#------------------------------------------------------------------------------ #$Date: 2021-07-05 20:37:49 +0300 (Mon, 05 Jul 2021) $ #$Revision: 267173 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/75/7707512.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707512 loop_ _publ_author_name 'Brach\ 2\s(I)' _cod_data_source_file d1dt01057c2.cif _cod_data_source_block 1@100K _cod_depositor_comments 'Adding full bibliography for 7707511--7707512.cif.' _cod_database_code 7707512 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.526 _shelx_estimated_absorpt_t_min 0.176 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C3(H3), C4(H4), C6(H6), C7(H7), C10(H10), C11(H11), C12(H12), C13(H13), C14(H14) ; _shelx_res_file ; TITL BB70 clathrate bb70.res created by SHELXL-2018/3 at 16:32:20 on 19-Oct-2020 CELL 1.54186 6.8681 7.3161 13.443 79.253 76.78 89.413 ZERR 1 0.0002 0.0002 0.0005 0.003 0.003 0.003 LATT 1 SFAC C H Fe N Pt UNIT 28 18 1 8 1 L.S. 8 0 0 PLAN 5 SIZE 0.05 0.13 0.18 TEMP -173.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.103600 1.189600 FVAR 0.59721 PT1 5 0.000000 0.500000 0.500000 10.50000 0.01890 0.02382 = 0.02291 -0.00508 -0.00288 0.00117 FE1 3 0.500000 1.000000 0.500000 10.50000 0.01845 0.02260 = 0.02030 -0.00480 -0.00123 0.00007 N1 4 0.314451 0.820003 0.482017 11.00000 0.02713 0.02581 = 0.01909 -0.00408 -0.00189 0.00278 N2 4 0.673156 0.798674 0.529974 11.00000 0.02320 0.03146 = 0.02213 -0.00309 -0.00063 -0.00170 N3 4 0.350839 0.967663 0.649526 11.00000 0.02139 0.02324 = 0.02232 -0.00473 0.00045 0.00151 C1 1 0.199605 0.700097 0.486384 11.00000 0.02429 0.02398 = 0.02392 -0.00774 -0.00480 -0.00220 C2 1 0.788137 0.682712 0.524868 11.00000 0.02175 0.02551 = 0.02251 -0.00244 -0.00489 0.00406 C3 1 0.152718 0.984262 0.674857 11.00000 0.02989 0.03213 = 0.02639 -0.00646 -0.00633 -0.00253 AFIX 43 H3 2 0.081068 0.993573 0.621560 11.00000 -1.20000 AFIX 0 C4 1 0.046136 0.988560 0.775956 11.00000 0.02894 0.03807 = 0.02653 -0.00229 0.00190 0.00257 AFIX 43 H4 2 -0.094807 1.001431 0.790933 11.00000 -1.20000 AFIX 0 C5 1 0.150648 0.973558 0.854953 11.00000 0.03738 0.03559 = 0.02215 -0.00607 0.00168 -0.00308 C6 1 0.354564 0.944685 0.830000 11.00000 0.03704 0.03470 = 0.02248 -0.00364 -0.00432 -0.00182 AFIX 43 H6 2 0.428330 0.926887 0.882634 11.00000 -1.20000 AFIX 0 C7 1 0.450170 0.942020 0.727122 11.00000 0.03024 0.02959 = 0.02156 -0.00441 -0.00258 -0.00460 AFIX 43 H7 2 0.589730 0.921542 0.710738 11.00000 -1.20000 AFIX 0 C8 1 0.046513 0.989460 0.958629 11.00000 0.03702 0.03123 = 0.02981 -0.00415 -0.00100 -0.00414 N4 4 -0.000416 0.497416 0.954259 11.00000 0.03615 0.04050 = 0.02932 -0.00764 -0.00204 -0.00806 C9 1 0.189927 0.457689 0.893217 11.00000 0.04061 0.03742 = 0.03182 -0.00957 -0.00015 -0.00521 C10 1 0.203635 0.476800 0.785939 11.00000 0.04668 0.03454 = 0.03145 -0.00273 -0.00552 -0.00533 AFIX 43 H10 2 0.090619 0.509976 0.757669 11.00000 -1.20000 AFIX 0 C11 1 0.387167 0.445977 0.721535 11.00000 0.04733 0.03554 = 0.03029 -0.00722 0.00372 -0.00392 AFIX 43 H11 2 0.399008 0.460948 0.648643 11.00000 -1.20000 AFIX 0 C12 1 0.552111 0.393974 0.762147 11.00000 0.04447 0.04144 = 0.03773 -0.01027 0.00040 -0.00615 AFIX 43 H12 2 0.676269 0.374130 0.717658 11.00000 -1.20000 AFIX 0 C13 1 0.532830 0.371178 0.869696 11.00000 0.03903 0.04376 = 0.04025 -0.01810 -0.00418 -0.00167 AFIX 43 H13 2 0.644947 0.334787 0.898137 11.00000 -1.20000 AFIX 0 C14 1 0.353286 0.400740 0.935275 11.00000 0.04382 0.04581 = 0.02935 -0.01044 -0.00659 -0.00425 AFIX 43 H14 2 0.341359 0.382421 1.008291 11.00000 -1.20000 AFIX 0 HKLF 4 REM BB70 clathrate REM wR2 = 0.1255, GooF = S = 1.069, Restrained GooF = 1.069 for all data REM R1 = 0.0493 for 2456 Fo > 4sig(Fo) and 0.0494 for all 2462 data REM 175 parameters refined using 0 restraints END WGHT 0.1034 1.2192 REM Highest difference peak 2.993, deepest hole -2.266, 1-sigma level 0.249 Q1 1 0.0492 0.5240 0.4280 11.00000 0.05 2.99 Q2 1 -0.0600 0.4133 0.4850 11.00000 0.05 2.56 Q3 1 0.9875 0.8271 0.5020 11.00000 0.05 2.25 Q4 1 0.4163 0.9592 0.5819 11.00000 0.05 1.04 Q5 1 0.8534 0.5782 0.6332 11.00000 0.05 0.96 ; _shelx_res_checksum 48413 _shelx_hkl_file ; -2 -3 -4 136.39 7.53 0 -3 -4 -8 240.44 18.36 0 -3 -3 -5 2490.15 31.04 0 0 -3 -3 755.25 12.85 0 1 -4 -7 316.38 14.64 0 -4 -3 -7 401.85 20.00 0 -4 -1 -4 298.84 11.54 0 -2 -4 -6 824.63 21.20 0 -1 -3 -3 1655.34 19.20 0 2 -2 -3 1168.37 13.70 0 -4 -2 -5 450.96 15.33 0 -1 -4 -5 471.56 15.00 0 -5 -2 -8 266.11 25.34 0 -3 -4 -7 346.01 18.33 0 -2 -2 -2 3800.28 25.79 0 2 -3 -5 536.04 13.51 0 -3 -2 -3 139.27 7.97 0 -2 -5 -11 50.36 14.61 0 -2 -5 -10 141.52 20.14 0 -2 -4 -5 919.70 20.68 0 -4 -3 -6 200.99 14.64 0 -2 -3 -3 288.69 10.29 0 -1 -5 -8 758.89 25.06 0 0 -5 -9 118.08 16.88 0 -5 -2 -7 334.45 24.79 0 -3 -4 -6 158.64 13.77 0 -3 -3 -4 1226.66 21.42 0 -5 -3 -9 273.25 30.03 0 -3 -5 -11 456.62 30.31 0 -1 -4 -4 276.36 10.43 0 0 -4 -4 1009.27 18.48 0 1 -4 -5 73.75 8.69 0 -3 -5 -9 375.24 24.91 0 -2 -5 -7 482.06 21.16 0 -1 -3 -2 3024.94 24.91 0 0 -5 -7 111.11 13.36 0 0 -3 -2 761.50 12.62 0 -5 -3 -8 269.41 25.92 0 -4 -3 -5 249.45 14.57 0 -2 -4 -4 1270.86 22.62 0 -1 -5 -6 528.95 19.79 0 2 -3 -4 775.54 15.08 0 -3 -5 -8 206.35 17.27 0 -2 -5 -6 411.90 19.29 0 0 -5 -6 224.73 14.71 0 -4 -1 -3 587.93 13.68 0 -1 -4 -3 808.63 16.65 0 -5 -3 -7 308.98 23.93 0 0 -4 -3 605.48 13.84 0 -4 -4 -6 665.20 24.87 0 -2 -2 -1 2912.86 23.26 0 1 -3 -2 1330.83 17.01 0 1 -2 -1 785.30 10.11 0 -3 -4 -4 437.33 16.31 0 -2 -5 -5 221.29 15.28 0 -2 -4 -3 724.37 17.73 0 -4 -3 -4 466.46 16.51 0 -1 -6 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14.52 0 1 0 -10 92.57 20.72 0 -3 1 -9 1195.09 37.36 0 0 -1 -8 402.06 19.08 0 0 0 -11 1076.67 39.61 0 -1 -1 -6 1617.08 27.40 0 -1 0 -11 1200.52 40.46 0 -1 -1 -8 643.60 24.77 0 -2 1 -12 367.78 32.10 0 0 -1 -3 908.51 13.20 0 2 -1 -5 184.79 10.27 0 -1 -1 -9 1605.11 39.01 0 2 0 -10 166.76 26.88 0 -1 1 -13 696.77 42.61 0 1 -1 -9 952.75 30.31 0 -4 2 -8 597.08 40.25 0 -3 0 -6 496.23 21.21 0 -1 6 0 232.53 15.41 0 0 6 -1 284.01 15.36 0 1 3 -3 878.50 17.00 0 0 3 -3 512.12 13.26 0 2 5 -2 187.00 13.76 0 2 6 -1 402.83 20.55 0 3 3 -2 1454.41 25.36 0 -1 2 -2 1027.55 14.25 0 0 1 -2 2398.58 18.08 0 1 2 -3 765.98 15.05 0 1 4 -3 130.00 11.22 0 1 7 0 196.98 18.43 0 2 1 -2 367.45 9.65 0 0 4 -3 962.84 21.33 0 3 2 -2 320.08 13.40 0 4 3 -1 29.61 13.36 0 0 2 -3 787.28 14.49 0 0 7 0 152.31 21.23 0 4 4 -1 573.89 27.76 0 -2 3 -1 615.94 14.75 0 -2 4 -1 967.09 22.57 0 -1 5 -2 1149.99 26.65 0 1 6 -2 140.29 17.47 0 0 6 -2 796.42 27.32 0 1 6 -3 46.82 17.29 0 2 3 -4 383.18 19.46 0 -2 4 -2 1336.51 27.75 0 -1 2 -3 193.09 8.63 0 0 6 -3 668.05 27.56 0 2 4 -4 1033.15 31.68 0 4 3 -2 195.12 20.91 0 -2 3 -2 637.00 16.13 0 0 2 -4 1675.04 24.70 0 0 5 -4 256.99 18.99 0 3 2 -3 15.30 10.76 0 3 5 -3 418.51 29.12 0 -1 4 -4 416.33 18.66 0 2 6 -3 365.19 23.19 0 -1 3 -4 751.70 19.46 0 0 7 -2 117.23 17.48 0 2 5 -4 56.56 18.36 0 1 3 -5 1823.49 33.48 0 -1 1 -2 3692.59 25.39 0 0 3 -5 157.55 13.01 0 0 4 -5 756.27 25.01 0 -2 4 -3 614.50 21.09 0 0 6 -4 529.96 25.73 0 1 6 -4 115.10 18.42 0 3 3 -4 1280.25 34.11 0 -2 3 -3 41.55 8.72 0 -1 2 -4 473.81 14.22 0 1 5 -5 855.21 30.71 0 2 4 -5 504.37 25.76 0 1 1 -4 1611.52 22.95 0 1 2 -5 305.62 13.23 0 4 4 -3 365.56 31.08 0 -2 2 -2 4482.48 33.12 0 -1 4 -5 315.00 17.44 0 0 2 -5 549.83 15.60 0 3 5 -4 386.56 29.47 0 4 3 -3 40.73 19.81 0 -1 6 -4 346.04 23.97 0 2 5 -5 147.97 21.03 0 3 2 -4 209.43 15.13 0 0 3 -6 137.27 14.48 0 0 4 -6 732.02 26.57 0 1 3 -6 568.20 22.64 0 1 6 -5 61.35 18.05 0 -2 3 -4 161.90 12.42 0 -2 5 -4 324.10 24.01 0 -1 2 -5 252.91 13.46 0 0 5 -6 169.80 21.75 0 1 5 -6 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134.97 16.62 0 2 8 2 456.77 19.69 0 -1 4 -4 457.57 19.23 0 1 7 -1 288.58 19.69 0 3 7 2 368.98 21.41 0 -3 5 -2 351.56 20.76 0 -3 6 -1 131.31 16.96 0 -3 7 1 360.82 21.78 0 2 6 -1 435.13 22.98 0 0 7 -1 207.45 16.19 0 0 8 1 213.91 16.22 0 2 4 -2 1135.32 30.62 0 3 5 0 267.29 21.27 0 -3 4 -2 381.97 20.02 0 -3 7 2 567.16 27.28 0 -1 5 -3 776.65 23.60 0 0 5 -3 290.28 17.29 0 2 8 3 575.07 21.16 0 3 6 1 125.42 18.19 0 -2 8 3 419.39 22.87 0 0 6 -2 801.49 25.26 0 1 8 2 29.14 11.98 0 3 7 3 327.81 19.21 0 -3 5 -1 496.31 21.75 0 -1 8 2 126.35 14.33 0 0 4 -3 1025.47 24.80 0 1 5 -2 1078.38 27.86 0 2 5 -1 225.36 17.81 0 -3 7 3 353.03 23.75 0 -1 4 -3 286.97 14.77 0 0 8 2 250.00 16.96 0 1 6 -1 83.51 14.18 0 2 6 0 515.28 22.77 0 2 8 4 447.47 19.10 0 0 7 0 143.98 14.95 0 -3 7 4 311.83 25.16 0 1 8 3 108.11 13.44 0 -3 4 -1 128.49 15.32 0 -3 6 1 194.72 17.43 0 -1 5 -2 1074.51 24.89 0 -1 6 -1 72.19 12.28 0 -1 8 3 106.56 14.41 0 0 5 -2 358.88 17.11 0 0 6 -1 331.05 17.50 0 3 5 1 445.27 22.63 0 3 7 4 391.03 19.56 0 0 8 3 224.46 17.09 0 2 4 -1 932.50 25.98 0 -3 5 0 634.06 23.45 0 -1 8 4 196.55 16.59 0 1 8 4 159.48 14.69 0 0 4 -2 1379.53 25.77 0 2 5 0 196.89 15.52 0 2 6 1 121.43 16.13 0 -1 4 -2 561.62 16.35 0 0 8 4 235.68 17.49 0 3 4 1 145.07 20.12 0 3 7 5 458.61 20.32 0 -1 6 0 232.17 14.33 0 -1 8 5 162.82 16.85 0 0 6 0 992.91 24.91 0 1 8 5 109.06 13.86 0 -2 7 3 196.40 17.72 0 -1 5 -1 901.61 22.02 0 -1 7 2 548.64 21.73 0 0 5 -1 529.30 18.04 0 -3 6 3 124.91 16.86 0 -1 8 6 36.82 14.38 0 0 7 2 179.66 14.63 0 0 8 5 78.44 15.28 0 3 5 2 429.25 21.36 0 1 4 -1 447.83 16.38 0 1 8 6 84.91 13.05 0 3 7 6 525.87 20.10 0 -2 5 0 230.68 14.19 0 -2 7 4 138.20 16.97 0 0 8 6 154.24 15.67 0 1 6 1 68.33 12.49 0 2 6 2 1143.26 28.11 0 -3 6 4 240.54 22.29 0 -1 6 1 226.07 14.16 0 0 6 1 1245.98 26.40 0 3 7 7 371.57 18.77 0 -2 6 2 665.41 22.58 0 -2 7 5 177.63 18.38 0 0 8 8 127.68 13.83 0 0 8 9 101.33 11.61 0 1 8 8 33.87 10.88 0 1 8 10 19.76 8.18 0 -3 6 5 129.96 19.19 0 -1 5 0 1347.59 24.88 0 0 5 0 70.45 10.71 0 1 8 9 53.59 10.12 0 -2 7 9 129.88 17.08 0 -1 7 4 400.68 21.66 0 1 7 4 555.68 21.72 0 3 4 2 366.57 19.97 0 3 5 3 441.16 20.51 0 3 7 8 303.66 15.09 0 -3 6 6 85.20 21.13 0 -2 4 0 1392.66 24.94 0 -2 7 7 64.59 18.03 0 -2 7 8 162.35 22.27 0 -2 6 3 282.76 18.49 0 -1 6 2 217.47 14.75 0 3 6 5 152.36 15.70 0 3 7 9 409.43 15.60 0 3 7 10 203.54 12.97 0 -3 5 3 377.92 20.22 0 -1 7 5 316.21 21.28 0 0 6 2 1196.64 26.46 0 1 5 1 1339.54 26.14 0 2 4 1 807.12 22.15 0 1 7 5 409.55 20.80 0 2 5 2 538.60 19.62 0 0 7 5 123.83 17.01 0 -2 6 4 409.39 20.69 0 -1 5 1 863.27 19.30 0 -1 7 6 353.31 23.60 0 -1 7 11 198.27 14.24 0 0 5 1 151.03 11.20 0 -2 5 2 586.90 19.05 0 -1 6 3 171.00 14.13 0 1 7 6 217.58 19.41 0 3 5 4 314.60 18.13 0 3 6 6 100.47 14.63 0 -1 7 7 287.84 22.86 0 0 6 3 1047.32 25.40 0 0 7 6 107.78 17.51 0 2 7 8 63.42 12.66 0 -2 4 1 1450.73 26.31 0 -3 5 5 329.32 21.88 0 -2 6 5 592.56 24.60 0 -2 6 11 305.60 18.85 0 1 5 2 1473.00 26.75 0 1 7 7 339.87 21.02 0 2 5 3 209.44 14.74 0 2 7 9 126.52 13.16 0 2 7 11 0.10 8.61 0 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191.84 18.16 0 2 6 13 182.32 11.50 0 -1 6 9 174.52 21.74 0 0 6 7 970.19 31.76 0 2 6 9 286.95 18.70 0 2 6 12 104.79 11.82 0 3 5 7 231.54 17.04 0 -3 4 6 56.65 19.41 0 -2 5 6 85.23 17.31 0 0 5 4 279.74 14.79 0 0 6 12 140.80 12.82 0 2 6 10 321.08 19.40 0 2 6 11 415.62 18.72 0 3 4 5 196.74 15.27 0 0 6 8 556.44 26.41 0 3 5 14 201.38 11.33 0 -2 5 7 89.35 19.56 0 0 6 9 454.66 25.86 0 1 6 9 207.24 19.13 0 1 6 12 179.45 14.21 0 3 5 8 216.45 16.55 0 -2 5 10 138.69 20.85 0 -1 5 5 651.72 21.45 0 1 5 5 847.29 24.06 0 1 6 10 107.26 17.17 0 1 6 11 214.20 17.67 0 2 5 15 89.02 7.60 0 -2 4 4 1185.44 26.36 0 -2 5 9 126.65 23.22 0 -1 4 3 460.33 16.30 0 -1 5 13 289.67 13.55 0 0 5 5 351.00 17.83 0 1 5 15 199.38 9.28 0 3 5 9 347.24 18.24 0 3 5 13 145.81 10.90 0 -1 5 6 1017.69 29.16 0 3 4 6 156.90 14.59 0 3 5 10 198.05 14.90 0 3 5 12 313.37 14.81 0 1 5 6 412.84 20.31 0 4 4 10 210.18 16.64 0 4 4 12 318.88 17.11 0 0 5 6 175.85 16.48 0 2 5 14 62.92 8.66 0 -2 4 12 338.95 17.93 0 1 5 14 333.84 13.34 0 2 5 8 87.14 14.79 0 3 4 15 112.58 9.27 0 -1 4 4 794.93 20.12 0 -1 5 8 563.53 28.55 0 1 4 4 492.42 15.89 0 2 4 5 1018.59 23.68 0 -1 4 14 36.74 7.41 0 -1 5 9 626.89 30.26 0 0 5 7 85.38 16.25 0 3 4 7 317.54 17.53 0 -4 5 9 146.39 14.83 0 -2 5 4 163.33 17.43 0 -4 5 8 160.28 17.52 0 -1 5 7 529.94 22.30 0 -1 5 9 654.44 23.70 0 -4 5 7 547.85 28.49 0 -2 5 10 140.24 14.28 0 -1 5 8 638.16 23.32 0 0 4 5 864.87 21.77 0 0 4 11 567.02 18.72 0 1 2 12 64.02 10.69 0 -3 5 5 375.82 23.22 0 -2 5 9 109.05 15.77 0 -1 4 12 127.59 12.03 0 1 1 12 390.59 16.30 0 -3 5 6 793.46 31.02 0 -3 5 8 182.18 17.54 0 -2 5 7 85.18 17.19 0 1 3 7 1442.20 26.70 0 1 3 8 944.32 22.62 0 -3 5 7 228.80 19.70 0 -1 1 14 337.79 11.88 0 0 2 13 479.15 15.18 0 0 3 12 143.86 12.43 0 0 4 7 1027.91 23.28 0 0 4 8 466.89 17.32 0 0 4 9 688.25 19.91 0 1 2 11 373.52 14.91 0 -4 3 12 45.85 5.53 0 -2 1 14 45.08 6.48 0 -1 3 13 510.06 15.08 0 -5 4 8 120.09 14.39 0 -2 3 13 170.51 9.66 0 -1 4 11 417.92 15.77 0 -3 4 11 108.08 10.06 0 0 1 13 141.13 10.48 0 1 1 11 235.55 15.10 0 1 2 10 70.21 10.12 0 -2 4 11 235.07 13.89 0 -1 4 10 0.35 10.68 0 0 3 11 168.49 12.85 0 -5 4 7 118.92 17.36 0 1 2 9 37.05 9.58 0 -5 4 6 160.22 25.06 0 -3 2 13 69.19 6.31 0 -2 4 3 490.65 20.10 0 -1 3 12 304.23 14.38 0 0 2 12 467.27 16.15 0 -3 3 12 415.22 12.86 0 -3 4 10 101.17 12.34 0 -2 4 10 275.14 16.46 0 -1 4 6 130.97 11.91 0 -1 4 8 352.27 17.11 0 0 3 10 321.36 14.47 0 1 2 8 33.89 7.60 0 -4 2 12 184.41 8.55 0 -2 2 13 494.76 13.59 0 1 1 10 911.83 20.55 0 -1 0 13 22.16 8.63 0 -1 1 13 581.57 15.21 0 0 3 9 263.55 13.23 0 -4 4 8 471.03 20.24 0 -3 4 3 237.27 20.04 0 -3 4 9 169.88 14.90 0 -1 3 11 744.28 20.53 0 0 0 12 460.30 17.33 0 0 3 8 315.02 13.45 0 -2 4 8 277.51 17.73 0 -4 4 4 757.40 30.44 0 -4 4 7 508.95 23.44 0 -3 4 8 154.04 16.37 0 -2 0 13 521.59 13.65 0 -2 4 7 675.06 23.27 0 -4 1 12 202.77 8.36 0 -4 4 5 805.90 31.23 0 -4 4 6 244.84 21.44 0 -3 4 4 217.79 19.29 0 -1 3 10 479.28 17.69 0 -5 2 10 62.38 7.19 0 -4 3 10 49.77 8.60 0 -3 4 5 71.87 16.46 0 -3 4 6 69.51 16.65 0 -2 2 12 588.18 16.55 0 0 1 11 247.49 13.35 0 -2 3 10 279.60 15.57 0 -1 1 12 518.78 15.66 0 -1 3 9 559.88 18.55 0 -3 3 10 596.90 18.66 0 -1 2 11 838.54 20.77 0 0 2 9 943.98 19.95 0 -4 3 9 65.45 10.81 0 -1 0 12 24.42 8.37 0 -1 3 8 892.04 22.01 0 -6 2 7 451.29 17.89 0 -3 -1 12 285.32 10.75 0 -1 3 7 573.70 18.07 0 0 2 8 653.01 16.61 0 -3 3 9 557.06 19.60 0 -2 -1 12 65.13 9.99 0 -2 2 11 641.41 18.53 0 -1 3 6 1150.66 23.14 0 0 1 10 388.95 15.06 0 -5 1 10 310.31 10.55 0 -5 2 9 85.75 8.53 0 -2 0 12 468.45 14.36 0 -1 2 10 259.28 13.85 0 -4 2 10 381.55 14.29 0 -2 3 8 330.23 17.05 0 -1 1 11 766.60 19.64 0 -5 3 5 251.98 23.25 0 -6 2 6 394.06 19.78 0 -5 3 4 506.46 30.12 0 -4 -1 11 140.42 8.68 0 -2 2 10 203.56 13.80 0 -2 3 7 346.77 17.95 0 0 1 9 275.08 12.42 0 -5 0 10 131.61 7.98 0 -3 1 11 482.96 16.00 0 -3 2 10 168.06 13.49 0 -2 1 11 171.43 12.56 0 -5 2 8 84.25 10.42 0 -3 3 7 687.45 23.43 0 -6 2 5 491.96 25.32 0 -4 3 6 363.90 21.90 0 -6 0 8 273.82 10.26 0 -5 1 9 306.87 12.12 0 -4 3 3 130.78 24.03 0 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395.67 16.07 0 -6 1 4 112.93 18.72 0 -5 2 2 157.99 27.24 0 -3 1 8 410.11 18.16 0 -2 1 8 322.23 15.84 0 -5 -1 8 360.52 14.15 0 -4 -1 9 154.96 11.94 0 -7 0 2 83.36 22.70 0 -5 1 6 438.29 19.02 0 -4 2 4 1178.92 33.95 0 -3 -3 9 529.41 16.52 0 -3 2 5 209.38 16.40 0 -2 -3 9 204.95 15.38 0 -6 -3 6 65.43 7.00 0 -5 0 7 187.73 14.07 0 -1 0 8 53.44 10.37 0 -7 0 1 142.42 30.58 0 -6 -1 6 83.91 9.73 0 -4 2 3 741.73 30.45 0 -2 -1 9 117.67 12.59 0 -2 1 7 123.45 12.22 0 -6 1 2 148.62 27.14 0 -4 2 2 1264.69 39.69 0 -3 -2 9 460.83 17.04 0 -3 1 7 567.31 20.33 0 -6 1 1 137.49 35.02 0 -5 -3 7 302.67 12.44 0 -4 -3 8 18.30 8.31 0 -4 -1 8 142.78 12.76 0 -4 1 6 926.82 25.62 0 -3 0 8 97.82 12.71 0 -5 -2 7 74.02 10.26 0 -5 0 6 92.72 10.28 0 -4 -2 8 474.86 17.31 0 -4 0 7 718.72 22.60 0 -4 1 5 217.52 16.54 0 -5 1 3 1023.77 33.83 0 -3 0 7 810.73 23.05 0 -2 0 7 764.54 20.89 0 -7 -1 1 223.85 24.97 0 -6 0 3 681.99 28.34 0 -5 0 5 490.10 20.81 0 -4 -1 7 216.47 15.12 0 -7 -3 2 357.71 14.79 0 -6 -4 4 237.18 11.16 0 -5 1 2 1205.33 39.45 0 -1 -1 7 794.01 20.29 0 -7 -1 0 315.64 31.43 0 -5 -2 6 56.49 11.52 0 -3 -4 7 93.17 11.68 0 -5 1 1 624.45 36.98 0 -2 -4 7 722.01 24.00 0 -7 -2 1 248.77 18.68 0 -7 -1 -1 477.09 41.00 0 -6 -3 4 288.39 13.95 0 -5 0 4 359.05 19.70 0 -5 1 0 1332.98 52.16 0 -4 1 3 390.59 21.18 0 -3 -5 6 251.65 14.81 0 -3 0 6 500.84 19.23 0 -3 1 4 706.71 20.36 0 -2 0 6 933.81 22.16 0 -6 -1 3 108.17 16.08 0 -6 0 1 998.46 41.28 0 -4 -4 6 192.65 12.96 0 -3 -3 7 308.45 16.36 0 -6 0 0 991.56 46.07 0 -4 1 2 481.51 24.00 0 -2 -2 7 737.50 21.14 0 -7 -2 0 154.81 20.26 0 -5 -3 5 126.33 12.78 0 -5 -2 5 300.19 16.84 0 -4 -5 5 237.78 12.93 0 -7 -4 0 127.00 11.23 0 -6 -5 2 43.05 7.51 0 -6 -2 3 278.42 16.99 0 -6 0 -1 361.38 39.19 0 -4 -3 6 163.81 14.18 0 -4 -2 6 176.65 12.83 0 -3 0 5 457.35 18.05 0 -6 -3 3 143.39 12.51 0 -5 -1 4 738.00 23.72 0 -4 0 4 1386.15 29.54 0 -7 -2 -1 86.80 22.26 0 -3 -4 6 195.18 14.45 0 -7 -2 -2 247.08 29.05 0 -5 -4 4 198.93 13.11 0 -3 -2 6 238.18 14.50 0 -7 -3 -1 355.48 21.90 0 -6 -4 2 309.73 14.70 0 -6 -2 2 324.82 19.18 0 -5 -2 4 161.73 12.79 0 -6 -3 2 218.26 15.07 0 -5 -5 3 369.66 14.47 0 -5 -1 3 820.73 25.13 0 -5 0 1 56.01 17.51 0 -4 -2 5 543.35 20.46 0 -4 0 3 1440.30 29.53 0 -2 -2 6 604.63 18.52 0 -4 -6 3 295.41 13.44 0 -3 -1 5 1177.02 25.30 0 -2 -3 6 466.44 18.15 0 -7 -4 -2 195.51 15.67 0 -4 -1 4 106.63 12.30 0 -2 5 8 78.39 18.60 0 -2 5 10 100.95 17.68 0 1 5 13 361.38 14.82 0 2 3 16 33.92 5.57 0 4 2 10 382.03 20.91 0 4 2 11 899.53 26.38 0 0 5 13 160.17 11.01 0 -1 5 7 539.50 23.29 0 1 5 9 571.18 21.61 0 1 5 12 246.06 15.24 0 3 3 7 1085.95 25.09 0 3 3 14 337.16 12.08 0 1 4 15 54.46 6.88 0 1 5 10 598.75 22.73 0 1 5 11 343.66 18.22 0 2 4 7 760.38 20.81 0 2 4 14 256.17 11.61 0 3 2 15 140.47 9.39 0 -1 5 8 584.53 24.97 0 0 4 15 375.79 10.95 0 0 5 8 219.54 17.23 0 0 5 12 84.83 12.21 0 -2 4 13 296.60 11.67 0 -1 5 10 254.73 19.69 0 0 5 9 123.14 16.24 0 0 5 11 138.53 16.36 0 1 3 16 278.10 9.63 0 3 3 8 823.04 23.14 0 2 2 16 208.91 9.07 0 1 4 6 211.82 12.90 0 2 4 12 201.82 13.73 0 3 3 9 1205.91 27.47 0 3 3 12 493.58 16.81 0 -2 4 5 1081.18 28.53 0 0 4 5 967.67 22.19 0 1 4 14 81.54 7.76 0 2 4 10 610.92 19.65 0 2 4 11 657.38 19.89 0 3 3 10 780.69 22.81 0 3 3 11 667.26 20.51 0 0 4 14 342.01 12.89 0 3 2 14 139.17 9.88 0 -2 4 12 354.04 15.19 0 -1 4 5 82.96 11.55 0 1 4 7 375.68 16.62 0 2 3 6 581.62 17.06 0 -2 3 14 179.38 8.66 0 -1 3 15 294.02 9.75 0 2 3 14 17.58 8.24 0 3 2 7 812.72 22.85 0 -3 3 12 448.47 17.55 0 -2 4 6 576.84 24.49 0 0 4 6 1316.38 27.14 0 1 2 16 32.99 5.98 0 3 2 13 272.62 12.64 0 -2 4 11 215.94 16.66 0 1 4 12 152.37 14.21 0 3 1 14 356.37 13.63 0 -1 4 6 132.95 13.80 0 0 2 16 147.66 7.02 0 0 3 15 80.62 7.34 0 1 4 9 140.10 13.59 0 1 4 10 73.66 12.71 0 1 4 11 382.87 18.31 0 2 3 7 229.59 12.78 0 2 3 13 118.93 11.27 0 -2 4 7 694.48 28.07 0 -2 4 10 200.03 19.81 0 0 4 7 1110.33 27.36 0 0 4 12 309.36 17.18 0 -2 4 8 245.09 22.50 0 -2 4 9 696.76 28.92 0 2 3 8 78.24 10.95 0 3 2 10 218.34 15.37 0 3 2 11 167.46 13.72 0 -1 4 7 379.65 20.54 0 0 4 8 555.56 22.27 0 0 4 11 569.18 22.67 0 1 3 14 486.80 15.79 0 -2 3 13 198.33 10.77 0 -1 3 14 289.59 11.46 0 -1 4 8 384.05 21.96 0 0 4 9 676.11 24.26 0 0 4 10 522.28 22.52 0 2 3 10 23.19 9.65 0 2 3 11 56.92 11.07 0 3 1 13 317.45 13.58 0 0 1 16 147.58 6.90 0 0 3 14 96.99 9.92 0 1 2 15 35.28 6.99 0 2 1 15 103.54 8.44 0 -1 2 15 208.33 8.58 0 1 3 13 764.44 20.47 0 -3 3 10 609.04 26.92 0 0 2 15 323.90 11.06 0 3 0 13 102.74 12.20 0 3 1 12 496.14 16.96 0 -2 3 12 205.09 12.86 0 -1 3 13 449.64 15.74 0 0 3 13 115.35 11.88 0 1 3 7 1732.76 28.07 0 1 3 12 393.11 17.92 0 3 1 8 705.61 24.04 0 3 1 11 634.92 20.02 0 1 2 14 24.90 8.80 0 1 3 11 382.26 17.52 0 2 1 14 87.19 9.57 0 3 1 10 613.74 21.33 0 -3 2 12 55.88 8.96 0 1 1 15 285.15 10.89 0 1 3 8 792.28 21.10 0 -2 3 11 218.87 15.94 0 -1 1 15 347.66 10.15 0 -1 2 14 101.83 8.81 0 -1 3 12 300.99 16.14 0 0 3 12 172.39 14.84 0 3 0 12 92.99 11.21 0 -3 1 13 250.98 9.82 0 0 3 11 171.00 15.08 0 -2 1 14 51.81 6.50 0 -2 3 6 410.28 21.97 0 -1 3 11 620.66 21.63 0 0 3 7 216.42 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389.63 16.42 0 -3 0 12 96.53 8.68 0 -2 1 12 60.58 9.90 0 -1 -2 14 118.54 6.68 0 -1 -1 14 237.31 9.14 0 0 -1 14 84.63 7.53 0 0 2 10 493.40 18.66 0 -2 0 13 483.41 13.36 0 -1 2 10 255.27 15.53 0 2 0 11 611.40 17.71 0 -4 0 10 347.30 14.43 0 -4 1 8 93.94 17.40 0 -2 2 9 1595.28 32.86 0 0 1 12 157.61 13.05 0 1 -3 13 307.55 11.72 0 1 1 11 169.82 12.45 0 2 -1 12 342.85 14.62 0 2 -2 12 222.27 12.84 0 -3 1 10 544.94 17.82 0 -2 -1 13 140.75 8.35 0 -1 0 13 23.65 8.53 0 0 0 13 552.11 16.41 0 1 -1 13 702.24 17.06 0 2 0 10 919.65 20.27 0 -2 -2 13 213.57 8.36 0 -2 1 11 185.48 13.27 0 -1 2 8 657.16 21.48 0 1 -2 13 30.62 7.89 0 1 0 12 293.23 14.48 0 1 1 10 866.34 20.82 0 -3 -2 12 79.83 6.56 0 -1 2 7 1009.69 24.90 0 0 1 11 239.67 14.08 0 -2 0 12 581.23 16.44 0 -1 -3 13 313.24 9.63 0 -1 1 11 769.65 21.20 0 0 -3 13 141.65 8.10 0 0 -1 13 163.50 10.45 0 1 1 9 1482.97 24.93 0 2 0 9 945.36 20.52 0 -4 -1 10 129.76 10.61 0 -4 0 9 486.06 17.78 0 -1 -1 13 332.86 12.13 0 -1 -2 13 117.73 8.07 0 0 -2 13 569.44 14.38 0 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572.47 17.17 0 1 -2 11 284.74 13.18 0 0 -1 11 186.39 11.82 0 -5 -3 7 431.40 15.18 0 -4 -3 9 40.90 7.64 0 -2 1 7 140.22 13.33 0 -1 -1 11 374.61 15.09 0 2 -2 9 1327.58 25.08 0 -2 -5 10 35.50 5.18 0 -2 -3 11 151.74 8.96 0 -2 -2 11 634.23 16.23 0 -1 -4 11 152.93 8.43 0 -1 1 7 1359.11 25.32 0 0 -4 11 462.47 13.31 0 -4 -1 8 131.97 11.95 0 -3 -2 10 19.56 7.88 0 -3 0 8 85.03 11.46 0 -2 0 9 1086.83 23.18 0 -1 -2 11 394.56 14.52 0 0 -5 10 178.80 9.40 0 -2 -1 10 120.83 11.21 0 -1 -3 11 468.02 14.25 0 1 -2 10 148.31 11.54 0 -5 -2 6 68.95 14.05 0 0 -1 10 444.99 15.65 0 1 -1 9 1884.88 27.65 0 1 -3 10 309.47 13.47 0 -5 -4 6 27.78 8.11 0 -4 -2 8 470.24 15.45 0 -3 0 7 836.26 21.48 0 -2 -4 10 263.23 10.67 0 -2 0 8 1086.31 23.13 0 -3 -4 9 250.60 9.98 0 -3 -2 9 442.38 15.47 0 -2 -3 10 268.13 12.23 0 -1 0 8 47.17 9.12 0 0 -4 10 281.32 12.56 0 0 -2 10 384.69 14.77 0 1 -1 8 1110.52 21.00 0 -4 -5 7 90.49 6.98 0 -2 -5 9 45.52 6.28 0 -1 -4 10 66.36 8.48 0 -1 -2 10 247.00 12.77 0 0 -1 9 309.06 13.34 0 1 -2 9 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0 8 83.72 11.83 0 -2 -5 7 42.16 10.18 0 -2 -2 9 417.85 16.28 0 0 -1 7 825.25 18.40 0 -5 -3 7 362.28 12.19 0 -4 -1 8 121.05 12.11 0 -2 -4 8 515.98 16.69 0 -5 0 6 131.21 12.83 0 -2 1 6 506.77 16.98 0 -1 -3 8 751.23 20.44 0 -1 -1 8 819.20 19.13 0 -1 0 7 411.02 14.20 0 0 -2 7 1393.88 24.55 0 -6 -1 5 143.46 13.35 0 -5 -5 5 116.87 8.79 0 -4 -4 7 470.30 14.22 0 -1 -5 6 284.52 15.99 0 -5 -4 6 15.35 6.63 0 -4 1 5 199.16 15.58 0 -3 -3 8 435.33 16.46 0 -2 -3 8 400.06 16.58 0 -2 -1 8 367.49 14.79 0 -1 -4 7 237.80 14.27 0 -6 -2 5 357.95 14.01 0 -3 -2 8 35.13 9.87 0 -3 0 7 845.74 22.07 0 -2 -2 8 805.02 20.61 0 -2 0 7 783.46 19.51 0 -5 0 5 473.56 18.76 0 -4 -1 7 216.82 14.34 0 -3 -5 6 254.64 12.25 0 -3 -4 7 101.99 10.83 0 -3 1 5 1570.30 29.27 0 -2 -5 6 91.92 10.66 0 -2 -4 7 726.77 20.47 0 -5 -3 6 474.07 15.55 0 -4 -6 4 280.03 11.39 0 -4 0 6 262.29 15.42 0 -1 -3 7 548.71 17.58 0 -7 -3 2 361.74 15.03 0 -7 -2 2 107.39 12.83 0 -6 -1 4 163.34 13.49 0 -1 -2 7 762.55 18.79 0 -3 -1 7 485.13 17.26 0 -1 -5 5 893.71 25.16 0 -5 -4 5 179.48 10.94 0 -4 -4 6 198.05 12.35 0 -3 -3 7 313.41 15.66 0 -2 -3 7 286.25 14.95 0 -2 0 6 928.73 20.54 0 -1 -4 6 200.83 14.33 0 -5 -5 4 152.21 9.48 0 -3 -6 4 161.55 11.06 0 -3 -2 7 153.09 12.56 0 -2 -2 7 840.96 20.61 0 -5 -1 5 195.69 14.68 0 -4 -3 6 143.39 12.81 0 -4 0 5 858.46 22.88 0 -3 -4 6 206.85 13.92 0 -2 -4 6 446.41 17.97 0 -6 -5 2 47.86 7.10 0 -6 -4 3 205.42 10.90 0 -6 -1 3 99.86 13.41 0 -5 -3 5 151.81 12.37 0 -5 -2 5 234.32 14.77 0 -4 -2 6 222.34 14.36 0 -3 -5 5 326.67 14.77 0 -2 -5 5 147.67 12.81 0 -1 -3 6 590.47 18.15 0 -7 -3 1 238.96 13.02 0 -7 -2 1 212.75 15.52 0 -4 -6 3 310.54 12.58 0 -3 -1 6 841.29 21.19 0 -6 -3 3 126.18 10.96 0 -5 -4 4 208.88 12.51 0 -3 -3 6 802.18 21.65 0 -3 -2 6 244.37 13.95 0 -2 -3 6 484.53 17.29 0 -1 -5 4 854.24 23.95 0 -1 -4 5 175.18 13.68 0 -6 -2 3 241.00 14.60 0 -5 -5 3 410.58 14.20 0 -5 0 3 200.45 17.19 0 -4 -5 4 177.22 12.04 0 -2 -2 6 611.68 17.87 0 -4 -1 5 310.45 16.10 0 -4 0 4 1354.64 27.36 0 -7 -2 0 148.36 17.23 0 -4 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403.06 26.83 0 -3 1 -8 914.81 35.54 0 -2 6 -9 257.32 19.18 0 -5 3 -6 170.44 26.88 0 -5 5 -6 235.91 25.71 0 -5 6 -4 38.88 25.39 0 -4 1 -3 562.32 29.33 0 -4 2 -8 373.33 26.66 0 -2 3 -10 63.51 22.60 0 -2 4 -10 322.90 28.64 0 -5 3 -2 425.89 34.69 0 -5 4 -6 293.63 27.70 0 -5 6 -3 97.80 31.75 0 -3 2 -9 304.14 26.63 0 -4 5 -8 38.51 17.71 0 -4 2 -7 734.32 34.45 0 -4 3 -8 283.95 27.00 0 -4 7 -5 208.32 18.18 0 -3 1 -7 599.36 28.43 0 -4 4 -8 395.93 27.92 0 -3 3 -9 705.93 33.58 0 -3 6 -8 50.56 13.60 0 -2 2 -9 1321.08 40.98 0 -1 2 -9 39.77 23.48 0 -5 4 -4 93.96 29.20 0 -5 4 -3 268.91 33.20 0 -5 4 -2 369.16 35.08 0 -5 5 -2 739.69 46.92 0 -3 4 -9 62.60 19.96 0 -3 1 -6 751.45 29.80 0 -3 2 -8 469.89 29.14 0 -2 5 -9 251.94 21.72 0 -4 3 -7 461.98 30.32 0 -4 5 -7 71.41 22.20 0 -4 6 -6 245.20 21.75 0 -4 7 -4 135.27 19.02 0 -4 2 -5 734.72 33.17 0 -4 4 -7 463.03 30.12 0 -3 7 -6 163.99 16.11 0 -2 6 -8 371.31 22.89 0 -4 2 -4 1250.56 39.51 0 -3 5 -8 428.64 24.99 0 -2 4 -9 732.76 32.10 0 -1 4 -9 99.94 22.43 0 -1 6 -8 76.48 19.13 0 -4 2 -3 1048.30 39.48 0 -4 2 -2 1481.02 45.58 0 -4 3 -6 445.16 28.79 0 -3 2 -7 365.84 25.50 0 -2 2 -8 837.17 32.32 0 -4 5 -6 80.22 22.67 0 -4 6 -5 252.42 23.87 0 -3 4 -8 240.51 23.36 0 -3 6 -7 55.96 12.38 0 -4 4 -6 496.40 30.17 0 -1 2 -8 48.27 20.00 0 -4 3 -5 640.23 29.69 0 -4 5 -5 267.70 26.20 0 -4 6 -4 455.04 29.32 0 -3 2 -6 616.27 27.85 0 -3 7 -5 252.71 19.09 0 -4 3 -4 183.80 22.88 0 -4 3 0 526.36 32.80 0 -4 4 -5 463.45 28.07 0 -3 5 -7 353.04 25.11 0 -2 7 -6 50.06 12.31 0 -2 8 -4 217.22 16.12 0 -3 4 -7 184.42 21.50 0 -3 6 -6 93.80 18.55 0 -3 8 -1 110.98 22.66 0 -2 6 -7 217.41 18.70 0 -1 5 -8 328.14 23.54 0 -4 3 -2 385.34 27.80 0 -4 3 -1 421.77 30.46 0 -4 5 -4 45.74 22.45 0 -3 8 0 66.15 24.24 0 -1 3 -8 827.76 32.66 0 0 7 -6 63.82 14.76 0 -4 4 -2 628.14 29.27 0 -3 8 3 72.37 16.60 0 -2 8 1 488.64 21.98 0 0 5 -3 307.94 19.66 0 -4 6 0 770.11 30.52 0 -4 7 3 153.95 27.01 0 -2 7 -1 189.81 16.76 0 -1 8 1 84.19 14.23 0 2 4 -1 847.35 29.91 0 2 7 2 174.84 18.86 0 2 8 5 492.25 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550.37 19.73 0 -2 7 2 222.26 16.68 0 0 8 5 60.81 14.06 0 -4 6 4 436.42 27.30 0 -2 5 -1 539.58 18.25 0 -1 6 0 264.88 15.97 0 1 8 7 59.53 12.07 0 2 7 5 123.51 14.95 0 -3 4 -1 142.83 12.90 0 -3 7 4 314.50 20.23 0 -1 5 -1 972.34 23.34 0 -1 7 2 524.07 20.89 0 -4 6 5 678.92 33.10 0 -1 8 6 49.23 13.47 0 0 8 6 154.46 15.13 0 1 8 8 30.83 10.22 0 1 8 9 62.95 10.08 0 2 6 3 535.61 22.49 0 -3 7 5 327.12 21.08 0 -2 7 3 197.93 17.03 0 -3 6 2 413.56 19.39 0 -3 7 8 119.38 18.74 0 -2 6 1 543.26 19.45 0 -1 8 8 60.15 11.60 0 -1 8 9 117.61 11.86 0 0 4 -1 403.91 16.02 0 0 6 1 1357.07 28.47 0 0 7 3 226.18 17.23 0 2 7 6 130.57 14.35 0 -3 7 7 307.90 21.12 0 -1 7 3 392.55 20.05 0 0 8 8 143.33 13.41 0 0 8 9 107.22 11.42 0 -1 6 1 234.55 14.51 0 0 5 0 48.95 8.45 0 -2 5 0 234.84 13.71 0 -2 7 4 136.35 16.60 0 -1 4 -1 100.59 9.89 0 2 7 7 274.82 17.68 0 -3 4 0 219.66 13.67 0 -3 5 1 451.79 18.50 0 -3 6 3 183.67 16.40 0 -1 5 0 1349.97 25.14 0 0 7 4 187.72 16.25 0 2 6 4 474.84 21.02 0 -2 6 2 619.39 20.72 0 -1 7 4 439.62 21.31 0 -4 5 4 222.68 21.71 0 -2 7 5 161.80 17.98 0 2 7 8 73.26 11.81 0 -1 6 2 219.89 14.43 0 2 7 9 110.99 13.58 0 2 7 11 14.11 9.69 0 0 7 5 138.94 16.25 0 2 5 3 207.66 15.61 0 2 7 10 100.92 11.49 0 -4 5 5 81.22 18.15 0 -3 5 2 482.96 19.53 0 -2 5 1 202.19 12.92 0 -2 7 10 126.79 12.89 0 2 6 5 430.61 20.07 0 -2 6 3 363.59 18.43 0 -2 7 7 43.08 16.07 0 -2 7 9 109.04 14.57 0 -4 5 6 348.13 27.56 0 -3 4 1 429.78 16.88 0 -3 6 5 137.65 17.41 0 -3 6 10 94.57 14.44 0 -1 4 0 529.45 15.76 0 -1 5 1 896.31 19.88 0 -1 7 6 344.91 21.75 0 0 6 3 1024.95 25.54 0 0 7 6 111.73 16.36 0 -1 6 3 179.52 15.19 0 1 7 12 130.51 10.46 0 -3 6 6 76.25 16.99 0 -1 7 7 285.11 21.02 0 -1 7 11 191.46 12.56 0 0 7 12 28.50 7.34 0 2 6 6 277.15 17.83 0 -3 6 7 299.06 23.23 0 -3 6 8 198.47 24.10 0 -3 6 9 183.51 19.13 0 -2 6 4 426.48 21.36 0 0 7 7 60.21 16.18 0 -2 5 2 622.29 18.82 0 -1 7 9 346.10 20.31 0 -1 7 10 190.69 15.08 0 0 5 2 426.25 15.57 0 0 7 8 112.71 16.88 0 2 5 4 197.92 15.43 0 -1 6 4 455.59 20.35 0 0 6 4 849.65 25.15 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15 459.29 14.61 0 3 4 13 191.98 14.71 0 -2 3 14 168.39 10.07 0 -1 5 9 606.30 31.14 0 -1 5 10 234.03 24.31 0 1 5 12 249.38 17.71 0 3 4 9 188.05 16.65 0 -1 4 14 44.86 7.56 0 0 4 15 375.26 12.18 0 0 5 12 82.85 12.00 0 1 5 10 635.95 26.19 0 1 5 11 308.12 21.00 0 3 4 10 130.01 16.99 0 3 4 12 49.96 13.34 0 0 5 9 128.75 19.51 0 0 5 10 224.14 21.03 0 0 5 11 132.35 17.63 0 3 4 11 66.52 12.68 0 -3 5 2 436.14 20.03 0 -2 6 4 403.12 21.26 0 -1 6 4 416.91 20.46 0 1 5 4 900.80 24.62 0 -3 6 5 133.24 17.64 0 3 4 10 158.57 17.00 0 1 6 8 201.91 16.31 0 -3 6 6 74.15 20.47 0 -3 6 10 102.93 14.39 0 -2 5 2 647.11 19.86 0 -1 6 13 36.06 6.51 0 -2 6 5 582.40 24.63 0 -2 6 12 263.64 11.39 0 -1 6 5 104.44 16.45 0 0 6 6 953.33 27.85 0 1 4 3 806.65 20.42 0 1 6 10 97.13 12.86 0 2 5 12 277.73 13.41 0 -3 6 9 190.41 19.70 0 1 5 5 790.89 23.24 0 2 5 9 351.78 18.46 0 2 5 11 47.15 10.66 0 -3 5 3 370.24 19.00 0 -3 6 8 187.50 19.33 0 0 6 7 888.04 26.91 0 2 5 10 121.26 13.48 0 -1 6 6 41.50 15.58 0 -2 6 11 272.91 13.91 0 0 5 4 254.51 14.80 0 0 6 8 533.92 22.48 0 1 4 15 60.49 8.87 0 2 4 6 911.15 24.38 0 0 6 9 419.47 20.93 0 0 6 10 413.98 20.05 0 -4 5 9 147.25 18.57 0 -2 6 9 415.23 21.34 0 -2 6 10 303.44 17.10 0 -1 6 11 144.41 13.16 0 1 4 4 434.93 15.65 0 1 5 13 383.92 14.18 0 2 4 13 334.34 13.76 0 -4 5 7 571.47 31.50 0 -4 5 8 182.44 24.36 0 -3 5 4 357.76 19.55 0 -1 6 9 200.97 18.25 0 1 5 7 831.19 23.11 0 -1 5 4 1160.16 26.57 0 0 5 5 350.92 17.15 0 1 5 8 688.79 21.48 0 2 4 12 212.42 12.68 0 -2 5 13 35.08 6.42 0 0 4 15 377.70 10.99 0 1 5 9 530.26 19.89 0 1 5 11 326.99 15.86 0 -3 5 5 373.96 21.35 0 0 5 13 202.48 11.45 0 1 4 5 491.25 16.95 0 2 4 9 862.64 24.11 0 2 4 10 701.78 21.56 0 2 4 11 728.33 20.54 0 -2 4 2 1385.73 25.25 0 -1 5 5 727.98 23.44 0 1 3 15 377.63 13.27 0 -3 5 6 743.07 28.97 0 -2 5 5 257.71 18.81 0 -2 5 12 35.07 8.38 0 0 5 7 86.27 13.05 0 0 5 12 91.68 12.10 0 2 3 13 134.80 12.29 0 -2 4 14 198.84 8.20 0 1 4 6 231.34 13.47 0 -3 5 7 197.38 20.90 0 -3 5 8 185.07 20.61 0 -3 5 9 331.69 21.96 0 -1 5 12 315.93 14.83 0 0 5 10 265.03 17.15 0 0 5 11 129.98 12.01 0 -3 4 3 244.40 16.25 0 -2 5 11 58.31 11.34 0 2 3 7 275.96 15.81 0 -4 4 10 435.55 18.17 0 -2 5 7 63.55 16.91 0 -1 5 7 559.50 23.94 0 -1 5 11 496.28 19.88 0 1 4 7 406.14 16.49 0 -2 4 3 559.61 18.53 0 -2 5 8 60.89 17.13 0 -2 5 9 84.49 16.70 0 -2 5 10 123.68 15.70 0 -1 5 8 633.50 25.29 0 -1 5 9 623.02 25.26 0 -1 5 10 286.93 18.32 0 0 3 15 70.49 7.03 0 1 4 12 150.63 12.65 0 2 3 8 73.71 12.65 0 -3 4 12 68.45 7.92 0 0 4 5 825.86 20.75 0 1 2 15 39.85 8.74 0 1 3 14 464.84 14.64 0 1 4 8 227.20 14.57 0 2 3 11 34.24 10.89 0 -4 4 9 565.86 24.80 0 -2 4 13 298.55 11.27 0 0 4 13 463.92 15.83 0 1 4 9 144.50 13.44 0 2 3 9 295.81 16.49 0 2 3 10 27.44 11.31 0 -4 4 6 235.06 23.08 0 -4 4 8 460.72 25.42 0 -3 4 4 209.16 16.80 0 -4 4 7 500.91 27.99 0 -1 4 13 74.83 10.09 0 -3 4 11 109.65 11.21 0 -2 4 4 1131.91 26.56 0 0 4 6 1258.16 25.76 0 0 4 12 319.02 16.32 0 -3 3 13 183.81 8.29 0 -2 3 14 174.45 8.54 0 -2 4 12 316.06 14.09 0 1 3 13 754.89 19.42 0 -4 3 11 16.63 7.62 0 -3 4 5 99.76 16.87 0 -1 4 5 83.37 12.22 0 -1 4 12 125.00 12.82 0 0 2 15 449.66 12.68 0 0 4 7 1122.08 25.43 0 0 4 11 596.25 21.42 0 2 2 12 178.31 12.60 0 -3 4 10 93.76 14.79 0 -1 3 14 267.02 11.06 0 -3 4 6 45.42 17.75 0 -2 4 11 201.96 15.14 0 0 4 9 670.86 22.27 0 1 2 14 32.72 8.47 0 1 3 12 364.99 15.46 0 -3 4 7 335.22 24.39 0 2 2 11 830.21 21.76 0 -2 4 10 275.81 18.04 0 -4 3 10 60.11 11.58 0 -3 3 12 355.28 12.64 0 -2 3 13 195.88 11.04 0 -1 4 7 265.15 15.70 0 -1 4 8 402.30 20.43 0 -1 4 9 164.74 17.80 0 -1 4 10 -4.30 10.14 0 1 3 11 380.71 16.25 0 -4 3 4 92.46 18.53 0 0 1 15 98.69 7.70 0 1 3 10 974.67 22.33 0 -4 3 9 56.16 17.73 0 -2 2 14 291.74 10.24 0 -1 1 15 353.26 10.22 0 1 2 13 96.88 11.01 0 -3 2 13 77.47 6.83 0 -3 3 3 2111.30 36.56 0 0 2 14 522.46 14.88 0 0 3 12 161.13 13.79 0 1 1 14 266.38 12.64 0 -4 3 5 33.87 18.89 0 -4 3 8 20.95 17.69 0 -3 3 11 543.94 18.28 0 -2 3 12 186.77 12.64 0 -1 2 14 96.20 8.65 0 -4 3 6 346.00 26.92 0 -1 3 12 306.15 15.45 0 0 3 11 185.37 14.50 0 1 2 12 31.98 10.44 0 -5 2 6 73.34 23.55 0 -3 3 4 1317.55 31.77 0 -2 1 14 52.58 6.37 0 -2 2 13 452.75 14.49 0 -2 3 11 238.14 15.90 0 -1 3 11 687.77 22.10 0 0 3 7 184.64 12.70 0 0 3 10 359.52 17.93 0 -3 2 12 62.46 8.47 0 -3 3 9 564.25 24.96 0 0 1 14 158.16 10.55 0 0 3 8 345.05 16.19 0 0 3 9 288.05 16.53 0 -3 1 13 245.83 9.62 0 -1 2 13 197.56 12.64 0 -3 3 6 1690.15 40.60 0 -2 0 14 205.48 8.46 0 -2 3 9 646.01 25.18 0 -1 3 6 1421.02 29.57 0 -1 3 9 570.71 22.36 0 1 2 10 63.04 10.82 0 -2 2 12 570.73 18.21 0 -2 3 6 411.82 20.61 0 -1 3 7 740.57 23.99 0 -1 3 8 908.59 26.38 0 1 2 8 39.59 9.49 0 1 2 9 40.60 9.07 0 -2 3 7 388.24 21.66 0 -1 2 12 150.62 13.03 0 1 1 12 394.32 16.40 0 -5 1 8 476.17 22.81 0 -2 1 13 110.54 9.72 0 0 -1 14 90.37 9.69 0 0 1 13 151.87 12.02 0 1 0 13 293.87 14.06 0 -4 2 8 438.57 24.26 0 -3 -1 13 241.54 9.51 0 -3 1 12 331.18 12.67 0 -4 2 4 1087.30 36.92 0 -3 2 10 146.21 13.97 0 -2 2 11 589.58 19.79 0 -1 -1 14 245.23 9.91 0 -1 1 13 667.75 18.28 0 -5 0 9 143.45 12.25 0 -5 1 7 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320.21 27.96 0 -2 6 0 514.51 18.87 0 -1 8 4 193.22 16.57 0 0 4 -2 1369.06 25.14 0 -3 5 0 635.37 21.64 0 -3 7 6 630.57 31.24 0 -2 5 -1 532.41 18.08 0 -2 7 2 223.50 16.54 0 -1 4 -2 683.97 18.40 0 0 8 4 252.42 17.74 0 1 7 2 457.10 19.85 0 2 8 7 393.23 17.47 0 1 8 5 120.33 13.79 0 -3 6 2 432.97 19.93 0 -1 6 0 223.17 14.02 0 -1 8 5 167.29 16.26 0 0 5 -1 496.80 17.50 0 0 6 0 1019.40 24.96 0 2 8 8 247.47 13.69 0 -2 7 3 194.08 16.70 0 -1 5 -1 917.00 21.91 0 -1 7 2 520.98 20.36 0 0 7 2 158.48 15.00 0 0 8 5 71.14 14.31 0 1 4 -1 450.52 17.22 0 -2 6 1 507.92 19.56 0 -1 8 6 49.69 13.27 0 1 8 6 101.73 13.48 0 2 6 2 1053.83 27.36 0 2 7 4 109.75 14.22 0 -3 4 0 268.98 15.67 0 -3 5 1 407.31 18.95 0 -1 8 7 113.68 14.80 0 -1 8 9 137.03 13.33 0 1 7 3 537.21 21.18 0 -3 6 3 173.29 16.81 0 -1 8 8 65.90 12.22 0 1 8 7 52.23 11.17 0 2 5 1 239.28 16.38 0 -2 7 4 127.52 16.29 0 -1 7 3 410.27 19.60 0 -1 6 1 154.87 10.73 0 0 4 -1 373.29 14.74 0 0 6 1 1242.32 26.42 0 0 7 3 236.48 17.00 0 0 8 7 211.27 16.28 0 1 8 8 42.33 10.45 0 1 8 10 25.84 8.22 0 -3 6 4 260.23 19.05 0 -2 6 2 562.08 20.84 0 0 5 0 72.91 10.31 0 0 8 8 132.66 14.11 0 0 8 9 106.37 11.67 0 1 8 9 45.71 10.23 0 2 7 5 118.25 14.33 0 -3 5 2 468.49 20.20 0 -3 4 1 458.07 18.73 0 -3 6 5 133.78 17.69 0 -1 7 4 402.70 21.06 0 1 6 2 24.41 9.49 0 3 7 9 373.13 15.78 0 3 7 10 228.65 14.30 0 -2 7 9 127.40 15.75 0 0 7 4 185.51 16.97 0 -3 6 6 89.26 19.32 0 -3 6 8 182.31 23.79 0 -2 7 8 148.03 18.19 0 -1 6 2 248.52 14.74 0 0 6 2 1154.35 25.47 0 2 5 2 528.79 19.57 0 -1 7 5 341.33 20.71 0 1 7 5 409.79 20.97 0 -1 5 1 1249.21 23.41 0 0 5 1 123.22 10.27 0 0 7 5 133.08 16.78 0 1 6 3 291.39 16.43 0 2 6 4 485.22 20.51 0 2 7 7 234.97 15.95 0 3 5 4 343.05 21.55 0 3 6 6 99.55 14.45 0 -3 4 2 461.57 19.15 0 -1 7 6 333.03 21.99 0 -3 5 4 370.15 19.82 0 2 7 8 79.63 12.65 0 -1 7 7 300.24 22.17 0 0 7 6 130.93 17.32 0 2 7 12 94.52 9.32 0 -2 4 1 1446.55 24.79 0 -1 7 8 263.26 20.83 0 -1 7 9 345.59 20.98 0 0 7 12 30.31 7.48 0 1 7 7 329.15 20.40 0 -3 5 5 393.02 22.08 0 -2 6 11 323.03 17.80 0 0 7 7 50.57 15.48 0 1 6 4 290.53 16.50 0 2 6 5 452.69 19.75 0 1 7 8 333.81 20.48 0 1 7 12 128.88 10.02 0 0 5 2 423.88 15.27 0 0 6 4 877.23 25.33 0 0 7 8 121.64 17.23 0 0 7 11 116.15 12.27 0 3 5 5 571.24 22.28 0 -2 6 10 368.69 22.02 0 0 7 9 44.51 14.91 0 1 7 9 260.42 18.40 0 1 7 10 309.57 17.43 0 1 7 11 156.26 13.23 0 -3 5 7 209.73 24.86 0 -3 5 8 218.58 26.43 0 -2 6 8 283.89 25.00 0 -2 6 9 441.14 26.46 0 -1 6 5 67.74 16.38 0 2 6 6 265.59 18.68 0 1 6 5 263.56 17.58 0 3 6 9 215.65 17.20 0 -3 4 4 215.96 17.90 0 0 6 5 531.55 23.67 0 1 5 3 1704.09 29.61 0 2 5 4 215.87 15.59 0 3 6 12 23.92 10.02 0 -1 5 3 934.23 23.03 0 3 6 10 80.07 12.75 0 3 6 11 72.23 11.38 0 0 5 3 367.81 15.41 0 3 5 6 478.20 22.08 0 1 6 6 240.75 19.39 0 1 6 14 119.63 9.09 0 -3 4 5 84.68 17.47 0 -2 5 5 282.04 19.99 0 -1 6 7 143.29 21.85 0 -1 6 11 131.81 16.82 0 -1 6 8 102.48 23.58 0 0 6 13 287.84 13.51 0 -3 4 6 65.76 21.63 0 -2 4 3 436.10 16.91 0 -1 6 9 224.05 26.01 0 -1 6 10 25.70 19.02 0 0 6 7 1014.74 36.13 0 1 5 4 1119.74 27.83 0 -6 -1 5 113.37 12.11 0 -5 0 6 128.56 11.84 0 -2 -5 7 32.21 7.94 0 -2 -4 8 454.26 14.89 0 -1 -1 8 801.17 18.17 0 -3 1 6 1000.21 22.74 0 -1 -3 8 738.27 19.50 0 0 -3 7 436.24 16.37 0 0 -2 7 1512.55 24.74 0 -4 1 5 174.49 14.96 0 -1 -2 8 315.75 14.02 0 -6 -3 5 114.72 8.48 0 -5 -5 5 118.01 7.91 0 -5 -4 6 18.71 6.44 0 -4 -4 7 478.73 13.98 0 -3 -3 8 476.90 16.54 0 -2 -1 8 346.52 14.44 0 -6 -2 5 377.32 14.05 0 -3 -6 5 115.38 9.42 0 -3 -2 8 29.97 9.54 0 -2 -3 8 398.26 15.75 0 -2 0 7 759.48 19.23 0 -1 -4 7 234.86 14.11 0 -2 -2 8 908.77 21.45 0 -6 -4 4 212.69 10.66 0 -1 -1 7 732.04 17.93 0 -7 -3 2 328.62 14.27 0 -6 -1 4 177.32 14.53 0 -5 -3 6 458.45 15.44 0 -4 -2 7 879.56 22.33 0 -4 1 4 181.49 16.49 0 -4 -6 4 283.32 11.39 0 -2 -5 6 101.22 10.99 0 -3 -1 7 513.56 17.90 0 -2 -1 7 85.14 10.44 0 -6 -3 4 251.05 12.03 0 -6 -2 4 224.13 13.18 0 -5 -4 5 170.57 10.83 0 -4 -4 6 198.24 12.52 0 -3 -3 7 302.32 15.74 0 -3 0 6 507.50 18.46 0 -2 0 6 904.92 20.69 0 -5 -5 4 158.23 9.77 0 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27.42 0 -6 -6 -3 286.09 13.11 0 -3 -7 -1 691.56 20.02 0 -7 -3 -3 344.73 19.11 0 -5 -6 -1 127.96 10.46 0 -5 0 0 540.18 23.71 0 -3 -6 1 139.85 11.64 0 -3 -4 3 138.04 12.28 0 -6 -1 -1 27.26 14.98 0 -2 -6 1 426.64 16.64 0 -1 -5 2 1071.82 24.92 0 -4 5 3 278.62 21.50 0 -3 5 2 508.55 22.88 0 -5 4 3 180.24 20.25 0 -3 6 10 100.77 14.64 0 -2 6 5 555.90 29.72 0 0 6 7 1012.43 33.60 0 -4 5 4 210.56 22.63 0 -3 6 7 294.79 28.25 0 -3 6 9 189.51 21.35 0 0 5 4 301.92 20.13 0 0 6 8 550.25 27.65 0 1 5 6 477.44 27.16 0 -5 3 2 512.64 29.44 0 -5 4 4 109.88 21.23 0 -5 4 9 100.12 17.42 0 -3 4 1 419.29 18.79 0 -2 6 6 456.32 30.08 0 0 6 9 404.92 25.75 0 0 6 10 429.82 24.74 0 -4 5 5 114.92 23.02 0 -4 5 10 158.34 15.98 0 -2 4 1 1453.62 29.28 0 -5 4 5 338.73 28.24 0 -5 4 8 128.04 23.12 0 -2 6 10 326.59 23.03 0 -4 5 6 362.08 30.30 0 -4 5 9 136.23 21.52 0 -2 6 8 270.54 27.49 0 -2 6 9 399.30 27.74 0 -1 6 10 20.48 18.18 0 -4 3 1 179.74 16.88 0 -4 5 7 519.66 34.43 0 -4 5 8 201.81 26.25 0 -3 5 4 409.08 25.91 0 -3 5 12 319.95 14.00 0 -5 3 3 458.10 26.81 0 -3 4 2 470.16 20.83 0 -2 5 4 185.09 19.73 0 1 5 8 685.80 29.58 0 -5 3 4 541.69 28.93 0 -4 4 11 392.95 17.91 0 -3 5 11 300.93 18.38 0 0 5 6 227.77 21.02 0 -5 3 9 423.05 26.04 0 -4 4 4 870.18 33.07 0 -3 5 6 773.26 35.70 0 -2 5 5 195.34 23.08 0 -5 3 5 274.46 27.30 0 -3 5 10 248.19 22.65 0 -1 5 13 307.79 15.66 0 -5 3 8 452.83 32.45 0 -3 4 3 250.31 19.28 0 -3 5 7 201.16 23.58 0 -3 5 8 207.54 28.87 0 -3 5 9 339.09 31.06 0 -2 5 12 24.26 10.80 0 -5 2 3 135.58 20.16 0 -5 3 7 448.82 33.88 0 -4 2 1 686.58 24.15 0 -4 4 5 790.78 35.37 0 -4 4 10 437.07 23.88 0 -2 5 6 88.00 20.78 0 -1 4 3 605.23 21.63 0 0 5 12 94.86 18.70 0 -2 4 3 457.02 20.58 0 -2 5 11 57.59 15.77 0 -2 5 7 72.18 22.06 0 -3 4 4 204.56 18.91 0 -3 4 12 48.91 10.20 0 -2 5 10 126.68 21.79 0 0 5 9 137.60 21.17 0 0 5 10 310.86 24.06 0 -5 2 4 121.89 21.14 0 -5 2 9 83.54 17.74 0 -5 2 8 69.16 22.04 0 -4 3 11 21.75 11.37 0 -3 4 5 67.48 17.93 0 -2 4 4 1080.25 29.76 0 -1 4 14 45.64 9.14 0 -5 2 6 61.86 25.15 0 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1771.18 47.23 0 -3 3 10 605.04 32.65 0 -2 3 4 772.25 24.71 0 0 3 14 86.34 12.65 0 -4 2 6 209.52 30.01 0 -3 3 7 767.88 38.95 0 -3 3 9 589.97 37.12 0 -1 5 2 1153.59 26.94 0 0 6 3 895.34 32.45 0 2 -1 -1 1147.02 12.24 0 4 3 5 251.08 15.87 0 0 2 3 442.24 9.13 0 0 4 4 1031.98 20.70 0 0 5 4 287.96 16.58 0 1 5 5 818.71 24.54 0 0 1 2 828.58 9.82 0 1 3 5 1076.99 19.67 0 3 4 6 146.52 14.65 0 0 3 4 890.93 16.75 0 2 4 6 894.78 23.08 0 2 5 6 379.73 19.52 0 2 2 5 1383.44 19.33 0 3 1 4 1506.70 18.26 0 4 4 6 652.88 27.99 0 -1 4 3 434.22 14.71 0 2 1 4 126.78 6.53 0 -2 3 0 175.46 7.87 0 4 3 6 232.01 17.40 0 0 4 5 1061.83 22.93 0 0 5 5 396.73 19.98 0 1 4 6 243.32 14.06 0 1 5 6 449.09 21.23 0 3 4 7 346.83 19.59 0 2 5 7 385.68 21.72 0 0 2 4 903.69 15.08 0 -2 4 1 1444.99 26.34 0 0 3 5 1000.77 19.29 0 3 2 6 297.55 12.79 0 -1 4 4 697.04 18.75 0 -1 5 4 1086.85 29.56 0 2 3 7 261.18 14.06 0 0 5 6 217.41 17.82 0 4 3 7 392.89 21.82 0 0 4 6 1369.67 27.42 0 3 1 5 2146.58 23.58 0 2 1 5 941.26 15.13 0 2 4 8 503.19 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622.08 17.02 0 -2 2 2 2639.16 25.37 0 3 2 10 224.47 16.25 0 -2 3 5 540.79 17.31 0 1 0 5 1031.19 15.17 0 -2 4 6 572.02 22.98 0 2 0 6 500.82 11.70 0 -2 2 3 1122.61 18.97 0 0 1 7 288.30 11.35 0 0 2 9 888.16 20.95 0 0 3 10 281.96 16.33 0 1 2 10 53.26 10.44 0 3 1 9 1247.29 24.29 0 -1 1 5 3436.40 31.14 0 1 0 6 1565.46 19.79 0 1 0 -1 2851.63 18.06 0 2 0 7 969.36 16.58 0 -1 2 8 663.47 18.26 0 0 1 8 277.79 10.82 0 3 0 7 373.37 11.08 0 0 0 5 3276.80 26.88 0 0 2 10 411.88 16.35 0 2 1 10 107.64 10.89 0 3 1 10 550.26 19.03 0 0 0 6 2884.91 27.38 0 1 1 10 790.26 19.71 0 -2 2 6 1492.48 25.54 0 -1 1 7 1346.99 22.54 0 -1 2 9 261.16 13.98 0 0 1 9 250.88 12.16 0 3 0 8 202.11 11.08 0 1 0 8 439.42 13.02 0 -2 3 8 335.96 17.67 0 2 1 11 264.35 15.29 0 0 0 7 2963.73 29.69 0 -2 2 7 1300.17 25.26 0 -1 1 8 1550.69 25.23 0 2 0 9 913.74 18.81 0 -1 0 3 326.77 8.91 0 3 0 9 408.78 15.54 0 1 0 9 569.28 15.56 0 -2 1 2 1084.63 13.72 0 -1 0 2 910.61 11.46 0 0 0 8 1803.65 24.89 0 -1 0 6 140.37 9.32 0 2 0 10 904.10 20.39 0 0 0 9 1349.70 23.35 0 1 -1 4 1856.09 16.76 0 2 -1 5 1220.43 14.18 0 3 0 10 0.32 10.14 0 -2 2 9 1722.89 32.75 0 -1 0 7 432.60 13.85 0 2 -1 6 772.00 12.65 0 -1 1 10 1044.66 23.86 0 2 -1 4 62.89 4.03 0 1 -1 3 2511.50 16.52 0 2 -1 7 486.19 11.54 0 -1 0 8 45.55 8.52 0 0 -1 5 621.80 13.01 0 0 -1 6 34.73 6.93 0 2 -1 8 110.89 8.24 0 -1 0 9 56.41 9.84 0 0 -1 7 802.29 16.92 0 1 0 0 427.05 4.42 0 3 0 2 1005.77 11.43 0 -3 2 6 144.57 15.13 0 -2 1 9 401.00 17.93 0 -3 2 3 309.90 10.21 0 -2 0 4 2663.29 27.12 0 -2 0 5 1123.74 20.30 0 0 -1 8 383.59 13.60 0 1 -1 9 1724.44 26.05 0 2 -1 9 279.19 12.21 0 -2 0 6 933.49 20.32 0 3 -1 6 847.98 13.54 0 3 -1 7 491.71 12.14 0 -2 0 3 1060.67 15.61 0 -2 0 7 769.98 20.29 0 -1 -1 6 1356.80 22.01 0 0 -1 9 310.70 13.87 0 1 -1 2 3810.38 16.61 0 1 -1 10 685.86 18.94 0 2 -1 10 150.00 11.90 0 -1 -1 7 707.69 17.64 0 0 -1 2 2349.27 16.17 0 3 -1 7 466.30 12.55 0 0 1 6 10.55 5.66 0 1 -1 3 2516.21 17.88 0 2 -1 6 759.35 13.71 0 2 1 10 90.64 9.56 0 0 3 8 280.71 11.79 0 0 4 8 509.29 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-1 515.95 25.10 0 -4 2 3 845.89 33.04 0 -3 2 5 185.24 18.53 0 -1 1 5 3243.13 36.56 0 1 3 8 882.39 26.63 0 2 3 7 257.43 18.50 0 -3 1 3 862.82 26.08 0 -1 4 9 188.23 23.94 0 -4 1 0 887.31 31.61 0 -4 3 5 29.66 21.92 0 1 4 9 140.64 23.25 0 -3 3 7 617.66 31.12 0 -2 0 1 613.01 14.86 0 -1 2 -7 147.01 20.41 0 -1 2 -6 207.71 19.89 0 0 2 -4 1718.49 27.12 0 1 2 -6 693.04 24.52 0 -4 0 -9 617.76 48.10 0 2 1 -2 392.85 7.92 0 -2 1 -3 506.33 11.90 0 1 2 -8 314.44 24.89 0 -4 0 -7 1294.36 43.64 0 -2 2 -8 825.12 40.02 0 -1 2 -4 525.53 17.13 0 -3 1 -5 1703.31 31.40 0 -2 2 -9 1173.89 47.79 0 -2 2 -6 1418.47 38.83 0 0 2 -10 308.20 30.60 0 1 2 -9 381.15 30.10 0 -2 2 -5 1855.85 35.11 0 -4 0 -6 1662.35 36.30 0 2 2 -6 556.71 21.71 0 -3 0 -3 144.15 6.42 0 2 2 -7 802.17 29.93 0 -4 1 -9 74.12 39.48 0 -3 1 -4 2155.01 27.59 0 -3 2 -9 277.81 37.16 0 -3 2 -8 433.90 39.03 0 -2 2 -4 3556.07 37.78 0 -4 1 -8 188.81 36.32 0 -2 1 -2 1766.19 17.26 0 -1 1 -1 8468.12 30.89 0 -2 3 -8 16.20 25.93 0 -2 3 -7 139.79 26.20 0 -1 2 -2 1170.20 16.82 0 -2 2 -3 1855.86 23.88 0 -2 3 -9 176.58 31.08 0 1 3 -6 586.29 25.49 0 1 3 -8 749.90 35.35 0 1 3 -5 1852.72 34.21 0 -4 2 -9 367.85 47.90 0 -3 1 -3 964.52 15.74 0 -2 3 -5 469.61 22.13 0 -4 2 -8 528.62 47.05 0 1 3 -4 1159.11 24.62 0 -3 3 -8 1022.10 51.47 0 -4 2 -7 632.20 39.66 0 -3 3 -6 973.04 36.54 0 -2 2 -2 4796.15 32.93 0 -4 2 -6 717.40 32.34 0 -1 4 -7 251.92 27.67 0 -3 3 -5 1377.07 33.39 0 -2 0 -1 679.25 6.65 0 -1 2 -1 48.27 4.52 0 0 3 -2 1500.03 21.53 0 0 4 -7 839.22 38.88 0 0 4 -6 879.04 34.73 0 -2 3 -3 55.67 9.40 0 -2 4 -7 510.01 35.66 0 -1 4 -5 378.54 22.47 0 2 2 -2 1896.30 18.22 0 -1 3 -2 939.07 17.30 0 -4 2 -5 710.10 25.30 0 -2 1 -1 605.46 9.17 0 -4 1 -4 94.74 8.86 0 -2 4 -5 477.80 25.71 0 1 3 -2 1147.77 18.65 0 -4 3 -7 437.25 39.54 0 1 4 -6 140.66 20.94 0 -3 1 -2 1044.30 13.94 0 -3 4 -7 156.36 31.77 0 -4 3 -6 416.77 31.25 0 -2 3 -2 715.32 16.35 0 -2 4 -4 1238.52 29.97 0 -1 4 -3 287.69 15.69 0 0 4 -3 1002.25 24.14 0 0 3 -1 404.73 10.58 0 2 3 -3 584.08 15.74 0 -4 2 -4 1198.84 24.78 0 -3 2 -2 588.27 13.35 0 -3 4 -5 157.94 20.51 0 -1 1 0 3217.52 16.70 0 0 2 0 9999.99 35.59 0 -4 3 -5 606.41 27.59 0 1 4 -3 128.88 12.68 0 -1 4 -2 758.51 19.68 0 -3 4 -4 293.23 19.24 0 -1 2 0 571.77 9.88 0 1 1 0 2124.90 10.45 0 -2 3 -1 588.05 14.08 0 0 5 -5 116.06 21.98 0 -2 4 -2 1407.39 25.95 0 -1 5 -4 438.30 24.95 0 2 3 -2 730.80 15.14 0 -4 2 -3 989.19 20.18 0 -2 5 -4 333.63 23.93 0 -1 4 -1 75.37 10.19 0 0 3 0 183.56 7.97 0 0 4 -1 350.68 13.91 0 -1 5 -3 774.51 26.91 0 -4 4 -5 460.78 31.33 0 -2 5 -3 127.18 16.56 0 -4 3 -3 313.98 16.65 0 -3 2 -1 192.78 8.28 0 -2 2 0 4557.60 28.06 0 -2 4 -1 970.54 21.37 0 1 5 -4 885.52 31.91 0 -4 4 -4 880.76 32.52 0 -3 5 -4 263.65 23.17 0 -3 1 -1 2390.19 18.65 0 1 5 -3 670.00 25.44 0 -2 5 -2 311.52 18.02 0 0 4 0 2737.77 29.39 0 -1 5 -1 886.42 24.37 0 -4 2 -2 1379.48 21.30 0 0 3 1 815.40 13.19 0 -4 3 -2 390.46 15.80 0 -2 4 0 1623.19 25.20 0 -1 3 1 1346.90 17.53 0 -1 6 -2 421.53 24.25 0 0 4 1 3365.37 31.38 0 0 5 0 77.55 11.07 0 1 5 -1 559.19 20.37 0 -4 1 -2 356.44 10.00 0 -4 4 -2 778.65 25.84 0 -3 3 0 3406.03 32.75 0 0 6 -2 813.92 31.38 0 -3 2 0 556.19 11.89 0 -2 3 1 524.88 12.60 0 1 2 1 1178.30 11.89 0 -2 2 1 3965.38 26.31 0 -2 5 0 186.03 12.74 0 -2 4 1 1471.08 23.80 0 0 1 1 374.59 5.56 0 -4 3 -1 400.98 15.33 0 0 6 -1 327.00 21.87 0 -1 5 1 872.31 20.92 0 -4 4 -1 1050.15 27.66 0 0 3 2 830.76 13.61 0 -2 5 1 201.90 14.59 0 0 2 2 102.73 5.81 0 -2 3 2 1156.36 18.06 0 -2 4 2 1264.39 22.51 0 -1 5 2 1183.03 24.78 0 -1 6 1 217.87 17.70 0 0 5 2 427.82 15.72 0 -4 3 0 533.77 17.05 0 -4 4 0 1007.72 26.90 0 -2 6 1 544.73 23.95 0 -3 2 1 535.48 12.02 0 -2 5 2 538.87 19.48 0 -1 4 3 668.69 16.48 0 2 4 1 813.58 19.18 0 -1 3 3 1375.50 19.02 0 -1 6 2 225.24 17.64 0 0 4 3 686.67 15.19 0 -1 5 3 899.25 22.41 0 -3 4 2 468.76 17.00 0 0 5 3 312.09 14.40 0 1 2 2 1782.02 16.00 0 -3 3 2 2184.27 27.75 0 -2 4 3 502.03 16.34 0 -3 5 2 432.07 20.53 0 -2 5 3 204.98 15.08 0 -4 4 1 402.04 20.50 0 1 1 1 3735.24 15.83 0 -1 6 3 171.41 16.42 0 1 3 3 1824.32 20.98 0 1 5 3 1601.78 27.78 0 1 6 2 14.54 14.76 0 -4 3 1 153.33 12.80 0 -1 2 3 1259.42 15.77 0 -2 6 3 284.85 20.12 0 -1 1 2 3336.60 19.26 0 -1 5 4 1058.79 24.56 0 0 2 3 401.48 8.72 0 -3 2 2 824.81 15.40 0 -3 4 3 221.51 14.57 0 -3 5 3 370.62 19.99 0 -1 3 4 1288.76 19.98 0 0 3 4 918.16 16.68 0 2 3 2 466.32 11.99 0 ; _shelx_hkl_checksum 81693 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pt1 Pt 0.000000 0.500000 0.500000 0.02211(17) Uani 1 2 d S . P . . Fe1 Fe 0.500000 1.000000 0.500000 0.0209(3) Uani 1 2 d S . P . . N1 N 0.3145(9) 0.8200(8) 0.4820(4) 0.0246(12) Uani 1 1 d . . . . . N2 N 0.6732(9) 0.7987(8) 0.5300(4) 0.0266(12) Uani 1 1 d . . . . . N3 N 0.3508(8) 0.9677(7) 0.6495(4) 0.0232(11) Uani 1 1 d . . . . . C1 C 0.1996(10) 0.7001(10) 0.4864(5) 0.0237(13) Uani 1 1 d . . . . . C2 C 0.7881(10) 0.6827(9) 0.5249(5) 0.0236(13) Uani 1 1 d . . . . . C3 C 0.1527(11) 0.9843(10) 0.6749(5) 0.0293(14) Uani 1 1 d . . . . . H3 H 0.081068 0.993573 0.621560 0.035 Uiso 1 1 calc R U . . . C4 C 0.0461(12) 0.9886(11) 0.7760(6) 0.0331(15) Uani 1 1 d . . . . . H4 H -0.094807 1.001431 0.790933 0.040 Uiso 1 1 calc R U . . . C5 C 0.1506(12) 0.9736(11) 0.8550(5) 0.0330(16) Uani 1 1 d . . . . . C6 C 0.3546(12) 0.9447(11) 0.8300(5) 0.0320(15) Uani 1 1 d . . . . . H6 H 0.428330 0.926887 0.882634 0.038 Uiso 1 1 calc R U . . . C7 C 0.4502(11) 0.9420(10) 0.7271(5) 0.0277(14) Uani 1 1 d . . . . . H7 H 0.589730 0.921542 0.710738 0.033 Uiso 1 1 calc R U . . . C8 C 0.0465(12) 0.9895(11) 0.9586(6) 0.0340(15) Uani 1 1 d . . . . . N4 N -0.0004(10) 0.4974(10) 0.9543(5) 0.0360(14) Uani 1 1 d . . . . . C9 C 0.1899(13) 0.4577(11) 0.8932(6) 0.0375(17) Uani 1 1 d . . . . . C10 C 0.2036(14) 0.4768(11) 0.7859(6) 0.0385(17) Uani 1 1 d . . . . . H10 H 0.090619 0.509976 0.757669 0.046 Uiso 1 1 calc R U . . . C11 C 0.3872(13) 0.4460(11) 0.7215(6) 0.0396(18) Uani 1 1 d . . . . . H11 H 0.399008 0.460948 0.648643 0.048 Uiso 1 1 calc R U . . . C12 C 0.5521(14) 0.3940(12) 0.7621(7) 0.0424(19) Uani 1 1 d . . . . . H12 H 0.676269 0.374130 0.717658 0.051 Uiso 1 1 calc R U . . . C13 C 0.5328(13) 0.3712(12) 0.8697(7) 0.0405(18) Uani 1 1 d . . . . . H13 H 0.644947 0.334787 0.898137 0.049 Uiso 1 1 calc R U . . . C14 C 0.3533(13) 0.4007(12) 0.9353(6) 0.0395(18) Uani 1 1 d . . . . . H14 H 0.341359 0.382421 1.008291 0.047 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pt1 0.0189(2) 0.0238(2) 0.0229(2) -0.00508(15) -0.00288(14) 0.00117(14) Fe1 0.0185(7) 0.0226(7) 0.0203(7) -0.0048(5) -0.0012(5) 0.0001(5) N1 0.027(3) 0.026(3) 0.019(3) -0.004(2) -0.002(2) 0.003(2) N2 0.023(3) 0.031(3) 0.022(3) -0.003(2) -0.001(2) -0.002(2) N3 0.021(3) 0.023(3) 0.022(3) -0.005(2) 0.000(2) 0.002(2) C1 0.024(3) 0.024(3) 0.024(3) -0.008(2) -0.005(2) -0.002(3) C2 0.022(3) 0.026(3) 0.023(3) -0.002(3) -0.005(2) 0.004(3) C3 0.030(4) 0.032(4) 0.026(3) -0.006(3) -0.006(3) -0.003(3) C4 0.029(4) 0.038(4) 0.027(3) -0.002(3) 0.002(3) 0.003(3) C5 0.037(4) 0.036(4) 0.022(3) -0.006(3) 0.002(3) -0.003(3) C6 0.037(4) 0.035(4) 0.022(3) -0.004(3) -0.004(3) -0.002(3) C7 0.030(4) 0.030(3) 0.022(3) -0.004(3) -0.003(2) -0.005(3) C8 0.037(4) 0.031(4) 0.030(3) -0.004(3) -0.001(3) -0.004(3) N4 0.036(4) 0.040(4) 0.029(3) -0.008(3) -0.002(2) -0.008(3) C9 0.041(4) 0.037(4) 0.032(4) -0.010(3) 0.000(3) -0.005(3) C10 0.047(5) 0.035(4) 0.031(4) -0.003(3) -0.006(3) -0.005(3) C11 0.047(5) 0.036(4) 0.030(4) -0.007(3) 0.004(3) -0.004(3) C12 0.044(5) 0.041(4) 0.038(4) -0.010(3) 0.000(3) -0.006(4) C13 0.039(4) 0.044(4) 0.040(4) -0.018(3) -0.004(3) -0.002(3) C14 0.044(5) 0.046(5) 0.029(4) -0.010(3) -0.007(3) -0.004(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Pt Pt -4.5932 6.9264 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 Pt1 C1 180.0 . 2_566 ? C1 Pt1 C2 88.4(3) . 1_455 ? C1 Pt1 C2 91.6(3) . 2_666 ? C1 Pt1 C2 88.4(3) 2_566 2_666 ? C1 Pt1 C2 91.6(3) 2_566 1_455 ? C2 Pt1 C2 180.0 2_666 1_455 ? N1 Fe1 N1 180.0 . 2_676 ? N1 Fe1 N3 88.0(2) 2_676 2_676 ? N1 Fe1 N3 92.0(2) . 2_676 ? N1 Fe1 N3 88.0(2) . . ? N1 Fe1 N3 92.0(2) 2_676 . ? N2 Fe1 N1 91.8(3) . 2_676 ? N2 Fe1 N1 88.2(3) 2_676 2_676 ? N2 Fe1 N1 88.2(3) . . ? N2 Fe1 N1 91.8(3) 2_676 . ? N2 Fe1 N2 180.0(2) . 2_676 ? N2 Fe1 N3 92.4(2) 2_676 2_676 ? N2 Fe1 N3 87.6(2) 2_676 . ? N2 Fe1 N3 87.6(2) . 2_676 ? N2 Fe1 N3 92.4(2) . . ? N3 Fe1 N3 180.0 2_676 . ? C1 N1 Fe1 170.1(5) . . ? C2 N2 Fe1 165.2(5) . . ? C3 N3 Fe1 120.9(5) . . ? C3 N3 C7 118.1(6) . . ? C7 N3 Fe1 120.8(4) . . ? N1 C1 Pt1 177.4(6) . . ? N2 C2 Pt1 173.4(5) . 1_655 ? N3 C3 H3 118.5 . . ? N3 C3 C4 123.0(7) . . ? C4 C3 H3 118.5 . . ? C3 C4 H4 120.6 . . ? C3 C4 C5 118.8(7) . . ? C5 C4 H4 120.6 . . ? C4 C5 C8 119.9(7) . . ? C6 C5 C4 118.3(6) . . ? C6 C5 C8 121.8(7) . . ? C5 C6 H6 120.3 . . ? C5 C6 C7 119.4(7) . . ? C7 C6 H6 120.3 . . ? N3 C7 C6 122.2(7) . . ? N3 C7 H7 118.9 . . ? C6 C7 H7 118.9 . . ? C8 C8 C5 175.9(12) 2_577 . ? N4 N4 C9 113.8(9) 2_567 . ? C10 C9 N4 115.8(8) . . ? C14 C9 N4 123.6(7) . . ? C14 C9 C10 120.6(8) . . ? C9 C10 H10 120.7 . . ? C11 C10 C9 118.6(8) . . ? C11 C10 H10 120.7 . . ? C10 C11 H11 119.4 . . ? C12 C11 C10 121.2(8) . . ? C12 C11 H11 119.4 . . ? C11 C12 H12 120.5 . . ? C11 C12 C13 119.0(8) . . ? C13 C12 H12 120.5 . . ? C12 C13 H13 119.4 . . ? C14 C13 C12 121.1(9) . . ? C14 C13 H13 119.4 . . ? C9 C14 H14 120.3 . . ? C13 C14 C9 119.4(8) . . ? C13 C14 H14 120.3 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pt1 C1 1.970(7) . ? Pt1 C1 1.970(7) 2_566 ? Pt1 C2 1.980(7) 1_455 ? Pt1 C2 1.980(7) 2_666 ? Fe1 N1 1.926(6) . ? Fe1 N1 1.926(6) 2_676 ? Fe1 N2 1.926(6) 2_676 ? Fe1 N2 1.926(6) . ? Fe1 N3 2.008(5) 2_676 ? Fe1 N3 2.008(5) . ? N1 C1 1.170(10) . ? N2 C2 1.154(10) . ? N3 C3 1.335(10) . ? N3 C7 1.356(9) . ? C3 H3 0.9500 . ? C3 C4 1.394(10) . ? C4 H4 0.9500 . ? C4 C5 1.399(11) . ? C5 C6 1.387(12) . ? C5 C8 1.439(10) . ? C6 H6 0.9500 . ? C6 C7 1.392(9) . ? C7 H7 0.9500 . ? C8 C8 1.186(16) 2_577 ? N4 N4 1.239(13) 2_567 ? N4 C9 1.434(11) . ? C9 C10 1.404(11) . ? C9 C14 1.395(13) . ? C10 H10 0.9500 . ? C10 C11 1.399(12) . ? C11 H11 0.9500 . ? C11 C12 1.387(14) . ? C12 H12 0.9500 . ? C12 C13 1.400(12) . ? C13 H13 0.9500 . ? C13 C14 1.383(12) . ? C14 H14 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Fe1 N3 C3 C4 -170.9(6) . . . . ? Fe1 N3 C7 C6 171.0(5) . . . . ? N3 C3 C4 C5 -0.5(12) . . . . ? C3 N3 C7 C6 -4.2(10) . . . . ? C3 C4 C5 C6 -3.5(11) . . . . ? C3 C4 C5 C8 176.0(7) . . . . ? C4 C5 C6 C7 3.6(11) . . . . ? C5 C6 C7 N3 0.3(11) . . . . ? C7 N3 C3 C4 4.3(10) . . . . ? C8 C5 C6 C7 -176.0(7) . . . . ? N4 N4 C9 C10 -171.2(8) 2_567 . . . ? N4 N4 C9 C14 9.8(13) 2_567 . . . ? N4 C9 C10 C11 178.0(7) . . . . ? N4 C9 C14 C13 -178.0(8) . . . . ? C9 C10 C11 C12 1.3(12) . . . . ? C10 C9 C14 C13 2.9(12) . . . . ? C10 C11 C12 C13 0.4(12) . . . . ? C11 C12 C13 C14 -0.4(13) . . . . ? C12 C13 C14 C9 -1.2(13) . . . . ? C14 C9 C10 C11 -2.9(12) . . . . ?