Crystallography Open Database

Information card for entry 7707504

Preview

Coordinates	7707504.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H32 B Cl N2
Calculated formula	C19 H32 B Cl N2
Title of publication	Synthesis, characterization, and reactivity of group 13 hydride complexes based on amido-amine ligands.
Authors of publication	Dehmel, Maximilian; Köhler, Angelina; Görls, Helmar; Kretschmer, Robert
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	24
Pages of publication	8434 - 8445
a	17.3711 ± 0.0002 Å
b	12.4969 ± 0.0002 Å
c	18.2513 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	3962.08 ± 0.09 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0372
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.083
Weighted residual factors for all reflections included in the refinement	0.0869
Goodness-of-fit parameter for all reflections included in the refinement	1.058
Diffraction radiation wavelength	1.54184 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
267144 (current)	2021-07-05	cif/ Updating files of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 Original log message: Adding full bibliography for 7707498--7707509.cif.	7707504.cif
265524	2021-05-27	cif/ Adding structures of 7707498, 7707499, 7707500, 7707501, 7707502, 7707503, 7707504, 7707505, 7707506, 7707507, 7707508, 7707509 via cif-deposit CGI script.	7707504.cif