Crystallography Open Database

Information card for entry 7707937

Preview

Coordinates	7707937.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	B2 O25 Pb6 Si8
Calculated formula	B2.036 O25 Pb6 Si7.964
Title of publication	High-temperature, high-pressure hydrothermal synthesis, crystal structure, and solid state NMR spectroscopy of a lead borosilicate with boron-silicon mixing: Pb<sub>6</sub>B<sub>2</sub>Si<sub>8</sub>O<sub>25</sub>.
Authors of publication	Chang, Ling-Wei; Lii, Kwang-Hwa
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	32
Pages of publication	11173 - 11179
a	9.509 ± 0.0002 Å
b	9.509 ± 0.0002 Å
c	42.3552 ± 0.0008 Å
α	90°
β	90°
γ	120°
Cell volume	3316.71 ± 0.12 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	167
Hermann-Mauguin space group symbol	R -3 c :H
Hall space group symbol	-R 3 2"c
Residual factor for all reflections	0.0183
Residual factor for significantly intense reflections	0.0147
Weighted residual factors for significantly intense reflections	0.0301
Weighted residual factors for all reflections included in the refinement	0.0309
Goodness-of-fit parameter for all reflections included in the refinement	1.126
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268742 (current)	2021-09-06	cif/ Updating files of 7707937 Original log message: Adding full bibliography for 7707937.cif.	7707937.cif
267903	2021-08-03	cif/ Adding structures of 7707937 via cif-deposit CGI script.	7707937.cif