#------------------------------------------------------------------------------
#$Date: 2021-05-09 04:32:20 +0300 (Sun, 09 May 2021) $
#$Revision: 265060 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/73/7707366.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7707366
loop_
_publ_author_name
'Masaryk, Luk\'a\<s'
'Nemec, Ivan'
'Kasparkova, Jana'
'Brabec, Viktor'
'Starha, Pavel'
_publ_section_title
;
 Unexpected solution behaviour of ester-functionalized half-sandwich
 Ru(II) and Ir(III) complexes
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/D1DT00466B
_journal_year                    2021
_chemical_formula_sum            'C22 H26 Cl F6 N2 O2 P Ru'
_chemical_formula_weight         631.94
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2014/7
_audit_update_record
;
2021-02-07 deposited with the CCDC.	2021-05-07 downloaded from the CCDC.
;
_cell_angle_alpha                95.433(2)
_cell_angle_beta                 91.504(2)
_cell_angle_gamma                107.988(2)
_cell_formula_units_Z            2
_cell_length_a                   9.3607(2)
_cell_length_b                   10.5073(3)
_cell_length_c                   13.3311(3)
_cell_measurement_reflns_used    3886
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      68.124
_cell_measurement_theta_min      3.422
_cell_volume                     1239.36(5)
_computing_cell_refinement       'CrysAlisPro 1.171.40.82a (Rigaku OD, 2020)'
_computing_data_collection       'CrysAlisPro 1.171.40.82a (Rigaku OD, 2020)'
_computing_data_reduction        'CrysAlisPro 1.171.40.82a (Rigaku OD, 2020)'
_computing_molecular_graphics    'Olex2 1.3-ac4 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 1.3-ac4 (Dolomanov et al., 2009)'
_computing_structure_refinement  'SHELXL 2018/3 (Sheldrick, 2015)'
_computing_structure_solution    'SHELXS  (Sheldrick, 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.987
_diffrn_measurement_device_type
'XtaLAB Synergy, Single source at home/near, HyPix3000'
_diffrn_measurement_method       '\w scans'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0465
_diffrn_reflns_av_unetI/netI     0.0519
_diffrn_reflns_Laue_measured_fraction_full 0.993
_diffrn_reflns_Laue_measured_fraction_max 0.987
_diffrn_reflns_limit_h_max       11
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            10328
_diffrn_reflns_point_group_measured_fraction_full 0.993
_diffrn_reflns_point_group_measured_fraction_max 0.987
_diffrn_reflns_theta_full        67.684
_diffrn_reflns_theta_max         68.242
_diffrn_reflns_theta_min         3.336
_diffrn_source                   'micro-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    7.352
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.844
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro 1.171.40.82a (Rigaku Oxford Diffraction, 2020)
Empirical absorption correction using spherical harmonics,
implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.693
_exptl_crystal_description       block
_exptl_crystal_F_000             636
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_refine_diff_density_max         0.577
_refine_diff_density_min         -0.800
_refine_diff_density_rms         0.076
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     386
_refine_ls_number_reflns         4489
_refine_ls_number_restraints     97
_refine_ls_restrained_S_all      1.063
_refine_ls_R_factor_all          0.0471
_refine_ls_R_factor_gt           0.0422
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[\s^2^(Fo^2^)+(0.0704P)^2^] where P=(Fo^2^+2Fc^2^)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1127
_refine_ls_wR_factor_ref         0.1172
_reflns_Friedel_coverage         0.000
_reflns_number_gt                3940
_reflns_number_total             4489
_reflns_threshold_expression     'I > 2\s(I)'
_cod_data_source_file            d1dt00466b2.cif
_cod_data_source_block           RuOH
_cod_database_code               7707366
_shelx_shelxl_version_number     2014/7
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_res_file
;

    shelx.res created by SHELXL-2014/7

TITL exp_11 in P1 #1                        New:P-1
CELL  1.54184   9.3607  10.5073  13.3311   95.433   91.504  107.988
ZERR     2.00   0.0002   0.0003   0.0003    0.002    0.002    0.002
LATT   1
SFAC  C    H    CL   F    N    O    P    RU
UNIT  44 52 2 12 4 4 2 2
MERG   2
EXYZ  C29 C29A
EADP  C29 C29A
SADI  P1 F1 P1 F1A P1 F2 P1 F2A P1 F3 P1 F3A P1
sadi  f4 p1 f4a p1 f5 p1 f5a p1 f6 p1 f6a
SIMU  F1 F1A F2 F2A F3 F3A F4 F4A F5 F5A F6 F6A
sadi c29 o1 c29 o1b
FMAP   2
PLAN   20
ACTA
BOND   $H
CONF
L.S.  24
WGHT    0.070400
FVAR       3.53785   0.73410   0.35129
C11   1    0.290795    0.273290    0.198902    11.00000    0.05944    0.04441 =
         0.07279    0.00358    0.01041   -0.00386
AFIX  43
H11   2    0.206733    0.203514    0.212363    11.00000   -1.20000
AFIX   0
C12   1    0.305133    0.403466    0.235262    11.00000    0.06199    0.04532 =
         0.07822    0.00627    0.01700    0.00375
AFIX  43
H12   2    0.229902    0.420102    0.273542    11.00000   -1.20000
AFIX   0
C14   1    0.530511    0.482892    0.160392    11.00000    0.05356    0.04519 =
         0.05150    0.00474    0.00655    0.00820
C15   1    0.521929    0.353921    0.122410    11.00000    0.05623    0.04352 =
         0.05954   -0.00015    0.00427    0.00921
AFIX  43
H15   2    0.597271    0.339147    0.083300    11.00000   -1.20000
AFIX   0
C16   1    0.400555    0.246221    0.142703    11.00000    0.06350    0.04036 =
         0.05638    0.00411   -0.00021    0.00839
C24   1    0.652472    0.602371    0.139509    11.00000    0.05287    0.04338 =
         0.05254    0.00230    0.00295    0.00596
C25   1    0.764060    0.599624    0.075822    11.00000    0.05564    0.04640 =
         0.06147    0.00136    0.00806    0.00969
AFIX  43
H25   2    0.768057    0.517536    0.045332    11.00000   -1.20000
AFIX   0
C26   1    0.871838    0.718516    0.056126    11.00000    0.05058    0.05564 =
         0.05534    0.00588    0.00372    0.00636
C27   1    0.860861    0.837879    0.103313    11.00000    0.06269    0.04809 =
         0.07280    0.01245    0.01452    0.00210
AFIX  43
H27   2    0.930506    0.919478    0.092359    11.00000   -1.20000
AFIX   0
C28   1    0.746591    0.835313    0.166434    11.00000    0.07032    0.03855 =
         0.07898    0.00328    0.01684    0.00329
AFIX  43
H28   2    0.739931    0.916479    0.196917    11.00000   -1.20000
AFIX   0
PART    1
C29   1    0.991286    0.711639   -0.014666    21.00000    0.05542    0.08808 =
         0.07236    0.00158    0.01365    0.00383
AFIX  23
H29A  2    1.055981    0.667803    0.015996    21.00000   -1.20000
H29B  2    0.943527    0.655773   -0.076004    21.00000   -1.20000
AFIX   0
PART    2
C29A  1    0.991286    0.711639   -0.014666   -21.00000    0.05542    0.08808 =
         0.07236    0.00158    0.01365    0.00383
AFIX  23
H29C  2    0.995930    0.776820   -0.062370   -21.00000   -1.20000
H29D  2    1.086896    0.740764    0.024308   -21.00000   -1.20000
AFIX   0
PART    0
C31   1    0.392241    0.105810    0.101869    11.00000    0.08266    0.04251 =
         0.07606    0.00091   -0.00037    0.00876
AFIX  23
H31A  2    0.389871    0.098603    0.028723    11.00000   -1.20000
H31B  2    0.480801    0.085808    0.125955    11.00000   -1.20000
AFIX   0
C63   1    0.580869    0.786243    0.415715    11.00000    0.07398    0.05719 =
         0.04912   -0.00487    0.00647    0.01247
C64   1    0.452674    0.674439    0.428617    11.00000    0.08626    0.05321 =
         0.05695    0.01013    0.01405    0.01389
AFIX  43
H64   2    0.466029    0.601944    0.458233    11.00000   -1.20000
AFIX   0
C65   1    0.306328    0.670638    0.397783    11.00000    0.07889    0.06704 =
         0.05961    0.00265    0.03121    0.01005
AFIX  43
H65   2    0.225273    0.596831    0.409146    11.00000   -1.20000
AFIX   0
C66   1    0.279365    0.776786    0.349720    11.00000    0.07219    0.07842 =
         0.06540   -0.00581    0.02106    0.02911
C67   1    0.407138    0.888869    0.336900    11.00000    0.08890    0.05356 =
         0.06666   -0.00413    0.01981    0.02734
AFIX  43
H67   2    0.393907    0.959974    0.305309    11.00000   -1.20000
AFIX   0
C69   1    0.551275    0.894839    0.370385    11.00000    0.08368    0.03793 =
         0.06104   -0.00721    0.01298    0.00389
AFIX  43
H69   2    0.631069    0.971671    0.363175    11.00000   -1.20000
AFIX   0
C71   1    0.737678    0.794333    0.446753    11.00000    0.08121    0.06690 =
         0.07498    0.00307    0.00598    0.01493
AFIX  13
H71   2    0.801884    0.833726    0.393526    11.00000   -1.20000
AFIX   0
C72   1    0.759518    0.662460    0.458542    11.00000    0.10024    0.09169 =
         0.15613    0.01221   -0.01185    0.03978
AFIX 137
H72A  2    0.708819    0.626330    0.516123    11.00000   -1.50000
H72B  2    0.865023    0.674269    0.468061    11.00000   -1.50000
H72C  2    0.718846    0.601450    0.399073    11.00000   -1.50000
AFIX   0
C73   1    0.788172    0.892915    0.543218    11.00000    0.11752    0.11247 =
         0.09892   -0.02306   -0.03094    0.03859
AFIX 137
H73A  2    0.721164    0.861938    0.595330    11.00000   -1.50000
H73B  2    0.786371    0.980526    0.529618    11.00000   -1.50000
H73C  2    0.888512    0.897840    0.564942    11.00000   -1.50000
AFIX   0
C74   1    0.122311    0.765769    0.309391    11.00000    0.08573    0.12632 =
         0.10416   -0.00520    0.01573    0.04995
AFIX 137
H74A  2    0.129266    0.822257    0.256005    11.00000   -1.50000
H74B  2    0.068327    0.794026    0.362780    11.00000   -1.50000
H74C  2    0.070039    0.674057    0.283890    11.00000   -1.50000
AFIX   0
CL1   3    0.337957    0.720756    0.110416    11.00000    0.08819    0.07745 =
         0.06249    0.00113    0.00195    0.03388
PART    1
F2    4    0.226210    0.823798    0.768151    31.00000    0.16425    0.15080 =
         0.15090   -0.09519    0.06652   -0.06446
F6    4    0.335085    0.754825    0.659137    31.00000    0.08137    0.22991 =
         0.18173    0.05794    0.04191    0.04315
F3    4    0.166897    0.829502    0.608210    31.00000    0.11404    0.08939 =
         0.25380    0.09087   -0.07335   -0.02685
F1    4    0.111091    0.606969    0.592625    31.00000    0.18683    0.09638 =
         0.10673   -0.03344    0.03057    0.02423
F4    4    0.011173    0.702860    0.706390    31.00000    0.05002    0.19931 =
         0.20946   -0.00846    0.05932   -0.00470
F5    4    0.176065    0.609031    0.756675    31.00000    0.15997    0.09584 =
         0.21313    0.04713   -0.09264    0.02135
PART    0
N1    5    0.643863    0.720110    0.185966    11.00000    0.05838    0.04122 =
         0.05494    0.00223    0.00941    0.00542
N2    5    0.424442    0.508173    0.217471    11.00000    0.05644    0.03874 =
         0.06094    0.00191    0.01190    0.00499
PART    1
O1    6    1.076392    0.830171   -0.039301    21.00000    0.08716    0.06697 =
         0.09085    0.00706    0.03968    0.00061
AFIX 147
H1    2    1.122795    0.818415   -0.088817    21.00000   -1.50000
AFIX   0
PART    2
O1B   6    0.980315    0.603635   -0.063186   -21.00000    0.09755    0.06599 =
         0.09478    0.01335    0.04975    0.01151
AFIX 147
H1B   2    1.042028    0.615434   -0.106691   -21.00000   -1.50000
AFIX   0
PART    0
O2    6    0.263186    0.013491    0.132937    11.00000    0.11627    0.04092 =
         0.14479   -0.00471    0.03834   -0.00623
AFIX   3
H32   2    0.257156   -0.063869    0.111517    11.00000   -1.50000
AFIX   0
P4    7    0.167168    0.717813    0.683023    11.00000    0.06517    0.06313 =
         0.07091    0.00756    0.01231    0.00635
RU1   8    0.453838    0.708378    0.269839    11.00000    0.05866    0.03880 =
         0.05569    0.00226    0.01203    0.00818
PART    2
F1A   4    0.038462    0.605398    0.622311   -31.00000    0.15657    0.11538 =
         0.17986    0.01815   -0.06776   -0.05033
F2A   4    0.289782    0.836080    0.749846   -31.00000    0.12845    0.08684 =
         0.13871    0.00281   -0.05630   -0.00458
F5A   4    0.050011    0.786478    0.724311   -31.00000    0.16729    0.22750 =
         0.19952    0.05601    0.06302    0.13870
F6A   4    0.287107    0.653357    0.650397   -31.00000    0.16585    0.14961 =
         0.15245    0.00543    0.05066    0.09897
F3A   4    0.189259    0.799753    0.592715   -31.00000    0.16507    0.10781 =
         0.07789    0.02896    0.03615    0.01993
F4A   4    0.140585    0.635777    0.773748   -31.00000    0.19963    0.15026 =
         0.13433    0.08433    0.07906    0.07374
HKLF    4

REM  exp_11 in P1 #1                        New:P-1
REM R1 =  0.0422 for    3940 Fo > 4sig(Fo)  and  0.0471 for all    4489 data
REM    386 parameters refined using     97 restraints

END

WGHT      0.0704      0.0000

REM Highest difference peak  0.577,  deepest hole -0.800,  1-sigma level  0.076
Q1    1   0.5326  0.6971  0.3272  11.00000  0.05    0.58
Q2    1   0.4586  0.6571  0.2003  11.00000  0.05    0.56
Q3    1   0.3988  0.7226  0.2070  11.00000  0.05    0.55
Q4    1   0.4490  0.7515  0.3394  11.00000  0.05    0.49
Q5    1   0.4334  0.6579  0.3617  11.00000  0.05    0.39
Q6    1   0.1261  0.6945  0.5844  11.00000  0.05    0.39
Q7    1   0.5234  0.8224  0.3383  11.00000  0.05    0.38
Q8    1   0.2953  0.7208  0.1591  11.00000  0.05    0.32
Q9    1   0.2049  0.6442  0.6185  11.00000  0.05    0.29
Q10   1   0.8460  1.0595  0.6055  11.00000  0.05    0.28
Q11   1   0.3136  0.6441  0.1236  11.00000  0.05    0.27
Q12   1   0.5785  0.7178  0.1230  11.00000  0.05    0.27
Q13   1   0.3518  0.6623  0.0356  11.00000  0.05    0.25
Q14   1   0.3540  0.5021  0.1640  11.00000  0.05    0.23
Q15   1   0.5513  0.6888  0.4224  11.00000  0.05    0.22
Q16   1   0.2482 -0.0033  0.1526  11.00000  0.05    0.22
Q17   1   0.5968  0.4084  0.0185  11.00000  0.05    0.22
Q18   1   0.5309  0.6719  0.5622  11.00000  0.05    0.22
Q19   1   0.5330  0.5151  0.2521  11.00000  0.05    0.22
Q20   1   0.5830  0.8388  0.6013  11.00000  0.05    0.22
;
_shelx_res_checksum              34581
_shelx_hkl_file
;
  -9   5   8 1252.89 151.200  46
  -9   6   8 9.78530 55.7061  46
  -9   7  -8 109.724 61.6414  53
  -9   7   7 10.4330 57.3798  46
  -9   8  -7 41.4661 54.5516  53
  -9   8   6-29.0361 62.0262  46
  -8  -2  -8 368.549 69.7392  17
  -8  -1  -9-23.7609 41.8892  17
  -8   0  -9 88.2225 52.0045  17
  -8   1 -10 19.3134 36.6603  29
  -8   2 -10 283.399 63.7530  29
  -8   3 -10 34.9314 42.3734  29
  -8   5   9 524.541 112.779  46
  -8   5  10 423.532 84.1219  46
  -8   6 -10 238.048 69.6429  53
  -8   6  -9 89.2871 80.4853  53
  -8   6   8-68.5586 79.4173  46
  -8   6   9 2297.79 214.571  46
  -8   6  10 152.495 57.0864  46
  -8   7  -9 137.438 68.7763  53
  -8   7   8 1562.49 175.433  46
  -8   7   9 17.2846 47.5366  46
  -8   8  -9 58.8532 47.3245   7
  -8   8  -9 136.437 63.1666  53
  -8   8  -8 895.155 127.901  53
  -8   8   6 476.135 110.335  46
  -8   8   7 937.201 133.301  46
  -8   8   8 476.776 86.4073  46
  -8   8   8 511.839 87.5310  27
  -8   9  -8 57.9991 48.3315   7
  -8   9  -7 812.311 112.601   7
  -8   9  -6 1733.61 180.756   7
  -8   9   6 736.393 121.320  27
  -8   9   7 570.473 91.5976  27
  -8  10   5 163.404 60.4954  27
  -8  11  -3 121.890 70.7876  30
  -8  11  -2 257.059 94.7184  30
  -8  11  -1 831.592 147.231  30
  -8  11   0 27.4696 66.9689  30
  -8  11   1 836.284 128.083  30
  -7  -3  -9 291.031 56.6504  17
  -7  -3  -8 1933.49 170.056  17
  -7  -2 -10 10.6270 36.6354  17
  -7  -2  -9 1676.32 158.338  17
  -7  -1 -10 624.282 93.9283  17
  -7   0 -11 39.1200 42.3914  29
  -7   0 -11 61.4735 41.5536  17
  -7   0 -10 885.451 116.526  17
  -7   1 -11 90.7783 49.3023  29
  -7   2 -12 595.608 80.5076  29
  -7   2 -11 8.23050 44.4506  29
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   1   7  -5 28458.2 1611.82   7
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   2   0   3 26405.6 1469.65  44
   2   0   4 95640.8 4976.78  36
   2   0   5 3335.34 392.977  36
   2   0   6 18630.5 1264.44  36
   2   0   7 149.275 109.949  36
   2   0   8 5750.23 615.273  36
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   2   7   4 28657.4 1606.95  23
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   2   7   6 8547.93 592.494  37
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   3  -4   6 9876.39 780.386  43
   3  -4   7 6659.79 657.000  43
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   3  -2   7 70.6848 66.1277  45
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   3  -1  -9 518.121 114.363  17
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   3  -1  -8 11537.7 681.861  17
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   3  -1  -5 31302.7 1813.95  18
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   3  -1  -2 27333.6 1605.74  18
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   3  -1   0 51223.3 2626.83  48
   3  -1   0 47795.0 2570.75  13
   3  -1   0 50611.1 2764.27   2
   3  -1   0 50083.8 2613.65  18
   3  -1   1 33137.6 1768.18  36
   3  -1   1 31153.8 1750.64  48
   3  -1   1 35644.5 1908.55   2
   3  -1   2 227.928 83.1645  36
   3  -1   2 23.6743 92.3076   2
   3  -1   3 38594.0 2098.17  36
   3  -1   4 229.144 104.417  36
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   3  -1   6 2875.80 400.092  36
   3  -1   7 6557.41 457.115  45
   3  -1   7 7885.04 731.236  36
   3  -1   8 2541.83 224.411  26
   3  -1   8 2442.13 238.989  45
   3  -1   9 6057.85 419.299  26
   3  -1   9 6452.50 442.076  45
   3  -1  10 6419.45 445.258  45
   3  -1  11 5794.39 410.626  45
   3  -1  12 2379.37 225.254  45
   3  -1  13 10.7712 50.0673  45
   3  -1  14 372.710 78.9079  45
   3  -1  15 112.050 47.7786  45
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   3   0  -5 47828.8 2615.33  13
   3   0  -5 45877.2 2681.00  39
   3   0  -4 5338.42 448.830  13
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   3   0  -3 81041.6 4064.76  13
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   3   0  -2 6415.62 544.509   2
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   3   0  -2 5485.54 484.920  39
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   3   0  -1 103846. 5287.57  20
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   3   0  -1 104919. 5465.88   2
   3   0  -1 106982. 5294.70  36
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   3   0   0 7410.93 642.328   2
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   3   0   1 1442.83 245.737   2
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   3   0   2 27431.9 1509.20   2
   3   0   3 8050.48 583.328  44
   3   0   3 8229.32 594.960  36
   3   0   4 38593.9 2166.91  44
   3   0   4 40588.2 2235.94  36
   3   0   5 3040.02 363.946  44
   3   0   5 2827.32 382.347  36
   3   0   6 27343.6 1693.17  44
   3   0   6 24673.4 1687.56  36
   3   0   7 373.675 182.678  44
   3   0   7 471.129 92.3696  26
   3   0   7 600.981 210.331  36
   3   0   7 298.260 88.0732  45
   3   0   8 205.617 151.216  44
   3   0   8 239.517 157.542  36
   3   0   8 116.532 59.6001  26
   3   0   8 65.4159 72.1717  45
   3   0   9 1345.13 304.065  36
   3   0   9 1984.73 206.832  45
   3   0   9 1774.41 187.857  26
   3   0  10 4367.60 340.561  45
   3   0  10 4511.96 332.959  26
   3   0  11 47.9093 63.5791  45
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   3   1  -2 79971.1 4098.49  13
   3   1  -1 48.4033 55.6280  13
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   3   1   3 31783.3 1911.75  36
   3   1   4 27655.9 1614.43  44
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   3   1   5 41885.0 2318.27  44
   3   1   5 37508.5 2352.48  36
   3   1   6 7923.45 700.526  44
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   3   1   8 4929.77 347.888  27
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   3   1  10 743.253 121.008  26
   3   1  11 7556.92 493.324  26
   3   1  12 192.683 74.1722  26
   3   1  13 767.905 110.297  26
   3   1  14 115.134 48.1975  26
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   3   2   6 3480.59 472.163  44
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   3   2   7 114.875 158.063  44
   3   2   7 109.579 67.2455  27
   3   2   7 222.685 153.210  36
   3   2   8 1567.75 369.532  44
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   3   2   9 874.517 134.923  26
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   3   2  10 10156.0 627.546  26
   3   2  11 2459.40 230.431  26
   3   2  12 2033.53 196.306  26
   3   2  13 9.15175 43.5902  26
   3   2  14 248.396 55.8439  26
   3   3 -15 1118.59 118.432   8
   3   3 -14 19.4454 57.1709   4
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   3   3   4 64474.1 3248.45  36
   3   3   4 60560.7 2913.41  34
   3   3   4 57920.4 3166.46  20
   3   3   5 11870.7 1049.20  36
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   3   3   6 10035.5 618.349  27
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   3   3   7 4075.84 596.082  36
   3   3   7 3551.20 320.839  26
   3   3   7 4549.93 333.875  27
   3   3   7 4320.08 618.052  44
   3   3   8 118.436 137.693  36
   3   3   8 210.049 205.871  44
   3   3   8 27.7468 67.7732  26
   3   3   8 146.465 79.6178  27
   3   3   9 5699.68 406.795  26
   3   3  10 545.506 108.762  26
   3   3  11 3051.00 253.743  26
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   3   4  -8 30141.5 1566.73  53
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   3   4   6 176.609 150.825  20
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   3   4   7 7674.52 515.042  27
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   3   5   2 25045.4 1449.47  34
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   3   6   4-15.1977 65.1292  37
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   3   6   5 4498.37 387.032  37
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   3   6   6-75.0643 89.3912  37
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   3   6   8 158.283 85.8332  37
   3   6   9 2145.47 212.650  37
   3   6  10 353.744 76.3196  37
   3   6  11 649.688 83.2232  37
   3   7 -12 870.955 98.6110  24
   3   7 -11 568.486 97.8116  24
   3   7 -11 489.119 91.7602   9
   3   7 -10 1280.37 160.359  24
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   3   7 -10 1699.38 192.046  53
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   3   7  -8 3488.96 303.887  24
   3   7  -8 3327.23 328.347  29
   3   7  -7 2312.63 257.384   6
   3   7  -7 2079.14 224.730  24
   3   7  -7 2725.66 272.748  29
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   4   0 -11 8759.71 560.474  17
   4   0 -11 8295.64 552.522  40
   4   0 -10 2651.51 258.352  32
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   4   0   5 27243.7 1738.37  36
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   4   0   7 89.5977 63.9083  12
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   4   0  13 323.259 73.4215  26
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   4   1  -8 73.8842 64.0428  40
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   4   1   3 14250.4 953.107  36
   4   1   3 12924.0 928.502  20
   4   1   4 19029.7 1204.93  36
   4   1   4 15585.0 1128.34  20
   4   1   5 8255.41 523.900  26
   4   1   5 9700.06 555.889  12
   4   1   5 7891.75 529.730  52
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   4   1   6 99.2354 67.0244  12
   4   1   6 106.197 123.420  36
   4   1   6 50.4736 65.6083  26
   4   1   7 2241.09 424.634  44
   4   1   7 1908.55 196.505  12
   4   1   7 1471.58 351.443  36
   4   1   7 1605.82 196.675  26
   4   1   8 65.1826 151.562  44
   4   1   8-59.2312 87.1951  36
   4   1   8 303.522 95.1304  26
   4   1   9 4788.49 366.956  26
   4   1  10 12.7096 61.9610  26
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   4   1  12 397.466 87.5996  26
   4   1  13 946.083 114.134  26
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   4   2   3 23692.0 1441.12  36
   4   2   4 2266.22 355.418  36
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   4   2   4 2500.37 222.844  37
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   4   2   5 33995.2 1894.11  52
   4   2   5 40542.2 1918.89  12
   4   2   5 33420.7 2183.02  20
   4   2   5 34230.2 1886.02  26
   4   2   5 39383.6 2300.49  36
   4   2   6 2799.72 263.765  26
   4   2   6 3047.35 492.041  36
   4   2   7 3497.17 303.901  26
   4   2   7 2679.65 500.675  36
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   4   2   8 5925.72 755.192  36
   4   2   9 1685.92 196.267  26
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   4   3  -8 459.181 127.749   4
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   4   3   0 17908.0 1050.18  14
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   4   3   1 1561.19 271.790  20
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   4   3   2 8744.06 724.808  20
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   4   3   3 6843.07 472.504  52
   4   3   3 6847.05 654.602  20
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   4   3   5-50.2161 104.394  20
   4   3   5 64.4223 61.3865  23
   4   3   5 28.5081 62.8732  37
   4   3   6 1080.20 315.892  20
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   4   3   6 1918.29 226.682  37
   4   3   7 201.299 170.893  36
   4   3   7 62.9698 69.5860  26
   4   3   7 277.343 216.242  20
   4   3   8 3138.68 289.013  26
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   4   3  10 1394.70 161.271  26
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   4   4  -9 190.144 104.635   4
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   4   4   0 16502.4 974.043  14
   4   4   1 8011.36 870.107  19
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   4   4   1 8460.45 716.367  20
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   4   4   3 37052.5 1978.93  37
   4   4   3 38562.0 2012.84  23
   4   4   3 36022.9 2277.60  20
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   4   4   5 17149.6 944.319  23
   4   4   6 92.8801 88.5911  37
   4   4   7 6020.95 480.792  37
   4   4   8 2348.55 259.218  37
   4   4   9 2714.31 260.300  37
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   4   4  11 347.734 69.9296  37
   4   4  11 271.323 63.4782  26
   4   5 -13 174.668 51.2872  24
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   4   5 -12 1480.81 159.486  24
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   4   5 -11 2134.06 216.541  24
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   4   5  -9 5026.66 435.566  53
   4   5  -9 5880.20 417.329   9
   4   5  -8 724.775 133.345  41
   4   5  -8 527.541 153.094  53
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   4   5  -7 11076.6 702.138  24
   4   5  -7 11998.9 727.832  41
   4   5  -7 11190.4 748.691  53
   4   5  -6 118.672 86.0316  29
   4   5  -6 70.7642 84.4538   6
   4   5  -6 148.983 73.2183  24
   4   5  -6 118.438 93.2281  41
   4   5  -5 13291.9 823.546  41
   4   5  -5 13531.8 841.841   6
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   4   5  -3 20133.6 1082.15  24
   4   5  -2 5642.81 400.989  41
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   4   5   1 2698.87 512.797  19
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   4   5   2 5373.20 418.501  23
   4   5   2 4186.61 529.640  20
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   4   5   3 1656.34 210.352  23
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   4   5   4 5903.42 444.186  23
   4   5   5 9445.39 636.871  37
   4   5   5 9356.13 615.154  23
   4   5   6 989.572 175.838  37
   4   5   7 18.5911 92.6703  37
   4   5   8 2702.35 272.239  37
   4   5   9 1353.52 162.780  37
   4   5  10 1597.38 156.095  37
   4   5  11 25.2122 32.7780  37
   4   6 -12 329.275 67.6659  24
   4   6 -11 559.377 99.1372  24
   4   6 -11 739.849 110.417   9
   4   6 -10 1988.71 209.343  24
   4   6 -10 2131.01 212.964   9
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   5   3   6 7545.95 547.527  37
   5   3   7 184.079 99.8218  37
   5   3   8 4851.73 391.308  37
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   5   4 -13 468.828 76.4319   8
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   6   1   4 5544.87 614.442  36
   6   1   4 5032.46 370.770  33
   6   1   4 4193.97 380.403  52
   6   1   5 59.3338 61.8298  22
   6   1   5 281.932 82.9995  23
   6   1   5 29.7636 69.3157  12
   6   1   5-54.9954 99.1023  36
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   6   1   5 82.1493 72.5857  52
   6   1   6 1230.03 164.647  12
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   6   1   7 6756.54 474.786  52
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   6   4   8 1337.90 148.685  37
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   6   5   2 1750.21 211.398  22
   6   5   2 1651.22 219.245  23
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   6   5   3 4084.20 365.010  22
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   6   5   4 319.313 98.5912  37
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   6   5   7 85.5098 56.7600  37
   6   5   7 65.7407 45.3370  22
   6   5   8 414.145 71.6311  37
   6   5   8 350.319 64.5613  33
   6   6  -9 2505.68 200.716   9
   6   6  -8 190.835 70.3257  10
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   6   6   3 14.5749 62.4818  22
   6   6   3 67.3269 61.0278  23
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   6   6   5 382.798 84.7274  22
   6   6   5 506.340 87.2563  23
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   6   7   0-50.2285 85.2840  21
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   6   7   4-8.60895 37.9707  22
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   7 -11   3 110.504 57.7321  15
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   7 -11   4 546.773 97.4931  15
   7 -11   5-21.0439 48.9170  15
   7 -10  -5-8.83024 46.7982  25
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   7 -10   1 1010.22 144.208  15
   7 -10   2 1090.86 182.034  16
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   7 -10   3 1073.12 162.931  16
   7 -10   3 1070.47 152.037  15
   7 -10   4 111.731 78.3613  15
   7 -10   5 1214.97 167.325  15
   7 -10   6 13.4708 56.0048  15
   7 -10   6 9.83105 45.6981  28
   7 -10   7 672.350 119.458  15
   7 -10   7 980.301 114.089  28
   7 -10   8 6.76438 28.1235  28
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   7  -9   0 647.789 121.899  15
   7  -9   1 1476.85 247.596  16
   7  -9   1 2096.17 216.989  15
   7  -9   2-64.3691 94.6122  16
   7  -9   2 14.8897 55.7981  15
   7  -9   3 267.290 104.962  16
   7  -9   3 62.2242 74.3679  15
   7  -9   4 258.333 94.0114  15
   7  -9   4 562.183 99.0600  28
   7  -9   5 214.075 94.4621  15
   7  -9   5 252.581 78.2023  28
   7  -9   6 1597.11 203.395  15
   7  -9   6 1644.86 177.545  28
   7  -9   7 539.315 123.418  15
   7  -9   7 484.855 92.9435  28
   7  -9   8 378.367 98.0610  15
   7  -8  -6 2485.90 228.885  25
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   7  -8  -4 453.684 99.4422  25
   7  -8  -3 2106.99 206.085  25
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   7  -8  -1 3133.79 345.534  16
   7  -8   0 3980.03 429.852  16
   7  -8   0 4961.79 366.646  15
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   7  -8   1 3137.27 283.273  15
   7  -8   2 2967.64 339.410  16
   7  -8   2 3412.69 298.352  15
   7  -8   3 549.828 98.5259  28
   7  -8   3 644.677 145.992  16
   7  -8   3 490.476 118.375  15
   7  -8   4 1414.17 199.084  15
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   7  -8   5 1381.16 200.992  15
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   7   0   5 8924.78 599.035  12
   7   0   5 8777.00 588.924  33
   7   0   5 8813.69 572.471  45
   7   0   6 33.5753 78.0683  52
   7   0   6 32.7384 65.9372  33
   7   0   6 93.9907 79.7995  12
   7   0   7 2689.74 255.076  52
   7   0   7 1931.43 230.714  33
   7   0   8 601.974 117.125  52
   7   0   8 540.965 110.696  33
   7   0   9 369.799 82.6238  33
   7   1 -12 336.120 63.0984  40
   7   1 -12 267.389 63.9927   8
   7   1 -11 2109.80 186.739  40
   7   1 -11 2445.45 209.526  32
   7   1 -11 2118.21 205.465   8
   7   1 -10 997.015 130.033  40
   7   1 -10 1051.50 152.209  32
   7   1 -10 1091.39 164.077   8
   7   1  -9 4205.89 341.192  32
   7   1  -9 4014.21 319.126   9
   7   1  -9 3342.29 335.964   8
   7   1  -8 445.921 110.122  41
   7   1  -8 168.341 95.2438  32
   7   1  -8 196.002 106.763   8
   7   1  -8 367.321 108.782   9
   7   1  -7 17965.4 1042.78   9
   7   1  -7 17866.6 1055.34   8
   7   1  -7 17472.4 1053.35  42
   7   1  -7 16785.5 1026.67  41
   7   1  -6 577.092 124.002   8
   7   1  -6 464.893 129.442   9
   7   1  -6 736.658 150.583  42
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   7   1  -5 23594.1 1315.90   8
   7   1  -5 20603.5 1329.46   9
   7   1  -5 25552.5 1358.54  42
   7   1  -5 25042.0 1377.55  41
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   7   1  -4 1661.95 212.749   9
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   7   1   0 18022.2 1059.48  22
   7   1   0 19057.0 1106.38  23
   7   1   0 19644.0 1055.56  33
   7   1   1 1256.65 168.297  22
   7   1   1 1104.45 186.414  23
   7   1   1 1169.79 151.600  33
   7   1   1 1215.07 163.242  52
   7   1   2 7667.91 552.078  22
   7   1   2 7715.73 577.495  23
   7   1   2 8096.55 527.916  33
   7   1   2 9047.04 566.445  52
   7   1   3 17.3763 65.1330  22
   7   1   3 17.8524 69.4411  23
   7   1   3 39.8214 61.7156  33
   7   1   3 32.1781 76.6440  12
   7   1   3 51.5275 75.7520  52
   7   1   4 752.597 140.711  22
   7   1   4 515.228 128.529  23
   7   1   4 681.584 131.127  33
   7   1   4 587.758 124.773  12
   7   1   4 431.785 132.743  52
   7   1   5 30.6931 57.5094  22
   7   1   5-15.8975 73.8924  33
   7   1   5-34.6729 91.8756  52
   7   1   6 2057.07 245.236  33
   7   1   6 2669.08 262.608  52
   7   1   7 108.161 74.0880  33
   7   1   7 270.063 89.1712  52
   7   1   8 1373.37 169.235  33
   7   1   8 1224.88 152.269  52
   7   1   9 19.3606 45.0042  33
   7   1  10 546.450 80.6167  33
   7   2 -11 690.877 101.146  32
   7   2 -11 451.688 91.5421   8
   7   2 -10 1216.16 155.518  32
   7   2 -10 1759.16 197.836   8
   7   2 -10 1583.96 165.821   9
   7   2  -9 312.629 94.4986  32
   7   2  -9 202.100 79.9456  41
   7   2  -9 178.134 91.4241   8
   7   2  -9 252.787 80.7277   9
   7   2  -8 1288.53 170.862  32
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   7   2  -8 1219.06 192.150   8
   7   2  -8 1200.45 171.190   9
   7   2  -7 254.455 105.371  41
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   7   2  -7 322.794 115.829  42
   7   2  -7 216.542 100.118   8
   7   2  -7 183.620 99.0286   9
   7   2  -6 3336.16 312.732  41
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   7   2  -6 3285.21 296.945   8
   7   2  -6 2750.57 289.777   9
   7   2  -5 88.9302 63.9625   8
   7   2  -5 163.815 92.9839   9
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   7   2  -5 211.200 103.965  42
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   7   2  -3 4913.75 400.861  42
   7   2  -3 4409.44 375.217  41
   7   2  -3 4214.50 387.717  14
   7   2  -2 911.999 201.472  21
   7   2  -2 765.284 162.082  42
   7   2  -2 887.583 160.813  10
   7   2  -1 1455.55 173.860  22
   7   2  -1 1543.84 255.156  21
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   7   2  -1 1453.51 207.639  10
   7   2   0 12568.9 752.320  22
   7   2   0 12288.1 791.541  23
   7   2   0 12118.3 848.881  21
   7   2   1 8927.33 597.122  22
   7   2   1 8530.22 630.842  23
   7   2   1 9998.13 669.253  21
   7   2   1 9141.25 636.442  14
   7   2   1 9297.30 576.630  33
   7   2   2 6030.75 459.414  22
   7   2   2 5896.87 478.791  23
   7   2   2 6946.31 470.106  52
   7   2   2 5746.82 456.033  14
   7   2   2 6397.01 431.920  33
   7   2   3 3634.74 338.229  22
   7   2   3 4143.94 352.769  23
   7   2   3 3957.78 320.147  33
   7   2   3 4190.28 354.487  52
   7   2   4 1497.90 184.348  23
   7   2   4 1132.70 177.728  22
   7   2   4 1163.41 163.985  33
   7   2   4 1114.56 181.131  52
   7   2   5 4525.61 366.295  22
   7   2   5 4983.05 369.081  23
   7   2   5 4225.96 366.257  33
   7   2   5 4856.59 384.216  52
   7   2   6 62.3727 59.4146  22
   7   2   6-16.0792 70.9020  33
   7   2   6-70.3128 70.0947  52
   7   2   7 2425.76 247.052  33
   7   2   8-45.7611 58.2931  33
   7   2   9 1151.68 127.040  33
   7   2  10-11.5811 26.9204  33
   7   3 -11 911.769 113.129   8
   7   3 -10 1934.77 201.290   8
   7   3 -10 1969.47 181.926   9
   7   3  -9 808.783 116.060  41
   7   3  -9 583.672 126.529   8
   7   3  -9 523.673 101.666   9
   7   3  -8 1440.69 198.365   8
   7   3  -8 1372.78 172.506   9
   7   3  -8 1392.74 167.604  41
   7   3  -7 5782.23 441.114   8
   7   3  -7 5439.19 428.670   9
   7   3  -7 6232.09 437.537  41
   7   3  -6-83.5538 86.8399  41
   7   3  -6 60.5910 72.1459   8
   7   3  -6 69.4146 86.4983   9
   7   3  -5 11344.1 747.646  42
   7   3  -5 12364.4 741.081  41
   7   3  -4 821.569 153.088  14
   7   3  -4 832.269 167.393  42
   7   3  -4 844.296 168.231  21
   7   3  -4 1006.57 185.438  10
   7   3  -4 888.453 157.416  41
   7   3  -3 1344.82 228.826  21
   7   3  -3 1561.46 219.922  10
   7   3  -3 1468.15 227.342  42
   7   3  -3 1679.17 210.387  41
   7   3  -3 1719.27 230.053  14
   7   3  -2 244.698 127.068  21
   7   3  -2 310.720 109.500  10
   7   3  -2 328.556 123.310  42
   7   3  -2 198.142 112.879  14
   7   3  -1 3669.65 413.001  21
   7   3  -1 4379.54 371.521  10
   7   3  -1 4262.15 394.274  14
   7   3   0 2881.71 312.636  14
   7   3   0 2985.61 267.077  22
   7   3   0 3007.15 299.957  23
   7   3   0 3082.17 342.868  21
   7   3   1 2153.58 242.246  14
   7   3   1 1813.31 208.222  22
   7   3   1 1894.85 245.535  21
   7   3   1 1366.52 212.837  23
   7   3   2 3247.32 298.902  22
   7   3   2 2816.65 297.567  23
   7   3   3 1669.32 220.092  22
   7   3   3 1805.50 218.575  23
   7   3   3 1503.48 177.462  33
   7   3   4 499.445 120.788  22
   7   3   4 684.409 123.484  23
   7   3   4 569.300 115.386  33
   7   3   5 1104.49 146.975  23
   7   3   5 1066.63 154.176  22
   7   3   5 920.298 148.935  37
   7   3   5 869.853 147.809  33
   7   3   6 1233.03 148.288  22
   7   3   6 976.684 155.407  33
   7   3   7 415.021 93.7267  33
   7   3   8 2077.38 185.666  33
   7   3   9 352.448 61.7105  33
   7   4 -10 7.55107 35.9661   9
   7   4  -9 859.090 116.301   9
   7   4  -9 921.671 116.465  41
   7   4  -8 65.9451 60.5376  41
   7   4  -8 70.0425 58.2830   9
   7   4  -7 1600.98 191.649   9
   7   4  -7 1820.90 201.657  41
   7   4  -6 1523.96 224.659  10
   7   4  -6 1649.75 202.048   9
   7   4  -6 1807.88 211.987  41
   7   4  -5 2021.44 272.226  10
   7   4  -5 2457.33 254.064  41
   7   4  -4 4918.43 416.244  21
   7   4  -4 4968.71 435.669  10
   7   4  -4 4475.55 374.441  41
   7   4  -4 4793.54 396.930  14
   7   4  -3 2465.51 292.741  21
   7   4  -3 1951.17 250.557  10
   7   4  -3 1994.03 216.293  41
   7   4  -3 1964.13 248.119  14
   7   4  -2 4629.70 418.426  14
   7   4  -2 4672.95 395.718  10
   7   4  -2 4737.90 452.997  21
   7   4  -1 21.3242 91.3796  14
   7   4  -1-17.4840 60.2683  10
   7   4  -1 26.5700 95.6610  21
   7   4   0 9566.84 664.964  23
   7   4   0 10865.0 730.491  21
   7   4   0 9924.16 685.032  14
   7   4   1 28.9045 65.5150  22
   7   4   1 57.2839 84.2300  23
   7   4   1 58.4167 75.7597  21
   7   4   1 51.9120 71.9761  14
   7   4   2 3947.75 342.581  22
   7   4   2 4403.64 369.197  23
   7   4   3 329.193 108.146  22
   7   4   3 353.470 101.154  23
   7   4   4 1617.06 198.709  22
   7   4   4 1705.14 190.580  23
   7   4   5 1722.77 190.662  22
   7   4   5 1795.77 183.380  23
   7   4   6 514.313 99.9595  33
   7   4   6 753.983 106.189  22
   7   4   7 1486.61 147.955  33
   7   4   7 1293.87 128.538  22
   7   5  -8 2105.76 187.220   9
   7   5  -7 1597.87 188.364  10
   7   5  -6 1181.65 183.200  10
   7   5  -5 2683.11 305.250  10
   7   5  -5 3300.60 278.372  41
   7   5  -4 1227.37 164.979  41
   7   5  -4 1156.84 179.681  21
   7   5  -4 1349.10 197.908  10
   7   5  -4 1126.86 170.743  14
   7   5  -3 1479.88 222.131  21
   7   5  -3 1169.65 181.830  10
   7   5  -3 1291.48 195.136  14
   7   5  -2 868.410 182.952  21
   7   5  -2 666.068 132.007  10
   7   5  -2 978.719 169.415  14
   7   5  -1 923.239 186.631  21
   7   5  -1 1029.60 177.942  14
   7   5   0 354.689 125.786  21
   7   5   0 292.515 97.1261  23
   7   5   0 455.493 120.667  14
   7   5   1 1021.46 144.092  22
   7   5   1 1119.42 172.913  23
   7   5   1 1134.35 169.919  21
   7   5   1 894.058 148.827  14
   7   5   2 82.9821 65.9684  22
   7   5   2 61.6360 69.8995  23
   7   5   3 2451.99 246.294  22
   7   5   3 3046.37 258.678  23
   7   5   4 12.1652 56.5494  22
   7   5   4-31.5657 50.1197  23
   7   5   5 1034.19 124.940  22
   7   5   6 276.577 57.2983  22
   7   6  -6-28.4860 59.2290  10
   7   6  -5 2180.17 237.599  10
   7   6  -4 1284.06 178.727  10
   7   6  -3 3310.36 307.211  21
   7   6  -3 2362.77 247.456  10
   7   6  -2 1296.06 208.890  21
   7   6  -2 1923.88 216.882  14
   7   6  -1 451.625 127.691  21
   7   6  -1 440.848 109.511  14
   7   6   0 2775.59 273.369  21
   7   6   1 260.729 84.4982  23
   7   6   2 2934.49 247.096  22
   7   6   2 3564.56 272.615  23
   7   6   3 97.8878 53.1361  22
   7   6   3 121.728 55.3130  23
   7   6   4 1404.81 138.288  22
   8 -11  -1 1080.14 109.886  25
   8 -11  -1 1124.84 140.817  16
   8 -11   0 155.333 48.9766  25
   8 -11   0 115.564 52.4468  15
   8 -11   0 142.019 73.8072  16
   8 -11   1 832.856 95.7992  25
   8 -11   1 885.986 113.197  15
   8 -11   1 679.901 123.355  16
   8 -11   2 71.6469 39.2132  25
   8 -11   2 174.615 56.7328  15
   8 -11   2 94.0937 64.8808  16
   8 -11   3 214.047 60.9851  15
   8 -10  -4 243.433 74.8013  41
   8 -10  -4 423.524 73.4789  25
   8 -10  -3 24.0555 39.9851  25
   8 -10  -2 1875.55 166.142  25
   8 -10  -2 1759.47 192.723  16
   8 -10  -1 97.7212 51.8201  25
   8 -10  -1 203.196 98.9917  16
   8 -10   0 2488.97 192.986  25
   8 -10   0 2048.33 205.890  15
   8 -10   0 2103.75 249.983  16
   8 -10   1 91.9574 56.2568  15
   8 -10   1 126.820 90.4414  16
   8 -10   2 570.783 103.147  15
   8 -10   2 712.812 139.129  16
   8 -10   3 57.2517 54.5647  15
   8 -10   3 12.7827 57.9371  16
   8 -10   4 80.0389 57.1280  15
   8 -10   5 626.566 108.466  15
   8 -10   6 31.2489 48.4393  15
   8  -9  -5 12.3223 62.7487  41
   8  -9  -5 26.9270 46.6544  25
   8  -9  -4 996.605 160.217  41
   8  -9  -4 1638.54 158.865  25
   8  -9  -3 1475.10 157.095  25
   8  -9  -2 652.650 132.772  16
   8  -9  -2 613.385 100.881  25
   8  -9  -1 2613.24 293.571  16
   8  -9  -1 2861.02 228.427  25
   8  -9   0-66.8927 101.068  16
   8  -9   1 1457.44 173.051  15
   8  -9   1 1330.79 221.162  16
   8  -9   2 79.5570 67.6946  15
   8  -9   2 154.030 106.004  16
   8  -9   3 189.600 80.3199  15
   8  -9   3 249.699 93.7727  16
   8  -9   4 1982.40 212.566  15
   8  -9   5 433.039 101.779  15
   8  -9   6 1233.54 164.593  15
   8  -9   7 637.854 116.117  15
   8  -9   7 630.755 95.7877  52
   8  -9   8 62.8998 38.5599  52
   8  -8  -6 683.670 124.466  41
   8  -8  -5 2197.85 247.718  41
   8  -8  -5 3000.43 237.773  25
   8  -8  -4 393.600 122.507  41
   8  -8  -4 459.687 96.2043  25
   8  -8  -2 634.003 147.317  16
   8  -8  -1 229.391 133.220  16
   8  -8   0 2603.49 324.575  16
   8  -8   1 277.758 131.926  16
   8  -8   2 2141.80 229.644  15
   8  -8   2 2444.26 285.453  16
   8  -8   3 59.8715 69.6703  15
   8  -8   3 105.347 94.8936  16
   8  -8   4 996.298 156.150  15
   8  -8   5 47.9723 76.1971  15
   8  -8   6 2017.46 226.384  15
   8  -8   7 163.202 78.8911  15
   8  -8   7 109.477 65.6804  52
   8  -8   8 393.062 97.4648  15
   8  -8   8 477.181 85.4336  52
   8  -8   9 86.8876 41.4385  52
   8  -7  -6 3833.09 335.400  41
   8  -7  -5-17.5786 81.7101  41
   8  -7  -4 2933.07 309.808  41
   8  -7  -3 861.852 158.505  16
   8  -7  -2 1380.68 212.248  16
   8  -7  -1 3185.48 358.785  16
   8  -7   0 195.675 139.664  16
   8  -7   1 5164.19 485.809  16
   8  -7   2 383.435 147.601  16
   8  -7   3 1925.11 233.219  16
   8  -7   3 1657.91 202.754  15
   8  -7   4 394.590 108.459  15
   8  -7   5 1782.53 224.021  15
   8  -7   6 363.606 113.792  15
   8  -7   7 1104.80 174.498  15
   8  -7   7 1364.36 165.867  52
   8  -7   8-21.1319 57.0707  52
   8  -7   9 87.3726 50.7418  52
   8  -7  10 102.828 43.6315  52
   8  -6 -10 137.686 46.8603  40
   8  -6  -7 2806.99 273.518  41
   8  -6  -6-17.2341 78.0803  41
   8  -6  -5 4055.79 372.711  41
   8  -6  -4 120.937 104.912  41
   8  -6  -3 2090.46 281.141  41
   8  -6  -3 2698.84 279.724  16
   8  -6  -2 606.562 157.716  16
   8  -6  -1 529.007 168.868  16
   8  -6  -1 455.480 118.930  42
   8  -6   0 2059.46 309.769  16
   8  -6   1 3172.37 369.260  16
   8  -6   2 1557.89 232.394  16
   8  -6   3 328.079 117.881  16
   8  -6   4 954.306 164.391  15
   8  -6   5 87.8362 70.9603  15
   8  -6   5 186.603 100.948  52
   8  -6   6 3645.36 347.205  15
   8  -6   6 4124.50 347.826  52
   8  -6   7 17.1785 77.8461  15
   8  -6   7 54.9337 71.3915  52
   8  -6   8 1101.72 146.708  52
   8  -6   9 38.9176 50.5962  52
   8  -6  10 187.862 57.6903  52
   8  -5 -10 284.231 67.0654  40
   8  -5  -9 582.821 107.928   5
   8  -5  -8 1445.61 180.543   5
   8  -5  -7 161.581 93.8711  41
   8  -5  -7 174.200 75.8939   5
   8  -5  -6 4726.72 411.320  41
   8  -5  -6 5607.56 394.481   5
   8  -5  -5 324.632 118.494  41
   8  -5  -4 3910.41 378.726  41
   8  -5  -3 175.999 108.118  16
   8  -5  -3 301.377 132.437  41
   8  -5  -2 5554.23 505.919  41
   8  -5  -2 5570.97 481.226  16
   8  -5  -2 5415.75 417.483  42
   8  -5  -1 1056.13 228.649  41
   8  -5  -1 1799.48 272.236  16
   8  -5  -1 1721.22 203.003  42
   8  -5   0 4457.65 464.655  16
   8  -5   0 5121.28 404.787  42
   8  -5   1 2545.93 326.126  16
   8  -5   2 2102.83 265.229  16
   8  -5   3 411.105 119.214  16
   8  -5   5 1892.92 238.129  15
   8  -5   5 2041.56 255.748  52
   8  -5   5 2403.88 228.672  45
   8  -5   6 70.6793 82.2699  15
   8  -5   6 180.808 85.6535  45
   8  -5   6 50.5696 80.4278  52
   8  -5   7 1817.77 206.168  45
   8  -5   7 1753.17 212.927  12
   8  -5   7 1374.80 185.081  52
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   8  -1   5 31.1133 82.4957  33
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   8  -1   7 27.1105 70.5564  12
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   8   0   0 2005.94 251.574  42
   8   0   1 5616.14 409.453  33
   8   0   1 6230.33 447.098  22
   8   0   2 535.570 110.141  33
   8   0   2 378.226 111.050  22
   8   0   2 476.436 110.706  52
   8   0   3 4513.92 370.601  12
   8   0   3 4384.51 340.690  33
   8   0   3 4171.33 363.010  22
   8   0   3 3761.35 352.692  52
   8   0   4-95.2723 73.8045  12
   8   0   4-14.7287 68.4590  33
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   8   0   6 59.2932 78.7207  52
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   8   1  -6 140.643 91.5008  42
   8   1  -6 68.6594 89.3450  41
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   8   1   1 2582.97 256.647  22
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   8   1   2 778.636 129.337  33
   8   1   2 866.519 155.061  22
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   8   1   3 2123.53 217.715  33
   8   1   3 2182.47 243.277  22
   8   1   3 2139.63 239.347  52
   8   1   4 1709.85 195.958  33
   8   1   4 1496.01 192.879  22
   8   1   4 1369.59 198.190  52
   8   1   5 120.093 81.0705  33
   8   1   5 67.3738 59.4172  22
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   8   1   7 227.605 76.5528  33
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   8   2  -6 5329.91 394.369  41
   8   2  -6 4591.32 386.594  42
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   8   2   1 3500.47 330.501  14
   8   2   2 2106.09 233.499  22
   8   2   2 2257.98 210.564  33
   8   2   2 1862.08 222.700  14
   8   2   3 1058.15 144.945  33
   8   2   3 1043.16 165.073  22
   8   2   4 40.2772 54.0435  33
   8   2   4-30.0864 56.3729  22
   8   2   5 1355.13 177.904  33
   8   2   5 1738.57 180.768  22
   8   2   6 188.661 73.4104  33
   8   2   6 199.632 60.8581  22
   8   2   7 1440.92 156.101  33
   8   2   8 314.088 62.2009  33
   8   3  -9 747.807 92.4811  41
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   8   3   0 38.1821 76.9481  14
   8   3   1 4883.23 370.877  22
   8   3   1 4906.36 393.454  14
   8   3   2-14.9864 60.3291  22
   8   3   3 2725.98 262.780  22
   8   3   4 609.640 112.222  22
   8   3   4 568.111 102.919  33
   8   3   5 1591.47 160.484  22
   8   3   5 1198.43 147.998  33
   8   3   6 964.204 109.356  22
   8   3   6 893.656 118.598  33
   8   3   7 460.496 71.6866  33
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   8   4   1 507.337 97.1103  22
   8   4   1 449.335 106.868  14
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   8   4   3 12.3308 52.8441  22
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   9  -9   5 1007.84 129.300  42
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   9  -8   3-16.1050 72.9616  42
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   9  -7   2-19.6275 81.5977  16
   9  -7   2 34.7194 88.3895  42
   9  -7   3 733.241 138.626  16
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   9  -7   6 61.7532 67.9417  12
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   9  -5  -1-47.0565 74.7078  42
   9  -5   0 4220.56 446.185  16
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   9  -5   1-24.6784 102.667  16
   9  -5   1-92.8177 98.4524  42
   9  -5   2 755.072 165.901  42
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   9  -5   3 189.644 112.057  42
   9  -5   4 477.414 135.190  42
   9  -5   5 767.488 144.027  12
   9  -5   5 620.126 136.727  52
   9  -5   6 332.196 106.691  12
   9  -5   6 419.752 106.478  52
   9  -5   7 1161.44 156.798  12
   9  -5   7 1369.12 156.223  52
   9  -5   8 345.112 78.6641  12
   9  -5   8 281.298 71.2262  52
   9  -5   9 430.195 69.2105  52
   9  -4  -9 154.315 51.2808  40
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   9  -4  -2 308.329 140.128  16
   9  -4  -1 5852.41 526.712  16
   9  -4  -1 5512.71 432.193  42
   9  -4   0-35.2126 91.5082  42
   9  -4   0-27.5574 137.368  16
   9  -4   1 3612.70 357.622  42
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   9  -4   1 4125.77 405.357  16
   9  -4   2 99.5699 99.6264  16
   9  -4   2 230.371 109.167  42
   9  -4   2 187.832 71.6550  33
   9  -4   3 391.631 131.721  42
   9  -4   4 798.857 157.518  42
   9  -4   4 690.496 146.212  12
   9  -4   5 332.918 110.262  52
   9  -4   5 234.057 96.9045  12
   9  -4   6 1079.13 161.049  52
   9  -4   6 1273.89 174.501  12
   9  -4   7 456.016 100.082  52
   9  -4   7 299.056 90.6205  12
   9  -4   8 17.8112 46.3417  52
   9  -4   8 106.528 62.9035  12
   9  -4   9 61.2763 43.1481  52
   9  -3  -9 418.532 84.1936  32
   9  -3  -9 435.772 74.1862  40
   9  -3  -8 123.387 68.2475  41
   9  -3  -7 1888.33 205.438  41
   9  -3  -6 677.586 141.007  41
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   9  -3  -4 73.8061 73.7100  42
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   9  -3  -2 810.044 185.700  41
   9  -3  -1 523.690 132.370  42
   9  -3  -1 414.935 176.494  16
   9  -3   0 4379.57 387.102  42
   9  -3   0 4436.89 329.578  33
   9  -3   0 4426.30 453.793  16
   9  -3   1 561.252 146.904  42
   9  -3   1 524.084 155.056  16
   9  -3   1 570.428 109.017  33
   9  -3   2 1371.06 221.308  42
   9  -3   2 2015.48 194.989  33
   9  -3   2 1450.10 209.604  12
   9  -3   2 1968.25 243.581  16
   9  -3   3 19.2464 74.8501  42
   9  -3   3-12.8329 56.5924  33
   9  -3   3 85.0670 82.9421  12
   9  -3   4 1290.70 188.199  12
   9  -3   4 1012.58 174.977  52
   9  -3   5 333.985 109.550  12
   9  -3   5 376.929 122.867  52
   9  -3   6 2112.41 229.542  12
   9  -3   6 2449.53 239.654  52
   9  -3   7 643.820 116.471  12
   9  -3   7 634.366 109.950  52
   9  -3   8 862.586 111.010  52
   9  -3   9 280.034 58.6672  52
   9  -2  -9 276.398 73.0883  32
   9  -2  -8 1775.72 181.419  41
   9  -2  -7-39.9541 73.2700  41
   9  -2  -6 5588.31 429.439  41
   9  -2  -5 500.738 113.632  42
   9  -2  -5 392.741 126.431  41
   9  -2  -4 2243.20 239.027  42
   9  -2  -4 2553.44 303.228  41
   9  -2  -3 1068.93 160.555  42
   9  -2  -3 969.035 195.484  41
   9  -2  -2 313.418 108.167  42
   9  -2  -1 4813.26 400.429  42
   9  -2  -1 4597.13 342.115  33
   9  -2   0 575.396 146.740  42
   9  -2   0 389.947 93.6360  33
   9  -2   1 2399.16 297.232  42
   9  -2   1 3282.07 262.515  33
   9  -2   2 19.8157 87.4170  42
   9  -2   2 75.0347 61.0210  33
   9  -2   3 1404.78 172.169  33
   9  -2   3 1513.22 201.652  12
   9  -2   4-16.6069 71.1688  52
   9  -2   4 40.8931 58.4175  33
   9  -2   4 15.4996 77.2604  12
   9  -2   5 1375.89 190.436  52
   9  -2   5 1692.46 188.894  33
   9  -2   5 1411.72 183.439  12
   9  -2   6 13.1839 72.5093  52
   9  -2   6-24.7770 64.3819  12
   9  -2   7 688.023 111.930  52
   9  -2   8 32.0135 39.9233  52
   9  -1  -9 363.735 79.6525  32
   9  -1  -9 280.679 65.3167  41
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   9  -1  -8 41.4865 53.9148  41
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   9  -1  -6-14.4287 63.6265  42
   9  -1  -6 62.1749 83.9463  41
   9  -1  -5 3449.77 304.646  42
   9  -1  -5 3346.38 330.478  41
   9  -1  -4 220.331 93.0321  42
   9  -1  -4 163.619 110.876  41
   9  -1  -3 1245.12 175.494  42
   9  -1  -3 756.798 171.755  41
   9  -1  -2 3561.40 327.420  42
   9  -1  -1 7765.78 552.808  42
   9  -1  -1 7225.99 478.225  33
   9  -1   0 1555.16 226.614  42
   9  -1   0 1732.34 182.174  33
   9  -1   1 5497.10 482.327  42
   9  -1   1 7064.84 442.986  33
   9  -1   2 693.178 119.998  33
   9  -1   3 376.220 99.8833  33
   9  -1   4 1336.84 192.652  52
   9  -1   4 2008.92 205.418  33
   9  -1   4 1690.33 196.716  12
   9  -1   5 14.5006 91.6853  52
   9  -1   5 26.4316 62.9623  33
   9  -1   5 49.3325 65.3776  12
   9  -1   6 2674.11 229.764  33
   9  -1   6 2152.32 219.213  52
   9  -1   7-26.5614 43.1817  33
   9  -1   7-28.1741 56.0867  52
   9  -1   8 839.507 98.8117  52
   9   0  -9 526.393 80.9064  41
   9   0  -9 653.445 90.3136  32
   9   0  -8 3071.22 240.167  32
   9   0  -8 2633.26 224.160  41
   9   0  -7 262.202 82.1838  41
   9   0  -7 247.633 79.4655  32
   9   0  -6 4401.52 353.753  42
   9   0  -6 4423.65 356.483  41
   9   0  -5 85.8643 94.5673  41
   9   0  -5 108.182 83.6018  42
   9   0  -4 3948.38 347.195  14
   9   0  -4 4532.38 359.037  42
   9   0  -4 3785.37 361.739  41
   9   0  -3 86.3108 87.9948  42
   9   0  -2 3431.91 328.002  42
   9   0  -1 39.5762 84.8430  42
   9   0  -1 65.3104 58.8513  33
   9   0   0 2443.64 278.651  42
   9   0   0 2475.78 222.957  33
   9   0   1 194.574 73.9496  33
   9   0   2 23.7154 56.4777  33
   9   0   2-15.8229 63.6934  22
   9   0   3 516.714 116.579  52
   9   0   3 782.733 127.026  33
   9   0   3 815.761 141.653  22
   9   0   4-43.4058 76.6867  52
   9   0   4 38.5568 62.6651  33
   9   0   4 53.3286 58.8007  22
   9   0   5 1470.83 173.674  33
   9   0   5 1477.03 177.573  52
   9   0   6 369.696 86.4959  33
   9   0   7 1080.21 120.711  33
   9   1  -8 165.855 56.4474  41
   9   1  -7 1171.80 144.364  41
   9   1  -6 1314.88 168.473  41
   9   1  -6 1416.28 177.042  42
   9   1  -5 2116.47 227.822  41
   9   1  -5 1927.07 221.916  42
   9   1  -4 509.576 113.290  14
   9   1  -4 554.195 127.043  41
   9   1  -4 566.538 133.409  42
   9   1  -3 1839.94 227.046  14
   9   1  -3 1452.84 207.545  42
   9   1  -2 252.113 115.863  14
   9   1  -2 117.615 100.178  42
   9   1  -1 5063.22 474.820  14
   9   1  -1 6925.06 501.541  42
   9   1   0 129.278 58.7994  33
   9   1   0 120.889 100.621  14
   9   1   1 1784.18 175.916  33
   9   1   1 1775.85 200.147  22
   9   1   1 1769.20 220.761  14
   9   1   2 1216.85 168.798  22
   9   1   2 1239.59 146.531  33
   9   1   3 424.704 102.463  22
   9   1   3 521.169 101.906  33
   9   1   4 1693.64 187.702  22
   9   1   4 2103.35 202.034  33
   9   1   5 233.090 64.0700  22
   9   1   5 111.592 58.5669  33
   9   1   6 1283.04 142.516  33
   9   2  -7 683.767 101.960  41
   9   2  -6 1075.73 141.958  41
   9   2  -5 572.516 114.911  41
   9   2  -4 1775.10 200.023  41
   9   2  -4 1652.16 210.212  42
   9   2  -4 1843.87 200.815  14
   9   2  -3 18.2489 84.9016  42
   9   2  -3 133.441 81.3975  14
   9   2  -2 1999.12 254.783  42
   9   2  -2 2413.32 266.995  14
   9   2  -1 77.3743 82.9791  14
   9   2   0 1824.59 226.388  14
   9   2   1 282.690 83.4830  22
   9   2   1 429.210 103.393  14
   9   2   2 557.061 108.660  22
   9   2   3 74.0286 56.1689  22
   9   2   3 152.472 57.1644  33
   9   2   4 1069.51 129.937  22
   9   2   4 886.193 119.115  33
   9   2   5 443.572 74.3896  22
   9   2   5 384.245 78.1052  33
   9   3  -6 2569.95 209.408  41
   9   3  -5 603.729 99.8938  41
   9   3  -4 1352.14 159.825  14
   9   3  -3 2112.29 224.844  14
   9   3  -2 49.2544 80.0727  14
   9   3  -1 3196.09 302.289  14
   9   3   0 174.325 81.7565  14
   9   3   1 2101.71 207.028  14
   9   3   1 2188.07 195.873  22
   9   3   2 21.0602 42.3993  22
   9   3   3 1273.99 140.897  22
   9   4  -2 307.850 86.6918  14
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  10  -8  -4 166.808 62.2137  41
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  10  -8   1 317.428 102.000  16
  10  -8   2 147.017 69.0090  42
  10  -8   2 184.897 75.1364  16
  10  -8   3 57.4081 57.2987  42
  10  -8   4 629.304 103.136  42
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  10  -7  -1 71.0332 84.6510  16
  10  -7   0 853.443 168.835  16
  10  -7   0 979.106 136.423  42
  10  -7   1-17.8632 89.0499  16
  10  -7   1 63.3909 60.4012  42
  10  -7   2 317.300 96.2938  16
  10  -7   2 373.120 101.944  42
  10  -7   3 569.490 120.569  42
  10  -7   4 60.5639 57.7674  42
  10  -7   4 60.6920 54.7089  12
  10  -7   5 736.105 104.391  42
  10  -7   5 614.309 97.2588  12
  10  -6  -6 156.275 62.3917  41
  10  -6  -5 966.301 134.265  41
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  10  -6  -3 934.511 145.137  16
  10  -6  -3 1004.74 167.423  41
  10  -6  -2 237.706 101.936  16
  10  -6  -2 197.235 104.309  41
  10  -6  -1 1745.85 193.376  42
  10  -6  -1 2311.44 269.484  16
  10  -6   0 65.3013 106.120  16
  10  -6   0 13.2413 61.5594  42
  10  -6   1 878.766 169.719  16
  10  -6   1 777.784 142.224  42
  10  -6   2 31.2369 74.3875  16
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  10  -6   3 186.040 93.0122  42
  10  -6   4 486.181 100.030  12
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  10  -6   5 162.023 64.5116  12
  10  -6   6-8.53051 43.4363  12
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  10  -5  -1 624.519 170.133  16
  10  -5  -1 654.554 123.553  42
  10  -5   0 828.661 183.754  16
  10  -5   0 851.881 144.302  42
  10  -5   1 20.1508 88.8590  16
  10  -5   1 16.1925 69.3945  42
  10  -5   2 540.257 119.883  12
  10  -5   2 544.875 131.529  42
  10  -5   3 276.363 92.6334  12
  10  -5   3 239.098 101.574  42
  10  -5   4 567.956 112.908  12
  10  -5   4 474.578 108.017  42
  10  -5   5 348.072 85.2194  12
  10  -5   6 365.434 77.3675  12
  10  -4  -7 465.000 85.1854  41
  10  -4  -6 791.317 121.196  41
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  10  -4  -3 772.363 162.892  41
  10  -4  -2 517.033 112.273  42
  10  -4  -1 919.294 148.649  42
  10  -4   0 379.605 114.231  42
  10  -4   1 634.497 140.402  42
  10  -4   2 30.6733 71.3027  12
  10  -4   2 34.6279 78.4539  42
  10  -4   3 470.982 106.892  12
  10  -4   3 410.514 112.728  42
  10  -4   4 47.1428 57.5004  12
  10  -4   5 986.723 131.953  12
  10  -4   6-8.61880 40.0745  12
  10  -4   6-35.8302 47.4830  52
  10  -4   7 222.382 53.9939  12
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  10  -3  -4 318.011 88.1703  42
  10  -3  -4 214.045 99.2091  41
  10  -3  -3 1405.80 170.983  42
  10  -3  -3 1194.20 191.859  41
  10  -3  -2 1046.47 152.481  42
  10  -3  -1 1111.36 168.124  42
  10  -3   0 1134.00 181.223  42
  10  -3   1 52.5235 85.3874  42
  10  -3   2 766.909 110.678  33
  10  -3   2 413.825 119.158  42
  10  -3   3 135.674 58.7500  33
  10  -3   3 117.083 70.5371  12
  10  -3   4 1264.49 141.263  33
  10  -3   4 1038.17 140.537  12
  10  -3   5 171.128 64.5851  12
  10  -3   6 831.455 108.156  52
  10  -3   6 785.657 100.184  12
  10  -2  -7-27.9592 48.4312  32
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  10  -2  -3 526.609 111.739  42
  10  -2  -2 997.096 155.658  42
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  10  -2   1 961.265 169.184  42
  10  -2   2 998.697 125.071  33
  10  -2   3 994.842 129.056  33
  10  -2   4 329.050 79.5905  33
  10  -2   4 270.217 73.5269  12
  10  -2   5 935.203 126.213  52
  10  -2   5 1122.83 123.539  33
  10  -2   6 267.812 64.2431  52
  10  -1  -7 1271.23 133.203  41
  10  -1  -7 1408.12 137.898  32
  10  -1  -6 362.834 81.5204  42
  10  -1  -6 226.167 74.2312  41
  10  -1  -6 189.513 62.6681  32
  10  -1  -5 1731.72 184.374  42
  10  -1  -5 1805.00 194.010  41
  10  -1  -4 102.276 66.6401  42
  10  -1  -4 111.697 80.9629  41
  10  -1  -3 2042.54 217.905  42
  10  -1  -2 725.274 138.832  42
  10  -1  -1 3147.28 304.524  42
  10  -1   0 1141.23 179.467  42
  10  -1   1 2968.53 234.767  33
  10  -1   2 61.4278 58.5996  14
  10  -1   2 67.3249 52.9895  33
  10  -1   3-9.81784 43.2943  33
  10  -1   4 113.736 54.2432  33
  10  -1   5 8.14817 37.8749  33
  10   0  -6 588.760 97.1216  41
  10   0  -5 280.871 78.8275  42
  10   0  -5 317.839 83.4378  41
  10   0  -4 638.624 118.422  42
  10   0  -3 57.6258 70.2571  42
  10   0  -3 27.9887 58.2119  14
  10   0  -2 1666.94 204.381  42
  10   0  -2 1417.81 196.529  14
  10   0  -1 101.613 88.0199  42
  10   0  -1-17.9812 89.6383  14
  10   0   0 2256.02 249.729  14
  10   0   1 41.4723 42.2597  33
  10   0   1 13.5378 61.3495  14
  10   0   2 766.973 102.781  33
  10   0   3 96.6631 50.2490  33
  10   0   4 92.1994 46.3182  33
  10   1  -4 181.595 74.9710  42
  10   1  -3 1223.10 166.841  42
  10   1  -3 1394.77 165.600  14
  10   1  -2 30.8328 71.6802  42
  10   1  -2 44.6939 65.7193  14
  10   1  -1 1457.44 188.427  14
  10   1   0 55.4408 62.8501  14
  10   1   1 1115.62 140.259  14
  10   1   2 35.3316 34.4910  33
  10   1   3 7.09094 32.1261  33
  10   2  -2 994.253 138.375  14
  10   2  -1 187.544 72.9349  14
  11  -6  -1 717.495 97.4658  42
  11  -6   0 129.228 57.9101  42
  11  -6   1 483.029 91.8618  42
  11  -5  -2 926.004 114.623  42
  11  -5  -1 365.631 82.6001  42
  11  -5   0 257.990 78.4342  42
  11  -5   1 22.8460 58.1725  42
  11  -5   2 183.538 67.9263  42
  11  -4  -3 93.1882 53.7527  42
  11  -4  -2 727.194 107.979  42
  11  -4  -1 204.654 71.5122  42
  11  -4   0 722.068 121.360  42
  11  -4   1 169.396 72.7185  42
  11  -4   2-63.9188 54.3326  42
  11  -3  -3 274.768 70.6016  42
  11  -3  -2 352.860 86.6817  42
  11  -3  -1 790.949 124.067  42
  11  -3   0 62.1231 63.3351  42
  11  -3   1-11.8362 55.0176  42
  11  -2  -3 9.55939 44.4346  42
  11  -2  -2 1585.01 175.521  14
  11  -2  -2 1630.69 172.212  42
  11  -2  -1 39.7638 66.1815  14
  11  -2  -1 120.888 67.7722  42
  11  -2   0 783.136 124.483  14
  11  -2   0 693.603 120.100  42
  11  -2   1 677.894 103.779  14
   0   0   0    0.00    0.00   0

TITL exp_11 in P1
REM P1 (#1 in standard setting)
CELL 1.54184   9.360712  10.507330  13.331112  95.4328  91.5040 107.9884
ZERR   10.00   0.000211   0.000296   0.000320   0.0021   0.0019   0.0022
LATT -1
SFAC C H N O P Cl Br Ir
UNIT 10.00 10.00 10.00 10.00 10.00 10.00 10.00 10.00
TREF
HKLF 4
END
;
_shelx_hkl_checksum              62752
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
C11 C 0.2908(5) 0.2733(4) 0.1989(3) 0.0636(10) Uani 1 1 d . . . . .
H11 H 0.2067 0.2035 0.2124 0.076 Uiso 1 1 calc R U . . .
C12 C 0.3051(5) 0.4035(4) 0.2353(3) 0.0646(10) Uani 1 1 d . . . . .
H12 H 0.2299 0.4201 0.2735 0.078 Uiso 1 1 calc R U . . .
C14 C 0.5305(4) 0.4829(4) 0.1604(3) 0.0517(8) Uani 1 1 d . . . . .
C15 C 0.5219(4) 0.3539(4) 0.1224(3) 0.0549(8) Uani 1 1 d . . . . .
H15 H 0.5973 0.3391 0.0833 0.066 Uiso 1 1 calc R U . . .
C16 C 0.4006(4) 0.2462(4) 0.1427(3) 0.0554(8) Uani 1 1 d . . . . .
C24 C 0.6525(4) 0.6024(4) 0.1395(3) 0.0519(8) Uani 1 1 d . . . . .
C25 C 0.7641(4) 0.5996(4) 0.0758(3) 0.0562(8) Uani 1 1 d . . . . .
H25 H 0.7681 0.5175 0.0453 0.067 Uiso 1 1 calc R U . . .
C26 C 0.8718(4) 0.7185(4) 0.0561(3) 0.0562(8) Uani 1 1 d . . . . .
C27 C 0.8609(5) 0.8379(4) 0.1033(3) 0.0641(10) Uani 1 1 d . . . . .
H27 H 0.9305 0.9195 0.0924 0.077 Uiso 1 1 calc R U . . .
C28 C 0.7466(5) 0.8353(4) 0.1664(3) 0.0657(10) Uani 1 1 d . . . . .
H28 H 0.7399 0.9165 0.1969 0.079 Uiso 1 1 calc R U . . .
C29 C 0.9913(5) 0.7116(5) -0.0147(4) 0.0765(13) Uani 0.734(9) 1 d D . P A 1
H29A H 1.0560 0.6678 0.0160 0.092 Uiso 0.734(9) 1 calc R U P A 1
H29B H 0.9435 0.6558 -0.0760 0.092 Uiso 0.734(9) 1 calc R U P A 1
C29A C 0.9913(5) 0.7116(5) -0.0147(4) 0.0765(13) Uani 0.266(9) 1 d . . P A 2
H29C H 0.9959 0.7768 -0.0624 0.092 Uiso 0.266(9) 1 calc R U P A 2
H29D H 1.0869 0.7408 0.0243 0.092 Uiso 0.266(9) 1 calc R U P A 2
C31 C 0.3922(5) 0.1058(4) 0.1019(4) 0.0700(11) Uani 1 1 d . . . . .
H31A H 0.3899 0.0986 0.0287 0.084 Uiso 1 1 calc R U . . .
H31B H 0.4808 0.0858 0.1260 0.084 Uiso 1 1 calc R U . . .
C63 C 0.5809(5) 0.7862(4) 0.4157(3) 0.0626(10) Uani 1 1 d . . . . .
C64 C 0.4527(5) 0.6744(4) 0.4286(3) 0.0668(10) Uani 1 1 d . . . . .
H64 H 0.4660 0.6019 0.4582 0.080 Uiso 1 1 calc R U . . .
C65 C 0.3063(5) 0.6706(5) 0.3978(3) 0.0712(12) Uani 1 1 d . . . . .
H65 H 0.2253 0.5968 0.4091 0.085 Uiso 1 1 calc R U . . .
C66 C 0.2794(5) 0.7768(5) 0.3497(4) 0.0713(11) Uani 1 1 d . . . . .
C67 C 0.4071(6) 0.8889(4) 0.3369(3) 0.0690(11) Uani 1 1 d . . . . .
H67 H 0.3939 0.9600 0.3053 0.083 Uiso 1 1 calc R U . . .
C69 C 0.5513(5) 0.8948(4) 0.3704(3) 0.0650(10) Uani 1 1 d . . . . .
H69 H 0.6311 0.9717 0.3632 0.078 Uiso 1 1 calc R U . . .
C71 C 0.7377(6) 0.7943(5) 0.4468(4) 0.0765(12) Uani 1 1 d . . . . .
H71 H 0.8019 0.8337 0.3935 0.092 Uiso 1 1 calc R U . . .
C72 C 0.7595(8) 0.6625(7) 0.4585(6) 0.114(2) Uani 1 1 d . . . . .
H72A H 0.7088 0.6263 0.5161 0.171 Uiso 1 1 calc R U . . .
H72B H 0.8650 0.6743 0.4681 0.171 Uiso 1 1 calc R U . . .
H72C H 0.7188 0.6014 0.3991 0.171 Uiso 1 1 calc R U . . .
C73 C 0.7882(8) 0.8929(8) 0.5432(5) 0.112(2) Uani 1 1 d . . . . .
H73A H 0.7212 0.8619 0.5953 0.168 Uiso 1 1 calc R U . . .
H73B H 0.7864 0.9805 0.5296 0.168 Uiso 1 1 calc R U . . .
H73C H 0.8885 0.8978 0.5649 0.168 Uiso 1 1 calc R U . . .
C74 C 0.1223(6) 0.7658(7) 0.3094(5) 0.1025(19) Uani 1 1 d . . . . .
H74A H 0.1293 0.8223 0.2560 0.154 Uiso 1 1 calc R U . . .
H74B H 0.0683 0.7940 0.3628 0.154 Uiso 1 1 calc R U . . .
H74C H 0.0700 0.6741 0.2839 0.154 Uiso 1 1 calc R U . . .
Cl1 Cl 0.33796(14) 0.72076(12) 0.11042(8) 0.0747(3) Uani 1 1 d . . . . .
F2 F 0.226(3) 0.824(2) 0.7682(16) 0.188(12) Uani 0.351(17) 1 d . U P B 1
F6 F 0.3351(16) 0.755(4) 0.6591(18) 0.163(9) Uani 0.351(17) 1 d . U P B 1
F3 F 0.167(2) 0.830(3) 0.608(2) 0.163(11) Uani 0.351(17) 1 d . U P B 1
F1 F 0.111(3) 0.607(2) 0.5926(15) 0.137(8) Uani 0.351(17) 1 d . U P B 1
F4 F 0.0112(15) 0.703(3) 0.7064(19) 0.164(9) Uani 0.351(17) 1 d . U P B 1
F5 F 0.176(3) 0.609(2) 0.757(2) 0.160(11) Uani 0.351(17) 1 d . U P B 1
N1 N 0.6439(4) 0.7201(3) 0.1860(2) 0.0539(7) Uani 1 1 d . . . . .
N2 N 0.4244(3) 0.5082(3) 0.2175(2) 0.0544(7) Uani 1 1 d . . . . .
O1 O 1.0764(6) 0.8302(5) -0.0393(4) 0.0865(18) Uani 0.734(9) 1 d D . P A 1
H1 H 1.1228 0.8184 -0.0888 0.130 Uiso 0.734(9) 1 calc R U P A 1
O1B O 0.9803(16) 0.6036(12) -0.0632(11) 0.088(5) Uani 0.266(9) 1 d D . P A 2
H1B H 1.0420 0.6154 -0.1067 0.132 Uiso 0.266(9) 1 calc R U P A 2
O2 O 0.2632(5) 0.0135(3) 0.1329(4) 0.1081(14) Uani 1 1 d . . . . .
H32 H 0.2572 -0.0639 0.1115 0.162 Uiso 1 1 d R U . . .
P4 P 0.16717(13) 0.71781(12) 0.68302(9) 0.0694(3) Uani 1 1 d . . . . .
Ru1 Ru 0.45384(3) 0.70838(3) 0.26984(2) 0.05270(13) Uani 1 1 d . . . . .
F1A F 0.0385(17) 0.6054(13) 0.6223(12) 0.173(6) Uani 0.649(17) 1 d . U P B 2
F2A F 0.2898(14) 0.8361(9) 0.7498(9) 0.129(4) Uani 0.649(17) 1 d . U P B 2
F5A F 0.0500(18) 0.7865(19) 0.7243(12) 0.177(6) Uani 0.649(17) 1 d . U P B 2
F6A F 0.2871(16) 0.6534(14) 0.6504(8) 0.145(4) Uani 0.649(17) 1 d . U P B 2
F3A F 0.1893(15) 0.7998(13) 0.5927(7) 0.120(4) Uani 0.649(17) 1 d . U P B 2
F4A F 0.1406(16) 0.6358(14) 0.7737(9) 0.151(5) Uani 0.649(17) 1 d . U P B 2
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
C11 0.059(2) 0.044(2) 0.073(2) 0.0036(17) 0.0104(18) -0.0039(17)
C12 0.062(2) 0.045(2) 0.078(3) 0.0063(18) 0.0170(19) 0.0037(17)
C14 0.0536(19) 0.0452(18) 0.0515(18) 0.0047(14) 0.0065(14) 0.0082(15)
C15 0.056(2) 0.0435(19) 0.060(2) -0.0002(15) 0.0043(15) 0.0092(15)
C16 0.064(2) 0.0404(18) 0.056(2) 0.0041(15) -0.0002(16) 0.0084(16)
C24 0.0529(18) 0.0434(18) 0.0525(18) 0.0023(14) 0.0029(14) 0.0060(15)
C25 0.056(2) 0.0464(19) 0.061(2) 0.0014(16) 0.0081(16) 0.0097(16)
C26 0.0506(18) 0.056(2) 0.055(2) 0.0059(16) 0.0037(15) 0.0064(16)
C27 0.063(2) 0.048(2) 0.073(2) 0.0124(18) 0.0145(18) 0.0021(17)
C28 0.070(2) 0.0386(19) 0.079(3) 0.0033(17) 0.017(2) 0.0033(17)
C29 0.055(2) 0.088(3) 0.072(3) 0.002(2) 0.0136(19) 0.004(2)
C29A 0.055(2) 0.088(3) 0.072(3) 0.002(2) 0.0136(19) 0.004(2)
C31 0.083(3) 0.043(2) 0.076(3) 0.0009(18) 0.000(2) 0.0088(19)
C63 0.074(2) 0.057(2) 0.0491(19) -0.0049(16) 0.0065(17) 0.0125(19)
C64 0.086(3) 0.053(2) 0.057(2) 0.0101(17) 0.0140(19) 0.014(2)
C65 0.079(3) 0.067(3) 0.060(2) 0.0027(19) 0.031(2) 0.010(2)
C66 0.072(3) 0.078(3) 0.065(2) -0.006(2) 0.021(2) 0.029(2)
C67 0.089(3) 0.054(2) 0.067(2) -0.0041(18) 0.020(2) 0.027(2)
C69 0.084(3) 0.0379(19) 0.061(2) -0.0072(16) 0.0130(19) 0.0039(18)
C71 0.081(3) 0.067(3) 0.075(3) 0.003(2) 0.006(2) 0.015(2)
C72 0.100(4) 0.092(4) 0.156(6) 0.012(4) -0.012(4) 0.040(4)
C73 0.118(5) 0.112(5) 0.099(4) -0.023(4) -0.031(4) 0.039(4)
C74 0.086(4) 0.126(5) 0.104(4) -0.005(4) 0.016(3) 0.050(4)
Cl1 0.0882(7) 0.0775(7) 0.0625(6) 0.0011(5) 0.0020(5) 0.0339(6)
F2 0.164(17) 0.151(14) 0.151(13) -0.095(11) 0.067(13) -0.064(12)
F6 0.081(8) 0.23(2) 0.182(16) 0.058(18) 0.042(8) 0.043(12)
F3 0.114(11) 0.089(11) 0.25(2) 0.091(13) -0.073(13) -0.027(9)
F1 0.19(2) 0.096(11) 0.107(9) -0.033(7) 0.031(11) 0.024(12)
F4 0.050(6) 0.20(2) 0.209(17) -0.008(17) 0.059(7) -0.005(9)
F5 0.160(15) 0.096(10) 0.21(2) 0.047(12) -0.093(16) 0.021(10)
N1 0.0584(17) 0.0412(15) 0.0549(16) 0.0022(12) 0.0094(13) 0.0054(13)
N2 0.0564(17) 0.0387(15) 0.0609(17) 0.0019(12) 0.0119(13) 0.0050(12)
O1 0.087(3) 0.067(3) 0.091(3) 0.007(2) 0.040(2) 0.001(2)
O1B 0.098(10) 0.066(8) 0.095(10) 0.013(7) 0.050(7) 0.012(7)
O2 0.116(3) 0.0409(16) 0.145(4) -0.0047(19) 0.038(3) -0.0062(18)
P4 0.0652(6) 0.0631(6) 0.0709(7) 0.0076(5) 0.0123(5) 0.0064(5)
Ru1 0.0587(2) 0.03880(17) 0.05569(19) 0.00226(11) 0.01203(12) 0.00818(12)
F1A 0.157(10) 0.115(7) 0.180(13) 0.018(8) -0.068(8) -0.050(7)
F2A 0.128(7) 0.087(4) 0.139(8) 0.003(5) -0.056(6) -0.005(5)
F5A 0.167(12) 0.227(14) 0.200(11) 0.056(12) 0.063(10) 0.139(11)
F6A 0.166(9) 0.150(8) 0.152(7) 0.005(7) 0.051(7) 0.099(8)
F3A 0.165(8) 0.108(7) 0.078(4) 0.029(4) 0.036(5) 0.020(5)
F4A 0.200(10) 0.150(9) 0.134(6) 0.084(6) 0.079(7) 0.074(7)
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru 0.0552 3.2960 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C16 C11 C12 119.9(3) . . ?
C16 C11 H11 120.1 . . ?
C12 C11 H11 120.1 . . ?
N2 C12 C11 122.3(4) . . ?
N2 C12 H12 118.8 . . ?
C11 C12 H12 118.8 . . ?
N2 C14 C15 121.8(3) . . ?
N2 C14 C24 115.1(3) . . ?
C15 C14 C24 123.1(3) . . ?
C14 C15 C16 119.8(4) . . ?
C14 C15 H15 120.1 . . ?
C16 C15 H15 120.1 . . ?
C11 C16 C15 118.0(4) . . ?
C11 C16 C31 122.4(4) . . ?
C15 C16 C31 119.6(4) . . ?
N1 C24 C25 121.3(3) . . ?
N1 C24 C14 114.4(3) . . ?
C25 C24 C14 124.3(3) . . ?
C24 C25 C26 120.8(4) . . ?
C24 C25 H25 119.6 . . ?
C26 C25 H25 119.6 . . ?
C27 C26 C25 117.4(4) . . ?
C27 C26 C29A 123.4(4) . . ?
C25 C26 C29A 119.2(4) . . ?
C27 C26 C29 123.4(4) . . ?
C25 C26 C29 119.2(4) . . ?
C28 C27 C26 119.7(4) . . ?
C28 C27 H27 120.2 . . ?
C26 C27 H27 120.2 . . ?
N1 C28 C27 122.7(4) . . ?
N1 C28 H28 118.7 . . ?
C27 C28 H28 118.7 . . ?
O1 C29 C26 114.8(5) . . ?
O1 C29 H29A 108.6 . . ?
C26 C29 H29A 108.6 . . ?
O1 C29 H29B 108.6 . . ?
C26 C29 H29B 108.6 . . ?
H29A C29 H29B 107.5 . . ?
O1B C29A C26 118.6(7) . . ?
O1B C29A H29C 107.7 . . ?
C26 C29A H29C 107.7 . . ?
O1B C29A H29D 107.7 . . ?
C26 C29A H29D 107.7 . . ?
H29C C29A H29D 107.1 . . ?
O2 C31 C16 110.0(4) . . ?
O2 C31 H31A 109.7 . . ?
C16 C31 H31A 109.7 . . ?
O2 C31 H31B 109.7 . . ?
C16 C31 H31B 109.7 . . ?
H31A C31 H31B 108.2 . . ?
C64 C63 C69 115.9(4) . . ?
C64 C63 C71 123.6(4) . . ?
C69 C63 C71 120.4(4) . . ?
C64 C63 Ru1 70.2(2) . . ?
C69 C63 Ru1 70.6(2) . . ?
C71 C63 Ru1 129.5(3) . . ?
C65 C64 C63 121.8(4) . . ?
C65 C64 Ru1 72.5(2) . . ?
C63 C64 Ru1 71.8(2) . . ?
C65 C64 H64 119.1 . . ?
C63 C64 H64 119.1 . . ?
Ru1 C64 H64 129.0 . . ?
C64 C65 C66 121.6(4) . . ?
C64 C65 Ru1 70.1(2) . . ?
C66 C65 Ru1 72.2(2) . . ?
C64 C65 H65 119.2 . . ?
C66 C65 H65 119.2 . . ?
Ru1 C65 H65 131.4 . . ?
C65 C66 C67 116.7(4) . . ?
C65 C66 C74 120.8(5) . . ?
C67 C66 C74 122.4(5) . . ?
C65 C66 Ru1 70.5(2) . . ?
C67 C66 Ru1 69.6(2) . . ?
C74 C66 Ru1 127.8(3) . . ?
C69 C67 C66 121.7(4) . . ?
C69 C67 Ru1 71.5(2) . . ?
C66 C67 Ru1 72.9(2) . . ?
C69 C67 H67 119.1 . . ?
C66 C67 H67 119.1 . . ?
Ru1 C67 H67 128.9 . . ?
C67 C69 C63 122.1(4) . . ?
C67 C69 Ru1 71.5(2) . . ?
C63 C69 Ru1 71.3(2) . . ?
C67 C69 H69 118.9 . . ?
C63 C69 H69 118.9 . . ?
Ru1 C69 H69 131.3 . . ?
C72 C71 C63 114.5(5) . . ?
C72 C71 C73 112.0(5) . . ?
C63 C71 C73 108.5(5) . . ?
C72 C71 H71 107.2 . . ?
C63 C71 H71 107.2 . . ?
C73 C71 H71 107.2 . . ?
C71 C72 H72A 109.5 . . ?
C71 C72 H72B 109.5 . . ?
H72A C72 H72B 109.5 . . ?
C71 C72 H72C 109.5 . . ?
H72A C72 H72C 109.5 . . ?
H72B C72 H72C 109.5 . . ?
C71 C73 H73A 109.5 . . ?
C71 C73 H73B 109.5 . . ?
H73A C73 H73B 109.5 . . ?
C71 C73 H73C 109.5 . . ?
H73A C73 H73C 109.5 . . ?
H73B C73 H73C 109.5 . . ?
C66 C74 H74A 109.5 . . ?
C66 C74 H74B 109.5 . . ?
H74A C74 H74B 109.5 . . ?
C66 C74 H74C 109.5 . . ?
H74A C74 H74C 109.5 . . ?
H74B C74 H74C 109.5 . . ?
C28 N1 C24 118.3(3) . . ?
C28 N1 Ru1 124.9(3) . . ?
C24 N1 Ru1 116.4(2) . . ?
C14 N2 C12 118.1(3) . . ?
C14 N2 Ru1 117.3(2) . . ?
C12 N2 Ru1 124.5(3) . . ?
C29 O1 H1 109.5 . . ?
C29A O1B H1B 109.5 . . ?
C31 O2 H32 111.3 . . ?
F4 P4 F2 92.0(12) . . ?
F3A P4 F6A 92.1(6) . . ?
F3A P4 F4A 178.4(7) . . ?
F6A P4 F4A 89.3(6) . . ?
F3A P4 F1A 90.0(7) . . ?
F6A P4 F1A 93.2(8) . . ?
F4A P4 F1A 89.3(8) . . ?
F4 P4 F6 172.0(14) . . ?
F2 P4 F6 82.9(12) . . ?
F4 P4 F1 90.1(11) . . ?
F2 P4 F1 177.9(12) . . ?
F6 P4 F1 95.0(12) . . ?
F3A P4 F5A 90.5(7) . . ?
F6A P4 F5A 175.9(7) . . ?
F4A P4 F5A 88.1(7) . . ?
F1A P4 F5A 89.9(8) . . ?
F3A P4 F2A 91.2(6) . . ?
F6A P4 F2A 90.9(6) . . ?
F4A P4 F2A 89.5(7) . . ?
F1A P4 F2A 175.7(8) . . ?
F5A P4 F2A 85.9(8) . . ?
F4 P4 F5 91.5(14) . . ?
F2 P4 F5 88.6(15) . . ?
F6 P4 F5 94.5(12) . . ?
F1 P4 F5 91.3(14) . . ?
F4 P4 F3 91.2(14) . . ?
F2 P4 F3 90.8(16) . . ?
F6 P4 F3 82.8(12) . . ?
F1 P4 F3 89.2(14) . . ?
F5 P4 F3 177.2(12) . . ?
N2 Ru1 N1 76.71(12) . . ?
N2 Ru1 C64 94.41(15) . . ?
N1 Ru1 C64 121.50(16) . . ?
N2 Ru1 C67 160.93(16) . . ?
N1 Ru1 C67 121.87(15) . . ?
C64 Ru1 C67 79.70(18) . . ?
N2 Ru1 C69 154.64(16) . . ?
N1 Ru1 C69 97.35(14) . . ?
C64 Ru1 C69 67.36(16) . . ?
C67 Ru1 C69 37.01(18) . . ?
N2 Ru1 C63 117.07(15) . . ?
N1 Ru1 C63 95.52(14) . . ?
C64 Ru1 C63 37.95(16) . . ?
C67 Ru1 C63 68.58(18) . . ?
C69 Ru1 C63 38.16(17) . . ?
N2 Ru1 C65 97.57(15) . . ?
N1 Ru1 C65 158.42(18) . . ?
C64 Ru1 C65 37.39(19) . . ?
C67 Ru1 C65 66.76(18) . . ?
C69 Ru1 C65 78.83(16) . . ?
C63 Ru1 C65 68.24(17) . . ?
N2 Ru1 C66 123.49(16) . . ?
N1 Ru1 C66 158.58(17) . . ?
C64 Ru1 C66 68.03(18) . . ?
C67 Ru1 C66 37.51(18) . . ?
C69 Ru1 C66 67.48(17) . . ?
C63 Ru1 C66 81.80(17) . . ?
C65 Ru1 C66 37.29(19) . . ?
N2 Ru1 Cl1 85.80(10) . . ?
N1 Ru1 Cl1 83.86(9) . . ?
C64 Ru1 Cl1 154.05(13) . . ?
C67 Ru1 Cl1 91.69(13) . . ?
C69 Ru1 Cl1 118.43(13) . . ?
C63 Ru1 Cl1 156.45(12) . . ?
C65 Ru1 Cl1 116.80(14) . . ?
C66 Ru1 Cl1 90.23(13) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C11 C16 1.371(6) . ?
C11 C12 1.372(6) . ?
C11 H11 0.9300 . ?
C12 N2 1.348(5) . ?
C12 H12 0.9300 . ?
C14 N2 1.342(5) . ?
C14 C15 1.378(5) . ?
C14 C24 1.468(5) . ?
C15 C16 1.387(5) . ?
C15 H15 0.9300 . ?
C16 C31 1.501(6) . ?
C24 N1 1.356(5) . ?
C24 C25 1.369(5) . ?
C25 C26 1.395(5) . ?
C25 H25 0.9300 . ?
C26 C27 1.383(6) . ?
C26 C29A 1.496(6) . ?
C26 C29 1.496(6) . ?
C27 C28 1.374(6) . ?
C27 H27 0.9300 . ?
C28 N1 1.346(5) . ?
C28 H28 0.9300 . ?
C29 O1 1.331(6) . ?
C29 H29A 0.9700 . ?
C29 H29B 0.9700 . ?
C29A O1B 1.226(12) . ?
C29A H29C 0.9700 . ?
C29A H29D 0.9700 . ?
C31 O2 1.397(6) . ?
C31 H31A 0.9700 . ?
C31 H31B 0.9700 . ?
C63 C64 1.424(6) . ?
C63 C69 1.436(6) . ?
C63 C71 1.489(7) . ?
C63 Ru1 2.200(4) . ?
C64 C65 1.407(7) . ?
C64 Ru1 2.179(4) . ?
C64 H64 0.9300 . ?
C65 C66 1.421(7) . ?
C65 Ru1 2.211(4) . ?
C65 H65 0.9300 . ?
C66 C67 1.423(7) . ?
C66 C74 1.518(7) . ?
C66 Ru1 2.234(4) . ?
C67 C69 1.391(7) . ?
C67 Ru1 2.191(4) . ?
C67 H67 0.9300 . ?
C69 Ru1 2.191(4) . ?
C69 H69 0.9300 . ?
C71 C72 1.484(8) . ?
C71 C73 1.537(8) . ?
C71 H71 0.9800 . ?
C72 H72A 0.9600 . ?
C72 H72B 0.9600 . ?
C72 H72C 0.9600 . ?
C73 H73A 0.9600 . ?
C73 H73B 0.9600 . ?
C73 H73C 0.9600 . ?
C74 H74A 0.9600 . ?
C74 H74B 0.9600 . ?
C74 H74C 0.9600 . ?
Cl1 Ru1 2.3935(11) . ?
F2 P4 1.477(17) . ?
F6 P4 1.548(14) . ?
F3 P4 1.61(2) . ?
F1 P4 1.552(18) . ?
F4 P4 1.465(15) . ?
F5 P4 1.60(2) . ?
N1 Ru1 2.103(3) . ?
N2 Ru1 2.084(3) . ?
O1 H1 0.8200 . ?
O1B H1B 0.8200 . ?
O2 H32 0.8199 . ?
P4 F3A 1.527(10) . ?
P4 F6A 1.532(8) . ?
P4 F4A 1.532(9) . ?
P4 F1A 1.546(9) . ?
P4 F5A 1.572(10) . ?
P4 F2A 1.585(9) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C16 C11 C12 N2 0.3(7) . . . . ?
N2 C14 C15 C16 0.3(6) . . . . ?
C24 C14 C15 C16 -177.9(3) . . . . ?
C12 C11 C16 C15 -1.6(6) . . . . ?
C12 C11 C16 C31 179.3(4) . . . . ?
C14 C15 C16 C11 1.3(6) . . . . ?
C14 C15 C16 C31 -179.5(4) . . . . ?
N2 C14 C24 N1 3.5(5) . . . . ?
C15 C14 C24 N1 -178.2(4) . . . . ?
N2 C14 C24 C25 -174.0(4) . . . . ?
C15 C14 C24 C25 4.3(6) . . . . ?
N1 C24 C25 C26 -0.6(6) . . . . ?
C14 C24 C25 C26 176.8(4) . . . . ?
C24 C25 C26 C27 0.0(6) . . . . ?
C24 C25 C26 C29A -179.4(4) . . . . ?
C24 C25 C26 C29 -179.4(4) . . . . ?
C25 C26 C27 C28 -0.1(6) . . . . ?
C29A C26 C27 C28 179.3(4) . . . . ?
C29 C26 C27 C28 179.3(4) . . . . ?
C26 C27 C28 N1 0.8(7) . . . . ?
C27 C26 C29 O1 -8.0(7) . . . . ?
C25 C26 C29 O1 171.4(5) . . . . ?
C27 C26 C29A O1B -170.3(10) . . . . ?
C25 C26 C29A O1B 9.1(11) . . . . ?
C11 C16 C31 O2 -2.1(6) . . . . ?
C15 C16 C31 O2 178.8(4) . . . . ?
C69 C63 C64 C65 0.6(6) . . . . ?
C71 C63 C64 C65 -179.7(4) . . . . ?
Ru1 C63 C64 C65 -54.8(4) . . . . ?
C69 C63 C64 Ru1 55.4(3) . . . . ?
C71 C63 C64 Ru1 -124.9(4) . . . . ?
C63 C64 C65 C66 1.7(6) . . . . ?
Ru1 C64 C65 C66 -52.9(4) . . . . ?
C63 C64 C65 Ru1 54.5(4) . . . . ?
C64 C65 C66 C67 -1.7(6) . . . . ?
Ru1 C65 C66 C67 -53.7(3) . . . . ?
C64 C65 C66 C74 175.0(4) . . . . ?
Ru1 C65 C66 C74 123.1(4) . . . . ?
C64 C65 C66 Ru1 51.9(4) . . . . ?
C65 C66 C67 C69 -0.5(6) . . . . ?
C74 C66 C67 C69 -177.1(4) . . . . ?
Ru1 C66 C67 C69 -54.5(4) . . . . ?
C65 C66 C67 Ru1 54.1(3) . . . . ?
C74 C66 C67 Ru1 -122.6(4) . . . . ?
C66 C67 C69 C63 2.8(6) . . . . ?
Ru1 C67 C69 C63 -52.4(4) . . . . ?
C66 C67 C69 Ru1 55.2(4) . . . . ?
C64 C63 C69 C67 -2.8(6) . . . . ?
C71 C63 C69 C67 177.5(4) . . . . ?
Ru1 C63 C69 C67 52.4(4) . . . . ?
C64 C63 C69 Ru1 -55.2(3) . . . . ?
C71 C63 C69 Ru1 125.1(4) . . . . ?
C64 C63 C71 C72 20.5(7) . . . . ?
C69 C63 C71 C72 -159.8(5) . . . . ?
Ru1 C63 C71 C72 -70.7(6) . . . . ?
C64 C63 C71 C73 -105.4(5) . . . . ?
C69 C63 C71 C73 74.3(6) . . . . ?
Ru1 C63 C71 C73 163.4(4) . . . . ?
C27 C28 N1 C24 -1.4(6) . . . . ?
C27 C28 N1 Ru1 -173.6(3) . . . . ?
C25 C24 N1 C28 1.2(6) . . . . ?
C14 C24 N1 C28 -176.4(4) . . . . ?
C25 C24 N1 Ru1 174.1(3) . . . . ?
C14 C24 N1 Ru1 -3.5(4) . . . . ?
C15 C14 N2 C12 -1.6(6) . . . . ?
C24 C14 N2 C12 176.7(4) . . . . ?
C15 C14 N2 Ru1 179.7(3) . . . . ?
C24 C14 N2 Ru1 -2.0(4) . . . . ?
C11 C12 N2 C14 1.4(7) . . . . ?
C11 C12 N2 Ru1 179.9(3) . . . . ?