -11 176.76 17.68 2 9 -10 129.00 12.83 2 9 -10 101.84 14.42 2 9 -10 96.15 13.22 2 9 -9 158.74 18.19 2 9 -9 167.41 15.42 2 9 -8 182.78 19.86 2 9 -8 186.16 16.66 2 9 -7 286.18 21.73 2 9 -7 283.16 25.47 2 9 -6 33.47 7.61 2 9 -6 41.34 9.62 2 9 -5 303.59 23.12 2 9 -5 298.92 26.47 2 9 -4 90.29 11.75 2 9 -2 421.62 30.15 2 9 -1 152.54 17.16 2 9 0 346.00 23.98 2 9 0 285.89 24.34 2 9 1 151.10 15.18 2 9 1 101.48 13.70 2 9 2 221.56 18.47 2 9 2 170.99 17.30 2 9 3 181.08 16.38 2 9 4 282.04 20.24 2 9 5 76.87 9.35 2 9 6 104.13 10.12 2 9 7 56.76 6.51 2 10 -12 102.42 11.14 2 10 -11 117.66 13.31 2 10 -10 68.37 10.71 2 10 -9 114.97 11.89 2 10 -9 123.33 15.05 2 10 -8 96.06 11.09 2 10 -8 96.73 13.79 2 10 -7 202.89 20.50 2 10 -7 195.00 17.09 2 10 -6 132.46 16.47 2 10 -6 124.20 13.42 2 10 0 59.99 9.09 2 10 1 217.75 17.69 2 10 2 28.94 5.86 2 10 3 322.66 20.79 2 10 4 10.04 3.37 2 10 5 132.14 10.55 2 11 -10 146.20 13.99 2 11 -9 27.35 6.44 2 11 -8 185.93 17.25 2 11 -8 170.52 13.66 2 11 -7 30.13 5.82 2 11 -7 37.67 7.82 2 11 -6 124.91 12.11 2 11 -5 1.77 2.27 2 11 1 7.10 2.79 2 11 2 166.64 12.47 2 12 -6 1.72 1.59 2 12 -5 113.65 9.76 2 12 -4 0.60 1.66 2 12 -3 86.47 8.33 2 12 -2 5.02 2.19 3 -13 2 93.40 10.63 3 -13 3 27.17 5.87 3 -13 4 109.25 12.26 3 -12 1 172.78 16.51 3 -11 -7 112.41 9.26 3 -11 0 207.27 19.00 3 -10 -8 423.88 22.83 3 -9 -10 8.11 2.48 3 -9 -9 333.63 20.10 3 -9 0 25.87 8.92 3 -9 1 759.16 55.52 3 -9 2 104.87 19.90 3 -9 3 195.65 27.49 3 -9 4 -2.65 3.92 3 -9 5 902.24 57.58 3 -8 -11 5.83 2.45 3 -8 -10 339.00 20.85 3 -8 -10 351.36 22.19 3 -8 -9 16.00 4.66 3 -8 -9 22.09 5.50 3 -8 -1 25.83 8.10 3 -8 0 792.56 53.73 3 -8 1 19.22 9.56 3 -8 2 1616.50 92.13 3 -8 3 45.62 12.66 3 -8 4 1391.83 75.95 3 -8 5 39.79 9.81 3 -7 -12 42.31 5.79 3 -7 -11 487.00 26.94 3 -7 -11 528.47 29.20 3 -7 -10 36.20 6.70 3 -7 -10 28.96 6.64 3 -7 -9 424.58 28.34 3 -7 -8 26.09 7.02 3 -7 -6 403.71 34.47 3 -7 -6 356.49 26.11 3 -7 -5 1065.01 63.31 3 -7 -5 1031.45 51.35 3 -7 -4 495.10 40.40 3 -7 -2 109.82 12.41 3 -7 -1 977.02 55.54 3 -7 0 253.57 26.41 3 -7 1 1412.32 77.91 3 -7 2 735.39 50.89 3 -7 3 1274.42 69.47 3 -7 4 484.82 34.87 3 -6 -13 216.79 14.14 3 -6 -12 135.66 12.06 3 -6 -12 137.60 13.26 3 -6 -11 74.35 9.73 3 -6 -11 104.58 12.08 3 -6 -10 343.40 23.89 3 -6 -10 388.36 26.42 3 -6 -9 204.83 19.26 3 -6 -8 916.54 45.90 3 -6 -7 419.69 26.85 3 -6 -7 411.37 33.88 3 -6 -7 376.18 26.92 3 -6 -6 1191.63 67.20 3 -6 -6 1265.64 60.75 3 -6 -6 1206.25 57.53 3 -6 -5 348.62 32.03 3 -6 -4 380.50 33.22 3 -6 -3 80.33 14.09 3 -6 -2 815.75 44.60 3 -6 -1 275.12 23.59 3 -6 0 1009.40 54.93 3 -6 1 1008.70 56.00 3 -6 2 1339.80 67.03 3 -6 3 820.39 45.63 3 -6 4 428.99 28.64 3 -5 -14 403.83 20.84 3 -5 -13 60.12 7.61 3 -5 -13 53.49 8.00 3 -5 -12 157.02 13.91 3 -5 -12 154.70 14.90 3 -5 -11 600.99 33.84 3 -5 -11 638.49 35.82 3 -5 -10 12.23 4.52 3 -5 -10 6.45 4.06 3 -5 -9 696.30 38.50 3 -5 -8 283.97 21.75 3 -5 -8 226.95 24.07 3 -5 -8 274.50 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1207.07 59.08 3 4 -10 1047.68 51.66 3 4 -9 8.05 5.07 3 4 -9 8.69 3.69 3 4 -9 14.38 4.58 3 4 -9 10.18 4.83 3 4 -8 1742.27 73.22 3 4 -8 1645.58 78.59 3 4 -8 1627.57 70.13 3 4 -8 1642.85 75.27 3 4 -7 7.62 5.05 3 4 -7 5.09 3.20 3 4 -7 1.77 2.28 3 4 -7 11.64 4.69 3 4 -6 1107.51 50.11 3 4 -6 1101.85 55.93 3 4 -6 1172.01 50.81 3 4 -6 1054.92 49.15 3 4 -6 1082.89 54.30 3 4 -5 4.41 2.67 3 4 -5 7.80 4.31 3 4 -5 2.39 2.22 3 4 -5 5.22 2.74 3 4 -5 3.71 2.90 3 4 -5 4.92 2.43 3 4 -4 1733.63 74.52 3 4 -4 1692.34 69.52 3 4 -4 1647.78 67.99 3 4 -4 1689.42 67.82 3 4 -3 111.59 13.08 3 4 -3 119.60 11.58 3 4 -2 1644.42 72.91 3 4 -2 1659.28 68.50 3 4 -1 256.70 21.51 3 4 -1 254.95 18.21 3 4 0 1328.22 65.17 3 4 0 1336.91 57.29 3 4 0 1265.34 54.73 3 4 1 280.90 26.76 3 4 1 328.41 20.35 3 4 2 755.25 52.40 3 4 2 959.17 43.11 3 4 3 2.22 3.28 3 4 3 4.65 3.08 3 4 4 374.01 24.27 3 4 4 367.87 25.39 3 4 5 32.12 6.89 3 4 5 43.46 8.21 3 4 6 1069.85 49.61 3 4 6 937.41 50.42 3 4 7 283.42 21.24 3 4 8 371.23 24.91 3 4 9 47.72 8.04 3 5 -16 26.26 4.91 3 5 -15 237.28 17.63 3 5 -14 39.14 6.81 3 5 -14 43.73 7.94 3 5 -13 551.30 32.39 3 5 -13 625.34 37.16 3 5 -13 610.52 35.11 3 5 -12 2.25 2.36 3 5 -12 1.24 2.61 3 5 -12 6.22 3.69 3 5 -11 672.65 37.76 3 5 -11 721.26 41.19 3 5 -10 12.48 4.92 3 5 -10 15.10 6.14 3 5 -9 680.29 36.56 3 5 -9 655.27 41.16 3 5 -9 620.73 37.84 3 5 -9 670.46 41.28 3 5 -8 514.38 29.21 3 5 -8 425.47 31.26 3 5 -8 400.12 28.39 3 5 -8 482.12 33.97 3 5 -7 604.04 32.16 3 5 -7 490.74 34.67 3 5 -7 555.00 37.09 3 5 -7 557.69 32.45 3 5 -7 525.99 29.54 3 5 -6 415.92 31.08 3 5 -6 435.43 26.54 3 5 -6 428.19 31.64 3 5 -6 420.14 26.72 3 5 -6 473.28 26.41 3 5 -5 824.23 54.87 3 5 -5 893.60 41.65 3 5 -5 856.63 42.39 3 5 -5 850.05 49.49 3 5 -4 254.75 27.70 3 5 -4 264.22 18.25 3 5 -4 211.11 20.42 3 5 -4 265.86 19.15 3 5 -4 230.61 23.47 3 5 -3 966.19 51.72 3 5 -3 996.51 46.34 3 5 -3 1100.38 63.03 3 5 -3 1049.40 48.05 3 5 -2 376.69 22.64 3 5 -2 345.20 26.84 3 5 -2 326.02 22.35 3 5 -2 371.73 33.22 3 5 -1 893.32 41.97 3 5 -1 883.02 50.53 3 5 -1 922.20 43.66 3 5 -1 817.36 44.28 3 5 -1 937.03 56.25 3 5 0 728.84 35.66 3 5 0 665.94 44.64 3 5 0 663.64 39.69 3 5 0 758.85 48.90 3 5 1 433.60 37.20 3 5 1 499.21 28.28 3 5 2 277.29 30.60 3 5 2 378.82 23.87 3 5 3 584.20 45.98 3 5 3 713.61 37.05 3 5 4 288.08 21.47 3 5 4 288.02 22.68 3 5 5 666.71 36.79 3 5 6 236.63 19.34 3 5 7 313.83 22.61 3 5 8 46.63 7.95 3 5 9 46.90 7.54 3 6 -15 20.39 4.73 3 6 -14 201.17 15.27 3 6 -14 172.65 16.31 3 6 -13 52.17 8.06 3 6 -13 64.97 10.56 3 6 -12 501.77 30.01 3 6 -11 227.75 20.87 3 6 -11 265.55 20.46 3 6 -10 359.32 29.76 3 6 -10 379.78 26.18 3 6 -9 773.99 43.75 3 6 -9 693.26 38.65 3 6 -9 687.64 43.36 3 6 -8 39.52 7.35 3 6 -8 30.34 8.17 3 6 -8 29.31 6.66 3 6 -8 28.00 7.97 3 6 -7 90.11 11.14 3 6 -7 105.53 14.36 3 6 -7 86.01 11.20 3 6 -7 89.14 13.98 3 6 -6 319.23 21.95 3 6 -6 321.22 28.07 3 6 -6 303.71 22.27 3 6 -5 231.89 27.21 3 6 -5 210.94 17.34 3 6 -5 209.21 23.19 3 6 -5 223.61 18.41 3 6 -4 605.03 33.22 3 6 -4 657.01 48.67 3 6 -4 595.83 33.83 3 6 -3 1084.31 49.63 3 6 -3 1138.88 66.84 3 6 -3 964.52 54.85 3 6 -2 564.72 43.76 3 6 -2 555.24 30.77 3 6 -2 495.11 35.86 3 6 -1 1037.08 54.76 3 6 -1 1207.35 67.81 3 6 -1 1164.33 51.95 3 6 -1 1083.77 61.21 3 6 0 299.59 25.17 3 6 0 277.12 28.54 3 6 1 125.48 13.20 3 6 1 95.16 17.14 3 6 2 279.96 21.11 3 6 2 233.70 27.45 3 6 3 54.62 9.18 3 6 4 222.37 18.88 3 6 5 488.41 30.22 3 6 6 140.97 14.54 3 6 7 268.28 19.84 3 6 8 120.04 11.93 3 6 9 83.55 9.02 3 6 9 67.24 8.10 3 6 10 103.55 9.03 3 7 -15 66.53 8.05 3 7 -14 160.85 14.76 3 7 -13 165.41 14.14 3 7 -13 179.38 16.99 3 7 -12 141.40 13.89 3 7 -12 151.39 16.53 3 7 -11 125.17 13.31 3 7 -10 187.55 18.09 3 7 -10 165.39 19.19 3 7 -10 183.10 16.86 3 7 -9 56.16 9.86 3 7 -9 54.76 9.05 3 7 -9 45.06 10.04 3 7 -8 410.51 28.86 3 7 -8 418.71 27.27 3 7 -8 392.13 31.12 3 7 -8 384.99 26.10 3 7 -7 39.80 8.06 3 7 -7 39.41 9.84 3 7 -7 44.50 8.11 3 7 -6 328.14 23.55 3 7 -6 335.93 29.18 3 7 -6 287.15 21.85 3 7 -5 610.37 45.77 3 7 -5 573.91 41.57 3 7 -5 593.07 33.85 3 7 -4 763.01 53.01 3 7 -4 780.18 40.73 3 7 -3 440.85 37.77 3 7 -3 403.92 26.42 3 7 -2 253.38 19.63 3 7 -2 291.01 29.52 3 7 -2 219.01 23.72 3 7 -1 120.22 18.17 3 7 -1 117.77 17.76 3 7 1 99.31 14.06 3 7 1 123.63 13.43 3 7 2 216.06 18.58 3 7 3 119.44 13.62 3 7 4 546.09 32.30 3 7 5 42.14 7.85 3 7 6 321.82 21.89 3 7 7 63.85 8.47 3 7 8 65.10 7.73 3 8 -14 54.58 7.70 3 8 -13 203.08 17.02 3 8 -13 186.85 13.99 3 8 -12 41.73 8.16 3 8 -12 27.01 5.62 3 8 -11 252.90 21.40 3 8 -11 229.81 17.99 3 8 -10 21.09 5.71 3 8 -10 28.81 7.68 3 8 -9 316.27 22.63 3 8 -9 289.24 25.66 3 8 -8 31.53 7.21 3 8 -8 38.66 9.58 3 8 -7 266.27 20.84 3 8 -7 265.77 20.98 3 8 -7 237.06 23.92 3 8 -6 167.48 16.12 3 8 -6 132.45 18.00 3 8 -6 163.04 16.31 3 8 -5 246.51 20.07 3 8 -4 6.83 4.14 3 8 -3 735.93 39.32 3 8 -2 19.34 5.43 3 8 1 295.82 22.13 3 8 2 16.72 5.25 3 8 3 327.81 23.01 3 8 4 6.93 3.89 3 8 5 312.49 20.65 3 8 6 0.74 1.74 3 8 7 178.32 12.79 3 9 -13 15.42 4.15 3 9 -12 166.08 14.62 3 9 -12 143.02 11.69 3 9 -11 19.02 5.33 3 9 -11 13.48 4.02 3 9 -10 184.54 15.26 3 9 -9 10.81 3.99 3 9 -9 4.31 3.69 3 9 -8 315.20 22.41 3 9 -8 320.36 26.22 3 9 -7 1.08 2.77 3 9 -7 -1.60 3.35 3 9 -6 318.21 23.04 3 9 -6 324.38 23.25 3 9 -5 29.84 6.82 3 9 -5 31.51 6.85 3 9 -4 461.03 28.69 3 9 -3 19.74 5.26 3 9 1 2.96 3.10 3 9 2 353.62 22.99 3 9 3 8.61 3.73 3 9 4 207.35 15.19 3 9 5 1.24 1.72 3 10 -11 116.04 9.74 3 10 -10 -0.68 1.60 3 10 -9 212.66 15.67 3 10 -8 0.84 1.98 3 10 -8 2.49 2.91 3 10 -7 257.64 18.59 3 10 -6 1.86 2.18 3 10 -5 134.16 13.23 3 10 -4 14.44 4.42 3 10 2 20.31 4.34 3 10 3 64.88 7.05 3 11 -8 102.43 9.07 3 11 -7 41.83 5.88 3 11 -6 118.15 10.51 3 11 -5 17.12 4.03 3 11 -4 91.30 9.24 3 11 -3 20.78 4.38 3 11 -2 53.80 6.74 3 11 -1 21.72 4.08 4 -13 1 255.62 17.83 4 -13 2 41.75 7.13 4 -13 3 129.09 12.92 4 -13 4 36.28 6.89 4 -13 5 117.76 12.63 4 -13 6 13.18 4.32 4 -13 7 128.46 12.48 4 -12 0 210.88 17.64 4 -12 1 1.11 2.01 4 -12 2 238.29 19.99 4 -12 3 11.97 4.71 4 -12 4 315.22 24.06 4 -12 5 3.79 3.50 4 -12 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55.46 4 2 -7 997.21 48.56 4 2 -7 1014.11 47.49 4 2 -7 1130.35 53.73 4 2 -6 1369.85 56.24 4 2 -6 1295.81 56.69 4 2 -6 1190.25 53.78 4 2 -6 1192.83 55.33 4 2 -5 326.27 21.37 4 2 -5 340.23 21.52 4 2 -4 1265.04 55.47 4 2 -4 1350.41 56.97 4 2 -3 35.00 6.55 4 2 -2 3418.33 128.73 4 2 -1 732.96 36.96 4 2 0 1047.74 52.17 4 2 1 851.77 46.02 4 2 2 564.49 36.16 4 2 3 325.27 21.97 4 2 4 1304.98 59.08 4 2 5 49.76 8.64 4 2 6 1346.79 62.86 4 2 7 669.98 37.01 4 2 8 274.46 21.34 4 2 9 191.48 17.29 4 2 10 62.42 9.20 4 3 -16 36.84 5.37 4 3 -15 143.78 12.90 4 3 -14 132.27 12.68 4 3 -14 124.11 12.96 4 3 -13 321.69 22.64 4 3 -13 339.97 23.93 4 3 -12 224.54 18.85 4 3 -11 511.80 34.60 4 3 -11 533.99 31.83 4 3 -10 217.05 22.02 4 3 -10 219.53 18.60 4 3 -9 904.97 47.31 4 3 -9 793.83 49.95 4 3 -9 968.06 46.77 4 3 -9 893.92 45.11 4 3 -8 158.77 15.78 4 3 -8 139.09 17.83 4 3 -8 166.41 15.70 4 3 -8 137.46 14.10 4 3 -7 399.66 26.35 4 3 -7 450.29 31.41 4 3 -7 419.69 25.99 4 3 -7 410.02 26.48 4 3 -6 406.06 25.29 4 3 -6 389.14 24.58 4 3 -6 409.20 28.36 4 3 -6 360.74 23.51 4 3 -5 814.38 40.65 4 3 -4 317.09 20.00 4 3 -4 353.53 22.48 4 3 -4 282.91 24.28 4 3 -3 1339.09 57.44 4 3 -3 1223.17 54.28 4 3 -2 505.64 27.99 4 3 -2 534.33 30.44 4 3 -2 554.00 34.03 4 3 -1 482.41 26.80 4 3 -1 520.58 29.45 4 3 0 784.25 38.42 4 3 0 807.47 41.07 4 3 0 762.47 45.27 4 3 1 431.25 25.04 4 3 1 342.98 29.85 4 3 2 108.11 11.43 4 3 2 111.05 11.86 4 3 2 83.96 14.76 4 3 3 180.75 16.01 4 3 4 499.30 29.84 4 3 5 322.29 23.02 4 3 6 757.24 40.36 4 3 7 341.77 24.14 4 3 8 356.98 24.48 4 3 9 45.89 8.07 4 3 10 21.48 5.10 4 4 -15 109.24 10.08 4 4 -15 108.97 10.57 4 4 -14 128.10 12.28 4 4 -14 129.75 12.76 4 4 -13 146.64 14.15 4 4 -12 345.45 25.70 4 4 -12 394.64 25.78 4 4 -11 239.90 22.38 4 4 -11 293.13 21.96 4 4 -10 181.88 19.92 4 4 -10 179.66 16.96 4 4 -9 464.93 35.18 4 4 -9 486.52 30.65 4 4 -9 533.62 31.57 4 4 -8 196.75 18.27 4 4 -8 165.14 20.06 4 4 -8 193.53 17.52 4 4 -8 215.42 18.23 4 4 -7 515.82 37.29 4 4 -7 550.44 32.80 4 4 -7 574.57 32.54 4 4 -6 634.12 33.91 4 4 -6 506.73 35.98 4 4 -6 553.18 31.66 4 4 -6 505.89 36.91 4 4 -5 370.96 24.97 4 4 -5 366.15 23.28 4 4 -5 423.08 29.69 4 4 -5 363.44 30.69 4 4 -5 372.50 24.11 4 4 -4 666.06 36.64 4 4 -4 687.85 35.01 4 4 -3 596.61 34.36 4 4 -3 638.00 33.12 4 4 -2 283.02 25.17 4 4 -2 328.04 22.98 4 4 -2 318.94 21.25 4 4 -1 1122.84 61.97 4 4 -1 1219.63 56.27 4 4 -1 1199.04 53.78 4 4 0 92.56 15.19 4 4 0 86.24 11.37 4 4 0 88.74 10.70 4 4 1 598.86 45.64 4 4 1 621.88 36.31 4 4 1 658.64 34.49 4 4 2 254.45 30.18 4 4 2 295.60 23.41 4 4 3 549.44 32.10 4 4 4 231.35 19.30 4 4 5 660.93 36.78 4 4 6 112.35 13.32 4 4 7 340.73 23.80 4 4 8 28.09 6.37 4 4 9 121.18 12.08 4 4 10 29.10 5.42 4 5 -15 22.50 4.18 4 5 -14 209.68 15.49 4 5 -14 199.86 16.53 4 5 -13 105.71 11.48 4 5 -12 432.16 28.42 4 5 -12 441.06 27.58 4 5 -11 227.19 20.77 4 5 -11 216.03 18.68 4 5 -10 457.42 32.73 4 5 -10 438.88 28.86 4 5 -9 365.21 29.25 4 5 -9 346.88 25.13 4 5 -8 437.58 33.07 4 5 -8 450.02 28.68 4 5 -8 371.63 26.69 4 5 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379.29 23.85 6 6 -1 0.87 2.03 6 6 0 311.85 20.11 6 7 -8 7.24 3.04 6 7 -7 208.79 14.51 6 7 -7 214.28 15.84 6 7 -6 15.27 4.01 6 7 -6 16.01 4.53 6 7 -5 296.99 18.35 6 7 -5 248.00 18.45 6 7 -4 7.40 3.01 6 7 -3 154.94 12.81 6 7 -2 11.91 3.54 6 7 -1 86.86 8.83 7 -12 0 53.53 6.77 7 -12 1 89.31 9.14 7 -12 1 80.26 9.57 7 -12 2 68.35 8.38 7 -12 2 58.69 8.62 7 -12 3 103.16 11.59 7 -12 4 52.65 7.78 7 -11 -3 89.28 8.95 7 -11 -2 89.18 9.50 7 -11 -1 143.60 13.17 7 -11 0 63.63 8.97 7 -11 0 71.80 10.46 7 -11 1 151.15 14.87 7 -11 1 130.73 15.67 7 -11 2 80.84 11.22 7 -11 2 88.26 13.27 7 -11 3 106.47 14.47 7 -11 4 85.33 11.80 7 -11 5 86.69 10.69 7 -10 -4 184.82 14.70 7 -10 -3 147.86 13.68 7 -10 -2 260.21 19.60 7 -10 -1 34.25 7.34 7 -10 -1 25.33 6.91 7 -10 0 188.37 18.69 7 -10 0 220.25 22.10 7 -10 1 6.02 3.87 7 -10 1 14.01 6.95 7 -10 2 206.35 21.41 7 -10 2 172.10 21.77 7 -10 3 47.67 10.81 7 -10 4 264.96 23.29 7 -9 -7 208.36 13.98 7 -9 -6 48.96 6.89 7 -9 -5 290.34 20.04 7 -9 -4 71.99 9.87 7 -9 -3 458.03 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-8 402.03 25.89 7 -6 -8 442.67 26.00 7 -6 -7 147.39 14.85 7 -6 -7 144.21 14.82 7 -6 -7 145.97 14.15 7 -6 -6 623.08 36.23 7 -6 -5 305.51 23.70 7 -6 -4 400.15 28.28 7 -6 -3 310.93 24.31 7 -6 -3 271.63 23.84 7 -6 -2 282.45 23.92 7 -6 -2 318.13 26.63 7 -6 -1 131.37 15.97 7 -6 -1 157.22 18.62 7 -6 0 424.96 32.68 7 -6 1 249.73 23.98 7 -6 2 463.29 33.23 7 -6 3 262.59 22.78 7 -5 -11 112.48 9.56 7 -5 -11 116.08 9.58 7 -5 -10 200.98 15.05 7 -5 -10 197.40 14.42 7 -5 -9 188.02 16.34 7 -5 -9 204.35 15.62 7 -5 -8 395.48 25.23 7 -5 -8 362.37 25.32 7 -5 -8 358.85 23.42 7 -5 -7 346.79 24.87 7 -5 -7 349.20 23.44 7 -5 -6 513.37 32.39 7 -5 -5 203.48 19.15 7 -5 -4 512.61 33.24 7 -5 -3 140.19 15.96 7 -5 -3 113.24 15.39 7 -5 -2 534.79 33.92 7 -5 -2 477.87 34.64 7 -5 -1 318.17 27.23 7 -5 0 496.67 35.29 7 -5 1 228.12 22.14 7 -5 2 319.81 25.88 7 -5 3 78.90 11.98 7 -4 -11 130.38 11.51 7 -4 -11 152.98 11.59 7 -4 -10 124.35 12.78 7 -4 -10 135.28 11.85 7 -4 -9 437.57 26.74 7 -4 -9 473.50 29.22 7 -4 -9 440.02 25.78 7 -4 -8 180.40 16.54 7 -4 -8 173.66 15.87 7 -4 -7 1046.43 52.07 7 -4 -6 17.18 5.73 7 -4 -5 340.04 25.88 7 -4 -4 156.37 16.91 7 -4 -3 250.57 21.80 7 -4 -3 223.66 22.10 7 -4 -2 318.84 27.15 7 -4 -1 335.38 28.24 7 -4 0 163.86 18.87 7 -4 1 617.62 39.23 7 -4 2 7.26 4.30 7 -4 3 469.43 31.61 7 -3 -12 181.81 12.21 7 -3 -12 171.95 12.23 7 -3 -11 32.54 5.67 7 -3 -11 52.51 7.46 7 -3 -10 549.77 30.15 7 -3 -10 537.09 31.58 7 -3 -9 58.24 8.94 7 -3 -9 45.48 7.84 7 -3 -8 909.38 46.13 7 -3 -8 883.52 45.14 7 -3 -7 8.86 4.20 7 -3 -7 7.83 3.71 7 -3 -6 395.82 27.93 7 -3 -6 373.35 25.34 7 -3 -5 55.80 9.95 7 -3 -4 173.00 17.75 7 -3 -4 188.26 19.57 7 -3 -3 318.76 24.57 7 -3 -3 309.16 26.34 7 -3 -2 1183.08 62.06 7 -3 -1 11.45 5.69 7 -3 0 1077.46 57.17 7 -3 1 30.12 7.95 7 -3 2 428.77 30.27 7 -3 11 1.10 1.53 7 -2 -12 21.85 4.30 7 -2 -12 30.73 5.11 7 -2 -11 535.87 28.84 7 -2 -11 521.50 29.27 7 -2 -10 5.88 3.41 7 -2 -10 2.21 3.27 7 -2 -9 671.42 36.08 7 -2 -9 614.80 35.04 7 -2 -8 33.24 7.33 7 -2 -8 32.69 7.07 7 -2 -7 633.05 36.79 7 -2 -7 601.74 34.81 7 -2 -6 28.66 7.39 7 -2 -6 19.88 5.72 7 -2 -5 503.31 32.27 7 -2 -4 118.05 14.20 7 -2 -3 1084.01 57.67 7 -2 -2 16.13 6.34 7 -2 -1 625.42 40.34 7 -2 0 284.65 24.49 7 -2 1 441.94 31.20 7 -2 10 20.83 4.37 7 -1 -12 356.94 20.70 7 -1 -11 51.01 7.97 7 -1 -10 447.59 29.08 7 -1 -10 567.88 30.74 7 -1 -9 80.77 10.82 7 -1 -8 485.49 30.40 7 -1 -8 478.68 30.01 7 -1 -8 490.19 33.09 7 -1 -7 56.86 9.67 7 -1 -7 49.79 8.64 7 -1 -6 585.65 35.10 7 -1 -5 30.95 7.29 7 -1 8 94.39 10.31 7 -1 9 37.31 5.84 7 -1 10 80.24 7.80 7 0 -12 21.40 4.51 7 0 -11 362.69 22.52 7 0 -10 86.61 10.77 7 0 -9 99.95 11.93 7 0 -9 94.15 13.67 7 0 -8 149.36 15.04 7 0 -8 136.74 16.97 7 0 -7 304.96 22.76 7 0 -7 327.85 26.21 7 0 -6 209.37 19.13 7 0 -5 667.09 37.34 7 0 -1 100.84 12.14 7 0 0 297.95 22.48 7 0 6 70.37 9.26 7 0 6 62.16 8.77 7 0 7 49.30 7.30 7 0 8 61.19 7.63 7 0 9 52.92 6.46 7 1 -12 148.28 11.86 7 1 -11 128.65 11.98 7 1 -10 172.56 17.20 7 1 -10 145.28 13.97 7 1 -9 170.92 18.58 7 1 -9 163.33 15.20 7 1 -8 245.38 23.28 7 1 -8 253.70 19.84 7 1 -7 314.81 24.49 7 1 -7 339.56 27.63 7 1 -6 329.50 24.81 7 1 -6 323.85 26.63 7 1 -5 411.14 27.96 7 1 -2 86.55 11.06 7 1 -1 496.43 30.28 7 1 0 251.45 20.34 7 1 1 137.74 14.63 7 1 2 198.98 17.97 7 1 3 216.05 18.44 7 1 4 21.16 5.53 7 1 5 155.60 13.85 7 1 6 21.01 4.91 7 1 7 119.90 10.92 7 1 8 47.68 6.08 7 2 -11 39.33 6.98 7 2 -11 40.66 6.21 7 2 -10 131.88 14.57 7 2 -10 154.73 13.37 7 2 -9 31.91 7.98 7 2 -9 37.77 6.74 7 2 -8 413.43 31.74 7 2 -8 433.88 27.29 7 2 -7 49.20 8.90 7 2 -7 44.29 10.28 7 2 -6 646.71 37.63 7 2 -6 666.83 41.36 7 2 -5 53.42 9.38 7 2 -5 56.47 11.33 7 2 -4 389.62 27.06 7 2 -4 389.73 28.97 7 2 -3 50.05 8.25 7 2 -2 148.09 14.70 7 2 -1 41.58 7.81 7 2 0 258.26 20.28 7 2 1 52.22 8.85 7 2 2 424.10 26.70 7 2 3 20.23 5.19 7 2 4 266.56 18.78 7 2 6 95.79 9.40 7 2 7 13.20 3.29 7 3 -11 187.19 14.47 7 3 -10 10.04 4.08 7 3 -9 354.29 25.10 7 3 -9 297.80 19.99 7 3 -8 36.28 7.52 7 3 -8 35.59 8.52 7 3 -8 39.37 6.87 7 3 -7 460.20 28.41 7 3 -7 342.85 28.32 7 3 -6 -1.18 2.48 7 3 -6 1.55 2.80 7 3 -5 223.56 19.26 7 3 -4 3.67 2.87 7 3 -3 335.25 22.78 7 3 -2 4.07 3.20 7 3 -1 412.49 26.17 7 3 0 16.16 4.99 7 3 1 288.58 20.60 7 3 2 7.17 3.64 7 3 3 166.43 13.92 7 4 -10 154.04 13.07 7 4 -9 0.94 2.21 7 4 -8 350.61 24.08 7 4 -8 343.52 22.50 7 4 -8 308.06 19.74 7 4 -7 21.42 5.26 7 4 -7 13.25 5.38 7 4 -6 274.10 20.60 7 4 -5 6.55 3.43 7 4 -4 156.96 15.65 7 4 -4 172.18 14.63 7 4 -3 7.21 3.99 7 4 -3 9.99 3.81 7 4 -2 182.90 15.50 7 4 -1 21.76 5.42 7 4 0 281.58 19.31 7 4 1 31.35 5.92 7 4 2 134.70 11.69 7 5 -8 10.08 3.46 7 5 -7 134.48 12.48 7 5 -6 31.70 6.21 7 5 -5 61.67 7.75 7 5 -5 56.33 8.33 7 5 -4 26.95 5.19 7 5 -4 18.46 4.94 7 5 -3 200.23 14.71 7 5 -3 147.28 14.70 7 5 -2 44.27 6.75 7 5 -1 230.75 16.17 7 5 0 38.58 5.98 7 5 1 102.33 9.27 7 6 -6 129.25 11.17 7 6 -5 15.02 3.52 7 6 -5 9.32 3.12 7 6 -4 136.64 10.68 7 6 -4 107.06 10.63 7 6 -3 26.85 4.62 7 6 -3 26.17 5.15 7 6 -2 96.87 8.77 7 6 -1 92.57 8.24 8 -10 -3 35.27 5.46 8 -10 -2 195.03 14.88 8 -10 -1 30.54 6.36 8 -10 -1 33.35 6.52 8 -10 0 174.82 17.23 8 -10 0 152.48 15.23 8 -10 1 16.39 5.86 8 -10 2 144.98 17.04 8 -10 3 3.84 3.29 8 -10 4 177.31 15.92 8 -9 -5 270.93 16.65 8 -9 -4 56.08 7.38 8 -9 -3 176.92 14.99 8 -9 -2 28.14 6.24 8 -9 -1 132.29 15.49 8 -9 -1 133.27 14.66 8 -9 0 105.62 15.15 8 -9 0 92.13 12.81 8 -9 1 163.17 20.05 8 -9 2 133.22 17.27 8 -9 3 187.91 18.95 8 -9 4 108.45 12.75 8 -8 -6 235.48 15.24 8 -8 -6 280.41 17.15 8 -8 -5 210.12 15.72 8 -8 -4 120.35 12.28 8 -8 -3 211.81 17.82 8 -8 -2 79.56 11.17 8 -8 -2 73.21 11.16 8 -8 -1 131.28 15.54 8 -8 -1 154.27 18.01 8 -8 0 170.52 20.28 8 -8 1 266.45 25.78 8 -8 2 100.63 15.04 8 -8 3 219.54 20.59 8 -7 -7 140.36 11.71 8 -7 -6 409.31 23.99 8 -7 -5 80.27 10.05 8 -7 -4 203.07 17.44 8 -7 -3 36.78 7.56 8 -7 -2 154.85 16.49 8 -7 -2 178.92 18.60 8 -7 -1 44.90 9.65 8 -7 0 436.39 33.37 8 -7 1 17.05 6.94 8 -7 2 370.42 28.48 8 -7 3 1.32 3.08 8 -6 -8 21.86 4.42 8 -6 -8 31.57 5.23 8 -6 -7 353.89 21.68 8 -6 -6 6.53 3.39 8 -6 -5 402.86 25.85 8 -6 -4 -1.16 2.10 8 -6 -3 440.59 29.28 8 -6 -3 456.90 30.71 8 -6 -2 11.72 4.74 8 -6 -2 13.85 5.60 8 -6 -1 596.82 39.39 8 -6 0 8.43 5.86 8 -6 1 526.18 35.90 8 -6 2 2.87 2.60 8 -6 3 232.62 20.24 8 -5 -9 11.00 3.09 8 -5 -9 8.13 3.03 8 -5 -8 414.16 24.13 8 -5 -8 453.82 25.91 8 -5 -7 30.58 6.11 8 -5 -7 27.89 6.25 8 -5 -6 524.00 30.52 8 -5 -5 19.09 5.43 8 -5 -4 399.41 27.20 8 -5 -3 -1.26 2.95 8 -5 -3 1.45 2.64 8 -5 -2 571.93 38.00 8 -5 -1 6.63 4.60 8 -5 0 495.74 34.97 8 -5 1 77.46 12.38 8 -5 2 283.37 23.65 8 -5 3 12.48 4.55 8 -4 -9 367.45 22.70 8 -4 -8 97.53 10.44 8 -4 -8 89.07 11.09 8 -4 -7 306.64 21.19 8 -4 -6 117.58 12.89 8 -4 -5 419.57 27.58 8 -4 -4 73.40 10.99 8 -4 -3 518.66 34.82 8 -4 -2 40.57 9.25 8 -4 -1 306.97 26.67 8 -4 0 101.25 14.65 8 -4 1 173.90 18.34 8 -4 2 36.44 8.21 8 -3 -10 231.76 14.94 8 -3 -10 230.72 16.06 8 -3 -9 129.57 12.92 8 -3 -9 130.39 11.82 8 -3 -8 261.39 18.53 8 -3 -8 237.10 17.64 8 -3 -7 263.16 19.69 8 -3 -6 407.95 26.64 8 -3 -5 196.48 17.70 8 -3 -4 307.80 23.00 8 -2 -10 178.24 13.43 8 -2 -10 158.79 13.35 8 -2 -9 119.00 12.45 8 -2 -9 141.15 12.59 8 -2 -8 169.11 14.77 8 -2 -7 133.53 14.99 8 -2 -7 171.00 15.38 8 -2 -7 134.73 13.45 8 -2 -6 248.86 19.77 8 -2 -6 247.87 18.85 8 -2 -5 337.25 23.96 8 -2 7 33.87 5.36 8 -2 7 38.02 5.64 8 -2 8 60.01 6.52 8 -1 -10 55.45 7.23 8 -1 -9 258.61 18.19 8 -1 -8 33.88 7.65 8 -1 -8 38.91 6.90 8 -1 -7 387.67 27.37 8 -1 -7 359.69 23.72 8 -1 -6 176.70 15.62 8 -1 -5 426.24 26.14 8 -1 0 24.62 5.94 8 -1 1 372.96 24.92 8 -1 2 32.65 7.11 8 -1 3 366.28 24.49 8 -1 4 12.32 4.23 8 -1 5 121.24 11.77 8 -1 6 1.35 1.87 8 -1 7 60.65 6.62 8 0 -10 181.53 13.57 8 0 -9 33.29 7.30 8 0 -9 37.53 6.33 8 0 -8 176.24 17.63 8 0 -8 178.88 15.00 8 0 -7 45.01 9.03 8 0 -7 40.28 7.14 8 0 -6 420.28 29.38 8 0 -6 399.53 25.14 8 0 0 308.21 21.77 8 0 1 4.12 3.05 8 0 2 245.77 18.98 8 0 3 13.01 4.58 8 0 4 177.55 14.42 8 0 5 13.02 3.82 8 0 6 96.01 8.63 8 1 -9 188.38 16.16 8 1 -9 173.02 13.70 8 1 -8 1.22 2.85 8 1 -8 3.27 2.42 8 1 -7 364.12 26.86 8 1 -7 337.00 21.91 8 1 -6 8.36 5.06 8 1 -5 390.62 28.44 8 1 -4 16.10 5.99 8 1 -1 235.16 17.85 8 1 0 18.97 5.29 8 1 1 366.01 23.47 8 1 2 50.01 7.81 8 1 3 141.87 12.52 8 1 4 6.65 2.88 8 1 5 51.97 6.10 8 2 -9 3.28 2.43 8 2 -9 1.85 1.82 8 2 -8 295.20 21.49 8 2 -8 283.89 18.08 8 2 -7 44.39 8.52 8 2 -7 34.68 5.99 8 2 -6 227.62 20.33 8 2 -5 109.48 13.66 8 2 -2 195.69 15.37 8 2 -1 23.65 5.29 8 2 0 248.11 17.70 8 2 1 59.66 8.02 8 2 2 55.29 7.29 8 2 3 29.43 4.99 8 3 -7 173.07 14.54 8 3 -7 139.66 11.36 8 3 -6 88.10 9.87 8 3 -3 73.34 8.26 8 3 -2 82.63 9.01 8 3 -1 90.80 9.48 8 3 0 154.06 12.35 8 3 1 80.13 8.28 8 3 2 53.60 6.22 8 4 -3 95.25 8.62 8 4 -2 67.13 7.22 9 -8 -2 0.88 2.06 9 -8 -1 219.27 18.94 9 -8 0 5.37 3.73 9 -8 1 302.26 24.02 9 -8 2 24.01 6.27 9 -8 3 178.92 15.13 9 -7 -4 278.62 17.97 9 -7 -3 26.56 5.38 9 -7 -2 302.41 22.05 9 -7 -1 9.03 4.49 9 -7 0 174.42 18.12 9 -7 1 27.34 7.01 9 -7 2 183.84 16.77 9 -6 -5 128.50 11.13 9 -6 -4 39.68 6.43 9 -5 -6 21.35 4.32 9 -5 -6 33.10 5.52 9 -5 -5 186.23 14.26 9 -4 -7 25.99 4.96 9 -4 -5 89.00 9.61 9 -4 4 111.69 11.23 9 -4 5 2.05 2.03 9 -3 -6 9.73 3.72 9 -3 3 195.96 15.05 9 -3 4 0.71 1.65 9 -3 5 145.99 11.24 9 -2 -6 389.31 24.47 9 -2 -5 5.85 3.39 9 -2 2 301.52 19.11 9 -2 3 10.42 3.35 9 -2 4 104.61 9.57 9 -1 -6 36.77 6.98 9 -1 -5 255.07 19.65 9 -1 -4 56.62 9.05 9 -1 2 87.03 8.84 9 -1 3 83.63 8.29 9 0 -6 114.49 12.16 9 0 -5 47.64 6.38 9 0 -5 67.61 9.52 9 0 -4 97.77 11.85 9 0 1 78.95 8.06 0 0 0 0.00 0.00 TITL lm_2020_03 in P1 REM P1 (#1 in standard setting) CELL 1.54184 8.075105 11.620071 14.454006 103.8004 92.7041 107.1225 ZERR 6.00 0.000193 0.000240 0.000248 0.0016 0.0017 0.0020 LATT -1 SFAC C H N O F P Cl Ir UNIT 6.00 6.00 6.00 6.00 36.00 6.00 6.00 6.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 7253 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C9 C 0.4532(8) 0.4634(5) 0.7450(4) 0.0524(13) Uani 1 1 d . . . . . H9 H 0.3692 0.4537 0.7869 0.063 Uiso 1 1 calc R U . . . C10 C 0.5326(8) 0.3721(5) 0.7194(4) 0.0549(13) Uani 1 1 d . . . . . H10 H 0.5039 0.3032 0.7446 0.066 Uiso 1 1 calc R U . . . C11 C 0.6549(7) 0.3845(5) 0.6561(3) 0.0461(11) Uani 1 1 d . . . . . C12 C 0.7537(9) 0.2915(5) 0.6250(5) 0.0619(15) Uani 1 1 d . . . . . H12A H 0.7528 0.2728 0.5559 0.074 Uiso 1 1 calc R U . . . H12B H 0.8744 0.3291 0.6542 0.074 Uiso 1 1 calc R U . . . C13 C 0.6921(7) 0.4872(5) 0.6192(3) 0.0424(10) Uani 1 1 d . . . . . H13 H 0.7734 0.4972 0.5759 0.051 Uiso 1 1 calc R U . . . C14 C 0.6074(6) 0.5755(4) 0.6473(3) 0.0357(9) Uani 1 1 d . . . . . C15 C 0.6329(6) 0.6841(4) 0.6084(3) 0.0361(9) Uani 1 1 d . . . . . C16 C 0.7426(6) 0.7101(5) 0.5402(3) 0.0417(10) Uani 1 1 d . . . . . H16 H 0.8112 0.6598 0.5191 0.050 Uiso 1 1 calc R U . . . C17 C 0.7505(7) 0.8107(5) 0.5034(3) 0.0460(11) Uani 1 1 d . . . . . C18 C 0.8739(9) 0.8387(6) 0.4306(4) 0.0614(15) Uani 1 1 d . . . . . H18A H 0.9935 0.8677 0.4614 0.074 Uiso 1 1 calc R U . . . H18B H 0.8583 0.7630 0.3802 0.074 Uiso 1 1 calc R U . . . C19 C 0.6483(8) 0.8839(5) 0.5373(4) 0.0569(14) Uani 1 1 d . . . . . H19 H 0.6508 0.9524 0.5141 0.068 Uiso 1 1 calc R U . . . C20 C 0.5428(8) 0.8547(5) 0.6056(4) 0.0523(13) Uani 1 1 d . . . . . H20 H 0.4731 0.9041 0.6270 0.063 Uiso 1 1 calc R U . . . C21 C 0.3948(7) 0.8926(4) 0.8368(3) 0.0486(12) Uani 1 1 d . . . . . C22 C 0.2171(7) 0.8155(5) 0.8159(3) 0.0485(12) Uani 1 1 d . . . . . C23 C 0.2009(7) 0.7102(5) 0.8550(3) 0.0486(12) Uani 1 1 d . . . . . C24 C 0.3666(7) 0.7240(5) 0.9011(3) 0.0487(12) Uani 1 1 d . . . . . C25 C 0.4911(7) 0.8332(5) 0.8863(3) 0.0496(12) Uani 1 1 d . . . . . C26 C 0.6810(8) 0.8873(7) 0.9258(4) 0.0726(18) Uani 1 1 d . . . . . H26A H 0.7245 0.8219 0.9351 0.109 Uiso 1 1 calc R U . . . H26B H 0.6949 0.9481 0.9861 0.109 Uiso 1 1 calc R U . . . H26C H 0.7452 0.9266 0.8813 0.109 Uiso 1 1 calc R U . . . C27 C 0.4088(10) 0.6412(6) 0.9581(4) 0.0733(19) Uani 1 1 d . . . . . H27A H 0.3203 0.5610 0.9399 0.110 Uiso 1 1 calc R U . . . H27B H 0.4129 0.6785 1.0254 0.110 Uiso 1 1 calc R U . . . H27C H 0.5201 0.6313 0.9454 0.110 Uiso 1 1 calc R U . . . C28 C 0.0322(8) 0.6091(6) 0.8533(4) 0.0672(17) Uani 1 1 d . . . . . H28A H -0.0265 0.5756 0.7888 0.101 Uiso 1 1 calc R U . . . H28B H -0.0411 0.6435 0.8942 0.101 Uiso 1 1 calc R U . . . H28C H 0.0571 0.5438 0.8756 0.101 Uiso 1 1 calc R U . . . C29 C 0.0697(9) 0.8399(7) 0.7664(5) 0.0760(19) Uani 1 1 d . . . . . H29A H 0.1118 0.8824 0.7186 0.114 Uiso 1 1 calc R U . . . H29B H 0.0212 0.8909 0.8125 0.114 Uiso 1 1 calc R U . . . H29C H -0.0189 0.7621 0.7361 0.114 Uiso 1 1 calc R U . . . C30 C 0.4705(10) 1.0168(6) 0.8159(5) 0.0713(18) Uani 1 1 d . . . . . H30A H 0.5896 1.0281 0.8044 0.107 Uiso 1 1 calc R U . . . H30B H 0.4662 1.0821 0.8699 0.107 Uiso 1 1 calc R U . . . H30C H 0.4041 1.0197 0.7602 0.107 Uiso 1 1 calc R U . . . N2 N 0.4923(5) 0.5655(4) 0.7119(3) 0.0406(9) Uani 1 1 d . . . . . N1 N 0.5351(5) 0.7583(4) 0.6429(3) 0.0411(9) Uani 1 1 d . . . . . O1 O 0.8426(8) 0.9303(5) 0.3903(3) 0.0875(16) Uani 1 1 d . . . . . H1 H 0.8531 0.9133 0.3329 0.131 Uiso 1 1 calc R U . . . O2 O 0.6818(7) 0.1800(4) 0.6508(4) 0.0845(14) Uani 1 1 d . . . . . H2 H 0.7405 0.1804 0.6988 0.127 Uiso 1 1 calc R U . . . F10 F 1.0052(9) 0.1422(5) 0.9322(4) 0.148(3) Uani 1 1 d . . . . . F11 F 1.2062(7) 0.1879(6) 0.8350(4) 0.130(2) Uani 1 1 d . . . . . F12 F 0.9252(6) 0.1069(4) 0.7760(3) 0.0887(12) Uani 1 1 d . . . . . F13 F 1.0722(7) 0.3051(4) 0.7862(3) 0.1015(14) Uani 1 1 d . . . . . F14 F 0.8710(7) 0.2590(6) 0.8820(4) 0.132(2) Uani 1 1 d . . . . . F15 F 1.1526(7) 0.3398(4) 0.9430(3) 0.1027(15) Uani 1 1 d . . . . . P4 P 1.0385(2) 0.22377(14) 0.86175(10) 0.0534(3) Uani 1 1 d . . . . . Cl1 Cl 0.15851(18) 0.58046(15) 0.61426(9) 0.0636(4) Uani 1 1 d . . . . . Ir1 Ir 0.37653(2) 0.70736(2) 0.74732(2) 0.03659(8) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C9 0.063(3) 0.050(3) 0.053(3) 0.017(2) 0.025(3) 0.024(3) C10 0.070(4) 0.042(3) 0.060(3) 0.019(2) 0.016(3) 0.023(3) C11 0.052(3) 0.042(3) 0.044(2) 0.004(2) 0.000(2) 0.022(2) C12 0.071(4) 0.051(3) 0.075(4) 0.017(3) 0.008(3) 0.035(3) C13 0.046(3) 0.044(3) 0.044(2) 0.011(2) 0.011(2) 0.025(2) C14 0.036(2) 0.039(2) 0.032(2) 0.0044(17) 0.0066(17) 0.0155(19) C15 0.036(2) 0.037(2) 0.035(2) 0.0032(17) 0.0074(17) 0.0146(19) C16 0.041(3) 0.046(3) 0.040(2) 0.008(2) 0.0141(19) 0.017(2) C17 0.054(3) 0.049(3) 0.034(2) 0.010(2) 0.013(2) 0.015(2) C18 0.074(4) 0.061(3) 0.053(3) 0.019(3) 0.032(3) 0.020(3) C19 0.081(4) 0.051(3) 0.051(3) 0.022(2) 0.027(3) 0.030(3) C20 0.069(4) 0.053(3) 0.053(3) 0.020(2) 0.025(3) 0.038(3) C21 0.059(3) 0.034(2) 0.046(3) -0.001(2) 0.017(2) 0.012(2) C22 0.049(3) 0.048(3) 0.047(3) 0.001(2) 0.020(2) 0.020(2) C23 0.046(3) 0.048(3) 0.040(2) -0.004(2) 0.021(2) 0.008(2) C24 0.062(3) 0.053(3) 0.030(2) 0.008(2) 0.013(2) 0.018(2) C25 0.045(3) 0.056(3) 0.035(2) -0.003(2) 0.009(2) 0.009(2) C26 0.059(4) 0.081(5) 0.059(3) 0.001(3) 0.004(3) 0.007(3) C27 0.107(6) 0.074(4) 0.039(3) 0.020(3) 0.010(3) 0.024(4) C28 0.056(3) 0.066(4) 0.062(3) 0.004(3) 0.028(3) 0.000(3) C29 0.064(4) 0.089(5) 0.085(4) 0.012(4) 0.010(3) 0.049(4) C30 0.091(5) 0.046(3) 0.072(4) 0.008(3) 0.029(3) 0.019(3) N2 0.049(2) 0.037(2) 0.0413(19) 0.0102(16) 0.0145(17) 0.0210(18) N1 0.045(2) 0.048(2) 0.0368(19) 0.0097(16) 0.0133(16) 0.0234(19) O1 0.130(5) 0.090(3) 0.068(3) 0.042(3) 0.049(3) 0.049(3) O2 0.100(4) 0.057(3) 0.104(4) 0.020(3) 0.000(3) 0.039(3) F10 0.185(6) 0.118(4) 0.107(4) 0.073(3) -0.029(4) -0.031(4) F11 0.083(3) 0.141(5) 0.164(5) 0.005(4) 0.009(3) 0.061(3) F12 0.095(3) 0.077(3) 0.075(2) 0.000(2) -0.005(2) 0.017(2) F13 0.127(4) 0.099(3) 0.080(3) 0.045(2) 0.016(3) 0.020(3) F14 0.083(3) 0.152(5) 0.150(5) -0.005(4) 0.039(3) 0.052(3) F15 0.110(4) 0.089(3) 0.072(2) 0.002(2) 0.003(2) -0.008(3) P4 0.0555(8) 0.0560(8) 0.0468(7) 0.0135(6) 0.0095(6) 0.0144(6) Cl1 0.0487(7) 0.0844(10) 0.0439(6) -0.0078(6) 0.0045(5) 0.0203(7) Ir1 0.03861(13) 0.03932(13) 0.03342(12) 0.00586(8) 0.01179(8) 0.01652(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ir Ir -4.7710 6.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 C9 C10 122.6(5) . . ? N2 C9 H9 118.7 . . ? C10 C9 H9 118.7 . . ? C11 C10 C9 119.2(5) . . ? C11 C10 H10 120.4 . . ? C9 C10 H10 120.4 . . ? C10 C11 C13 118.7(5) . . ? C10 C11 C12 123.5(5) . . ? C13 C11 C12 117.7(5) . . ? O2 C12 C11 112.6(5) . . ? O2 C12 H12A 109.1 . . ? C11 C12 H12A 109.1 . . ? O2 C12 H12B 109.1 . . ? C11 C12 H12B 109.1 . . ? H12A C12 H12B 107.8 . . ? C11 C13 C14 119.5(4) . . ? C11 C13 H13 120.3 . . ? C14 C13 H13 120.3 . . ? N2 C14 C13 121.7(4) . . ? N2 C14 C15 115.1(4) . . ? C13 C14 C15 123.1(4) . . ? N1 C15 C16 121.2(4) . . ? N1 C15 C14 114.5(4) . . ? C16 C15 C14 124.2(4) . . ? C17 C16 C15 120.2(4) . . ? C17 C16 H16 119.9 . . ? C15 C16 H16 119.9 . . ? C19 C17 C16 118.2(4) . . ? C19 C17 C18 122.6(5) . . ? C16 C17 C18 119.2(5) . . ? O1 C18 C17 110.6(5) . . ? O1 C18 H18A 109.5 . . ? C17 C18 H18A 109.5 . . ? O1 C18 H18B 109.5 . . ? C17 C18 H18B 109.5 . . ? H18A C18 H18B 108.1 . . ? C20 C19 C17 119.3(5) . . ? C20 C19 H19 120.4 . . ? C17 C19 H19 120.4 . . ? N1 C20 C19 123.3(5) . . ? N1 C20 H20 118.4 . . ? C19 C20 H20 118.4 . . ? C22 C21 C25 108.0(4) . . ? C22 C21 C30 126.8(6) . . ? C25 C21 C30 125.1(5) . . ? C22 C21 Ir1 70.1(3) . . ? C25 C21 Ir1 69.4(3) . . ? C30 C21 Ir1 128.2(4) . . ? C21 C22 C23 107.9(5) . . ? C21 C22 C29 127.0(6) . . ? C23 C22 C29 125.0(5) . . ? C21 C22 Ir1 71.8(3) . . ? C23 C22 Ir1 70.1(3) . . ? C29 C22 Ir1 125.7(4) . . ? C24 C23 C22 108.2(5) . . ? C24 C23 C28 126.5(5) . . ? C22 C23 C28 125.2(5) . . ? C24 C23 Ir1 72.5(3) . . ? C22 C23 Ir1 71.0(3) . . ? C28 C23 Ir1 126.0(3) . . ? C23 C24 C25 108.6(5) . . ? C23 C24 C27 126.7(5) . . ? C25 C24 C27 124.7(5) . . ? C23 C24 Ir1 69.6(3) . . ? C25 C24 Ir1 69.4(3) . . ? C27 C24 Ir1 127.6(4) . . ? C24 C25 C21 107.1(5) . . ? C24 C25 C26 127.3(5) . . ? C21 C25 C26 125.1(5) . . ? C24 C25 Ir1 72.0(3) . . ? C21 C25 Ir1 71.7(3) . . ? C26 C25 Ir1 127.7(4) . . ? C25 C26 H26A 109.5 . . ? C25 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C25 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C24 C27 H27A 109.5 . . ? C24 C27 H27B 109.5 . . ? H27A C27 H27B 109.5 . . ? C24 C27 H27C 109.5 . . ? H27A C27 H27C 109.5 . . ? H27B C27 H27C 109.5 . . ? C23 C28 H28A 109.5 . . ? C23 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C23 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C22 C29 H29A 109.5 . . ? C22 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C22 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C21 C30 H30A 109.5 . . ? C21 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C21 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C9 N2 C14 118.2(4) . . ? C9 N2 Ir1 124.7(3) . . ? C14 N2 Ir1 117.0(3) . . ? C20 N1 C15 117.7(4) . . ? C20 N1 Ir1 125.5(3) . . ? C15 N1 Ir1 116.7(3) . . ? C18 O1 H1 109.5 . . ? C12 O2 H2 109.5 . . ? F10 P4 F14 90.9(4) . . ? F10 P4 F15 91.4(3) . . ? F14 P4 F15 91.7(3) . . ? F10 P4 F11 91.8(4) . . ? F14 P4 F11 176.7(3) . . ? F15 P4 F11 90.2(3) . . ? F10 P4 F13 178.4(3) . . ? F14 P4 F13 89.7(3) . . ? F15 P4 F13 90.1(3) . . ? F11 P4 F13 87.6(3) . . ? F10 P4 F12 90.3(3) . . ? F14 P4 F12 89.1(3) . . ? F15 P4 F12 178.1(3) . . ? F11 P4 F12 88.9(3) . . ? F13 P4 F12 88.2(2) . . ? N2 Ir1 N1 76.52(15) . . ? N2 Ir1 C23 121.48(19) . . ? N1 Ir1 C23 161.95(19) . . ? N2 Ir1 C25 111.06(19) . . ? N1 Ir1 C25 109.38(18) . . ? C23 Ir1 C25 64.90(19) . . ? N2 Ir1 C22 160.42(18) . . ? N1 Ir1 C22 123.06(18) . . ? C23 Ir1 C22 38.9(2) . . ? C25 Ir1 C22 64.9(2) . . ? N2 Ir1 C21 147.5(2) . . ? N1 Ir1 C21 100.00(17) . . ? C23 Ir1 C21 64.42(19) . . ? C25 Ir1 C21 38.9(2) . . ? C22 Ir1 C21 38.1(2) . . ? N2 Ir1 C24 100.38(17) . . ? N1 Ir1 C24 145.14(19) . . ? C23 Ir1 C24 37.9(2) . . ? C25 Ir1 C24 38.6(2) . . ? C22 Ir1 C24 64.0(2) . . ? C21 Ir1 C24 63.92(19) . . ? N2 Ir1 Cl1 85.13(12) . . ? N1 Ir1 Cl1 85.81(12) . . ? C23 Ir1 Cl1 96.44(14) . . ? C25 Ir1 Cl1 159.64(15) . . ? C22 Ir1 Cl1 95.62(15) . . ? C21 Ir1 Cl1 127.17(16) . . ? C24 Ir1 Cl1 128.88(15) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C9 N2 1.343(6) . ? C9 C10 1.382(7) . ? C9 H9 0.9300 . ? C10 C11 1.377(8) . ? C10 H10 0.9300 . ? C11 C13 1.381(7) . ? C11 C12 1.523(7) . ? C12 O2 1.401(8) . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C13 C14 1.388(6) . ? C13 H13 0.9300 . ? C14 N2 1.349(6) . ? C14 C15 1.466(6) . ? C15 N1 1.359(6) . ? C15 C16 1.384(6) . ? C16 C17 1.381(7) . ? C16 H16 0.9300 . ? C17 C19 1.377(7) . ? C17 C18 1.510(7) . ? C18 O1 1.406(7) . ? C18 H18A 0.9700 . ? C18 H18B 0.9700 . ? C19 C20 1.373(7) . ? C19 H19 0.9300 . ? C20 N1 1.341(6) . ? C20 H20 0.9300 . ? C21 C22 1.423(8) . ? C21 C25 1.446(8) . ? C21 C30 1.501(8) . ? C21 Ir1 2.189(5) . ? C22 C23 1.441(8) . ? C22 C29 1.492(8) . ? C22 Ir1 2.168(5) . ? C23 C24 1.414(8) . ? C23 C28 1.509(7) . ? C23 Ir1 2.156(4) . ? C24 C25 1.437(8) . ? C24 C27 1.505(8) . ? C24 Ir1 2.192(4) . ? C25 C26 1.501(8) . ? C25 Ir1 2.158(5) . ? C26 H26A 0.9600 . ? C26 H26B 0.9600 . ? C26 H26C 0.9600 . ? C27 H27A 0.9600 . ? C27 H27B 0.9600 . ? C27 H27C 0.9600 . ? C28 H28A 0.9600 . ? C28 H28B 0.9600 . ? C28 H28C 0.9600 . ? C29 H29A 0.9600 . ? C29 H29B 0.9600 . ? C29 H29C 0.9600 . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? N2 Ir1 2.098(4) . ? N1 Ir1 2.105(4) . ? O1 H1 0.8200 . ? O2 H2 0.8200 . ? F10 P4 1.532(4) . ? F11 P4 1.569(5) . ? F12 P4 1.605(4) . ? F13 P4 1.590(4) . ? F14 P4 1.545(5) . ? F15 P4 1.568(4) . ? Cl1 Ir1 2.4024(13) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N2 C9 C10 C11 -1.1(9) . . . . ? C9 C10 C11 C13 -0.9(8) . . . . ? C9 C10 C11 C12 178.4(5) . . . . ? C10 C11 C12 O2 12.8(8) . . . . ? C13 C11 C12 O2 -167.9(5) . . . . ? C10 C11 C13 C14 0.6(7) . . . . ? C12 C11 C13 C14 -178.7(5) . . . . ? C11 C13 C14 N2 1.7(7) . . . . ? C11 C13 C14 C15 -177.1(4) . . . . ? N2 C14 C15 N1 -0.5(6) . . . . ? C13 C14 C15 N1 178.4(4) . . . . ? N2 C14 C15 C16 -178.8(4) . . . . ? C13 C14 C15 C16 0.1(7) . . . . ? N1 C15 C16 C17 -2.1(7) . . . . ? C14 C15 C16 C17 176.1(4) . . . . ? C15 C16 C17 C19 0.7(8) . . . . ? C15 C16 C17 C18 178.8(5) . . . . ? C19 C17 C18 O1 -11.7(8) . . . . ? C16 C17 C18 O1 170.2(5) . . . . ? C16 C17 C19 C20 -0.1(9) . . . . ? C18 C17 C19 C20 -178.2(6) . . . . ? C17 C19 C20 N1 1.0(10) . . . . ? C25 C21 C22 C23 1.8(5) . . . . ? C30 C21 C22 C23 -175.5(5) . . . . ? Ir1 C21 C22 C23 61.1(3) . . . . ? C25 C21 C22 C29 179.3(5) . . . . ? C30 C21 C22 C29 2.0(8) . . . . ? Ir1 C21 C22 C29 -121.4(5) . . . . ? C25 C21 C22 Ir1 -59.3(3) . . . . ? C30 C21 C22 Ir1 123.4(5) . . . . ? C21 C22 C23 C24 1.2(5) . . . . ? C29 C22 C23 C24 -176.4(5) . . . . ? Ir1 C22 C23 C24 63.3(3) . . . . ? C21 C22 C23 C28 176.7(4) . . . . ? C29 C22 C23 C28 -0.9(8) . . . . ? Ir1 C22 C23 C28 -121.1(5) . . . . ? C21 C22 C23 Ir1 -62.2(3) . . . . ? C29 C22 C23 Ir1 120.3(5) . . . . ? C22 C23 C24 C25 -3.7(5) . . . . ? C28 C23 C24 C25 -179.2(5) . . . . ? Ir1 C23 C24 C25 58.6(3) . . . . ? C22 C23 C24 C27 175.2(5) . . . . ? C28 C23 C24 C27 -0.2(8) . . . . ? Ir1 C23 C24 C27 -122.4(5) . . . . ? C22 C23 C24 Ir1 -62.4(3) . . . . ? C28 C23 C24 Ir1 122.2(5) . . . . ? C23 C24 C25 C21 4.8(5) . . . . ? C27 C24 C25 C21 -174.2(5) . . . . ? Ir1 C24 C25 C21 63.6(3) . . . . ? C23 C24 C25 C26 177.1(5) . . . . ? C27 C24 C25 C26 -1.9(8) . . . . ? Ir1 C24 C25 C26 -124.1(5) . . . . ? C23 C24 C25 Ir1 -58.8(3) . . . . ? C27 C24 C25 Ir1 122.2(5) . . . . ? C22 C21 C25 C24 -4.1(5) . . . . ? C30 C21 C25 C24 173.3(5) . . . . ? Ir1 C21 C25 C24 -63.8(3) . . . . ? C22 C21 C25 C26 -176.5(5) . . . . ? C30 C21 C25 C26 0.8(8) . . . . ? Ir1 C21 C25 C26 123.7(5) . . . . ? C22 C21 C25 Ir1 59.7(3) . . . . ? C30 C21 C25 Ir1 -122.9(5) . . . . ? C10 C9 N2 C14 3.4(8) . . . . ? C10 C9 N2 Ir1 179.8(4) . . . . ? C13 C14 N2 C9 -3.7(7) . . . . ? C15 C14 N2 C9 175.2(4) . . . . ? C13 C14 N2 Ir1 179.6(3) . . . . ? C15 C14 N2 Ir1 -1.5(5) . . . . ? C19 C20 N1 C15 -2.3(8) . . . . ? C19 C20 N1 Ir1 -179.8(5) . . . . ? C16 C15 N1 C20 2.8(7) . . . . ? C14 C15 N1 C20 -175.5(4) . . . . ? C16 C15 N1 Ir1 -179.4(3) . . . . ? C14 C15 N1 Ir1 2.2(5) . . . . ?