Crystallography Open Database

Information card for entry 7707866

Preview

Coordinates	7707866.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H116 Co2 Gd2 N4 O32
Calculated formula	C54 H112 Co2 Gd2 N4 O32
Title of publication	From tetranuclear to pentanuclear [Co-Ln] (Ln = Gd, Tb, Dy, Ho) complexes across the lanthanide series: effect of varying sequence of ligand addition.
Authors of publication	Basak, Dipmalya; Smythe, Lucy; Herchel, Radovan; Murrie, Mark; Nemec, Ivan; Ray, Debashis
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	34
Pages of publication	11861 - 11877
a	9.208 ± 0.005 Å
b	13.808 ± 0.01 Å
c	15.878 ± 0.009 Å
α	105.21 ± 0.03°
β	99.6 ± 0.02°
γ	102.95 ± 0.04°
Cell volume	1843 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0446
Residual factor for significantly intense reflections	0.0376
Weighted residual factors for significantly intense reflections	0.0891
Weighted residual factors for all reflections included in the refinement	0.0922
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268816 (current)	2021-09-06	cif/ Updating files of 7707862, 7707863, 7707864, 7707865, 7707866 Original log message: Adding full bibliography for 7707862--7707866.cif.	7707866.cif
267688	2021-07-22	cif/ Adding structures of 7707862, 7707863, 7707864, 7707865, 7707866 via cif-deposit CGI script.	7707866.cif