#------------------------------------------------------------------------------ #$Date: 2021-08-04 04:05:38 +0300 (Wed, 04 Aug 2021) $ #$Revision: 267927 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/79/7707948.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707948 loop_ _publ_author_name 'Malik, Deesha D.' 'Chandra, Anirban' 'Seo, Mi Sook' 'Lee, Yong-Min' 'Farquhar, Erik R.' 'mebs, stefan' 'Dau, Holger' 'Ray, Kallol' 'Nam, Wonwoo' _publ_section_title ; Formation of cobalt-oxygen intermediates by dioxygen activation at a mononuclear nonheme cobalt(II) center ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT01996A _journal_year 2021 _chemical_formula_moiety 'C21 H48 Co N10, 2(C24 H20 B)' _chemical_formula_sum 'C69 H88 B2 Co N10' _chemical_formula_weight 1138.04 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _audit_update_record ; 2021-06-18 deposited with the CCDC. 2021-08-03 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 91.831(5) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 17.8342(17) _cell_length_b 19.1569(18) _cell_length_c 18.2002(17) _cell_measurement_reflns_used 159628 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 32.826 _cell_measurement_theta_min 1.544 _cell_volume 6214.9(10) _computing_cell_refinement 'Bruker SMART' _computing_data_collection 'Bruker SMART' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_temperature 120(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.985 _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0848 _diffrn_reflns_av_unetI/netI 0.0574 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.985 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 159628 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.985 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 32.826 _diffrn_reflns_theta_min 1.544 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.326 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour purple _exptl_crystal_density_diffrn 1.216 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 2436 _exptl_crystal_size_max 0.300 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.100 _exptl_transmission_factor_max 0.746 _exptl_transmission_factor_min 0.654 _refine_diff_density_max 0.963 _refine_diff_density_min -0.825 _refine_diff_density_rms 0.063 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.062 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 751 _refine_ls_number_reflns 22747 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.062 _refine_ls_R_factor_all 0.0873 _refine_ls_R_factor_gt 0.0497 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0418P)^2^+3.2469P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1080 _refine_ls_wR_factor_ref 0.1277 _reflns_Friedel_coverage 0.000 _reflns_number_gt 16027 _reflns_number_total 22747 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt01996a2.cif _cod_data_source_block CCDC-2090593 _cod_depositor_comments ; The following automatic conversions were performed: data item '_exptl_crystal_density_meas' value 'not measured' was changed to '?' -- the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas ; _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 7707948 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.908 _shelx_estimated_absorpt_t_max 0.968 _shelx_res_file ; TITL KJ007-1.res in P2(1)/n KJ007-1.res created by SHELXL-2016/6 at 15:45:16 on 08-Nov-2017 CELL 0.71073 17.8342 19.1569 18.2002 90.000 91.831 90.000 ZERR 4.000 0.0017 0.0018 0.0017 0.000 0.005 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N Co B UNIT 276 352 40 4 8 L.S. 10 ACTA CONF BOND $H FMAP 2 PLAN 1 SIZE 0.30 0.20 0.10 TEMP -153.000 WGHT 0.041800 3.246900 FVAR 0.21296 CO1 4 0.482294 0.224182 0.299515 11.00000 0.01521 0.01853 = 0.01720 0.00150 0.00186 0.00012 N1 3 0.383901 0.187294 0.341882 11.00000 0.01753 0.02531 = 0.01906 0.00234 0.00113 -0.00035 N2 3 0.523348 0.218898 0.401611 11.00000 0.01617 0.02102 = 0.01795 0.00043 0.00167 -0.00052 N3 3 0.482669 0.137789 0.238954 11.00000 0.01927 0.02110 = 0.01674 -0.00005 0.00271 -0.00324 N4 3 0.419865 0.303362 0.263675 11.00000 0.01565 0.02359 = 0.02617 0.00382 0.00168 0.00182 N5 3 0.651998 0.207767 0.388835 11.00000 0.01661 0.02853 = 0.03034 -0.00538 0.00293 -0.00411 N6 3 0.608539 0.248653 0.498729 11.00000 0.02332 0.02442 = 0.02571 -0.00483 -0.00500 0.00198 N7 3 0.538375 0.047511 0.170673 11.00000 0.03135 0.01936 = 0.01925 -0.00071 0.00210 0.00156 N8 3 0.566840 0.163080 0.147529 11.00000 0.02477 0.02141 = 0.02441 0.00085 0.00869 0.00029 N9 3 0.396996 0.381619 0.165106 11.00000 0.03517 0.02684 = 0.02824 0.00660 -0.00855 0.00027 N10 3 0.504424 0.391275 0.239406 11.00000 0.02622 0.02313 = 0.03002 0.00361 -0.00234 -0.00296 B1 5 0.742794 0.488818 0.574643 11.00000 0.02025 0.02728 = 0.02052 -0.00036 -0.00085 -0.00333 B2 5 0.758636 0.433396 0.079100 11.00000 0.02299 0.01978 = 0.01905 0.00081 0.00406 -0.00013 C1 1 0.403246 0.161548 0.417266 11.00000 0.01962 0.02914 = 0.01683 0.00205 0.00418 -0.00316 AFIX 23 H1A 2 0.423424 0.113493 0.414768 11.00000 -1.20000 H1B 2 0.357721 0.160603 0.446984 11.00000 -1.20000 AFIX 0 C2 1 0.461597 0.209793 0.452924 11.00000 0.01997 0.02743 = 0.01778 -0.00219 0.00440 -0.00164 AFIX 23 H2A 2 0.438695 0.255573 0.463775 11.00000 -1.20000 H2B 2 0.481070 0.189308 0.499687 11.00000 -1.20000 AFIX 0 C3 1 0.358368 0.131627 0.290456 11.00000 0.02058 0.03201 = 0.02048 0.00164 0.00038 -0.00848 AFIX 23 H3A 2 0.332044 0.152810 0.247240 11.00000 -1.20000 H3B 2 0.322643 0.100565 0.315137 11.00000 -1.20000 AFIX 0 C4 1 0.424811 0.089338 0.265426 11.00000 0.02548 0.02446 = 0.01872 0.00109 0.00242 -0.00845 AFIX 23 H4A 2 0.445679 0.061151 0.306833 11.00000 -1.20000 H4B 2 0.408614 0.057178 0.225405 11.00000 -1.20000 AFIX 0 C5 1 0.330969 0.247094 0.342323 11.00000 0.01677 0.03511 = 0.03495 0.00550 0.00612 0.00367 AFIX 23 H5A 2 0.341874 0.276775 0.385894 11.00000 -1.20000 H5B 2 0.278858 0.229713 0.345085 11.00000 -1.20000 AFIX 0 C6 1 0.339195 0.289641 0.272656 11.00000 0.01579 0.03601 = 0.04101 0.01130 0.00150 0.00335 AFIX 23 H6A 2 0.318433 0.263493 0.229723 11.00000 -1.20000 H6B 2 0.311512 0.334227 0.276409 11.00000 -1.20000 AFIX 0 C7 1 0.592887 0.225375 0.429407 11.00000 0.02029 0.01656 = 0.02138 0.00034 -0.00055 -0.00114 C8 1 0.720419 0.249218 0.392279 11.00000 0.02692 0.05828 = 0.06414 -0.02187 0.01422 -0.02128 AFIX 137 H8A 2 0.714580 0.287831 0.426951 11.00000 -1.50000 H8B 2 0.730143 0.267971 0.343400 11.00000 -1.50000 H8C 2 0.762601 0.219760 0.408805 11.00000 -1.50000 AFIX 0 C9 1 0.645904 0.159546 0.327598 11.00000 0.02190 0.03843 = 0.02988 -0.01000 0.00243 0.00058 AFIX 137 H9A 2 0.602806 0.128651 0.334005 11.00000 -1.50000 H9B 2 0.691814 0.131580 0.325705 11.00000 -1.50000 H9C 2 0.638970 0.185796 0.281666 11.00000 -1.50000 AFIX 0 C10 1 0.672314 0.222563 0.542985 11.00000 0.03233 0.03482 = 0.03848 -0.00410 -0.01574 0.00412 AFIX 137 H10A 2 0.691091 0.179515 0.521033 11.00000 -1.50000 H10B 2 0.656402 0.212934 0.593022 11.00000 -1.50000 H10C 2 0.712235 0.257735 0.544591 11.00000 -1.50000 AFIX 0 C11 1 0.565689 0.304338 0.532258 11.00000 0.03502 0.02927 = 0.03088 -0.01119 -0.00534 0.00464 AFIX 137 H11A 2 0.532222 0.325823 0.494967 11.00000 -1.50000 H11B 2 0.600181 0.339688 0.552670 11.00000 -1.50000 H11C 2 0.535852 0.284945 0.571681 11.00000 -1.50000 AFIX 0 C12 1 0.528187 0.115861 0.187684 11.00000 0.01980 0.02085 = 0.01716 0.00032 0.00009 -0.00043 C13 1 0.643006 0.148748 0.123691 11.00000 0.02625 0.03507 = 0.03632 -0.00158 0.01284 -0.00176 AFIX 137 H13A 2 0.660800 0.104711 0.145392 11.00000 -1.50000 H13B 2 0.676438 0.186766 0.139767 11.00000 -1.50000 H13C 2 0.642727 0.145181 0.069969 11.00000 -1.50000 AFIX 0 C14 1 0.545016 0.235735 0.143514 11.00000 0.04048 0.02466 = 0.03433 0.00695 0.01576 0.00335 AFIX 137 H14A 2 0.490288 0.239366 0.145231 11.00000 -1.50000 H14B 2 0.561927 0.255925 0.097423 11.00000 -1.50000 H14C 2 0.568048 0.261140 0.185168 11.00000 -1.50000 AFIX 0 C15 1 0.547287 0.024333 0.094909 11.00000 0.03657 0.02752 = 0.02378 -0.00552 0.00398 0.00367 AFIX 137 H15A 2 0.532141 0.061933 0.061073 11.00000 -1.50000 H15B 2 0.515764 -0.016770 0.085296 11.00000 -1.50000 H15C 2 0.599931 0.012301 0.087577 11.00000 -1.50000 AFIX 0 C16 1 0.547769 -0.006526 0.226987 11.00000 0.04275 0.02211 = 0.02911 0.00411 -0.00312 0.00116 AFIX 137 H16A 2 0.555359 0.015476 0.275264 11.00000 -1.50000 H16B 2 0.591462 -0.035369 0.216251 11.00000 -1.50000 H16C 2 0.502781 -0.035892 0.227179 11.00000 -1.50000 AFIX 0 C17 1 0.439490 0.357490 0.223175 11.00000 0.02314 0.02083 = 0.02321 -0.00009 -0.00093 0.00303 C18 1 0.551580 0.419141 0.182098 11.00000 0.03936 0.03351 = 0.04740 0.00872 0.00859 -0.01007 AFIX 137 H18A 2 0.530006 0.406563 0.133698 11.00000 -1.50000 H18B 2 0.602159 0.399465 0.187746 11.00000 -1.50000 H18C 2 0.554192 0.470081 0.186423 11.00000 -1.50000 AFIX 0 C19 1 0.539871 0.387276 0.312342 11.00000 0.03712 0.03102 = 0.04065 0.00248 -0.01436 -0.00552 AFIX 137 H19A 2 0.501615 0.378388 0.348668 11.00000 -1.50000 H19B 2 0.565255 0.431506 0.323812 11.00000 -1.50000 H19C 2 0.576634 0.349239 0.313707 11.00000 -1.50000 AFIX 0 C20 1 0.393108 0.455053 0.144146 11.00000 0.06401 0.03157 = 0.05379 0.01652 -0.02035 0.00428 AFIX 137 H20A 2 0.419194 0.483370 0.181817 11.00000 -1.50000 H20B 2 0.340476 0.469588 0.139636 11.00000 -1.50000 H20C 2 0.417041 0.461538 0.096902 11.00000 -1.50000 AFIX 0 C21 1 0.352951 0.335129 0.117411 11.00000 0.04750 0.04617 = 0.03329 0.00318 -0.01499 -0.00742 AFIX 137 H21A 2 0.366994 0.286617 0.127986 11.00000 -1.50000 H21B 2 0.362729 0.345796 0.065933 11.00000 -1.50000 H21C 2 0.299485 0.341686 0.126212 11.00000 -1.50000 AFIX 0 C22 1 0.691113 0.442668 0.630710 11.00000 0.02240 0.02976 = 0.01842 -0.00187 -0.00297 -0.00568 C23 1 0.711290 0.376250 0.657049 11.00000 0.02423 0.03456 = 0.02228 0.00279 -0.00537 -0.00374 AFIX 43 H23 2 0.756612 0.356025 0.641114 11.00000 -1.20000 AFIX 0 C24 1 0.667847 0.338525 0.705578 11.00000 0.03280 0.04059 = 0.02598 0.00979 -0.00647 -0.00714 AFIX 43 H24 2 0.684507 0.294214 0.722924 11.00000 -1.20000 AFIX 0 C25 1 0.600425 0.365581 0.728528 11.00000 0.03440 0.05095 = 0.02309 0.00754 0.00019 -0.01459 AFIX 43 H25 2 0.570286 0.339993 0.761168 11.00000 -1.20000 AFIX 0 C26 1 0.577832 0.430492 0.703051 11.00000 0.02719 0.04949 = 0.02846 -0.00067 0.00635 -0.00388 AFIX 43 H26 2 0.531293 0.449354 0.717498 11.00000 -1.20000 AFIX 0 C27 1 0.622897 0.468387 0.656335 11.00000 0.02802 0.03480 = 0.02901 -0.00042 0.00394 -0.00174 AFIX 43 H27 2 0.606851 0.513565 0.641127 11.00000 -1.20000 AFIX 0 C28 1 0.792287 0.437250 0.521918 11.00000 0.02454 0.02468 = 0.02309 -0.00119 0.00153 -0.00631 C29 1 0.776680 0.427369 0.446471 11.00000 0.03030 0.02699 = 0.02404 -0.00090 0.00206 -0.00798 AFIX 43 H29 2 0.734790 0.450878 0.424446 11.00000 -1.20000 AFIX 0 C30 1 0.819836 0.384660 0.402465 11.00000 0.04117 0.03178 = 0.02528 -0.00703 0.00750 -0.01527 AFIX 43 H30 2 0.807549 0.380576 0.351472 11.00000 -1.20000 AFIX 0 C31 1 0.880167 0.348300 0.432241 11.00000 0.03293 0.02835 = 0.04146 -0.01108 0.01330 -0.01094 AFIX 43 H31 2 0.908830 0.318201 0.402596 11.00000 -1.20000 AFIX 0 C32 1 0.898144 0.356621 0.506523 11.00000 0.02801 0.03239 = 0.04278 -0.00643 0.00369 -0.00143 AFIX 43 H32 2 0.939645 0.332153 0.528050 11.00000 -1.20000 AFIX 0 C33 1 0.855725 0.400567 0.549535 11.00000 0.02610 0.03267 = 0.02846 -0.00373 -0.00067 -0.00171 AFIX 43 H33 2 0.870127 0.406165 0.599895 11.00000 -1.20000 AFIX 0 C34 1 0.687774 0.537861 0.521390 11.00000 0.02200 0.02964 = 0.02067 -0.00085 0.00097 -0.00104 C35 1 0.621102 0.510645 0.489123 11.00000 0.02628 0.03390 = 0.02871 0.00247 -0.00402 -0.00527 AFIX 43 H35 2 0.606592 0.464511 0.501498 11.00000 -1.20000 AFIX 0 C36 1 0.575544 0.548403 0.439888 11.00000 0.02358 0.04605 = 0.02792 -0.00130 -0.00249 0.00114 AFIX 43 H36 2 0.530804 0.528014 0.419939 11.00000 -1.20000 AFIX 0 C37 1 0.595127 0.615310 0.419963 11.00000 0.02851 0.04130 = 0.02361 0.00215 0.00265 0.01277 AFIX 43 H37 2 0.564704 0.640846 0.385630 11.00000 -1.20000 AFIX 0 C38 1 0.659868 0.644749 0.450783 11.00000 0.03151 0.02997 = 0.03085 0.00370 0.00520 0.00469 AFIX 43 H38 2 0.673948 0.690834 0.437755 11.00000 -1.20000 AFIX 0 C39 1 0.704269 0.606688 0.500881 11.00000 0.02491 0.02917 = 0.02628 -0.00056 0.00234 -0.00101 AFIX 43 H39 2 0.747708 0.628332 0.522131 11.00000 -1.20000 AFIX 0 C40 1 0.800365 0.540391 0.621890 11.00000 0.02016 0.02340 = 0.02207 -0.00018 -0.00190 0.00088 C41 1 0.863103 0.570006 0.588658 11.00000 0.02538 0.03183 = 0.02712 -0.00237 0.00263 -0.00391 AFIX 43 H41 2 0.875190 0.554770 0.540795 11.00000 -1.20000 AFIX 0 C42 1 0.908246 0.620582 0.622688 11.00000 0.02204 0.02979 = 0.03917 0.00075 0.00026 -0.00445 AFIX 43 H42 2 0.949626 0.639448 0.597759 11.00000 -1.20000 AFIX 0 C43 1 0.892898 0.643451 0.692898 11.00000 0.02784 0.02374 = 0.03578 -0.00190 -0.01056 -0.00086 AFIX 43 H43 2 0.922929 0.678474 0.716210 11.00000 -1.20000 AFIX 0 C44 1 0.833103 0.614328 0.728285 11.00000 0.03186 0.02549 = 0.02478 -0.00342 -0.00559 0.00387 AFIX 43 H44 2 0.822493 0.628793 0.776787 11.00000 -1.20000 AFIX 0 C45 1 0.787959 0.563677 0.693359 11.00000 0.02428 0.02507 = 0.02190 -0.00023 0.00000 0.00068 AFIX 43 H45 2 0.747377 0.544394 0.719160 11.00000 -1.20000 AFIX 0 C46 1 0.724422 0.490835 0.136595 11.00000 0.01934 0.02068 = 0.02181 -0.00111 0.00484 -0.00163 C47 1 0.684700 0.549892 0.110052 11.00000 0.02651 0.02314 = 0.02717 0.00100 0.00393 0.00104 AFIX 43 H47 2 0.680733 0.557213 0.058448 11.00000 -1.20000 AFIX 0 C48 1 0.651111 0.597844 0.156023 11.00000 0.02743 0.02214 = 0.04225 -0.00086 0.00723 0.00279 AFIX 43 H48 2 0.623477 0.635939 0.135555 11.00000 -1.20000 AFIX 0 C49 1 0.657908 0.590115 0.231595 11.00000 0.03359 0.02657 = 0.03979 -0.00987 0.01447 -0.00262 AFIX 43 H49 2 0.634378 0.622242 0.263262 11.00000 -1.20000 AFIX 0 C50 1 0.699425 0.534978 0.260329 11.00000 0.03596 0.03065 = 0.02472 -0.00604 0.00683 -0.00388 AFIX 43 H50 2 0.706004 0.530014 0.312068 11.00000 -1.20000 AFIX 0 C51 1 0.731707 0.486571 0.213429 11.00000 0.02458 0.02471 = 0.02267 -0.00163 0.00310 -0.00087 AFIX 43 H51 2 0.759851 0.449088 0.234515 11.00000 -1.20000 AFIX 0 C52 1 0.691007 0.389960 0.033796 11.00000 0.02706 0.02425 = 0.01917 0.00158 0.00535 -0.00477 C53 1 0.704181 0.322875 0.005723 11.00000 0.03125 0.02648 = 0.02863 -0.00374 0.00804 -0.00690 AFIX 43 H53 2 0.751174 0.301403 0.016969 11.00000 -1.20000 AFIX 0 C54 1 0.651920 0.286262 -0.037716 11.00000 0.04508 0.03399 = 0.03073 -0.00698 0.00737 -0.01343 AFIX 43 H54 2 0.663739 0.241076 -0.055469 11.00000 -1.20000 AFIX 0 C55 1 0.582873 0.315688 -0.054979 11.00000 0.04643 0.04567 = 0.02895 -0.00270 -0.00338 -0.01822 AFIX 43 H55 2 0.546965 0.291152 -0.084754 11.00000 -1.20000 AFIX 0 C56 1 0.566801 0.381465 -0.028235 11.00000 0.03321 0.04652 = 0.03570 0.00333 -0.00742 -0.00608 AFIX 43 H56 2 0.519404 0.402187 -0.039414 11.00000 -1.20000 AFIX 0 C57 1 0.620062 0.417556 0.015187 11.00000 0.03169 0.03073 = 0.02700 0.00142 -0.00133 -0.00142 AFIX 43 H57 2 0.607665 0.462648 0.032811 11.00000 -1.20000 AFIX 0 C58 1 0.806389 0.478281 0.019814 11.00000 0.02303 0.01681 = 0.02131 0.00053 0.00472 0.00308 C59 1 0.789377 0.481260 -0.055592 11.00000 0.02629 0.02002 = 0.02207 0.00205 0.00337 0.00220 AFIX 43 H59 2 0.746997 0.456191 -0.074397 11.00000 -1.20000 AFIX 0 C60 1 0.831946 0.519459 -0.104448 11.00000 0.04082 0.02329 = 0.02306 0.00398 0.00785 0.00229 AFIX 43 H60 2 0.817272 0.521100 -0.155057 11.00000 -1.20000 AFIX 0 C61 1 0.895168 0.554844 -0.079770 11.00000 0.03790 0.02381 = 0.03736 0.00739 0.01522 -0.00147 AFIX 43 H61 2 0.925504 0.579186 -0.113249 11.00000 -1.20000 AFIX 0 C62 1 0.913754 0.554264 -0.004911 11.00000 0.03008 0.02427 = 0.04316 0.00438 0.00236 -0.00578 AFIX 43 H62 2 0.956857 0.578697 0.013205 11.00000 -1.20000 AFIX 0 C63 1 0.869303 0.517996 0.043179 11.00000 0.03072 0.02312 = 0.02651 0.00068 0.00007 -0.00252 AFIX 43 H63 2 0.881812 0.519993 0.094266 11.00000 -1.20000 AFIX 0 C64 1 0.812305 0.376305 0.123958 11.00000 0.02698 0.01927 = 0.01830 -0.00100 0.00378 0.00129 C65 1 0.890529 0.372001 0.120735 11.00000 0.02852 0.02316 = 0.02225 0.00184 0.00137 -0.00059 AFIX 43 H65 2 0.915681 0.403383 0.089482 11.00000 -1.20000 AFIX 0 C66 1 0.933237 0.323569 0.161471 11.00000 0.02943 0.02912 = 0.03208 0.00108 -0.00368 0.00219 AFIX 43 H66 2 0.986270 0.323086 0.157979 11.00000 -1.20000 AFIX 0 C67 1 0.898592 0.276299 0.206887 11.00000 0.04311 0.02621 = 0.02699 0.00317 -0.00288 0.00600 AFIX 43 H67 2 0.927423 0.243624 0.235073 11.00000 -1.20000 AFIX 0 C68 1 0.821371 0.277519 0.210461 11.00000 0.04663 0.02371 = 0.02941 0.00746 0.00960 0.00382 AFIX 43 H68 2 0.796634 0.244743 0.240466 11.00000 -1.20000 AFIX 0 C69 1 0.779646 0.326567 0.170285 11.00000 0.03192 0.02443 = 0.03008 0.00455 0.01019 0.00341 AFIX 43 H69 2 0.726661 0.326551 0.174248 11.00000 -1.20000 AFIX 0 HKLF 4 REM KJ007-1.res in P2(1)/n REM R1 = 0.0497 for 16027 Fo > 4sig(Fo) and 0.0873 for all 22747 data REM 751 parameters refined using 0 restraints END WGHT 0.0417 3.2603 REM Highest difference peak 0.963, deepest hole -0.825, 1-sigma level 0.063 Q1 1 0.5704 0.2573 0.2587 11.00000 0.05 0.96 ; _shelx_res_checksum 49980 _shelx_hkl_file ; 1 0 0 -0.10 0.10 -1 0 0 0.00 0.20 2 0 0 51.69 3.80 -2 0 0 47.00 3.80 -3 0 0 -0.50 0.60 3 0 0 -0.40 0.50 -5 0 0 0.90 1.00 -6 0 0 26.40 2.70 -6 0 0 27.40 2.70 -6 0 0 31.50 2.60 6 0 0 32.80 2.60 6 0 0 29.50 2.60 7 0 0 0.90 0.90 -7 0 0 -1.00 0.80 7 0 0 -0.10 0.90 -7 0 0 0.20 0.80 -7 0 0 -2.30 0.90 7 0 0 0.20 1.00 -7 0 0 -1.30 0.70 8 0 0 193.18 13.80 -8 0 0 181.98 13.80 -8 0 0 170.38 13.70 8 0 0 169.68 13.70 -8 0 0 173.68 13.80 8 0 0 189.78 13.70 -9 0 0 -1.00 0.90 9 0 0 -1.00 1.20 9 0 0 -0.80 1.00 9 0 0 -0.60 1.10 -9 0 0 0.70 1.00 -10 0 0 358.36 28.80 -10 0 0 397.06 28.80 10 0 0 331.27 28.80 -10 0 0 377.36 28.90 10 0 0 401.66 28.80 -10 0 0 420.96 28.70 -11 0 0 -1.50 1.30 11 0 0 0.00 1.30 11 0 0 -0.30 1.30 -11 0 0 0.60 1.10 -11 0 0 0.90 1.00 -11 0 0 1.20 1.30 11 0 0 -0.10 1.10 -12 0 0 7.30 1.40 -12 0 0 -0.40 1.10 12 0 0 1.20 1.30 -12 0 0 -0.50 1.30 12 0 0 0.30 1.20 -12 0 0 -1.30 1.40 13 0 0 -1.10 1.50 -13 0 0 -1.00 1.20 -13 0 0 -4.40 1.40 13 0 0 -1.50 1.30 -13 0 0 -2.10 1.10 -13 0 0 -0.60 1.40 -14 0 0 1.00 1.40 14 0 0 0.20 1.60 14 0 0 3.50 1.70 -14 0 0 1.70 1.90 -14 0 0 -1.30 1.60 -14 0 0 4.20 1.60 -15 0 0 -0.30 1.80 -15 0 0 -2.50 2.00 -15 0 0 0.60 2.00 15 0 0 0.60 1.60 15 0 0 -1.60 1.50 -15 0 0 0.00 1.30 16 0 0 88.29 7.60 16 0 0 89.99 7.40 -16 0 0 84.49 7.40 -16 0 0 70.79 7.60 -16 0 0 85.59 7.50 -16 0 0 107.59 7.40 17 0 0 0.60 1.80 -17 0 0 8.80 2.60 17 0 0 1.00 1.80 -17 0 0 -0.60 2.30 -17 0 0 1.50 1.90 -17 0 0 1.70 1.60 -18 0 0 6.70 1.90 18 0 0 10.30 2.40 18 0 0 8.10 2.50 -18 0 0 10.10 2.40 -18 0 0 13.50 2.50 -18 0 0 11.10 2.60 -19 0 0 2.60 2.10 19 0 0 3.60 2.20 -19 0 0 0.40 1.90 -19 0 0 -4.10 2.60 -19 0 0 5.70 2.50 -20 0 0 6.70 2.40 -20 0 0 3.30 2.40 -20 0 0 -1.40 2.90 -21 0 0 -1.00 3.00 -21 0 0 5.50 2.80 -22 0 0 75.39 7.10 -22 0 0 75.29 7.80 -23 0 0 -1.50 3.60 -23 0 0 5.80 2.90 -24 0 0 47.90 6.10 -24 0 0 47.80 5.40 -25 0 0 9.00 3.30 -25 0 0 2.40 4.10 -26 0 0 11.50 4.60 -27 0 0 3.10 3.50 -27 0 0 4.70 4.80 0 -1 0 0.10 0.10 0 1 0 0.20 0.20 -1 -1 0 212.88 18.80 1 -1 0 256.67 18.80 -1 1 0 244.08 18.80 1 1 0 278.97 18.80 -2 -1 0 25.50 1.90 2 -1 0 23.20 1.90 -2 -1 0 25.60 1.90 2 1 0 21.80 1.80 -2 1 0 18.10 1.90 3 -1 0 11.90 1.40 -3 -1 0 13.30 1.30 -3 1 0 10.80 1.40 3 1 0 12.90 1.30 -4 -1 0 68.09 4.70 4 -1 0 56.79 4.80 4 1 0 63.29 4.80 -4 1 0 53.69 4.80 -5 -1 0 11.00 1.50 5 -1 0 18.40 1.80 5 1 0 14.50 1.70 -5 1 0 19.90 1.80 6 -1 0 11.80 1.50 6 -1 0 10.90 1.50 -6 -1 0 12.20 1.50 -6 -1 0 14.40 1.40 -6 -1 0 10.80 1.40 -6 1 0 10.20 1.40 -6 1 0 12.10 1.40 -6 1 0 13.60 1.50 6 1 0 12.20 1.40 -7 -1 0 79.69 6.60 7 -1 0 82.39 6.70 7 -1 0 88.79 6.60 -7 -1 0 92.59 6.70 -7 -1 0 80.19 6.70 -7 -1 0 74.49 6.60 -7 1 0 87.49 6.60 -7 1 0 93.29 6.70 7 1 0 89.99 6.70 -7 1 0 87.49 6.60 -7 1 0 80.99 6.70 7 1 0 85.19 6.60 7 1 0 83.19 6.60 8 -1 0 50.89 4.10 -8 -1 0 49.70 4.20 8 -1 0 45.20 3.90 -8 -1 0 44.40 4.10 -8 -1 0 59.19 4.00 -8 1 0 41.10 4.00 -8 1 0 50.09 4.10 -8 1 0 46.70 3.90 8 1 0 49.99 4.10 -8 1 0 42.30 4.10 8 1 0 42.00 3.90 9 -1 0 -0.60 1.10 -9 -1 0 0.60 1.00 9 -1 0 0.50 1.00 -9 1 0 0.70 0.90 9 1 0 2.70 1.20 9 1 0 0.60 1.00 -9 1 0 4.50 1.20 -9 1 0 5.70 1.40 9 1 0 1.00 1.10 -10 -1 0 75.49 6.20 10 -1 0 87.49 6.30 -10 -1 0 81.69 6.40 10 -1 0 82.79 6.20 -10 -1 0 75.59 6.00 -10 -1 0 85.49 6.40 -10 1 0 83.89 6.40 10 1 0 62.79 6.20 -10 1 0 66.99 6.20 -10 1 0 76.39 6.30 -10 1 0 73.59 6.10 10 1 0 85.19 6.30 -11 -1 0 42.90 4.00 11 -1 0 47.50 4.00 11 -1 0 42.30 3.80 -11 -1 0 48.80 4.00 -11 -1 0 40.10 3.80 -11 -1 0 48.20 3.60 -11 1 0 44.40 4.00 11 1 0 39.60 3.90 -11 1 0 49.60 3.80 11 1 0 41.20 3.90 11 1 0 54.79 4.00 -11 1 0 43.00 3.90 -11 1 0 31.10 4.00 12 -1 0 245.58 18.20 -12 -1 0 208.18 18.10 12 -1 0 247.58 18.00 -12 -1 0 248.28 18.10 -12 -1 0 240.48 18.20 -12 1 0 192.98 18.00 -12 1 0 198.38 17.90 12 1 0 252.07 18.10 12 1 0 272.07 18.10 12 1 0 250.77 18.10 -12 1 0 231.68 18.20 -12 1 0 254.17 18.20 -13 -1 0 16.70 2.00 -13 -1 0 12.50 2.00 -13 -1 0 14.60 2.20 13 -1 0 11.90 2.10 13 -1 0 15.30 2.00 -13 -1 0 11.10 2.20 13 1 0 13.80 2.20 13 1 0 17.20 2.10 -13 1 0 15.80 1.90 -13 1 0 15.30 2.10 -13 1 0 15.30 2.20 13 1 0 15.70 2.20 -13 1 0 10.20 2.20 14 -1 0 133.99 10.00 -14 -1 0 112.29 9.60 -14 -1 0 123.89 10.00 -14 -1 0 118.49 9.80 14 -1 0 113.09 9.70 -14 -1 0 126.59 10.00 14 1 0 128.29 9.90 -14 1 0 132.89 9.90 14 1 0 129.69 9.70 -14 1 0 129.09 9.70 -14 1 0 107.89 9.80 -15 -1 0 5.20 2.20 15 -1 0 6.90 2.10 -15 -1 0 6.80 2.00 -15 -1 0 6.90 1.60 -15 -1 0 6.30 1.90 15 -1 0 6.60 1.80 15 1 0 6.40 1.70 -15 1 0 8.00 1.90 -15 1 0 10.80 1.70 -15 1 0 6.70 1.80 -15 1 0 4.90 2.20 15 1 0 7.60 1.80 -16 -1 0 34.60 4.00 16 -1 0 30.50 3.60 16 -1 0 35.30 3.90 -16 -1 0 38.00 4.00 -16 -1 0 36.60 3.50 -16 -1 0 36.50 3.80 16 1 0 31.80 3.80 -16 1 0 25.40 3.90 -16 1 0 40.90 4.10 -16 1 0 34.00 3.80 16 1 0 37.90 3.70 -16 1 0 38.10 3.80 -17 -1 0 56.19 5.40 17 -1 0 57.09 5.50 17 -1 0 53.99 5.30 -17 -1 0 46.60 5.00 -17 -1 0 45.60 5.20 17 1 0 52.19 5.30 -17 1 0 71.29 5.90 -17 1 0 52.59 5.30 17 1 0 58.09 5.50 -17 1 0 63.19 5.30 -17 1 0 56.29 5.00 -18 -1 0 94.69 8.50 -18 -1 0 108.19 8.20 18 -1 0 91.99 8.10 -18 -1 0 103.09 8.70 18 -1 0 106.29 8.80 -18 -1 0 93.69 8.40 -18 -1 0 85.99 8.20 18 1 0 91.59 8.30 18 1 0 106.39 8.50 -18 1 0 106.09 8.10 -18 1 0 99.19 8.50 -18 1 0 93.79 8.40 -18 1 0 92.59 8.60 -19 -1 0 -0.90 2.10 -19 -1 0 -1.00 1.70 19 -1 0 0.40 2.30 -19 -1 0 -1.00 2.60 -19 -1 0 -0.80 2.00 -19 1 0 0.90 2.10 -19 1 0 -1.40 2.60 -19 1 0 1.40 2.00 -19 1 0 2.40 2.20 -20 -1 0 27.60 4.50 -20 -1 0 38.30 4.10 -20 -1 0 35.60 4.30 -20 1 0 44.80 4.60 -20 1 0 39.70 4.80 -21 -1 0 -1.30 3.10 -21 -1 0 4.30 2.90 -21 -1 0 -0.80 2.30 -21 1 0 -0.10 2.40 -21 1 0 -1.60 3.10 -22 -1 0 19.10 3.30 -22 -1 0 26.20 4.30 -22 -1 0 15.90 3.60 -22 1 0 20.60 3.80 -22 1 0 17.30 4.20 -23 -1 0 6.60 2.80 -23 -1 0 2.20 3.60 -23 1 0 3.20 2.90 -23 1 0 -0.90 3.60 -24 -1 0 10.30 3.40 -24 -1 0 5.60 4.00 -24 1 0 4.40 3.10 -24 1 0 0.50 3.70 -25 -1 0 26.80 4.20 -25 -1 0 23.70 5.10 -25 1 0 20.90 4.90 -25 1 0 31.60 4.60 -26 -1 0 11.10 4.70 -26 1 0 20.60 4.00 -26 1 0 11.10 4.70 -27 -1 0 4.20 4.80 -27 1 0 0.10 4.40 -27 1 0 17.20 4.30 0 -2 0 1.80 0.40 0 2 0 2.70 0.40 1 -2 0 121.09 9.90 -1 2 0 135.59 10.00 1 2 0 139.19 9.90 -2 -2 0 2327.37 169.18 2 2 0 2219.88 169.08 2 2 0 2212.78 169.08 -2 2 0 2274.37 169.08 3 -2 0 60.89 4.90 -3 -2 0 55.69 4.70 -3 -2 0 61.89 4.80 -3 2 0 62.29 4.80 3 2 0 63.09 4.80 3 2 0 65.69 4.80 4 -2 0 28.70 2.50 -4 -2 0 27.40 2.40 -4 -2 0 28.80 2.30 -4 2 0 21.50 2.50 4 2 0 23.60 2.30 -5 -2 0 991.50 75.19 5 -2 0 895.91 75.19 -5 -2 0 1092.09 75.19 5 2 0 1037.50 75.19 -6 -2 0 532.55 40.40 -6 -2 0 478.05 40.40 -6 -2 0 576.34 40.50 -6 -2 0 595.24 40.40 6 -2 0 554.74 40.50 -6 2 0 562.64 40.40 6 2 0 495.85 40.40 -6 2 0 514.15 40.40 7 -2 0 13.50 1.60 -7 -2 0 12.90 1.60 -7 -2 0 12.90 1.70 7 -2 0 17.30 1.80 -7 -2 0 15.70 1.60 -7 -2 0 15.00 1.60 -7 2 0 15.70 1.60 7 2 0 16.30 1.60 -7 2 0 12.00 1.60 -7 2 0 14.40 1.50 7 2 0 14.50 1.60 7 2 0 12.40 1.50 8 -2 0 79.59 7.00 -8 -2 0 83.19 6.90 8 -2 0 96.69 6.90 -8 -2 0 80.19 7.00 -8 -2 0 86.99 7.00 8 2 0 97.39 6.90 8 2 0 89.19 6.90 -8 2 0 87.09 6.90 -8 2 0 92.19 6.90 -8 2 0 94.29 6.90 8 2 0 80.49 6.90 9 -2 0 9.00 1.50 -9 -2 0 9.10 1.30 9 -2 0 11.40 1.40 -9 -2 0 7.20 1.20 9 2 0 6.10 1.30 -9 2 0 4.80 1.20 9 2 0 11.40 1.50 -9 2 0 9.20 1.60 -9 2 0 11.00 1.50 -9 2 0 8.30 1.40 9 2 0 8.70 1.40 10 -2 0 9.20 1.40 -10 -2 0 8.70 1.40 -10 -2 0 9.60 1.70 -10 -2 0 10.70 1.20 10 -2 0 8.20 1.50 -10 -2 0 9.60 1.50 10 2 0 7.40 1.50 -10 2 0 8.40 1.40 10 2 0 6.50 1.40 10 2 0 7.50 1.40 -10 2 0 7.60 1.70 -10 2 0 7.40 1.30 -10 2 0 9.20 1.50 11 -2 0 265.47 21.50 -11 -2 0 270.17 21.40 -11 -2 0 303.27 21.50 -11 -2 0 299.27 21.60 -11 -2 0 297.47 21.60 11 -2 0 280.17 21.60 -11 2 0 287.67 21.50 11 2 0 268.77 21.50 11 2 0 271.67 21.50 11 2 0 287.47 21.60 -11 2 0 271.07 21.50 -11 2 0 298.07 21.50 -12 -2 0 313.87 22.80 -12 -2 0 265.57 22.80 12 -2 0 320.37 22.70 -12 -2 0 286.37 22.50 12 -2 0 258.17 22.80 -12 -2 0 265.67 22.60 12 2 0 320.87 22.80 -12 2 0 321.77 22.70 -12 2 0 311.67 22.70 -12 2 0 326.87 22.90 13 -2 0 0.00 1.50 -13 -2 0 -1.10 1.60 13 -2 0 0.10 1.50 -13 -2 0 1.60 1.40 -13 -2 0 0.20 1.70 -13 2 0 0.50 1.50 -13 2 0 -2.10 1.60 -13 2 0 0.50 1.40 13 2 0 2.10 1.30 13 2 0 0.90 1.50 13 2 0 -0.20 1.50 -13 2 0 -1.50 1.40 -14 -2 0 -2.70 1.70 -14 -2 0 -1.50 1.40 -14 -2 0 -0.90 1.80 14 -2 0 -1.40 1.60 14 -2 0 -0.40 1.50 -14 -2 0 -0.90 1.50 14 2 0 -0.30 1.70 -14 2 0 -4.20 1.70 14 2 0 -0.40 1.40 14 2 0 -2.10 1.50 -14 2 0 -1.40 1.50 -14 2 0 2.10 1.50 -14 2 0 2.90 1.70 -15 -2 0 10.10 2.40 15 -2 0 8.60 2.20 -15 -2 0 15.00 2.40 -15 -2 0 11.00 2.00 15 -2 0 10.90 2.00 -15 -2 0 10.50 1.70 -15 -2 0 10.00 2.10 -15 2 0 8.00 2.40 15 2 0 11.00 2.00 -15 2 0 15.30 1.90 15 2 0 11.50 2.30 15 2 0 13.40 2.00 -15 2 0 13.20 2.20 -15 2 0 11.70 2.10 -16 -2 0 122.29 9.80 -16 -2 0 127.89 10.10 -16 -2 0 106.29 10.00 16 -2 0 139.59 10.10 16 -2 0 120.79 9.80 -16 -2 0 96.99 9.60 16 2 0 130.29 9.90 -16 2 0 121.69 10.10 -16 2 0 125.29 9.90 -16 2 0 131.29 9.80 -16 2 0 121.89 9.80 16 2 0 121.89 9.70 17 -2 0 59.29 5.70 -17 -2 0 56.49 5.30 -17 -2 0 54.79 5.00 -17 -2 0 62.09 5.80 -17 -2 0 53.99 5.50 -17 -2 0 50.69 5.50 17 -2 0 43.30 5.10 -17 2 0 64.19 5.30 -17 2 0 56.89 5.30 17 2 0 63.09 5.30 -17 2 0 59.59 5.80 17 2 0 49.10 5.10 -17 2 0 60.19 5.20 -18 -2 0 8.50 2.20 -18 -2 0 1.80 2.50 -18 -2 0 6.50 2.20 18 -2 0 7.60 2.40 -18 -2 0 6.70 1.80 -18 -2 0 6.40 2.60 18 2 0 5.60 2.10 -18 2 0 12.70 2.40 18 2 0 5.40 2.10 -18 2 0 5.70 2.20 -18 2 0 8.30 2.80 -18 2 0 6.40 2.10 -19 -2 0 50.39 5.80 19 -2 0 56.39 5.50 -19 -2 0 66.59 5.40 -19 -2 0 60.89 5.50 -19 -2 0 46.10 5.90 -19 2 0 58.09 5.40 -19 2 0 37.40 4.90 -19 2 0 49.90 5.80 -20 -2 0 19.20 3.70 -20 -2 0 21.40 3.30 -20 -2 0 18.60 3.40 -20 2 0 23.30 3.80 -20 2 0 19.40 3.30 -21 -2 0 1.50 2.30 -21 -2 0 1.90 3.10 -21 -2 0 -3.10 2.70 -21 2 0 -0.80 3.00 -21 2 0 0.50 2.70 -22 -2 0 53.79 5.70 -22 -2 0 67.79 6.80 -22 -2 0 47.30 5.90 -22 2 0 61.69 6.00 -22 2 0 48.70 6.10 -23 -2 0 8.60 2.80 -23 -2 0 7.60 3.80 -23 -2 0 8.30 3.00 -23 2 0 2.40 3.70 -23 2 0 9.90 3.50 -24 -2 0 48.20 5.00 -24 -2 0 39.30 5.70 -24 2 0 39.00 5.70 -24 2 0 41.30 5.10 -25 -2 0 3.00 4.20 -25 -2 0 5.80 3.50 -25 2 0 -2.20 3.90 -25 2 0 10.70 3.50 -26 -2 0 48.40 6.70 -26 2 0 80.09 7.30 -26 2 0 39.20 6.40 -27 -2 0 6.00 5.70 -27 2 0 -1.40 5.30 0 -3 0 0.60 0.60 0 3 0 0.90 0.60 1 -3 0 448.76 37.20 -1 -3 0 490.45 37.20 -1 3 0 549.95 37.20 -2 -3 0 24.10 2.30 2 -3 0 22.40 2.40 -2 -3 0 33.30 2.30 2 3 0 28.20 2.30 -2 3 0 27.00 2.40 -3 -3 0 12.70 1.50 -3 -3 0 14.60 1.50 3 -3 0 15.10 1.70 3 3 0 12.50 1.50 3 3 0 14.10 1.50 -3 3 0 9.60 1.40 -4 -3 0 874.11 57.29 -4 -3 0 692.53 57.19 4 -3 0 673.43 57.29 4 3 0 839.12 57.29 4 3 0 744.83 57.19 -5 -3 0 58.79 5.00 -5 -3 0 62.49 5.00 -5 -3 0 62.89 5.00 -5 3 0 65.49 5.00 5 3 0 64.59 5.00 6 -3 0 170.08 12.90 -6 -3 0 148.39 12.80 -6 -3 0 159.98 12.80 6 -3 0 189.88 12.80 -6 -3 0 181.78 12.90 -6 -3 0 166.28 12.80 -6 3 0 176.58 12.80 -6 3 0 142.49 12.80 -6 3 0 168.98 12.80 6 3 0 178.88 12.80 -7 -3 0 371.26 28.10 -7 -3 0 369.16 28.10 7 -3 0 341.37 28.10 -7 -3 0 367.06 28.00 -7 -3 0 369.06 28.10 7 -3 0 395.96 28.10 -7 -3 0 386.46 28.20 -7 -3 0 379.26 28.00 -7 3 0 369.86 28.10 -7 3 0 378.26 28.10 -7 3 0 378.76 28.10 7 3 0 368.76 28.10 -8 -3 0 295.27 21.80 8 -3 0 300.37 21.90 -8 -3 0 302.27 21.80 -8 -3 0 317.57 21.70 -8 -3 0 306.67 21.80 -8 -3 0 268.77 21.90 -8 3 0 313.57 21.90 8 3 0 275.67 21.70 8 3 0 271.37 21.80 -8 3 0 269.37 21.70 8 3 0 251.07 21.80 -9 -3 0 395.96 28.80 -9 -3 0 363.16 28.60 9 -3 0 388.26 28.70 9 -3 0 390.66 28.80 -9 -3 0 374.96 28.80 -9 3 0 420.66 28.80 9 3 0 409.16 28.70 9 3 0 380.86 28.70 -9 3 0 354.96 28.70 -9 3 0 369.16 28.70 -9 3 0 336.77 28.70 9 3 0 388.16 28.70 -10 -3 0 174.88 11.90 10 -3 0 129.09 11.90 -10 -3 0 150.88 12.10 -10 -3 0 173.98 12.10 10 -3 0 163.88 12.10 -10 -3 0 132.59 11.90 -10 -3 0 167.98 11.90 -10 3 0 167.68 12.00 10 3 0 167.48 11.90 -10 3 0 140.69 11.90 10 3 0 127.09 11.90 -10 3 0 180.88 12.10 10 3 0 151.18 12.00 -10 3 0 150.68 11.90 11 -3 0 4.50 1.40 -11 -3 0 4.90 1.10 -11 -3 0 3.10 1.10 -11 -3 0 0.90 1.50 -11 -3 0 1.00 1.40 -11 -3 0 2.30 1.30 11 -3 0 3.30 1.30 -11 3 0 3.40 1.10 11 3 0 2.30 1.30 11 3 0 3.20 1.30 -11 3 0 4.40 1.20 -11 3 0 -0.10 1.40 -11 3 0 2.30 1.30 11 3 0 3.10 1.20 12 -3 0 157.98 12.70 -12 -3 0 139.69 12.40 -12 -3 0 177.48 12.40 -12 -3 0 137.79 12.60 -12 -3 0 164.38 12.60 -12 -3 0 168.98 12.60 12 -3 0 148.49 12.50 12 3 0 177.78 12.60 -12 3 0 159.68 12.40 -12 3 0 173.68 12.60 12 3 0 172.38 12.50 12 3 0 172.78 12.50 -12 3 0 139.99 12.50 -12 3 0 168.98 12.50 -13 -3 0 6.90 1.80 -13 -3 0 9.40 1.40 -13 -3 0 5.00 1.60 -13 -3 0 3.50 1.90 13 -3 0 7.20 1.70 13 -3 0 6.70 1.80 -13 -3 0 4.30 1.50 -13 3 0 3.20 1.90 13 3 0 8.10 1.70 -13 3 0 1.80 1.60 -13 3 0 10.00 1.70 -13 3 0 6.90 1.50 13 3 0 8.20 1.60 13 3 0 9.00 1.80 -14 -3 0 25.10 2.90 -14 -3 0 21.80 3.00 -14 -3 0 27.50 3.20 14 -3 0 24.30 2.90 14 -3 0 31.10 3.30 -14 -3 0 26.10 2.80 -14 3 0 24.50 2.80 14 3 0 23.80 2.80 14 3 0 20.90 2.80 -14 3 0 25.90 2.80 -14 3 0 22.90 3.10 14 3 0 25.70 2.80 -14 3 0 22.30 2.70 -15 -3 0 40.20 4.40 15 -3 0 39.00 4.00 15 -3 0 47.00 4.60 -15 -3 0 32.20 3.90 -15 -3 0 37.20 4.10 -15 -3 0 39.90 4.10 15 3 0 44.40 4.20 15 3 0 40.10 4.30 -15 3 0 44.70 3.90 15 3 0 40.70 3.90 -15 3 0 44.90 4.00 -15 3 0 39.50 4.10 -15 3 0 36.00 4.10 -16 -3 0 14.60 2.30 16 -3 0 8.30 2.70 -16 -3 0 15.10 2.80 16 -3 0 15.90 2.50 -16 -3 0 16.20 2.60 -16 -3 0 15.90 2.80 -16 3 0 16.30 2.30 16 3 0 20.30 2.70 16 3 0 17.50 2.40 16 3 0 16.40 2.50 -16 3 0 17.90 2.30 -16 3 0 16.90 2.60 -16 3 0 19.10 2.90 -17 -3 0 22.20 2.70 -17 -3 0 21.50 2.90 17 -3 0 25.90 3.30 -17 -3 0 19.60 2.90 -17 -3 0 15.90 3.00 17 -3 0 16.70 2.90 -17 -3 0 17.80 2.90 -17 3 0 19.70 2.70 -17 3 0 18.80 3.20 17 3 0 24.00 2.90 -17 3 0 22.60 3.00 17 3 0 21.00 2.90 18 -3 0 57.19 5.50 -18 -3 0 53.09 5.50 -18 -3 0 61.49 5.20 -18 -3 0 49.30 5.60 -18 -3 0 51.49 5.20 -18 -3 0 50.49 5.70 18 3 0 58.49 5.30 -18 3 0 49.60 5.10 -18 3 0 63.29 5.80 18 3 0 56.89 5.60 -18 3 0 47.40 5.30 -19 -3 0 65.19 6.30 19 -3 0 52.99 6.40 -19 -3 0 80.29 6.70 -19 3 0 59.69 6.70 -19 3 0 69.79 6.10 -19 3 0 80.89 6.50 -20 -3 0 6.10 2.80 -20 -3 0 12.50 3.50 -20 -3 0 8.20 2.50 20 -3 0 3.70 4.40 -20 3 0 15.20 3.50 -20 3 0 8.90 2.40 -20 3 0 8.60 2.80 -21 -3 0 -2.50 3.00 -21 -3 0 2.00 2.70 -21 -3 0 4.70 2.70 -21 3 0 2.80 3.30 -21 3 0 -0.60 2.60 -22 -3 0 9.00 2.70 -22 -3 0 9.10 3.10 -22 3 0 11.00 3.10 -22 3 0 5.60 3.60 -23 -3 0 32.10 5.20 -23 -3 0 36.00 4.70 -23 -3 0 40.70 4.50 -23 3 0 41.80 4.80 -23 3 0 33.70 5.10 -24 -3 0 10.80 3.40 -24 -3 0 8.50 3.30 -24 -3 0 8.20 4.10 -24 3 0 -1.10 3.70 -24 3 0 13.00 3.40 -25 -3 0 45.00 6.40 -25 3 0 52.49 6.60 -25 3 0 56.09 6.20 -26 -3 0 31.90 5.70 -26 3 0 30.70 4.80 -26 3 0 27.70 5.20 0 -4 0 44.20 3.70 0 4 0 45.10 3.70 1 -4 0 208.68 15.70 -1 -4 0 193.28 15.60 -1 4 0 204.48 15.70 1 4 0 223.38 15.70 -2 -4 0 58.79 4.30 2 -4 0 54.19 4.40 -2 4 0 50.19 4.40 -3 -4 0 419.96 31.00 -3 4 0 386.86 31.10 3 4 0 432.86 31.00 -4 -4 0 1576.34 116.49 -4 -4 0 1508.35 116.49 4 4 0 1645.74 116.49 4 4 0 1499.15 116.49 5 -4 0 20.10 2.20 -5 -4 0 19.40 2.00 5 -4 0 22.30 2.00 -5 -4 0 20.70 1.90 -5 -4 0 20.40 2.10 -5 -4 0 20.40 2.10 -5 -4 0 26.00 2.20 -5 4 0 15.20 2.10 5 4 0 25.30 2.20 5 4 0 18.10 2.00 5 4 0 17.80 2.10 -5 4 0 21.10 2.00 -5 4 0 20.40 2.00 -6 -4 0 35.90 3.40 -6 -4 0 40.50 3.40 -6 -4 0 40.30 3.30 -6 -4 0 46.00 3.40 6 -4 0 32.90 3.40 6 -4 0 40.70 3.60 -6 -4 0 41.10 3.40 6 4 0 45.70 3.40 6 4 0 36.80 3.40 6 4 0 36.20 3.40 6 4 0 42.50 3.40 -6 4 0 45.90 3.40 -6 4 0 40.80 3.40 -6 4 0 34.70 3.30 -7 -4 0 38.10 3.20 -7 -4 0 39.10 3.20 -7 -4 0 46.00 3.50 -7 -4 0 37.00 3.30 7 -4 0 27.60 3.60 -7 -4 0 35.30 3.30 -7 -4 0 28.90 3.10 -7 4 0 41.40 3.30 7 4 0 36.10 3.30 -7 4 0 38.50 3.30 7 4 0 37.30 3.20 7 4 0 38.90 3.20 -8 -4 0 17.50 1.90 -8 -4 0 26.00 2.20 -8 -4 0 13.20 1.80 -8 -4 0 25.20 2.20 8 -4 0 17.30 1.90 8 -4 0 17.40 2.00 8 4 0 12.40 1.80 8 4 0 14.10 1.80 -8 4 0 19.70 2.10 8 4 0 17.80 1.90 -9 -4 0 6.80 1.60 -9 -4 0 8.00 1.40 9 -4 0 7.00 1.50 -9 -4 0 6.60 1.30 9 -4 0 7.40 1.40 -9 -4 0 7.50 1.30 -9 -4 0 6.40 1.40 9 4 0 7.70 1.20 -9 4 0 6.20 1.40 9 4 0 5.10 1.20 -9 4 0 8.80 1.40 -9 4 0 6.30 1.30 -9 4 0 8.50 1.20 9 4 0 7.90 1.20 -10 -4 0 0.30 1.40 -10 -4 0 0.90 1.20 -10 -4 0 1.50 1.00 -10 -4 0 2.00 1.20 10 -4 0 -1.10 1.30 -10 -4 0 2.40 1.10 10 -4 0 1.90 1.20 -10 4 0 -0.70 1.20 -10 4 0 1.50 1.20 10 4 0 0.50 1.00 -10 4 0 0.60 1.10 10 4 0 0.30 1.10 -10 4 0 1.60 1.00 10 4 0 1.70 1.30 -11 -4 0 469.75 31.60 -11 -4 0 360.46 31.40 11 -4 0 456.15 31.60 11 -4 0 361.46 31.40 -11 -4 0 419.56 31.60 -11 4 0 344.27 31.40 -11 4 0 430.36 31.40 -11 4 0 432.46 31.50 11 4 0 447.96 31.40 11 4 0 388.36 31.40 11 4 0 448.66 31.50 -11 4 0 446.16 31.50 -12 -4 0 19.50 2.60 12 -4 0 18.80 2.50 -12 -4 0 19.90 2.30 -12 -4 0 21.50 2.30 -12 -4 0 22.10 2.20 12 -4 0 22.00 2.40 -12 -4 0 16.30 2.40 -12 4 0 17.30 2.40 12 4 0 22.50 2.40 -12 4 0 18.30 2.30 -12 4 0 21.70 2.40 12 4 0 19.70 2.20 12 4 0 19.50 2.30 -12 4 0 20.30 2.40 13 -4 0 105.99 8.10 -13 -4 0 82.39 7.80 -13 -4 0 90.69 8.20 13 -4 0 96.59 8.30 -13 -4 0 92.89 8.30 -13 -4 0 100.19 8.00 -13 -4 0 110.49 8.10 13 4 0 102.99 8.10 -13 4 0 99.59 8.10 -13 4 0 105.49 8.20 -13 4 0 104.89 8.00 13 4 0 113.19 8.20 13 4 0 98.99 8.10 -13 4 0 101.19 8.10 -14 -4 0 43.50 4.30 14 -4 0 43.60 4.50 -14 -4 0 40.40 4.00 -14 -4 0 47.80 4.00 -14 -4 0 38.80 4.50 14 -4 0 38.20 4.20 -14 4 0 43.80 3.90 14 4 0 45.60 4.10 -14 4 0 35.90 4.30 -14 4 0 38.70 4.10 14 4 0 39.30 4.10 -14 4 0 43.80 4.00 14 4 0 34.50 4.00 15 -4 0 2.90 1.80 -15 -4 0 2.10 1.80 -15 -4 0 5.70 2.30 -15 -4 0 5.70 2.20 15 -4 0 1.10 1.90 -15 -4 0 4.20 1.90 -15 4 0 1.50 1.60 15 4 0 2.30 1.80 -15 4 0 7.80 2.10 -15 4 0 4.40 2.30 15 4 0 5.30 1.80 15 4 0 5.30 1.70 -16 -4 0 -2.70 2.10 16 -4 0 -2.00 1.90 16 -4 0 -0.30 1.80 -16 -4 0 -0.20 2.20 -16 -4 0 -0.10 1.90 -16 -4 0 -1.80 1.70 -16 4 0 1.90 2.20 -16 4 0 -1.40 1.70 16 4 0 0.20 1.80 16 4 0 1.20 1.80 16 4 0 -1.60 1.90 -16 4 0 -0.40 1.60 -17 -4 0 3.50 2.40 17 -4 0 0.40 1.90 -17 -4 0 2.70 2.10 -17 -4 0 1.00 2.00 17 -4 0 0.30 2.40 -17 -4 0 -1.70 2.30 -17 4 0 -0.30 2.40 -17 4 0 2.50 2.20 17 4 0 1.70 1.80 17 4 0 3.30 2.10 -17 4 0 1.40 2.00 17 4 0 1.90 1.90 -18 -4 0 -2.50 2.40 -18 -4 0 0.60 2.10 -18 -4 0 -1.20 1.80 -18 -4 0 -1.50 1.70 18 -4 0 -0.40 2.00 -18 -4 0 0.20 2.70 -18 4 0 2.20 1.90 -18 4 0 -1.30 2.50 -18 4 0 1.00 2.20 18 4 0 -3.60 2.40 19 -4 0 9.10 2.60 -19 -4 0 10.00 3.00 -19 -4 0 5.00 2.20 -19 -4 0 7.60 2.80 -19 4 0 0.60 2.80 -19 4 0 6.40 2.60 -19 4 0 7.90 2.20 -20 -4 0 75.69 7.10 -20 -4 0 74.29 7.30 20 -4 0 66.19 6.90 -20 -4 0 66.09 6.50 -20 4 0 57.09 6.30 -20 4 0 82.49 6.80 -20 4 0 82.09 7.20 -21 -4 0 3.80 3.20 -21 -4 0 2.90 2.40 -21 -4 0 2.20 3.30 -21 4 0 3.00 2.80 -21 4 0 4.40 3.20 -22 -4 0 8.30 3.20 -22 -4 0 6.30 2.80 -22 4 0 3.50 3.40 -23 -4 0 7.90 3.90 -23 -4 0 4.10 3.00 -23 -4 0 4.50 3.20 -23 4 0 11.20 3.30 -23 4 0 7.30 3.70 -24 -4 0 5.20 3.50 -24 -4 0 4.70 4.00 -24 4 0 0.20 3.60 -25 -4 0 8.80 3.90 -25 -4 0 11.60 4.50 -25 4 0 8.60 4.00 -25 4 0 13.60 3.80 -26 -4 0 9.00 4.80 -26 4 0 16.00 3.90 -26 4 0 -0.10 4.00 0 -5 0 0.80 1.00 0 5 0 -1.70 0.90 -1 -5 0 1343.87 97.39 1 -5 0 1117.49 97.39 1 5 0 1481.55 97.39 -1 5 0 1265.87 97.39 -2 5 0 415.46 28.40 2 5 0 340.97 28.40 3 -5 0 838.32 56.89 -3 -5 0 732.53 56.79 -3 -5 0 757.02 56.79 -3 -5 0 722.93 56.79 3 5 0 741.13 56.79 -3 5 0 757.32 56.79 -4 -5 0 258.97 19.10 4 -5 0 258.07 19.10 -4 -5 0 263.07 19.10 -4 -5 0 255.77 19.10 -4 -5 0 245.08 19.10 -4 5 0 251.87 19.10 -4 5 0 244.28 19.10 -4 5 0 232.08 19.10 4 5 0 265.17 19.10 -5 -5 0 201.38 14.80 -5 -5 0 199.58 14.70 -5 -5 0 205.98 14.70 -5 -5 0 200.98 14.70 5 -5 0 216.48 14.90 -5 -5 0 192.78 14.80 5 5 0 217.18 14.80 5 5 0 162.48 14.70 5 5 0 176.38 14.70 -5 5 0 181.78 14.70 -5 5 0 172.68 14.70 5 5 0 206.58 14.80 6 -5 0 358.16 27.20 6 -5 0 374.56 27.30 -6 -5 0 334.77 27.20 -6 -5 0 357.76 27.30 -6 -5 0 364.46 27.20 -6 -5 0 350.56 27.20 -6 -5 0 352.56 27.20 6 5 0 352.36 27.20 -6 5 0 350.76 27.20 -6 5 0 411.36 27.20 6 5 0 365.86 27.30 6 5 0 376.26 27.20 6 5 0 372.66 27.20 6 5 0 339.77 27.20 -6 5 0 363.26 27.20 -7 -5 0 128.79 10.60 -7 -5 0 147.89 10.50 -7 -5 0 124.39 10.50 -7 -5 0 135.69 10.60 7 -5 0 147.69 10.70 7 -5 0 142.99 10.60 -7 -5 0 134.09 10.70 7 5 0 145.99 10.60 7 5 0 149.69 10.50 -7 5 0 135.69 10.60 -7 5 0 128.59 10.50 -7 5 0 124.49 10.50 7 5 0 140.59 10.50 -8 -5 0 53.29 4.50 -8 -5 0 54.19 4.60 8 -5 0 53.99 4.60 -8 -5 0 62.09 4.80 -8 -5 0 57.09 4.50 -8 -5 0 60.29 4.60 -8 5 0 46.40 4.60 8 5 0 51.29 4.60 8 5 0 58.69 4.50 -8 5 0 57.69 4.60 -8 5 0 50.59 4.60 8 5 0 53.79 4.60 9 -5 0 1.60 1.30 -9 -5 0 1.20 1.10 -9 -5 0 3.40 1.00 -9 -5 0 3.50 1.10 9 -5 0 4.40 1.20 -9 -5 0 2.00 1.50 -9 -5 0 4.00 1.20 9 5 0 4.60 1.20 9 5 0 1.90 1.10 -9 5 0 3.40 1.40 9 5 0 2.00 1.10 -9 5 0 3.90 1.20 -9 5 0 3.80 1.30 -9 5 0 3.20 0.90 -10 -5 0 67.49 5.70 -10 -5 0 71.09 5.60 -10 -5 0 63.39 5.80 -10 -5 0 66.19 5.70 -10 -5 0 70.19 5.50 10 -5 0 70.59 5.80 10 -5 0 65.99 5.70 10 5 0 70.59 5.50 10 5 0 60.29 5.50 10 5 0 69.29 5.60 -10 5 0 77.39 5.60 -10 5 0 65.79 5.60 -10 5 0 70.99 5.70 -10 5 0 68.89 5.50 11 -5 0 20.00 2.30 -11 -5 0 22.90 2.20 11 -5 0 20.80 2.60 -11 -5 0 17.40 2.20 -11 -5 0 20.40 2.20 -11 -5 0 19.70 2.30 -11 -5 0 15.30 2.50 -11 5 0 20.00 2.20 11 5 0 16.60 2.20 11 5 0 16.20 2.20 -11 5 0 19.00 2.30 -11 5 0 23.50 2.40 -11 5 0 21.60 2.30 11 5 0 20.30 2.20 12 -5 0 29.90 3.30 -12 -5 0 36.90 3.50 -12 -5 0 30.00 3.10 -12 -5 0 35.90 3.30 12 -5 0 31.60 3.70 -12 -5 0 32.10 3.70 -12 -5 0 28.10 3.40 12 5 0 30.10 3.20 -12 5 0 27.40 3.20 -12 5 0 31.50 3.50 -12 5 0 38.50 3.20 -12 5 0 35.40 3.40 12 5 0 34.70 3.20 12 5 0 41.60 3.40 -13 -5 0 72.19 6.10 -13 -5 0 73.59 6.30 13 -5 0 64.39 6.10 -13 -5 0 70.19 6.30 13 -5 0 78.29 6.50 -13 -5 0 64.39 6.00 -13 -5 0 75.99 5.90 13 5 0 79.49 6.20 13 5 0 69.19 6.10 -13 5 0 80.19 6.10 -13 5 0 74.19 6.20 -13 5 0 73.99 6.30 -13 5 0 59.09 6.00 13 5 0 86.59 6.30 14 -5 0 59.69 5.40 -14 -5 0 56.99 5.30 -14 -5 0 51.99 5.50 -14 -5 0 54.79 5.40 -14 -5 0 65.99 5.20 14 -5 0 55.39 5.10 -14 -5 0 53.79 4.90 14 5 0 56.09 5.20 -14 5 0 55.29 5.20 14 5 0 60.39 5.20 -14 5 0 59.09 5.40 -14 5 0 54.29 5.00 14 5 0 64.79 5.20 -15 -5 0 -2.50 2.20 -15 -5 0 1.70 1.60 15 -5 0 3.30 2.00 -15 -5 0 0.80 2.00 15 -5 0 -0.70 1.80 -15 -5 0 1.20 1.70 15 5 0 2.50 2.00 15 5 0 -0.10 1.70 -15 5 0 0.70 1.80 -15 5 0 1.50 1.60 -15 5 0 0.00 2.00 15 5 0 2.90 1.80 16 -5 0 79.29 7.20 -16 -5 0 94.19 7.80 -16 -5 0 72.99 7.50 -16 -5 0 89.59 7.30 -16 -5 0 84.89 7.10 16 -5 0 91.79 7.60 -16 5 0 82.39 7.20 -16 5 0 82.39 7.60 16 5 0 97.09 7.40 16 5 0 87.39 7.20 -16 5 0 91.79 7.50 16 5 0 72.49 7.40 17 -5 0 8.90 2.20 -17 -5 0 6.80 3.10 -17 -5 0 14.70 2.90 -17 -5 0 6.20 2.20 -17 -5 0 9.20 2.30 -17 5 0 8.50 2.10 17 5 0 8.80 2.10 17 5 0 6.80 2.30 -17 5 0 11.40 2.70 -17 5 0 9.00 2.70 -18 -5 0 41.60 4.50 -18 -5 0 29.40 4.40 -18 -5 0 40.80 4.40 18 -5 0 44.00 4.30 -18 5 0 30.70 4.10 -18 5 0 45.40 4.40 -18 5 0 44.00 4.60 18 5 0 38.60 4.20 19 -5 0 26.90 3.60 -19 -5 0 22.50 3.80 -19 -5 0 31.20 4.00 -19 -5 0 21.10 3.40 -19 5 0 28.10 3.70 -19 5 0 26.50 3.90 -19 5 0 28.00 3.30 -20 -5 0 11.80 3.30 20 -5 0 4.00 2.80 -20 -5 0 9.00 2.70 -20 -5 0 8.40 3.10 -20 5 0 10.30 3.20 -20 5 0 8.60 2.40 -20 5 0 7.10 2.80 -21 -5 0 0.40 2.60 -21 -5 0 -2.70 3.10 -21 -5 0 1.10 3.00 -21 5 0 5.50 2.80 -21 5 0 -0.30 3.00 -22 -5 0 7.30 3.30 -22 -5 0 2.30 3.20 -22 5 0 3.40 3.30 -22 5 0 18.40 3.70 -23 -5 0 13.60 4.10 -23 -5 0 12.80 3.60 -23 5 0 21.20 4.00 -23 5 0 5.80 4.00 -24 -5 0 5.20 3.80 -24 -5 0 4.70 4.20 -24 5 0 1.20 4.00 -24 5 0 17.00 4.00 -25 -5 0 11.60 3.70 -25 -5 0 13.00 4.50 -25 5 0 12.10 4.10 -25 5 0 9.20 4.30 -26 -5 0 9.00 4.70 -26 -5 0 6.50 3.60 -26 5 0 6.70 3.60 -26 5 0 2.10 3.80 0 -6 0 51.79 3.80 0 6 0 39.30 3.70 0 6 0 40.30 3.60 -1 -6 0 116.29 8.10 -1 6 0 107.69 8.10 1 6 0 88.29 8.10 -2 -6 0 145.09 10.80 2 -6 0 133.09 10.80 -2 -6 0 139.59 10.70 -2 6 0 138.89 10.70 2 6 0 147.69 10.80 2 6 0 141.59 10.80 3 -6 0 85.69 6.70 -3 -6 0 81.39 6.70 -3 -6 0 89.59 6.70 -3 -6 0 79.89 6.60 -3 6 0 71.59 6.70 3 6 0 80.99 6.70 3 6 0 101.99 6.70 -3 6 0 86.69 6.70 -3 6 0 92.49 6.70 -4 -6 0 269.37 21.30 -4 -6 0 275.97 21.20 -4 -6 0 270.17 21.20 4 6 0 260.17 21.20 -4 6 0 312.57 21.20 4 6 0 285.47 21.20 -4 6 0 296.17 21.20 -5 -6 0 229.78 20.80 -5 -6 0 300.57 20.80 -5 -6 0 256.17 20.90 5 -6 0 300.27 21.00 -5 -6 0 238.68 20.80 5 6 0 273.77 20.90 5 6 0 289.77 20.80 5 6 0 312.37 20.90 -5 6 0 287.57 20.80 -5 6 0 272.87 20.80 -6 -6 0 268.77 19.20 6 -6 0 214.58 19.30 -6 -6 0 236.88 19.20 -6 -6 0 242.18 19.20 -6 -6 0 232.28 19.20 6 6 0 257.17 19.10 6 6 0 264.47 19.20 6 6 0 267.17 19.20 6 6 0 242.58 19.20 6 6 0 261.67 19.20 -6 6 0 284.37 19.20 -6 6 0 266.87 19.20 -7 -6 0 36.00 3.40 -7 -6 0 30.60 3.30 7 -6 0 48.30 3.80 7 6 0 40.30 3.40 -7 6 0 32.90 3.50 -7 6 0 43.70 3.40 -7 6 0 39.10 3.40 7 6 0 37.50 3.30 7 6 0 43.60 3.40 7 6 0 34.90 3.30 -8 -6 0 1.30 1.10 -8 -6 0 -0.10 1.00 8 -6 0 0.20 1.30 -8 -6 0 0.50 0.90 -8 -6 0 2.40 1.10 8 -6 0 0.50 1.10 -8 -6 0 -0.30 1.30 -8 6 0 -1.40 1.10 -8 6 0 0.40 1.00 8 6 0 -0.30 1.00 -8 6 0 1.90 1.00 8 6 0 0.50 1.10 8 6 0 0.10 1.00 9 -6 0 181.18 13.40 -9 -6 0 179.38 13.30 -9 -6 0 186.28 13.40 -9 -6 0 150.68 13.20 -9 -6 0 180.18 13.50 -9 -6 0 185.48 13.40 9 -6 0 200.28 13.50 -9 6 0 146.19 13.30 9 6 0 163.88 13.30 9 6 0 166.38 13.30 -9 6 0 173.38 13.30 -9 6 0 178.48 13.20 9 6 0 172.28 13.30 10 -6 0 49.90 5.20 -10 -6 0 56.99 4.90 -10 -6 0 59.89 5.10 -10 -6 0 60.99 4.90 10 -6 0 52.79 5.00 -10 -6 0 53.29 5.20 -10 -6 0 58.99 5.00 -10 6 0 70.09 5.00 -10 6 0 61.69 5.10 10 6 0 60.29 4.90 -10 6 0 69.59 4.90 10 6 0 62.99 5.10 10 6 0 52.99 4.90 -10 6 0 63.29 5.10 11 -6 0 26.80 2.70 -11 -6 0 21.90 2.40 -11 -6 0 18.70 2.40 -11 -6 0 22.20 2.30 -11 -6 0 23.30 2.60 -11 -6 0 22.10 2.30 11 -6 0 23.00 2.60 11 6 0 20.60 2.40 -11 6 0 25.60 2.40 -11 6 0 18.70 2.50 -11 6 0 19.90 2.40 -11 6 0 15.40 2.30 11 6 0 22.90 2.40 11 6 0 19.30 2.20 -12 -6 0 23.40 2.80 -12 -6 0 23.50 2.80 12 -6 0 26.80 3.00 -12 -6 0 22.30 2.50 12 -6 0 29.30 2.90 -12 -6 0 32.50 2.90 -12 -6 0 24.60 2.80 -12 6 0 26.20 2.80 12 6 0 21.60 2.60 12 6 0 20.30 2.50 12 6 0 28.80 3.00 -12 6 0 35.10 2.90 -12 6 0 22.20 2.80 -13 -6 0 26.80 2.50 -13 -6 0 16.80 2.90 13 -6 0 20.00 2.90 -13 -6 0 21.40 2.60 -13 -6 0 20.50 2.70 -13 -6 0 21.20 2.60 13 -6 0 17.00 2.60 -13 6 0 22.40 2.70 13 6 0 20.50 2.60 -13 6 0 26.10 2.80 -13 6 0 21.00 2.50 13 6 0 25.60 2.60 13 6 0 24.60 2.60 -14 -6 0 7.80 2.10 -14 -6 0 3.80 2.30 14 -6 0 6.70 2.10 -14 -6 0 10.50 1.80 14 -6 0 6.30 1.90 -14 -6 0 9.50 2.00 -14 -6 0 5.90 1.70 14 6 0 6.50 1.80 -14 6 0 7.40 2.20 -14 6 0 9.10 2.00 14 6 0 11.10 1.80 14 6 0 9.90 2.10 -14 6 0 8.20 2.10 -15 -6 0 47.90 4.80 15 -6 0 51.29 5.10 -15 -6 0 43.60 4.60 -15 -6 0 46.60 5.10 -15 -6 0 46.90 4.70 -15 -6 0 57.79 4.60 15 -6 0 39.30 4.50 -15 6 0 48.70 4.80 -15 6 0 51.59 4.70 -15 6 0 50.99 4.70 15 6 0 31.40 4.30 15 6 0 54.89 4.60 15 6 0 48.30 4.60 16 -6 0 18.30 3.10 16 -6 0 22.90 3.00 -16 -6 0 20.50 3.50 -16 -6 0 21.50 2.80 -16 -6 0 28.20 3.40 -16 -6 0 25.00 3.00 16 6 0 25.90 3.20 16 6 0 21.30 3.20 16 6 0 28.40 3.00 -16 6 0 23.70 3.00 -16 6 0 24.90 3.30 -16 6 0 25.70 3.20 -17 -6 0 4.70 2.60 17 -6 0 1.50 2.30 -17 -6 0 2.20 2.60 -17 -6 0 2.80 3.10 -17 -6 0 5.80 2.10 17 6 0 -0.80 2.00 -17 6 0 4.30 2.50 -17 6 0 3.70 1.90 -17 6 0 4.40 2.20 17 6 0 0.70 2.00 18 -6 0 13.80 2.60 -18 -6 0 13.40 3.00 -18 -6 0 5.40 2.90 -18 -6 0 10.20 2.40 18 6 0 9.10 2.50 -18 6 0 13.10 2.70 -18 6 0 12.20 2.50 -18 6 0 14.00 2.90 -19 -6 0 31.40 4.70 19 -6 0 36.70 4.40 -19 -6 0 39.80 4.80 -19 -6 0 37.20 4.10 -19 6 0 38.80 4.20 19 6 0 42.00 4.50 -19 6 0 50.19 4.90 -19 6 0 54.89 5.20 -20 -6 0 1.00 2.20 -20 -6 0 0.80 3.30 20 -6 0 0.50 2.40 -20 -6 0 1.60 3.00 -20 6 0 5.10 2.70 -20 6 0 3.60 2.90 -20 6 0 0.30 2.20 -21 -6 0 20.80 4.10 -21 -6 0 21.60 4.90 -21 -6 0 17.10 3.90 -21 6 0 26.20 4.00 -21 6 0 29.30 4.10 -22 -6 0 2.70 3.40 -22 -6 0 23.00 4.30 -22 6 0 11.30 3.20 -22 6 0 6.80 3.30 -23 -6 0 8.40 4.40 -23 -6 0 -5.30 3.50 -23 6 0 4.50 3.20 -23 6 0 0.70 3.30 -24 -6 0 7.80 4.40 -24 -6 0 -0.40 3.30 -24 6 0 -2.10 3.40 -24 6 0 10.60 3.50 -25 -6 0 4.40 4.30 -25 -6 0 4.60 3.60 -25 6 0 13.40 3.70 -25 6 0 3.40 3.70 -26 -6 0 4.60 3.60 -26 -6 0 8.70 4.70 -26 6 0 3.10 3.70 -26 6 0 10.00 3.80 0 -7 0 1.00 0.90 0 -7 0 0.50 0.80 0 7 0 -1.00 1.00 0 7 0 0.10 0.70 1 -7 0 88.09 6.00 -1 -7 0 74.49 6.00 -1 -7 0 64.19 6.10 -1 7 0 80.69 6.00 1 7 0 68.79 6.00 1 7 0 83.99 6.10 -2 -7 0 62.29 5.00 -2 -7 0 66.69 4.90 2 -7 0 68.19 5.00 -2 -7 0 58.89 4.90 -2 7 0 62.49 4.90 2 7 0 63.49 4.90 -2 7 0 50.29 4.90 -3 -7 0 329.17 22.70 -3 -7 0 321.17 22.70 3 7 0 257.97 22.70 3 7 0 297.97 22.70 -4 -7 0 51.59 4.00 -4 -7 0 47.00 3.90 -4 -7 0 52.89 4.00 -4 -7 0 46.80 3.90 4 -7 0 34.80 4.10 -4 -7 0 42.80 4.00 4 7 0 49.80 4.00 -4 7 0 51.29 4.00 -4 7 0 41.00 4.00 4 7 0 47.60 3.90 4 7 0 53.99 3.90 -5 -7 0 369.26 30.00 -5 -7 0 407.06 29.90 -5 -7 0 426.86 30.00 -5 -7 0 373.96 29.90 -5 -7 0 363.96 29.90 5 -7 0 443.46 30.10 -5 7 0 419.36 29.90 5 7 0 345.17 29.90 5 7 0 395.36 29.90 5 7 0 418.06 30.00 -5 7 0 374.26 29.90 5 7 0 380.16 29.90 -5 7 0 454.35 30.00 -6 -7 0 47.50 4.10 -6 -7 0 62.99 4.30 -6 -7 0 52.19 4.10 6 7 0 51.99 4.10 -6 7 0 35.80 4.20 6 7 0 47.70 4.10 -6 7 0 51.39 4.20 6 7 0 45.10 4.10 -7 -7 0 1.60 1.00 -7 -7 0 2.60 1.10 7 -7 0 1.50 1.40 -7 -7 0 2.50 1.10 -7 7 0 0.30 1.10 7 7 0 -0.20 1.00 7 7 0 0.40 1.00 -7 7 0 4.40 1.10 -7 7 0 -0.60 1.10 7 7 0 1.50 1.00 -8 -7 0 177.58 13.80 -8 -7 0 193.88 13.80 8 -7 0 202.78 14.00 -8 -7 0 171.98 13.90 -8 -7 0 183.58 13.80 8 7 0 168.08 13.70 8 7 0 164.78 13.80 -8 7 0 161.68 13.70 -8 7 0 195.88 13.80 8 7 0 182.88 13.70 8 7 0 179.58 13.70 -9 -7 0 235.58 19.00 9 -7 0 254.17 19.00 -9 -7 0 228.98 18.80 -9 -7 0 283.27 18.80 -9 -7 0 213.68 18.90 -9 -7 0 269.57 18.90 9 7 0 251.27 18.90 -9 7 0 260.67 18.90 9 7 0 256.37 18.90 -9 7 0 232.18 18.90 -9 7 0 249.38 18.90 9 7 0 243.28 18.80 -10 -7 0 -2.70 1.20 -10 -7 0 -0.80 1.00 -10 -7 0 -0.80 1.10 10 -7 0 -0.20 1.50 -10 -7 0 -0.90 1.20 -10 -7 0 -0.80 1.50 10 7 0 -0.30 1.20 -10 7 0 -1.20 1.30 -10 7 0 -0.20 1.20 10 7 0 -1.30 1.20 -10 7 0 2.00 1.20 10 7 0 -0.70 1.10 -11 -7 0 8.00 2.10 -11 -7 0 9.90 1.70 11 -7 0 11.90 2.00 11 -7 0 12.10 1.90 -11 -7 0 9.60 1.50 -11 -7 0 9.50 1.80 -11 -7 0 9.10 1.60 11 7 0 9.10 1.60 11 7 0 8.00 1.70 -11 7 0 7.10 1.70 -11 7 0 10.20 1.80 11 7 0 12.30 1.80 -11 7 0 12.20 1.70 -12 -7 0 6.70 1.60 12 -7 0 9.20 2.00 -12 -7 0 6.50 1.50 -12 -7 0 6.50 1.60 -12 -7 0 4.00 1.60 12 -7 0 8.30 1.80 -12 -7 0 3.90 1.70 12 7 0 9.80 1.60 12 7 0 8.20 1.60 -12 7 0 6.80 1.60 -12 7 0 5.20 1.80 12 7 0 3.90 1.50 -12 7 0 8.30 1.80 13 -7 0 14.20 2.70 -13 -7 0 12.00 2.10 -13 -7 0 17.10 2.00 -13 -7 0 16.30 2.10 -13 -7 0 13.70 2.60 -13 -7 0 17.20 2.30 13 -7 0 16.40 2.30 13 7 0 11.40 2.20 13 7 0 13.40 2.10 13 7 0 11.20 2.00 -13 7 0 14.80 2.30 -13 7 0 11.10 2.00 -13 7 0 14.30 2.30 14 -7 0 28.80 3.70 -14 -7 0 39.80 3.90 -14 -7 0 36.60 3.70 -14 -7 0 23.90 3.20 -14 -7 0 31.40 3.90 -14 -7 0 34.40 3.60 14 -7 0 34.00 3.60 14 7 0 31.40 3.60 -14 7 0 38.40 3.50 14 7 0 31.40 3.40 14 7 0 32.20 3.40 -14 7 0 33.00 3.80 -14 7 0 37.10 3.80 -15 -7 0 62.69 5.50 -15 -7 0 58.99 5.60 15 -7 0 56.89 6.10 -15 -7 0 59.29 5.70 -15 -7 0 54.69 6.00 15 -7 0 57.79 5.50 -15 -7 0 59.59 5.30 -15 7 0 63.89 5.70 -15 7 0 70.39 5.50 15 7 0 62.69 5.50 15 7 0 58.29 5.50 15 7 0 62.49 5.50 -15 7 0 62.89 5.60 -16 -7 0 23.50 3.30 16 -7 0 22.70 3.00 -16 -7 0 25.20 3.10 -16 -7 0 20.20 2.70 -16 -7 0 18.60 3.40 -16 7 0 26.40 2.90 -16 7 0 21.30 3.10 16 7 0 26.20 3.10 16 7 0 18.90 2.90 -16 7 0 25.60 3.30 -17 -7 0 0.20 2.00 17 -7 0 4.60 2.40 -17 -7 0 2.10 2.60 -17 -7 0 0.10 2.40 -17 7 0 3.40 1.90 -17 7 0 0.40 2.20 17 7 0 0.90 2.10 17 7 0 -0.60 2.00 -17 7 0 6.50 2.40 -18 -7 0 2.70 1.90 -18 -7 0 -1.20 2.70 18 -7 0 1.50 2.20 -18 -7 0 2.10 2.60 -18 7 0 3.70 2.20 -18 7 0 1.20 2.40 -18 7 0 1.50 2.30 18 7 0 3.40 2.40 -19 -7 0 10.10 3.10 -19 -7 0 2.60 3.00 -19 -7 0 5.40 2.20 19 -7 0 8.50 2.70 -19 7 0 6.70 2.30 -19 7 0 5.60 2.70 -19 7 0 7.00 2.80 19 7 0 7.30 3.40 20 -7 0 -0.60 2.40 -20 -7 0 -2.40 3.30 -20 -7 0 2.40 3.10 -20 7 0 0.60 2.60 -20 7 0 -1.90 2.30 -20 7 0 -1.80 2.70 -21 -7 0 28.90 4.50 -21 -7 0 19.20 4.10 -21 7 0 21.70 3.60 -21 7 0 25.50 4.00 -21 7 0 29.70 4.00 -22 -7 0 13.10 4.00 -22 -7 0 10.00 3.60 -22 7 0 9.20 3.30 -22 7 0 8.90 3.30 -23 -7 0 5.50 3.50 -23 -7 0 9.50 4.00 -23 7 0 2.10 3.20 -23 7 0 2.80 3.30 -24 -7 0 -1.10 3.40 -24 -7 0 9.80 4.20 -24 7 0 6.30 3.60 -24 7 0 2.20 3.40 -25 -7 0 14.10 4.80 -25 -7 0 9.20 4.00 -25 7 0 12.30 4.00 -25 7 0 17.40 4.00 -26 -7 0 4.50 3.80 -26 -7 0 9.60 5.20 -26 7 0 7.00 3.80 -26 7 0 3.90 3.70 0 -8 0 503.35 39.90 0 -8 0 485.35 40.00 0 8 0 539.65 39.90 0 8 0 600.54 40.00 1 -8 0 54.29 3.90 -1 -8 0 53.19 3.90 1 -8 0 38.20 4.00 -1 -8 0 59.69 4.10 -1 8 0 37.20 4.00 -1 8 0 46.20 4.00 1 8 0 45.80 4.00 1 8 0 47.80 3.90 -2 -8 0 26.20 2.90 2 -8 0 31.00 3.10 -2 -8 0 25.50 2.80 -2 -8 0 31.20 2.80 2 -8 0 31.50 2.70 2 8 0 29.20 3.20 -2 8 0 35.50 2.80 2 8 0 31.00 2.60 -2 8 0 35.70 2.80 2 8 0 33.30 2.80 -3 -8 0 346.37 24.90 -3 -8 0 332.67 25.00 -3 -8 0 317.97 24.90 3 -8 0 325.27 25.00 3 -8 0 328.67 24.90 -3 8 0 351.06 24.90 3 8 0 329.07 24.90 -3 8 0 346.87 25.00 3 8 0 295.57 24.90 -4 -8 0 1.20 1.00 -4 -8 0 3.30 0.80 4 -8 0 1.90 1.50 -4 -8 0 1.80 1.10 -4 -8 0 2.70 1.00 4 8 0 2.50 0.90 -4 8 0 -0.90 1.10 4 8 0 0.00 1.00 -4 8 0 2.10 1.10 4 8 0 2.30 0.80 -5 -8 0 104.19 7.60 -5 -8 0 95.09 7.50 -5 -8 0 108.69 7.70 -5 -8 0 98.79 7.60 -5 8 0 88.99 7.50 5 8 0 98.59 7.60 5 8 0 87.79 7.40 -5 8 0 94.99 7.60 -6 -8 0 163.68 14.30 -6 -8 0 197.68 14.40 6 -8 0 191.18 14.40 -6 -8 0 186.28 14.20 -6 8 0 190.08 14.20 -6 8 0 172.38 14.30 -6 8 0 208.48 14.30 6 8 0 199.28 14.30 6 8 0 174.18 14.30 -7 -8 0 330.87 24.10 7 8 0 351.96 24.10 7 8 0 341.37 24.20 7 8 0 252.97 24.00 -8 -8 0 131.89 9.80 8 -8 0 146.69 10.00 -8 -8 0 122.89 9.80 -8 -8 0 130.79 9.90 8 8 0 114.79 9.80 -8 8 0 106.69 9.80 8 8 0 128.09 9.80 -8 8 0 141.99 9.80 8 8 0 112.19 9.70 -9 -8 0 37.40 3.60 -9 -8 0 40.20 3.30 -9 -8 0 34.80 3.80 -9 -8 0 30.80 3.60 -9 -8 0 39.70 3.50 9 -8 0 38.50 3.90 -9 8 0 31.70 3.50 -9 8 0 43.50 3.50 9 8 0 43.30 3.40 9 8 0 36.50 3.60 -9 8 0 40.80 3.60 -10 -8 0 25.00 3.10 -10 -8 0 29.10 3.00 -10 -8 0 29.40 3.10 -10 -8 0 35.00 3.00 10 -8 0 33.40 3.40 -10 -8 0 31.00 2.90 10 8 0 28.40 3.00 -10 8 0 27.90 3.00 -10 8 0 21.20 2.90 10 8 0 28.70 3.00 10 8 0 26.30 2.90 -10 8 0 33.60 3.00 -11 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0 9.10 2.40 15 8 0 0.30 1.90 -15 8 0 1.30 1.70 -15 8 0 1.10 2.00 -16 -8 0 15.50 3.20 -16 -8 0 9.20 2.00 -16 -8 0 15.00 2.80 -16 -8 0 13.10 2.60 16 8 0 10.70 2.40 16 8 0 10.20 2.30 -16 8 0 12.30 2.60 -16 8 0 8.90 2.20 -16 8 0 11.20 2.50 -17 -8 0 156.98 12.70 -17 -8 0 150.58 12.80 -17 8 0 157.48 12.60 -17 8 0 161.98 12.60 17 8 0 151.58 12.50 -18 -8 0 22.00 3.80 -18 -8 0 26.20 3.60 -18 8 0 29.90 3.50 -18 8 0 23.20 3.30 -18 8 0 12.60 2.70 -19 -8 0 16.10 3.70 -19 -8 0 18.70 3.50 -19 8 0 17.20 3.20 -19 8 0 19.80 3.30 -19 8 0 11.80 2.60 -20 -8 0 3.70 3.10 -20 -8 0 -0.60 3.10 -20 8 0 5.70 2.80 -20 8 0 3.70 2.30 -20 8 0 5.70 2.70 -21 -8 0 6.70 3.50 -21 -8 0 20.00 3.90 -21 8 0 9.80 3.20 -21 8 0 9.20 2.60 -21 8 0 12.70 3.30 -22 -8 0 4.10 3.60 -22 -8 0 3.80 4.10 -22 8 0 6.90 3.30 -22 8 0 1.90 2.90 -23 -8 0 12.60 4.00 -23 -8 0 14.00 4.40 -23 8 0 17.20 3.80 -23 8 0 14.20 3.60 -24 -8 0 10.50 4.50 -24 -8 0 16.60 4.60 -24 8 0 20.70 4.30 -24 8 0 16.10 3.90 -25 -8 0 0.50 3.80 -25 -8 0 19.40 4.80 -25 8 0 3.70 3.50 -25 8 0 10.50 4.30 -26 -8 0 16.10 4.50 -26 -8 0 20.70 5.20 -26 8 0 19.00 4.20 -26 8 0 17.20 4.60 0 -9 0 0.30 0.90 0 -9 0 -2.50 1.10 0 9 0 0.70 0.90 0 9 0 0.60 1.10 -1 -9 0 187.78 14.90 -1 -9 0 198.68 14.80 -1 -9 0 204.88 14.80 1 -9 0 216.18 14.80 1 -9 0 186.78 15.00 1 9 0 207.18 14.80 -1 9 0 171.78 14.80 -1 9 0 186.48 14.90 -2 -9 0 1.30 1.10 -2 -9 0 0.10 1.00 2 -9 0 1.60 0.90 -2 9 0 -1.10 1.20 -2 9 0 -2.60 0.90 2 9 0 -1.70 1.10 2 9 0 0.20 0.90 -3 -9 0 91.69 6.90 -3 -9 0 80.39 6.80 3 -9 0 85.09 6.70 -3 -9 0 89.69 6.70 3 -9 0 85.89 7.10 -3 -9 0 92.19 6.90 3 9 0 90.29 6.70 3 9 0 68.19 6.80 -3 9 0 94.59 6.90 3 9 0 86.99 6.70 -3 9 0 85.99 6.80 4 -9 0 27.80 2.70 -4 -9 0 18.90 1.80 -4 -9 0 15.20 1.90 4 -9 0 18.00 1.80 -4 -9 0 22.80 2.30 -4 -9 0 21.10 2.30 4 9 0 23.40 2.00 -4 9 0 16.40 1.90 -4 9 0 14.90 2.00 4 9 0 12.80 1.80 4 9 0 16.00 1.90 -4 9 0 17.40 1.90 -5 -9 0 370.66 27.30 -5 -9 0 386.06 27.20 5 -9 0 378.66 27.10 -5 -9 0 342.27 27.20 5 -9 0 422.16 27.40 -5 9 0 376.66 27.20 5 9 0 308.57 27.20 5 9 0 312.57 27.20 5 9 0 324.17 27.10 -5 9 0 383.86 27.20 -5 9 0 363.16 27.10 -6 -9 0 10.00 1.40 -6 -9 0 9.70 1.50 -6 -9 0 8.40 1.60 -6 -9 0 9.80 1.50 6 -9 0 4.70 1.80 -6 9 0 7.60 1.50 -6 9 0 7.80 1.20 -6 9 0 9.40 1.50 6 9 0 9.30 1.30 6 9 0 7.90 1.30 6 9 0 6.80 1.40 -7 -9 0 291.37 22.80 -7 -9 0 302.17 22.90 -7 -9 0 261.67 22.80 7 -9 0 291.67 23.00 -7 -9 0 322.57 22.80 -7 9 0 303.27 22.80 7 9 0 293.47 22.80 7 9 0 330.57 22.80 7 9 0 310.07 22.80 -7 9 0 306.07 22.90 8 -9 0 30.40 3.50 -8 -9 0 28.90 3.00 -8 -9 0 30.60 2.90 -8 -9 0 27.30 3.30 -8 -9 0 38.60 3.20 8 9 0 25.50 2.90 8 9 0 31.20 3.00 8 9 0 34.90 3.20 -8 9 0 28.20 2.90 -8 9 0 32.30 3.10 -8 9 0 32.40 3.10 -9 -9 0 124.69 10.80 -9 -9 0 143.99 11.00 -9 -9 0 141.39 10.90 -9 -9 0 137.39 10.80 9 9 0 150.88 10.90 -9 9 0 127.79 10.90 -9 9 0 138.99 10.90 9 9 0 137.19 10.70 -9 9 0 149.59 10.90 10 -9 0 21.50 2.90 -10 -9 0 27.70 2.90 -10 -9 0 19.70 2.60 -10 -9 0 28.00 2.80 -10 -9 0 26.40 2.70 -10 -9 0 21.10 2.90 -10 9 0 30.40 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150.78 13.90 -10 -10 0 66.79 5.60 -10 -10 0 72.69 5.80 10 -10 0 89.09 6.20 -10 -10 0 67.69 6.10 -10 -10 0 57.69 5.80 -10 -10 0 62.89 5.80 10 10 0 60.29 5.70 -10 10 0 76.79 5.70 -10 10 0 66.49 5.80 10 10 0 68.79 5.80 -11 -10 0 96.19 7.40 -11 -10 0 89.59 7.50 -11 -10 0 95.19 7.60 -11 -10 0 90.19 7.90 -11 -10 0 85.09 7.50 11 -10 0 93.99 7.80 -11 10 0 81.79 7.40 -11 10 0 75.49 7.50 11 10 0 108.49 7.50 11 10 0 89.69 7.50 -11 10 0 108.79 7.70 -12 -10 0 11.00 1.70 12 -10 0 13.80 2.70 -12 -10 0 10.20 2.00 -12 -10 0 9.00 2.50 -12 -10 0 9.20 2.00 -12 -10 0 12.40 2.10 -12 10 0 10.40 2.20 -12 10 0 14.10 2.00 -12 10 0 10.70 2.10 12 10 0 14.50 2.10 12 10 0 9.40 2.00 -13 -10 0 24.10 2.90 -13 -10 0 23.20 2.70 -13 -10 0 16.10 2.90 -13 -10 0 27.70 2.90 13 -10 0 28.90 3.30 -13 -10 0 23.10 2.90 -13 10 0 20.80 3.00 -13 10 0 24.40 2.90 13 10 0 25.30 2.80 13 10 0 25.60 2.90 -13 10 0 33.10 3.20 -14 -10 0 19.90 2.90 -14 -10 0 21.70 3.40 -14 -10 0 16.70 2.40 -14 -10 0 19.50 2.80 -14 10 0 20.80 2.70 14 10 0 17.10 2.50 -14 10 0 22.50 3.00 -14 10 0 16.00 2.60 14 10 0 21.20 2.80 -15 -10 0 73.89 6.60 -15 -10 0 62.39 6.30 -15 -10 0 71.89 7.00 -15 10 0 79.19 6.70 -15 10 0 65.39 6.60 15 10 0 77.79 6.40 -15 10 0 80.79 6.50 -16 -10 0 1.70 2.80 -16 -10 0 6.00 2.20 -16 -10 0 -0.10 2.30 -16 10 0 2.30 2.00 -16 10 0 5.10 2.00 16 10 0 0.00 2.10 -16 10 0 1.60 2.30 -17 -10 0 80.59 8.20 -17 10 0 95.29 7.70 -17 10 0 79.79 7.80 -17 10 0 97.89 7.80 -18 -10 0 8.50 3.20 -18 -10 0 0.50 3.20 -18 10 0 1.40 2.20 -18 10 0 3.80 2.60 -18 10 0 6.40 2.40 -19 -10 0 18.40 3.50 -19 -10 0 10.50 3.70 -19 10 0 18.60 3.30 -19 10 0 20.60 3.40 -19 10 0 14.10 2.90 -20 -10 0 15.80 3.80 -20 -10 0 5.20 3.60 -20 10 0 7.90 2.90 -20 10 0 9.60 3.10 -20 10 0 3.80 2.70 -21 -10 0 12.70 4.00 -21 -10 0 18.80 4.00 -21 10 0 15.50 3.00 -21 10 0 15.90 3.60 -21 10 0 16.90 3.40 -22 -10 0 0.50 3.70 -22 -10 0 8.40 4.30 -22 10 0 6.60 3.00 -22 10 0 -0.20 3.10 -23 -10 0 41.40 5.50 -23 -10 0 30.90 5.70 -23 10 0 24.30 4.60 -23 10 0 35.70 4.60 -24 -10 0 10.60 4.30 -24 -10 0 18.00 4.60 -24 10 0 8.50 3.80 -24 10 0 10.40 3.60 -25 -10 0 0.20 4.00 -25 -10 0 11.10 5.20 -25 10 0 7.10 3.50 -25 10 0 1.40 3.50 0 -11 0 2.40 1.10 0 -11 0 -1.90 1.10 0 -11 0 -1.00 0.90 0 11 0 -0.10 1.20 0 11 0 -0.70 0.80 0 11 0 -1.30 1.00 1 -11 0 625.14 45.70 -1 -11 0 612.84 45.70 -1 -11 0 577.54 45.70 1 11 0 644.44 45.70 1 11 0 557.94 45.60 -1 11 0 596.64 45.70 1 11 0 643.44 45.70 -2 -11 0 74.89 6.20 2 -11 0 68.39 5.90 -2 -11 0 67.89 5.80 -2 -11 0 85.99 6.00 -2 -11 0 70.89 6.00 -2 11 0 80.09 6.00 -2 11 0 73.79 5.80 -2 11 0 70.69 6.10 2 11 0 72.79 6.10 2 11 0 77.79 5.90 -2 11 0 79.69 6.00 2 11 0 75.09 5.90 -3 -11 0 164.08 11.50 3 -11 0 148.89 11.50 -3 -11 0 148.19 11.60 -3 -11 0 153.18 11.60 3 11 0 162.68 11.50 3 11 0 146.09 11.60 3 11 0 132.59 11.50 -3 11 0 145.29 11.60 4 -11 0 7.10 1.20 4 -11 0 3.20 1.60 -4 -11 0 6.10 1.40 -4 -11 0 9.10 1.40 -4 -11 0 4.70 1.40 -4 -11 0 7.10 1.10 4 11 0 5.90 1.40 4 11 0 6.90 1.20 -4 11 0 9.80 1.50 4 11 0 6.10 1.20 -4 11 0 7.40 1.10 -4 11 0 8.40 1.40 -5 -11 0 140.79 11.70 -5 -11 0 145.89 11.70 5 -11 0 120.69 11.80 5 -11 0 168.08 11.50 5 11 0 169.48 11.60 -5 11 0 127.79 11.60 -5 11 0 165.28 11.70 5 11 0 167.18 11.70 6 -11 0 14.50 2.20 -6 -11 0 11.60 1.50 -6 -11 0 11.40 1.90 -6 -11 0 16.80 1.90 -6 -11 0 9.60 1.60 6 -11 0 11.70 1.40 -6 11 0 12.80 1.80 -6 11 0 11.50 1.50 6 11 0 11.50 1.50 6 11 0 11.30 1.70 -6 11 0 9.30 1.80 6 11 0 10.10 1.70 -7 -11 0 179.88 13.40 7 -11 0 187.38 13.60 -7 -11 0 167.68 13.20 -7 -11 0 173.88 13.50 7 -11 0 161.38 13.10 -7 -11 0 157.58 13.30 -7 11 0 184.88 13.30 7 11 0 189.48 13.30 -7 11 0 179.18 13.40 7 11 0 173.28 13.30 -7 11 0 144.99 13.30 7 11 0 175.38 13.30 -8 -11 0 38.80 3.70 -8 -11 0 37.20 3.50 8 -11 0 36.80 4.10 -8 -11 0 35.00 3.60 -8 -11 0 37.90 3.90 -8 11 0 38.50 3.40 8 11 0 29.40 3.50 -8 11 0 45.00 3.70 8 11 0 30.20 3.40 -8 11 0 38.40 3.60 8 11 0 39.00 3.40 -9 -11 0 172.98 12.10 -9 -11 0 166.68 12.10 9 -11 0 126.79 12.30 -9 -11 0 132.19 12.00 -9 -11 0 153.88 12.20 9 11 0 137.09 11.90 -9 11 0 149.88 12.10 9 11 0 166.38 12.10 -9 11 0 171.48 12.10 9 11 0 160.18 12.00 -9 11 0 164.48 12.00 -10 -11 0 1.80 2.10 -10 -11 0 -0.90 1.50 -10 -11 0 1.70 1.70 -10 -11 0 1.50 1.60 10 -11 0 1.10 2.10 10 11 0 1.80 1.40 -10 11 0 4.40 1.40 -10 11 0 0.90 1.70 10 11 0 1.00 1.50 -10 11 0 -0.20 1.60 -11 -11 0 13.40 2.00 -11 -11 0 10.00 2.00 -11 -11 0 13.90 2.20 11 -11 0 15.40 2.70 -11 -11 0 16.70 1.90 -11 -11 0 12.80 2.60 -11 11 0 12.40 2.30 11 11 0 10.70 2.00 -11 11 0 13.30 2.20 -11 11 0 15.60 2.00 11 11 0 8.90 2.20 -12 -11 0 51.39 4.70 -12 -11 0 56.09 4.50 -12 -11 0 48.30 4.90 -12 -11 0 43.10 4.80 12 -11 0 36.30 5.00 -12 -11 0 55.39 5.00 -12 11 0 54.39 4.80 -12 11 0 60.59 4.90 12 11 0 53.69 4.90 12 11 0 46.10 4.60 -12 11 0 49.10 4.70 -13 -11 0 0.40 2.40 -13 -11 0 -0.70 1.90 -13 -11 0 0.20 1.80 -13 -11 0 1.00 1.80 -13 11 0 -1.40 1.90 -13 11 0 -0.60 1.80 -13 11 0 2.00 1.60 13 11 0 -1.40 1.60 -14 -11 0 35.50 3.60 -14 -11 0 36.50 3.80 -14 -11 0 29.50 4.00 -14 11 0 34.20 3.70 -14 11 0 29.60 3.50 -14 11 0 21.40 3.50 14 11 0 35.50 3.60 -15 -11 0 57.39 5.60 -15 -11 0 50.29 6.20 -15 -11 0 73.79 5.90 15 11 0 76.99 5.90 -15 11 0 56.99 5.70 -15 11 0 53.29 5.80 -15 11 0 63.49 5.70 -16 -11 0 23.50 3.30 -16 -11 0 25.40 3.20 -16 -11 0 18.90 3.70 -16 11 0 24.00 3.30 -16 11 0 26.80 3.20 -16 11 0 24.50 3.10 16 11 0 20.20 3.00 -17 -11 0 37.80 4.60 -17 -11 0 38.20 5.10 -17 -11 0 39.60 4.40 -17 11 0 46.80 4.90 -17 11 0 46.60 4.60 -17 11 0 43.60 4.70 -18 -11 0 3.00 3.30 -18 -11 0 1.50 2.80 -18 11 0 7.10 2.80 -18 11 0 1.90 2.60 -18 11 0 10.80 2.60 -19 -11 0 14.50 3.40 -19 -11 0 6.20 3.50 -19 11 0 12.20 2.90 -19 11 0 17.20 2.90 -19 11 0 10.80 3.00 -20 -11 0 4.10 3.70 -20 11 0 5.30 3.00 -20 11 0 -1.40 2.40 -20 11 0 6.20 2.70 -21 -11 0 -1.80 3.50 -21 -11 0 3.70 3.30 -21 11 0 0.10 3.10 -21 11 0 6.60 3.10 -21 11 0 -0.30 2.50 -22 -11 0 3.10 3.70 -22 -11 0 0.50 3.70 -22 11 0 3.30 3.50 -22 11 0 6.90 3.00 -23 -11 0 7.50 4.40 -23 -11 0 13.90 4.40 -23 11 0 11.10 3.70 -23 11 0 13.00 3.80 -24 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40.90 5.20 -15 -12 0 55.59 5.30 -15 -12 0 54.29 5.10 -15 12 0 57.09 5.10 15 12 0 45.60 5.10 -15 12 0 51.49 4.90 -15 12 0 46.70 5.10 -16 -12 0 7.60 2.30 -16 -12 0 4.20 3.10 -16 -12 0 6.70 2.60 -16 12 0 7.00 2.60 -16 12 0 7.20 2.40 -16 12 0 10.50 2.50 16 12 0 5.00 2.50 -17 -12 0 19.60 2.90 -17 -12 0 16.30 3.30 -17 -12 0 16.60 3.80 -17 12 0 21.00 3.00 -17 12 0 17.80 3.00 -17 12 0 18.70 3.20 -18 -12 0 63.59 6.10 -18 -12 0 44.40 6.00 -18 12 0 52.69 5.60 -18 12 0 49.80 5.80 -18 12 0 66.29 5.70 -19 -12 0 22.70 4.30 -19 -12 0 23.90 4.20 -19 12 0 16.50 3.70 -19 12 0 9.30 2.90 -19 12 0 17.30 3.10 -20 -12 0 11.60 3.40 -20 -12 0 1.50 3.60 -20 12 0 4.20 3.00 -20 12 0 13.90 3.00 -20 12 0 6.20 2.90 -21 -12 0 19.30 4.10 -21 -12 0 12.30 4.20 -21 12 0 9.90 3.50 -21 12 0 17.80 3.40 -21 12 0 11.70 3.30 -22 -12 0 17.00 4.30 -22 -12 0 -0.10 4.00 -22 12 0 7.40 3.70 -23 -12 0 -5.90 3.80 -23 -12 0 9.00 4.70 -23 12 0 2.30 3.40 -24 -12 0 10.00 4.60 -24 -12 0 16.50 4.70 -24 12 0 8.50 4.20 0 -13 0 -0.50 1.00 0 -13 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14.50 1.70 4 14 0 12.20 2.00 -4 14 0 13.60 1.90 5 -14 0 98.29 7.80 -5 -14 0 95.99 7.60 -5 -14 0 88.09 7.40 -5 -14 0 92.59 7.50 5 -14 0 76.79 7.30 5 14 0 96.79 7.30 -5 14 0 92.49 7.50 5 14 0 94.99 7.50 -6 -14 0 12.60 2.00 -6 -14 0 9.60 2.40 -6 -14 0 12.20 2.10 6 -14 0 9.90 2.30 -6 -14 0 13.10 1.70 6 -14 0 10.40 1.70 6 14 0 7.30 1.90 -6 14 0 8.10 1.90 -6 14 0 11.00 1.80 6 14 0 8.00 1.70 -7 -14 0 2.80 1.90 7 -14 0 4.10 2.30 -7 -14 0 3.70 1.60 -7 -14 0 3.60 1.80 -7 -14 0 4.00 1.40 7 14 0 4.70 1.80 -7 14 0 3.40 1.80 7 14 0 4.40 1.50 7 14 0 2.00 1.50 -7 14 0 3.10 1.70 -8 -14 0 178.18 14.00 -8 -14 0 177.08 13.70 8 -14 0 193.48 14.30 -8 -14 0 160.78 13.90 -8 -14 0 188.68 13.90 8 14 0 176.08 13.80 8 14 0 178.68 13.90 -8 14 0 167.88 13.90 -9 -14 0 2.40 1.90 -9 -14 0 2.10 1.70 -9 -14 0 0.90 2.00 -9 -14 0 1.60 1.50 9 -14 0 3.60 2.20 9 14 0 2.70 1.70 -9 14 0 3.90 1.80 9 14 0 1.90 1.80 -9 14 0 1.30 1.80 -10 -14 0 48.40 4.90 -10 -14 0 42.20 5.10 10 -14 0 56.89 5.90 -10 -14 0 48.90 4.70 -10 14 0 57.39 4.90 -10 14 0 44.60 4.80 10 14 0 55.19 4.80 -11 -14 0 71.89 6.40 -11 -14 0 82.79 7.00 -11 -14 0 79.39 6.60 11 14 0 55.89 6.30 -11 14 0 84.99 6.60 -11 14 0 75.19 6.50 -12 -14 0 7.40 2.40 -12 -14 0 10.00 2.40 -12 -14 0 8.40 2.00 -12 14 0 11.30 2.30 -12 14 0 9.20 2.20 12 14 0 4.10 2.10 -13 -14 0 95.49 8.60 -13 -14 0 97.69 8.70 -13 14 0 97.49 8.70 -13 14 0 128.49 8.80 13 14 0 104.19 8.60 -14 -14 0 -2.50 2.60 -14 -14 0 -2.00 2.20 -14 -14 0 -3.60 2.00 14 14 0 -1.70 2.20 -14 14 0 0.50 2.10 -14 14 0 -1.50 2.20 -15 -14 0 37.20 4.30 -15 -14 0 45.30 4.90 -15 -14 0 37.20 4.90 -15 14 0 37.10 4.40 15 14 0 36.60 4.20 -15 14 0 47.20 4.70 -16 -14 0 21.20 3.60 -16 -14 0 26.70 4.30 -16 -14 0 21.80 3.30 -16 14 0 26.50 3.70 -16 14 0 28.30 3.70 -17 -14 0 0.20 2.70 -17 -14 0 3.20 2.40 -17 -14 0 4.30 3.00 -17 14 0 5.10 2.80 -17 14 0 3.10 2.50 -18 -14 0 0.60 2.40 -18 -14 0 10.20 3.90 -18 14 0 -0.20 2.50 -18 14 0 0.70 2.70 -19 -14 0 10.40 3.30 -19 -14 0 7.40 3.90 -19 14 0 4.40 3.00 -19 14 0 9.40 2.90 -20 -14 0 0.70 3.90 -20 -14 0 9.70 3.50 -20 14 0 5.50 3.20 -20 14 0 2.00 2.80 -21 -14 0 17.00 4.00 -21 -14 0 5.20 4.20 -21 14 0 -2.20 3.20 -21 14 0 4.40 2.80 -22 -14 0 2.80 4.70 -22 -14 0 16.60 4.60 -22 14 0 1.80 3.40 -22 14 0 8.70 3.50 -23 -14 0 15.40 4.40 -23 -14 0 -2.10 4.30 -23 14 0 1.30 3.80 0 -15 0 0.20 1.30 0 -15 0 1.70 1.60 0 -15 0 1.30 1.40 0 15 0 -1.30 1.60 0 15 0 1.60 1.30 1 -15 0 66.99 5.10 1 -15 0 69.59 5.60 -1 -15 0 65.09 5.10 -1 -15 0 59.59 5.50 -1 -15 0 55.29 5.10 1 15 0 48.00 5.00 -1 15 0 58.09 5.00 1 15 0 54.99 5.30 -1 15 0 57.69 5.30 -2 -15 0 0.60 1.80 2 -15 0 4.70 1.90 2 15 0 -1.10 1.60 -2 15 0 1.20 1.50 -2 15 0 0.40 1.70 2 15 0 0.80 1.20 -3 -15 0 125.89 9.30 -3 -15 0 114.39 9.30 3 -15 0 138.49 9.30 3 -15 0 137.99 9.70 -3 -15 0 92.39 9.30 3 15 0 128.09 9.30 -3 15 0 109.69 9.20 3 15 0 106.69 9.20 -3 15 0 104.99 9.40 4 -15 0 54.59 4.50 -4 -15 0 44.70 4.60 -4 -15 0 40.40 4.70 -4 -15 0 48.60 4.60 4 15 0 48.10 4.60 -4 15 0 54.09 4.70 -4 15 0 52.89 4.70 4 15 0 52.99 4.40 -5 -15 0 3.30 1.50 -5 -15 0 3.70 1.90 5 -15 0 3.30 1.90 -5 -15 0 -0.70 1.70 5 -15 0 2.70 1.40 5 15 0 0.50 1.60 5 15 0 1.10 1.40 -5 15 0 0.90 1.80 -5 15 0 1.90 1.60 -6 -15 0 151.98 12.10 -6 -15 0 143.59 12.10 -6 -15 0 159.78 12.20 6 -15 0 174.08 12.40 6 -15 0 170.48 12.10 6 15 0 151.88 12.50 -6 15 0 161.98 12.10 6 15 0 126.79 12.00 -6 15 0 142.69 12.10 -7 -15 0 18.80 2.60 7 -15 0 17.30 2.90 -7 -15 0 21.10 2.80 -7 -15 0 22.60 2.90 -7 15 0 23.00 2.80 7 15 0 20.10 2.70 -7 15 0 24.30 2.80 -8 -15 0 10.30 2.40 -8 -15 0 15.40 2.30 8 -15 0 15.50 2.80 -8 -15 0 9.80 2.30 -8 15 0 9.20 2.30 8 15 0 16.10 2.30 -8 15 0 13.40 2.20 -9 -15 0 8.60 2.50 -9 -15 0 5.30 2.20 -9 15 0 5.80 2.10 9 15 0 6.10 2.00 -9 15 0 5.40 2.00 -10 -15 0 28.10 3.30 -10 -15 0 24.60 3.50 -10 15 0 28.90 3.30 -10 15 0 28.00 3.30 10 15 0 23.70 3.20 -11 -15 0 5.70 2.60 -11 -15 0 11.10 3.50 -11 -15 0 7.60 2.40 11 15 0 9.00 2.20 -11 15 0 9.20 2.30 -11 15 0 6.80 2.20 -12 -15 0 73.59 6.70 -12 -15 0 69.49 7.10 -12 -15 0 79.19 6.50 -12 15 0 70.49 6.70 12 15 0 70.69 6.60 -12 15 0 84.99 6.80 -13 -15 0 10.80 3.10 -13 -15 0 12.30 2.40 -13 -15 0 11.10 2.70 13 15 0 16.90 2.90 -13 15 0 15.90 2.80 -13 15 0 16.20 2.70 -14 -15 0 12.40 2.80 -14 -15 0 17.30 3.60 -14 -15 0 13.40 2.90 14 15 0 17.40 2.80 -14 15 0 19.80 3.00 -14 15 0 14.00 2.80 -15 -15 0 -1.70 3.00 -15 -15 0 -2.40 2.40 -15 -15 0 -0.70 2.20 15 15 0 -0.60 2.50 -15 15 0 -0.80 2.40 -15 15 0 1.40 2.20 -16 -15 0 36.50 5.00 -16 -15 0 49.50 5.90 -16 -15 0 51.59 5.70 -16 15 0 58.19 5.50 -16 15 0 55.49 5.40 -17 -15 0 1.50 2.70 -17 -15 0 11.00 3.50 -17 -15 0 12.20 3.90 -17 15 0 -0.30 2.70 -17 15 0 -2.10 2.70 -18 -15 0 13.20 3.60 -18 -15 0 12.60 4.10 -18 -15 0 9.00 2.70 -18 15 0 -2.80 2.40 -18 15 0 -0.10 2.80 -19 -15 0 13.70 4.40 -19 -15 0 16.00 3.70 -19 15 0 10.50 3.40 -19 15 0 15.80 3.20 -20 -15 0 14.70 4.60 -20 -15 0 21.40 4.20 -20 15 0 21.90 3.50 -20 15 0 19.90 3.90 -21 -15 0 13.20 4.00 -21 -15 0 9.50 4.60 -21 15 0 9.00 3.50 -21 15 0 9.90 3.40 -22 -15 0 7.30 4.50 -22 15 0 1.70 3.00 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24.00 2.90 10 11 3 20.50 2.80 -10 11 -3 22.90 2.90 -11 -11 -3 7.40 1.90 11 -11 3 6.60 2.40 -11 -11 -3 7.80 2.30 -11 -11 -3 4.80 2.00 -11 -11 -3 5.70 1.80 11 11 3 8.30 2.00 11 11 3 4.00 2.10 -11 11 -3 4.40 1.90 -11 11 -3 6.00 2.00 11 11 3 6.00 2.00 -12 -11 -3 5.30 2.00 -12 -11 -3 7.40 2.00 12 -11 3 8.20 2.40 -12 -11 -3 7.80 1.90 -12 -11 -3 7.40 2.40 -12 -11 -3 7.50 1.90 12 11 3 8.70 2.20 -12 11 -3 8.00 2.10 12 11 3 9.30 2.10 12 11 3 8.90 2.20 -12 11 -3 11.80 2.30 -13 -11 -3 92.49 8.20 -13 -11 -3 105.59 8.00 -13 -11 -3 95.89 7.70 -13 -11 -3 97.19 8.00 -13 -11 -3 95.29 7.80 13 11 3 89.49 8.00 13 11 3 78.39 7.70 -13 11 -3 97.39 7.90 -13 11 -3 92.29 7.90 13 11 3 89.99 7.80 -14 -11 -3 40.70 4.30 -14 -11 -3 46.00 4.70 -14 -11 -3 37.30 4.40 -14 -11 -3 45.30 4.60 -14 -11 -3 44.00 4.20 14 11 3 35.70 4.20 14 11 3 39.70 4.50 -14 11 -3 48.70 4.60 -14 11 -3 41.80 4.50 -15 -11 -3 -0.40 2.50 -15 -11 -3 -1.50 2.10 -15 -11 -3 0.90 1.80 -15 -11 -3 -0.80 1.90 -15 -11 -3 7.30 2.30 -15 11 -3 -0.30 2.10 15 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4.00 3 12 -3 46.10 4.10 -3 12 3 44.20 4.10 2 -12 -3 14.60 1.80 -2 -12 3 16.50 2.10 -2 -12 3 16.20 2.00 2 -12 -3 18.40 2.30 -2 -12 3 19.20 2.10 2 -12 -3 16.40 1.90 -2 12 3 15.00 2.00 -2 12 3 17.10 1.90 2 12 -3 15.80 1.80 2 12 -3 16.30 2.00 -2 12 3 15.80 1.90 -2 12 3 17.00 2.10 -1 -12 3 43.00 4.00 1 -12 -3 50.69 4.40 -1 -12 3 40.10 4.10 -1 -12 3 54.79 4.20 1 -12 -3 46.30 4.00 1 -12 -3 46.30 4.00 -1 12 3 44.20 4.10 -1 12 3 43.90 4.00 1 12 -3 38.60 3.80 -1 12 3 54.59 4.20 -1 12 3 54.19 4.00 0 -12 3 157.58 12.00 0 -12 -3 132.89 12.00 0 -12 -3 156.48 12.10 0 -12 3 178.28 12.10 0 -12 3 142.89 12.10 0 -12 -3 150.58 12.20 0 12 3 152.28 12.10 0 12 -3 145.99 12.10 0 12 3 167.08 12.10 0 12 3 163.48 12.10 0 12 3 176.18 12.20 1 -12 3 2.10 1.20 -1 -12 -3 3.90 1.20 1 -12 3 2.30 1.40 -1 -12 -3 2.50 1.50 -1 -12 -3 2.30 1.20 1 12 3 3.60 1.40 -1 12 -3 5.80 1.10 1 12 3 3.90 1.30 1 12 3 4.40 1.10 -1 12 -3 5.00 1.40 1 12 3 4.90 1.40 -2 -12 -3 399.76 28.90 -2 -12 -3 378.86 28.80 2 -12 3 408.56 28.80 -2 -12 -3 368.06 28.80 2 -12 3 374.06 28.70 2 12 3 369.66 28.80 2 12 3 376.16 28.90 2 12 3 373.36 28.80 2 12 3 332.07 28.80 -2 12 -3 427.26 28.80 3 -12 3 11.30 1.60 -3 -12 -3 11.90 1.80 -3 -12 -3 9.90 1.70 -3 -12 -3 11.80 1.80 3 -12 3 9.90 1.80 3 12 3 11.50 1.70 3 12 3 9.80 1.80 3 12 3 9.10 1.60 -3 12 -3 14.80 1.60 3 12 3 10.30 1.80 -3 12 -3 10.40 1.80 4 -12 3 66.59 5.80 -4 -12 -3 61.09 5.40 -4 -12 -3 70.59 5.60 4 -12 3 52.59 5.30 -4 -12 -3 81.79 5.70 -4 -12 -3 73.19 5.40 4 12 3 64.09 5.50 4 12 3 60.99 5.40 4 12 3 68.49 5.40 -4 12 -3 59.99 5.40 -4 12 -3 61.09 5.40 5 -12 3 26.20 2.70 -5 -12 -3 27.10 2.90 -5 -12 -3 26.60 3.10 5 -12 3 29.20 3.10 -5 -12 -3 27.60 2.70 -5 -12 -3 29.60 3.10 5 12 3 31.80 2.90 5 12 3 23.80 2.80 -5 12 -3 33.50 2.80 5 12 3 19.80 2.60 -5 12 -3 23.60 2.80 -6 -12 -3 106.19 8.40 -6 -12 -3 102.99 8.50 -6 -12 -3 101.09 8.30 6 -12 3 79.89 8.60 -6 12 -3 117.79 8.50 6 12 3 111.49 8.40 6 12 3 124.69 8.50 -6 12 -3 92.79 8.30 6 12 3 107.69 8.40 -7 -12 -3 1.10 1.50 -7 -12 -3 3.20 1.40 7 -12 3 2.40 1.80 -7 -12 -3 1.90 1.60 -7 -12 -3 3.70 1.70 7 12 3 2.50 1.60 -7 12 -3 2.00 1.70 -7 12 -3 3.80 1.60 7 12 3 5.60 1.70 7 12 3 3.60 1.50 -8 -12 -3 187.28 15.30 8 -12 3 196.78 15.40 -8 -12 -3 204.98 15.20 -8 -12 -3 206.08 15.40 8 12 3 215.08 15.20 8 12 3 177.38 15.20 8 12 3 200.78 15.30 -8 12 -3 186.38 15.20 -9 -12 -3 17.10 2.20 9 -12 3 12.60 2.50 -9 -12 -3 14.20 2.10 -9 -12 -3 10.70 2.10 -9 -12 -3 14.00 2.10 -9 12 -3 10.20 2.20 9 12 3 14.80 2.20 9 12 3 13.10 2.20 9 12 3 14.20 2.10 -9 12 -3 9.00 2.10 10 -12 3 -0.10 2.00 -10 -12 -3 0.90 1.70 -10 -12 -3 0.70 1.80 -10 -12 -3 4.50 2.10 -10 -12 -3 1.40 1.80 10 12 3 1.00 1.70 10 12 3 2.40 1.80 -10 12 -3 0.40 1.80 -10 12 -3 -0.40 1.70 10 12 3 -0.40 1.70 -11 -12 -3 0.90 1.80 -11 -12 -3 3.00 1.70 -11 -12 -3 5.90 2.00 11 -12 3 2.00 2.10 -11 -12 -3 3.90 2.20 -11 12 -3 1.80 1.90 -11 12 -3 2.00 1.90 11 12 3 4.20 1.90 11 12 3 3.40 1.80 11 12 3 7.20 2.00 -12 -12 -3 49.10 5.60 -12 -12 -3 50.89 5.30 -12 -12 -3 64.99 5.80 -12 -12 -3 63.09 5.60 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1076.79 79.39 -8 0 4 1052.79 79.39 8 0 -4 1036.90 79.49 -7 0 4 -3.00 0.80 7 0 -4 -0.50 0.90 -7 0 4 -1.80 1.30 -7 0 4 -0.30 1.10 -7 0 4 -1.10 0.80 -7 0 4 0.50 0.90 -6 0 4 -0.10 0.90 6 0 -4 0.20 0.70 -6 0 4 -0.20 0.70 -6 0 4 1.60 1.00 -6 0 4 1.80 1.10 -5 0 4 1.00 0.90 -5 0 4 1.30 1.00 -5 0 4 0.10 0.70 5 0 -4 0.60 0.70 -4 0 4 98.39 7.80 -4 0 4 95.49 7.50 4 0 -4 99.59 7.50 -3 0 4 -0.40 0.60 -2 0 4 49.40 4.00 2 0 -4 52.39 4.00 1 0 -4 -0.40 0.50 -1 0 4 -0.10 0.60 1 0 -4 0.20 0.60 0 0 4 247.38 19.30 0 0 -4 275.87 19.30 0 0 4 250.67 19.30 0 0 -4 252.07 19.30 -1 0 -4 0.40 0.70 -1 0 -4 -0.50 0.70 1 0 4 0.00 0.70 1 0 4 -0.20 0.80 2 0 4 1578.84 118.39 -2 0 -4 1628.14 118.39 -2 0 -4 1543.35 118.39 3 0 4 1.90 1.00 -3 0 -4 1.90 0.90 -3 0 -4 1.20 1.00 4 0 4 855.81 60.09 -4 0 -4 753.02 59.99 -4 0 -4 810.92 60.09 4 0 4 767.92 59.99 -4 0 -4 772.82 60.09 4 0 4 848.62 59.99 -5 0 -4 -0.40 0.80 5 0 4 1.60 1.00 -5 0 -4 -0.30 1.00 5 0 4 -0.40 1.00 5 0 4 0.70 0.90 -5 0 -4 -0.10 0.80 5 0 4 0.70 1.00 6 0 4 13.10 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142.79 11.50 10 -2 4 148.49 11.50 -10 -2 -4 137.89 11.40 -10 -2 -4 148.89 11.20 -10 2 -4 138.69 11.40 10 2 4 146.39 11.50 10 2 4 153.98 11.60 10 2 4 168.88 11.60 10 2 4 146.09 11.50 -10 2 -4 158.48 11.40 -10 2 -4 143.89 11.40 11 -2 4 2.10 1.50 -11 -2 -4 5.20 1.40 -11 -2 -4 4.20 1.50 11 -2 4 2.90 1.60 11 -2 4 4.10 1.50 -11 -2 -4 3.00 1.50 -11 -2 -4 2.30 1.00 -11 -2 -4 0.60 1.40 11 2 4 3.40 1.50 -11 2 -4 1.70 1.30 11 2 4 1.90 1.50 -11 2 -4 2.30 1.30 -11 2 -4 2.50 1.30 -11 2 -4 -1.30 1.40 11 2 4 2.80 1.50 12 -2 4 392.26 28.90 12 -2 4 408.26 29.00 12 -2 4 395.16 28.90 -12 -2 -4 378.96 28.90 -12 -2 -4 385.76 28.90 -12 -2 -4 383.66 28.80 -12 -2 -4 358.16 28.90 12 2 4 391.16 28.90 -12 2 -4 372.36 28.90 12 2 4 362.86 28.90 12 2 4 313.97 28.80 -12 2 -4 389.56 28.80 -12 2 -4 408.86 28.80 -13 -2 -4 1.20 1.60 -13 -2 -4 1.10 1.60 13 -2 4 -1.60 1.80 13 -2 4 2.10 1.60 -13 -2 -4 0.10 1.60 13 -2 4 -0.20 1.70 -13 -2 -4 -1.80 1.60 -13 2 -4 -2.20 1.50 13 2 4 0.70 1.60 -13 2 -4 0.20 1.50 -13 2 -4 -3.30 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12 3 -4 24.90 2.60 -12 3 4 21.90 2.70 -12 3 4 26.10 2.70 -12 3 4 23.10 2.60 -11 -3 4 68.29 7.10 11 -3 -4 90.09 6.90 -11 -3 4 83.29 6.80 11 -3 -4 79.49 7.10 -11 -3 4 93.69 7.00 -11 -3 4 85.79 7.20 -11 3 4 87.89 6.80 11 3 -4 94.29 6.80 -11 3 4 102.29 6.90 -11 3 4 81.89 7.00 -11 3 4 86.29 7.10 -11 3 4 97.49 7.10 11 3 -4 77.29 6.90 -10 -3 4 37.10 4.00 -10 -3 4 44.70 3.70 10 -3 -4 43.10 3.70 -10 -3 4 42.70 3.70 -10 -3 4 40.50 4.00 -10 3 4 44.00 3.60 10 3 -4 44.30 3.70 -10 3 4 47.00 4.00 -10 3 4 46.80 3.60 -10 3 4 43.90 3.80 10 3 -4 45.20 3.60 -10 3 4 44.10 3.90 -9 -3 4 11.20 1.70 -9 -3 4 6.60 1.10 -9 -3 4 9.80 1.10 -9 -3 4 6.40 1.20 -9 -3 4 5.80 1.70 9 -3 -4 8.40 1.50 9 3 -4 6.60 1.10 -9 3 4 5.20 1.60 -9 3 4 6.70 1.50 -9 3 4 7.20 1.10 -9 3 4 6.60 1.40 -9 3 4 6.70 1.10 8 -3 -4 159.28 11.60 -8 -3 4 151.38 11.50 -8 -3 4 151.88 11.70 -8 -3 4 160.08 11.50 -8 -3 4 134.09 11.40 -8 -3 4 146.49 11.50 -8 3 4 139.49 11.40 -8 3 4 154.18 11.60 8 3 -4 137.59 11.40 -8 3 4 148.49 11.60 -8 3 4 164.88 11.40 -8 3 4 152.28 11.50 -7 -3 4 191.88 15.30 -7 -3 4 205.08 15.40 7 -3 -4 191.18 15.40 -7 -3 4 208.78 15.30 -7 -3 4 182.58 15.20 -7 3 4 213.08 15.40 -7 3 4 216.08 15.30 7 3 -4 185.68 15.20 -7 3 4 213.58 15.40 -7 3 4 210.88 15.20 -6 -3 4 113.69 9.10 -6 -3 4 106.19 8.80 6 -3 -4 119.69 9.10 -6 -3 4 122.59 9.00 -6 -3 4 117.09 9.00 6 3 -4 112.39 8.80 -6 3 4 121.79 9.20 -6 3 4 130.89 9.00 -6 3 4 118.59 9.00 -6 3 4 105.89 9.00 -6 3 4 119.59 8.90 -5 -3 4 181.98 12.70 -5 -3 4 165.18 12.60 5 -3 -4 185.58 12.70 -5 -3 4 142.49 12.50 -5 -3 4 161.88 12.50 -5 3 4 176.58 12.60 5 3 -4 167.78 12.50 -5 3 4 170.18 12.70 -5 3 4 164.58 12.70 -5 3 4 152.28 12.70 -4 -3 4 1423.16 104.29 -4 -3 4 1324.17 104.09 -4 -3 4 1275.77 104.29 -4 -3 4 1241.28 104.09 4 -3 -4 1439.96 104.29 -4 3 4 1381.16 104.29 -4 3 4 1518.65 104.29 -4 3 4 1478.05 104.29 -4 3 4 1505.25 104.29 4 3 -4 1354.36 104.09 -3 -3 4 195.58 15.70 3 -3 -4 214.48 15.70 -3 3 4 218.68 15.70 -3 3 4 200.68 15.70 2 -3 -4 284.27 22.40 -2 3 4 310.87 22.50 -1 -3 4 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29.10 3.90 -12 -11 4 40.30 4.40 -12 11 4 38.00 3.70 -12 11 4 39.90 3.90 -12 11 4 36.40 3.90 11 -11 -4 7.70 2.30 -11 -11 4 12.00 2.70 -11 -11 4 14.50 2.30 -11 -11 4 2.40 1.90 -11 11 4 2.80 1.60 -11 11 4 4.80 1.90 -11 11 4 5.30 1.90 -10 -11 4 1.30 2.10 10 -11 -4 2.20 2.00 -10 -11 4 4.10 1.70 -10 -11 4 2.00 1.80 -10 11 4 0.50 1.50 10 11 -4 2.30 1.40 -10 11 4 1.50 1.60 -10 11 4 2.00 1.60 9 -11 -4 3.60 2.00 -9 -11 4 1.80 1.80 9 -11 -4 0.50 1.30 -9 11 4 4.10 1.60 -9 11 4 2.70 1.60 9 11 -4 0.70 1.40 -9 11 4 2.60 1.50 8 -11 -4 22.00 2.20 -8 -11 4 19.20 2.20 -8 -11 4 17.80 2.70 -8 -11 4 22.20 2.50 8 -11 -4 14.80 2.60 -8 11 4 22.50 2.40 -8 11 4 20.40 2.40 -8 11 4 21.40 2.50 -8 11 4 21.40 2.10 8 11 -4 19.30 2.20 -7 -11 4 62.69 6.30 7 -11 -4 76.89 6.00 -7 -11 4 73.09 6.50 -7 -11 4 79.99 6.10 -7 -11 4 65.89 6.10 7 -11 -4 65.09 6.40 -7 11 4 81.39 6.30 -7 11 4 78.89 6.20 -7 11 4 76.69 6.30 7 11 -4 86.49 6.10 -7 11 4 88.79 6.30 -6 -11 4 1.90 1.40 6 -11 -4 1.70 1.00 -6 -11 4 1.10 1.00 -6 -11 4 1.30 1.70 6 -11 -4 3.30 1.70 -6 -11 4 3.60 1.20 -6 11 4 1.10 1.50 -6 11 4 1.90 1.10 -6 11 4 0.20 1.20 -6 11 4 0.10 1.40 6 11 -4 1.40 1.20 -5 -11 4 160.78 13.40 5 -11 -4 180.98 13.30 5 -11 -4 169.68 13.50 -5 -11 4 151.88 13.40 -5 11 4 190.88 13.40 -5 11 4 175.98 13.30 -5 11 4 175.58 13.40 -5 11 4 180.98 13.40 -4 -11 4 6.00 1.50 -4 -11 4 4.50 1.70 4 -11 -4 6.60 1.20 -4 -11 4 5.60 1.20 4 -11 -4 6.20 1.60 4 11 -4 8.60 1.30 -4 11 4 4.00 1.30 -4 11 4 8.10 1.60 -4 11 4 4.30 1.40 -4 11 4 7.40 1.50 -3 -11 4 2.60 1.10 3 -11 -4 2.10 1.50 -3 -11 4 0.40 1.30 -3 -11 4 -1.30 1.30 3 -11 -4 2.70 1.10 3 -11 -4 0.40 1.10 -3 11 4 2.30 1.10 -3 11 4 1.60 1.30 -3 11 4 -1.00 1.20 -3 11 4 1.30 1.10 3 11 -4 2.40 1.10 2 -11 -4 118.39 10.60 -2 -11 4 137.79 10.50 -2 -11 4 116.89 10.50 2 -11 -4 143.69 10.50 2 -11 -4 128.89 10.50 -2 11 4 146.99 10.60 -2 11 4 147.19 10.50 -2 11 4 145.59 10.60 2 11 -4 127.89 10.50 -2 11 4 147.59 10.60 -1 -11 4 46.10 3.90 1 -11 -4 45.70 3.80 1 -11 -4 35.80 4.10 1 -11 -4 50.79 3.90 -1 -11 4 41.10 3.80 -1 11 4 46.40 3.90 -1 11 4 41.90 3.80 -1 11 4 49.40 3.90 1 11 -4 36.00 3.60 -1 11 4 44.10 3.90 1 11 -4 54.69 3.90 0 -11 -4 6.40 1.30 0 -11 4 4.40 1.30 0 -11 -4 4.70 1.20 0 -11 -4 4.70 1.50 0 -11 4 5.70 1.30 0 -11 4 3.20 1.20 0 11 -4 3.30 1.00 0 11 4 4.10 1.30 0 11 4 4.50 1.40 0 11 4 5.30 1.40 0 11 -4 3.00 1.30 0 11 4 4.40 1.20 -1 -11 -4 37.30 3.50 1 -11 4 33.00 3.30 -1 -11 -4 29.00 3.20 -1 -11 -4 41.10 3.40 1 -11 4 34.10 3.10 1 11 4 32.90 3.10 1 11 4 35.90 3.30 1 11 4 30.40 3.20 1 11 4 33.90 3.30 -1 11 -4 38.40 3.30 -2 -11 -4 3.80 1.10 -2 -11 -4 3.70 1.50 2 -11 4 7.60 1.50 2 -11 4 6.80 1.30 -2 -11 -4 5.00 1.50 2 11 4 4.40 1.50 -2 11 -4 3.90 1.40 -2 11 -4 8.40 1.10 2 11 4 3.80 1.40 2 11 4 3.50 1.20 2 11 4 5.10 1.50 -3 -11 -4 1.20 1.40 3 -11 4 1.60 1.50 -3 -11 -4 2.20 1.20 3 -11 4 1.50 1.10 -3 -11 -4 1.40 1.20 3 11 4 1.20 1.30 -3 11 -4 -0.30 1.30 -3 11 -4 3.30 1.10 3 11 4 -0.40 1.10 3 11 4 0.20 1.20 3 11 4 2.30 1.40 4 -11 4 1.30 1.10 -4 -11 -4 2.20 1.50 -4 -11 -4 2.30 1.30 -4 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6 78.19 7.50 -15 0 6 0.30 1.60 -15 0 6 -2.20 1.50 -15 0 6 3.50 2.10 -14 0 6 163.28 12.90 -14 0 6 162.48 13.30 -14 0 6 177.68 13.30 -13 0 6 1.10 1.20 13 0 -6 -1.10 1.30 -13 0 6 1.60 1.90 -13 0 6 -0.30 2.00 -13 0 6 4.30 1.80 -12 0 6 31.30 3.60 -12 0 6 45.00 4.30 -12 0 6 42.80 3.90 -12 0 6 46.70 4.00 12 0 -6 46.20 3.80 -11 0 6 3.20 1.50 -11 0 6 0.60 1.10 -11 0 6 0.40 1.20 11 0 -6 0.70 1.20 -11 0 6 -1.10 1.50 -10 0 6 502.05 42.80 -10 0 6 618.74 43.00 -10 0 6 590.74 42.80 -9 0 6 0.90 1.10 -9 0 6 -0.50 1.30 9 0 -6 0.20 0.90 -9 0 6 -0.60 1.20 -9 0 6 -1.50 0.90 -9 0 6 -1.30 1.10 -8 0 6 32.00 3.00 -8 0 6 32.00 2.70 -8 0 6 35.10 2.80 -8 0 6 29.40 2.70 8 0 -6 21.50 2.70 -8 0 6 30.90 3.10 7 0 -6 -0.80 0.90 -7 0 6 -3.50 1.30 -7 0 6 -1.40 0.80 -7 0 6 1.20 1.00 -7 0 6 -1.80 1.10 -7 0 6 -0.90 0.80 -6 0 6 169.78 13.00 6 0 -6 163.18 12.80 -6 0 6 177.98 12.80 -6 0 6 161.18 12.90 -6 0 6 169.08 12.80 5 0 -6 -1.00 0.60 -5 0 6 0.40 0.90 -5 0 6 0.40 1.00 -5 0 6 0.20 1.10 -5 0 6 0.60 0.70 -4 0 6 106.79 8.30 4 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202.68 15.60 7 -4 9 214.38 15.60 -7 -4 -9 208.48 15.60 -7 -4 -9 229.18 15.70 7 -4 9 210.48 15.40 -7 -4 -9 206.58 15.40 7 -4 9 205.08 15.60 7 -4 9 189.68 15.50 7 -4 9 185.58 15.30 7 4 9 176.08 15.40 7 4 9 218.68 15.70 -7 4 -9 201.58 15.50 -7 4 -9 196.58 15.40 7 4 9 208.48 15.60 -7 4 -9 206.38 15.50 7 4 9 211.58 15.60 -7 4 -9 181.18 15.40 7 4 9 207.58 15.60 8 -4 9 0.10 1.30 -8 -4 -9 0.90 1.50 -8 -4 -9 2.10 1.40 8 -4 9 0.00 1.40 8 -4 9 0.40 1.50 -8 -4 -9 -1.00 1.30 -8 -4 -9 -0.30 0.90 8 -4 9 -1.20 1.50 -8 4 -9 -1.20 1.10 8 4 9 -0.30 1.10 -8 4 -9 0.20 1.30 8 4 9 1.50 1.60 -8 4 -9 0.90 1.40 8 4 9 0.20 1.20 8 4 9 0.60 1.50 8 4 9 -0.60 1.40 8 4 9 1.70 1.50 9 -4 9 88.99 7.80 -9 -4 -9 92.09 7.90 9 -4 9 96.89 7.80 9 -4 9 103.49 7.80 -9 -4 -9 94.69 7.50 -9 -4 -9 95.99 7.80 9 -4 9 89.59 7.90 -9 -4 -9 93.99 7.90 9 4 9 97.19 7.80 9 4 9 103.89 7.80 9 4 9 97.99 7.90 -9 4 -9 94.09 7.60 -9 4 -9 90.49 7.70 -9 4 -9 96.09 7.80 9 4 9 89.99 7.90 9 4 9 99.09 7.80 10 -4 9 6.80 2.00 -10 -4 -9 5.60 1.40 -10 -4 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13.20 1.90 -9 5 9 15.30 1.90 -9 5 9 13.00 2.10 -9 5 9 13.70 1.90 -8 -5 9 62.19 5.90 -8 -5 9 78.59 6.10 -8 -5 9 74.99 6.30 8 -5 -9 62.69 6.00 -8 5 9 78.59 6.20 -8 5 9 77.09 6.10 -8 5 9 73.69 6.20 -8 5 9 79.29 6.00 -7 -5 9 32.70 3.50 7 -5 -9 35.60 3.60 -7 -5 9 37.80 3.20 -7 -5 9 37.80 3.70 -7 5 9 34.30 3.60 -7 5 9 32.80 3.40 -7 5 9 38.60 3.40 -7 5 9 36.60 3.10 -7 5 9 39.80 3.70 -6 -5 9 4.00 1.10 -6 -5 9 5.50 1.60 6 -5 -9 5.10 1.30 -6 -5 9 5.50 1.50 -6 5 9 5.20 1.00 -6 5 9 5.20 1.30 -6 5 9 5.80 1.50 -6 5 9 7.40 1.50 -6 5 9 4.10 1.50 -5 -5 9 230.98 17.20 5 -5 -9 224.88 17.20 -5 -5 9 238.78 17.30 -5 -5 9 202.48 17.00 -5 5 9 232.88 17.20 -5 5 9 235.98 17.20 -5 5 9 219.88 17.10 -5 5 9 218.58 17.00 -5 5 9 222.48 17.30 -4 -5 9 10.60 1.70 4 -5 -9 8.00 1.40 -4 -5 9 9.70 1.20 4 -5 -9 8.30 1.50 -4 -5 9 8.40 1.60 -4 5 9 8.40 1.50 -4 5 9 8.50 1.20 -4 5 9 9.30 1.70 -4 5 9 9.20 1.50 -4 5 9 9.60 1.70 -3 -5 9 105.29 8.50 3 -5 -9 115.19 8.60 -3 -5 9 117.69 8.70 3 -5 -9 119.29 8.80 -3 -5 9 119.89 8.70 -3 5 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11 12 10.10 2.30 1 11 12 7.10 2.40 1 11 12 5.80 1.80 -2 -11 -12 14.90 2.70 -2 -11 -12 16.90 2.40 2 -11 12 14.50 2.20 -2 -11 -12 17.30 2.30 2 11 12 17.10 2.50 2 11 12 15.80 2.80 2 11 12 14.00 2.50 2 11 12 15.70 2.60 2 11 12 14.50 2.50 -2 11 -12 15.00 2.10 -3 -11 -12 38.10 4.10 -3 -11 -12 36.70 4.00 3 -11 12 36.10 3.70 -3 -11 -12 38.10 3.50 3 11 12 36.20 4.10 -3 11 -12 39.10 3.70 3 11 12 28.10 3.80 3 11 12 42.10 3.70 3 11 12 31.70 4.00 3 11 12 29.50 3.60 -4 -11 -12 2.50 2.10 -4 -11 -12 0.20 1.70 -4 -11 -12 5.90 2.10 4 11 12 2.90 2.00 4 11 12 -0.30 2.10 4 11 12 3.20 1.90 4 11 12 2.00 2.00 -4 11 -12 2.80 1.70 4 11 12 4.60 2.30 -5 -11 -12 95.59 8.50 -5 -11 -12 111.19 9.10 -5 -11 -12 100.49 8.30 5 11 12 99.79 8.50 5 11 12 96.89 8.70 5 11 12 102.09 8.40 5 11 12 99.49 8.50 6 -11 12 18.80 2.50 -6 -11 -12 12.00 2.70 -6 -11 -12 14.10 2.50 -6 -11 -12 13.60 2.30 6 11 12 14.00 2.70 -6 11 -12 13.80 2.40 6 11 12 17.70 3.00 6 11 12 13.10 2.60 6 11 12 11.00 2.60 -7 -11 -12 16.10 2.40 -7 -11 -12 16.40 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-2.40 3.80 -6 -3 27 -7.10 3.40 -6 3 27 5.90 6.20 -6 3 27 -0.70 4.10 -5 -3 27 19.50 4.30 5 -3 -27 23.60 3.90 -5 -3 27 22.50 4.70 -5 3 27 14.30 4.20 -5 3 27 16.70 5.30 -4 -3 27 -3.90 4.30 -4 -3 27 -2.40 3.40 4 -3 -27 -2.40 2.90 -4 3 27 1.80 3.60 -4 3 27 1.60 4.10 3 -3 -27 3.20 3.00 -3 -3 27 1.70 3.50 -3 3 27 1.20 3.60 -3 3 27 6.70 4.30 2 -3 -27 4.70 3.50 -2 -3 27 0.00 3.40 -2 3 27 5.70 4.20 -2 3 27 1.40 3.60 2 3 -27 -2.00 2.80 -1 -3 27 19.80 4.40 1 -3 -27 19.90 3.80 1 3 -27 25.00 4.10 -1 3 27 30.10 5.10 -1 3 27 16.90 4.90 0 -3 -27 13.60 3.40 0 -3 27 12.60 4.20 0 -3 -27 11.80 3.80 0 3 27 18.00 4.60 0 3 27 12.60 4.10 0 3 -27 10.40 3.20 1 -3 27 3.90 3.50 -1 -3 -27 4.00 3.30 -1 -3 -27 0.50 3.40 1 3 27 8.10 4.60 -1 3 -27 0.90 4.40 1 3 27 10.20 3.80 -2 -3 -27 32.10 4.20 -2 -3 -27 29.90 5.00 2 3 27 19.30 4.60 2 3 27 28.20 5.30 -3 -3 -27 5.40 3.40 -3 -3 -27 3.10 3.00 3 3 27 7.60 4.10 3 3 27 5.60 4.70 -5 -4 27 1.70 3.60 5 -4 -27 6.70 3.40 -5 4 27 3.80 3.90 -5 4 27 4.20 4.40 -4 -4 27 -2.40 3.50 4 -4 -27 2.70 3.20 -4 4 27 2.20 3.80 -4 4 27 2.00 4.10 -3 -4 27 11.20 3.90 3 -4 -27 6.90 3.30 -3 4 27 4.30 3.80 -3 4 27 5.70 4.30 2 -4 -27 1.30 3.00 -2 -4 27 -1.20 3.40 -2 4 27 -8.00 3.40 -2 4 27 1.90 4.20 1 -4 -27 -3.90 3.70 1 -4 -27 2.00 3.30 -1 -4 27 -1.00 3.90 1 4 -27 -0.70 2.70 -1 4 27 2.60 4.20 -1 4 27 2.50 3.60 0 -4 -27 1.30 3.00 0 -4 -27 6.80 4.00 0 -4 27 5.70 3.60 0 4 27 6.60 4.10 0 4 -27 3.90 2.80 0 4 27 2.20 3.70 1 -4 27 11.00 4.70 -1 -4 -27 13.30 3.60 -1 -4 -27 13.20 4.00 1 4 27 13.00 5.10 1 4 27 11.40 4.10 -2 -4 -27 0.00 2.90 -2 -4 -27 2.10 3.40 2 4 27 4.20 3.70 2 4 27 5.30 4.20 -3 -4 -27 7.20 4.10 -3 -4 -27 8.00 3.40 3 4 27 10.20 3.80 3 4 27 10.10 4.30 4 -5 -27 17.20 4.40 -4 -5 27 10.80 4.30 -4 5 27 11.50 4.20 -4 5 27 12.20 4.40 -4 5 27 14.10 5.30 3 -5 -27 7.70 3.40 -3 -5 27 -0.60 4.00 -3 5 27 12.10 4.10 -3 5 27 9.50 4.10 -3 5 27 7.40 4.30 2 -5 -27 2.30 3.00 -2 -5 27 7.10 4.00 -2 5 27 4.90 3.70 -2 5 27 4.00 4.30 -2 5 27 1.30 3.70 1 -5 -27 0.90 4.00 1 -5 -27 2.20 3.40 -1 -5 27 3.30 3.50 -1 5 27 4.60 4.20 -1 5 27 1.20 3.70 -1 5 27 3.30 3.60 0 -5 -27 4.50 4.00 0 -5 -27 2.70 3.00 0 -5 27 3.60 3.50 0 5 27 1.50 4.70 0 5 27 6.10 4.30 0 5 -27 2.30 2.90 0 5 27 9.00 4.20 -1 -5 -27 2.30 3.60 -1 -5 -27 4.30 3.10 1 5 27 2.30 3.80 1 5 27 8.80 4.80 1 5 27 2.20 4.70 -2 -5 -27 1.30 3.60 -2 -5 -27 -0.30 2.90 2 5 27 0.50 4.10 2 5 27 5.00 4.30 -3 -6 27 3.90 3.60 -3 6 27 4.70 4.10 2 -6 -27 10.90 3.60 2 -6 -27 6.40 4.20 -2 -6 27 6.40 3.70 -2 6 27 12.80 4.20 -2 6 27 10.40 3.90 -2 6 27 6.00 4.30 1 -6 -27 -0.30 4.00 -1 -6 27 0.80 3.80 1 -6 -27 -2.30 2.90 -1 6 27 4.30 3.70 -1 6 27 1.30 4.10 -1 6 27 1.50 3.70 0 -6 27 -0.70 3.40 0 -6 -27 0.80 4.10 0 -6 -27 -2.60 3.20 0 6 27 -2.00 4.00 0 6 27 6.10 4.30 0 6 27 2.50 4.00 1 6 27 -2.20 3.60 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 5759 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.48229(2) 0.22418(2) 0.29952(2) 0.01695(5) Uani 1 1 d . . . . . N1 N 0.38390(7) 0.18729(7) 0.34188(6) 0.0206(2) Uani 1 1 d . . . . . N2 N 0.52335(6) 0.21890(6) 0.40161(6) 0.0184(2) Uani 1 1 d . . . . . N3 N 0.48267(7) 0.13779(6) 0.23895(6) 0.0190(2) Uani 1 1 d . . . . . N4 N 0.41986(7) 0.30336(7) 0.26367(7) 0.0218(2) Uani 1 1 d . . . . . N5 N 0.65200(7) 0.20777(7) 0.38883(7) 0.0251(3) Uani 1 1 d . . . . . N6 N 0.60854(7) 0.24865(7) 0.49873(7) 0.0246(3) Uani 1 1 d . . . . . N7 N 0.53838(8) 0.04751(7) 0.17067(7) 0.0233(2) Uani 1 1 d . . . . . N8 N 0.56684(7) 0.16308(7) 0.14753(7) 0.0234(2) Uani 1 1 d . . . . . N9 N 0.39700(8) 0.38162(7) 0.16511(8) 0.0303(3) Uani 1 1 d . . . . . N10 N 0.50442(8) 0.39128(7) 0.23941(7) 0.0265(3) Uani 1 1 d . . . . . B1 B 0.74279(9) 0.48882(9) 0.57464(9) 0.0227(3) Uani 1 1 d . . . . . B2 B 0.75864(9) 0.43340(9) 0.07910(9) 0.0205(3) Uani 1 1 d . . . . . C1 C 0.40325(8) 0.16155(8) 0.41727(7) 0.0218(3) Uani 1 1 d . . . . . H1A H 0.423424 0.113493 0.414768 0.026 Uiso 1 1 calc R U . . . H1B H 0.357721 0.160603 0.446984 0.026 Uiso 1 1 calc R U . . . C2 C 0.46160(8) 0.20979(8) 0.45292(8) 0.0216(3) Uani 1 1 d . . . . . H2A H 0.438695 0.255573 0.463775 0.026 Uiso 1 1 calc R U . . . H2B H 0.481070 0.189308 0.499687 0.026 Uiso 1 1 calc R U . . . C3 C 0.35837(8) 0.13163(8) 0.29046(8) 0.0244(3) Uani 1 1 d . . . . . H3A H 0.332044 0.152810 0.247240 0.029 Uiso 1 1 calc R U . . . H3B H 0.322643 0.100565 0.315137 0.029 Uiso 1 1 calc R U . . . C4 C 0.42481(8) 0.08934(8) 0.26543(8) 0.0229(3) Uani 1 1 d . . . . . H4A H 0.445679 0.061151 0.306833 0.027 Uiso 1 1 calc R U . . . H4B H 0.408614 0.057178 0.225405 0.027 Uiso 1 1 calc R U . . . C5 C 0.33097(9) 0.24709(9) 0.34232(9) 0.0288(3) Uani 1 1 d . . . . . H5A H 0.341874 0.276775 0.385894 0.035 Uiso 1 1 calc R U . . . H5B H 0.278858 0.229713 0.345085 0.035 Uiso 1 1 calc R U . . . C6 C 0.33920(8) 0.28964(9) 0.27266(10) 0.0309(4) Uani 1 1 d . . . . . H6A H 0.318433 0.263493 0.229723 0.037 Uiso 1 1 calc R U . . . H6B H 0.311512 0.334227 0.276409 0.037 Uiso 1 1 calc R U . . . C7 C 0.59289(8) 0.22538(7) 0.42941(8) 0.0194(2) Uani 1 1 d . . . . . C8 C 0.72042(11) 0.24922(13) 0.39228(13) 0.0495(6) Uani 1 1 d . . . . . H8A H 0.714580 0.287831 0.426951 0.074 Uiso 1 1 calc R U . . . H8B H 0.730143 0.267971 0.343400 0.074 Uiso 1 1 calc R U . . . H8C H 0.762601 0.219760 0.408805 0.074 Uiso 1 1 calc R U . . . C9 C 0.64590(9) 0.15955(10) 0.32760(9) 0.0300(3) Uani 1 1 d . . . . . H9A H 0.602806 0.128651 0.334005 0.045 Uiso 1 1 calc R U . . . H9B H 0.691814 0.131580 0.325705 0.045 Uiso 1 1 calc R U . . . H9C H 0.638970 0.185796 0.281666 0.045 Uiso 1 1 calc R U . . . C10 C 0.67231(10) 0.22256(10) 0.54298(10) 0.0356(4) Uani 1 1 d . . . . . H10A H 0.691091 0.179515 0.521033 0.053 Uiso 1 1 calc R U . . . H10B H 0.656402 0.212934 0.593022 0.053 Uiso 1 1 calc R U . . . H10C H 0.712235 0.257735 0.544591 0.053 Uiso 1 1 calc R U . . . C11 C 0.56569(10) 0.30434(9) 0.53226(9) 0.0319(4) Uani 1 1 d . . . . . H11A H 0.532222 0.325823 0.494967 0.048 Uiso 1 1 calc R U . . . H11B H 0.600181 0.339688 0.552670 0.048 Uiso 1 1 calc R U . . . H11C H 0.535852 0.284945 0.571681 0.048 Uiso 1 1 calc R U . . . C12 C 0.52819(8) 0.11586(8) 0.18768(7) 0.0193(3) Uani 1 1 d . . . . . C13 C 0.64301(9) 0.14875(10) 0.12369(10) 0.0323(4) Uani 1 1 d . . . . . H13A H 0.660800 0.104711 0.145392 0.048 Uiso 1 1 calc R U . . . H13B H 0.676438 0.186766 0.139767 0.048 Uiso 1 1 calc R U . . . H13C H 0.642727 0.145181 0.069969 0.048 Uiso 1 1 calc R U . . . C14 C 0.54502(11) 0.23574(9) 0.14351(10) 0.0328(4) Uani 1 1 d . . . . . H14A H 0.490288 0.239366 0.145231 0.049 Uiso 1 1 calc R U . . . H14B H 0.561927 0.255925 0.097423 0.049 Uiso 1 1 calc R U . . . H14C H 0.568048 0.261140 0.185168 0.049 Uiso 1 1 calc R U . . . C15 C 0.54729(10) 0.02433(9) 0.09491(8) 0.0292(3) Uani 1 1 d . . . . . H15A H 0.532141 0.061933 0.061073 0.044 Uiso 1 1 calc R U . . . H15B H 0.515764 -0.016770 0.085296 0.044 Uiso 1 1 calc R U . . . H15C H 0.599931 0.012301 0.087577 0.044 Uiso 1 1 calc R U . . . C16 C 0.54777(11) -0.00653(9) 0.22699(9) 0.0314(3) Uani 1 1 d . . . . . H16A H 0.555359 0.015476 0.275264 0.047 Uiso 1 1 calc R U . . . H16B H 0.591462 -0.035369 0.216251 0.047 Uiso 1 1 calc R U . . . H16C H 0.502781 -0.035892 0.227179 0.047 Uiso 1 1 calc R U . . . C17 C 0.43949(8) 0.35749(8) 0.22318(8) 0.0224(3) Uani 1 1 d . . . . . C18 C 0.55158(11) 0.41914(10) 0.18210(11) 0.0399(4) Uani 1 1 d . . . . . H18A H 0.530006 0.406563 0.133698 0.060 Uiso 1 1 calc R U . . . H18B H 0.602159 0.399465 0.187746 0.060 Uiso 1 1 calc R U . . . H18C H 0.554192 0.470081 0.186423 0.060 Uiso 1 1 calc R U . . . C19 C 0.53987(11) 0.38728(10) 0.31234(10) 0.0366(4) Uani 1 1 d . . . . . H19A H 0.501615 0.378388 0.348668 0.055 Uiso 1 1 calc R U . . . H19B H 0.565255 0.431506 0.323812 0.055 Uiso 1 1 calc R U . . . H19C H 0.576634 0.349239 0.313707 0.055 Uiso 1 1 calc R U . . . C20 C 0.39311(14) 0.45505(11) 0.14415(13) 0.0503(6) Uani 1 1 d . . . . . H20A H 0.419194 0.483370 0.181817 0.075 Uiso 1 1 calc R U . . . H20B H 0.340476 0.469588 0.139636 0.075 Uiso 1 1 calc R U . . . H20C H 0.417041 0.461538 0.096902 0.075 Uiso 1 1 calc R U . . . C21 C 0.35295(12) 0.33513(11) 0.11741(10) 0.0427(5) Uani 1 1 d . . . . . H21A H 0.366994 0.286617 0.127986 0.064 Uiso 1 1 calc R U . . . H21B H 0.362729 0.345796 0.065933 0.064 Uiso 1 1 calc R U . . . H21C H 0.299485 0.341686 0.126212 0.064 Uiso 1 1 calc R U . . . C22 C 0.69111(8) 0.44267(8) 0.63071(8) 0.0236(3) Uani 1 1 d . . . . . C23 C 0.71129(9) 0.37625(9) 0.65705(8) 0.0272(3) Uani 1 1 d . . . . . H23 H 0.756612 0.356025 0.641114 0.033 Uiso 1 1 calc R U . . . C24 C 0.66785(10) 0.33852(10) 0.70558(9) 0.0333(4) Uani 1 1 d . . . . . H24 H 0.684507 0.294214 0.722924 0.040 Uiso 1 1 calc R U . . . C25 C 0.60042(10) 0.36558(11) 0.72853(9) 0.0362(4) Uani 1 1 d . . . . . H25 H 0.570286 0.339993 0.761168 0.043 Uiso 1 1 calc R U . . . C26 C 0.57783(10) 0.43049(11) 0.70305(9) 0.0349(4) Uani 1 1 d . . . . . H26 H 0.531293 0.449354 0.717498 0.042 Uiso 1 1 calc R U . . . C27 C 0.62290(9) 0.46839(10) 0.65634(9) 0.0305(3) Uani 1 1 d . . . . . H27 H 0.606851 0.513565 0.641127 0.037 Uiso 1 1 calc R U . . . C28 C 0.79229(9) 0.43725(8) 0.52192(8) 0.0241(3) Uani 1 1 d . . . . . C29 C 0.77668(9) 0.42737(9) 0.44647(8) 0.0271(3) Uani 1 1 d . . . . . H29 H 0.734790 0.450878 0.424446 0.033 Uiso 1 1 calc R U . . . C30 C 0.81984(10) 0.38466(9) 0.40247(9) 0.0326(4) Uani 1 1 d . . . . . H30 H 0.807549 0.380576 0.351472 0.039 Uiso 1 1 calc R U . . . C31 C 0.88017(10) 0.34830(9) 0.43224(10) 0.0340(4) Uani 1 1 d . . . . . H31 H 0.908830 0.318201 0.402596 0.041 Uiso 1 1 calc R U . . . C32 C 0.89814(10) 0.35662(10) 0.50652(10) 0.0343(4) Uani 1 1 d . . . . . H32 H 0.939645 0.332153 0.528050 0.041 Uiso 1 1 calc R U . . . C33 C 0.85573(9) 0.40057(9) 0.54953(9) 0.0291(3) Uani 1 1 d . . . . . H33 H 0.870127 0.406165 0.599895 0.035 Uiso 1 1 calc R U . . . C34 C 0.68777(8) 0.53786(8) 0.52139(8) 0.0241(3) Uani 1 1 d . . . . . C35 C 0.62110(9) 0.51065(9) 0.48912(9) 0.0297(3) Uani 1 1 d . . . . . H35 H 0.606592 0.464511 0.501498 0.036 Uiso 1 1 calc R U . . . C36 C 0.57554(9) 0.54840(10) 0.43989(9) 0.0326(4) Uani 1 1 d . . . . . H36 H 0.530804 0.528014 0.419939 0.039 Uiso 1 1 calc R U . . . C37 C 0.59513(9) 0.61531(10) 0.41996(9) 0.0311(4) Uani 1 1 d . . . . . H37 H 0.564704 0.640846 0.385630 0.037 Uiso 1 1 calc R U . . . C38 C 0.65987(10) 0.64475(9) 0.45078(9) 0.0307(3) Uani 1 1 d . . . . . H38 H 0.673948 0.690834 0.437755 0.037 Uiso 1 1 calc R U . . . C39 C 0.70427(9) 0.60669(9) 0.50088(9) 0.0268(3) Uani 1 1 d . . . . . H39 H 0.747708 0.628332 0.522131 0.032 Uiso 1 1 calc R U . . . C40 C 0.80036(8) 0.54039(8) 0.62189(8) 0.0219(3) Uani 1 1 d . . . . . C41 C 0.86310(9) 0.57001(9) 0.58866(9) 0.0281(3) Uani 1 1 d . . . . . H41 H 0.875190 0.554770 0.540795 0.034 Uiso 1 1 calc R U . . . C42 C 0.90825(9) 0.62058(9) 0.62269(10) 0.0303(3) Uani 1 1 d . . . . . H42 H 0.949626 0.639448 0.597759 0.036 Uiso 1 1 calc R U . . . C43 C 0.89290(9) 0.64345(9) 0.69290(9) 0.0294(3) Uani 1 1 d . . . . . H43 H 0.922929 0.678474 0.716210 0.035 Uiso 1 1 calc R U . . . C44 C 0.83310(9) 0.61433(8) 0.72829(9) 0.0275(3) Uani 1 1 d . . . . . H44 H 0.822493 0.628793 0.776787 0.033 Uiso 1 1 calc R U . . . C45 C 0.78796(9) 0.56368(8) 0.69336(8) 0.0238(3) Uani 1 1 d . . . . . H45 H 0.747377 0.544394 0.719160 0.029 Uiso 1 1 calc R U . . . C46 C 0.72442(8) 0.49084(8) 0.13660(8) 0.0205(3) Uani 1 1 d . . . . . C47 C 0.68470(9) 0.54989(8) 0.11005(9) 0.0255(3) Uani 1 1 d . . . . . H47 H 0.680733 0.557213 0.058448 0.031 Uiso 1 1 calc R U . . . C48 C 0.65111(9) 0.59784(9) 0.15602(10) 0.0305(3) Uani 1 1 d . . . . . H48 H 0.623477 0.635939 0.135555 0.037 Uiso 1 1 calc R U . . . C49 C 0.65791(10) 0.59012(9) 0.23160(10) 0.0330(4) Uani 1 1 d . . . . . H49 H 0.634378 0.622242 0.263262 0.040 Uiso 1 1 calc R U . . . C50 C 0.69942(10) 0.53498(9) 0.26033(9) 0.0303(3) Uani 1 1 d . . . . . H50 H 0.706004 0.530014 0.312068 0.036 Uiso 1 1 calc R U . . . C51 C 0.73171(9) 0.48657(8) 0.21343(8) 0.0239(3) Uani 1 1 d . . . . . H51 H 0.759851 0.449088 0.234515 0.029 Uiso 1 1 calc R U . . . C52 C 0.69101(9) 0.38996(8) 0.03380(8) 0.0234(3) Uani 1 1 d . . . . . C53 C 0.70418(10) 0.32287(9) 0.00572(9) 0.0286(3) Uani 1 1 d . . . . . H53 H 0.751174 0.301403 0.016969 0.034 Uiso 1 1 calc R U . . . C54 C 0.65192(11) 0.28626(10) -0.03772(10) 0.0365(4) Uani 1 1 d . . . . . H54 H 0.663739 0.241076 -0.055469 0.044 Uiso 1 1 calc R U . . . C55 C 0.58287(12) 0.31569(11) -0.05498(10) 0.0405(4) Uani 1 1 d . . . . . H55 H 0.546965 0.291152 -0.084754 0.049 Uiso 1 1 calc R U . . . C56 C 0.56680(11) 0.38146(11) -0.02824(10) 0.0387(4) Uani 1 1 d . . . . . H56 H 0.519404 0.402187 -0.039414 0.046 Uiso 1 1 calc R U . . . C57 C 0.62006(10) 0.41756(9) 0.01519(9) 0.0299(3) Uani 1 1 d . . . . . H57 H 0.607665 0.462648 0.032811 0.036 Uiso 1 1 calc R U . . . C58 C 0.80639(8) 0.47828(7) 0.01981(8) 0.0203(3) Uani 1 1 d . . . . . C59 C 0.78938(9) 0.48126(8) -0.05559(8) 0.0227(3) Uani 1 1 d . . . . . H59 H 0.746997 0.456191 -0.074397 0.027 Uiso 1 1 calc R U . . . C60 C 0.83195(10) 0.51946(8) -0.10445(9) 0.0289(3) Uani 1 1 d . . . . . H60 H 0.817272 0.521100 -0.155057 0.035 Uiso 1 1 calc R U . . . C61 C 0.89517(10) 0.55484(9) -0.07977(10) 0.0327(4) Uani 1 1 d . . . . . H61 H 0.925504 0.579186 -0.113249 0.039 Uiso 1 1 calc R U . . . C62 C 0.91375(10) 0.55426(9) -0.00491(10) 0.0325(4) Uani 1 1 d . . . . . H62 H 0.956857 0.578697 0.013205 0.039 Uiso 1 1 calc R U . . . C63 C 0.86930(9) 0.51800(8) 0.04318(9) 0.0268(3) Uani 1 1 d . . . . . H63 H 0.881812 0.519993 0.094266 0.032 Uiso 1 1 calc R U . . . C64 C 0.81231(8) 0.37631(8) 0.12396(8) 0.0215(3) Uani 1 1 d . . . . . C65 C 0.89053(9) 0.37200(8) 0.12073(8) 0.0246(3) Uani 1 1 d . . . . . H65 H 0.915681 0.403383 0.089482 0.030 Uiso 1 1 calc R U . . . C66 C 0.93324(10) 0.32357(9) 0.16147(9) 0.0303(3) Uani 1 1 d . . . . . H66 H 0.986270 0.323086 0.157979 0.036 Uiso 1 1 calc R U . . . C67 C 0.89859(11) 0.27630(9) 0.20689(9) 0.0322(3) Uani 1 1 d . . . . . H67 H 0.927423 0.243624 0.235073 0.039 Uiso 1 1 calc R U . . . C68 C 0.82137(11) 0.27752(9) 0.21046(9) 0.0331(4) Uani 1 1 d . . . . . H68 H 0.796634 0.244743 0.240466 0.040 Uiso 1 1 calc R U . . . C69 C 0.77965(10) 0.32657(8) 0.17028(9) 0.0286(3) Uani 1 1 d . . . . . H69 H 0.726661 0.326551 0.174248 0.034 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.01521(8) 0.01853(9) 0.01720(8) 0.00150(7) 0.00186(6) 0.00012(7) N1 0.0175(5) 0.0253(6) 0.0191(5) 0.0023(4) 0.0011(4) -0.0004(5) N2 0.0162(5) 0.0210(6) 0.0180(5) 0.0004(4) 0.0017(4) -0.0005(4) N3 0.0193(5) 0.0211(6) 0.0167(5) 0.0000(4) 0.0027(4) -0.0032(4) N4 0.0157(5) 0.0236(6) 0.0262(6) 0.0038(5) 0.0017(4) 0.0018(5) N5 0.0166(6) 0.0285(7) 0.0303(6) -0.0054(5) 0.0029(5) -0.0041(5) N6 0.0233(6) 0.0244(6) 0.0257(6) -0.0048(5) -0.0050(5) 0.0020(5) N7 0.0314(7) 0.0194(6) 0.0192(5) -0.0007(4) 0.0021(5) 0.0016(5) N8 0.0248(6) 0.0214(6) 0.0244(6) 0.0008(5) 0.0087(5) 0.0003(5) N9 0.0352(7) 0.0268(7) 0.0282(7) 0.0066(5) -0.0086(5) 0.0003(6) N10 0.0262(6) 0.0231(6) 0.0300(7) 0.0036(5) -0.0023(5) -0.0030(5) B1 0.0203(7) 0.0273(8) 0.0205(7) -0.0004(6) -0.0008(6) -0.0033(6) B2 0.0230(7) 0.0198(7) 0.0191(7) 0.0008(5) 0.0041(5) -0.0001(6) C1 0.0196(6) 0.0291(8) 0.0168(6) 0.0020(5) 0.0042(5) -0.0032(5) C2 0.0200(6) 0.0274(7) 0.0178(6) -0.0022(5) 0.0044(5) -0.0016(5) C3 0.0206(7) 0.0320(8) 0.0205(6) 0.0016(5) 0.0004(5) -0.0085(6) C4 0.0255(7) 0.0245(7) 0.0187(6) 0.0011(5) 0.0024(5) -0.0084(6) C5 0.0168(7) 0.0351(9) 0.0350(8) 0.0055(7) 0.0061(6) 0.0037(6) C6 0.0158(7) 0.0360(9) 0.0410(9) 0.0113(7) 0.0015(6) 0.0033(6) C7 0.0203(6) 0.0166(6) 0.0214(6) 0.0003(5) -0.0005(5) -0.0011(5) C8 0.0269(9) 0.0583(13) 0.0641(14) -0.0219(11) 0.0142(9) -0.0213(9) C9 0.0219(7) 0.0384(9) 0.0299(8) -0.0100(7) 0.0024(6) 0.0006(6) C10 0.0323(9) 0.0348(9) 0.0385(9) -0.0041(7) -0.0157(7) 0.0041(7) C11 0.0350(9) 0.0293(8) 0.0309(8) -0.0112(6) -0.0053(6) 0.0046(7) C12 0.0198(6) 0.0209(7) 0.0172(6) 0.0003(5) 0.0001(5) -0.0004(5) C13 0.0262(8) 0.0351(9) 0.0363(9) -0.0016(7) 0.0128(6) -0.0018(7) C14 0.0405(9) 0.0247(8) 0.0343(8) 0.0070(6) 0.0158(7) 0.0034(7) C15 0.0366(9) 0.0275(8) 0.0238(7) -0.0055(6) 0.0040(6) 0.0037(7) C16 0.0428(10) 0.0221(8) 0.0291(8) 0.0041(6) -0.0031(7) 0.0012(7) C17 0.0231(7) 0.0208(7) 0.0232(7) -0.0001(5) -0.0009(5) 0.0030(5) C18 0.0394(10) 0.0335(10) 0.0474(11) 0.0087(8) 0.0086(8) -0.0101(8) C19 0.0371(9) 0.0310(9) 0.0407(10) 0.0025(7) -0.0144(7) -0.0055(7) C20 0.0640(14) 0.0316(10) 0.0538(12) 0.0165(9) -0.0204(11) 0.0043(9) C21 0.0475(11) 0.0462(11) 0.0333(9) 0.0032(8) -0.0150(8) -0.0074(9) C22 0.0224(7) 0.0298(8) 0.0184(6) -0.0019(5) -0.0030(5) -0.0057(6) C23 0.0242(7) 0.0346(9) 0.0223(7) 0.0028(6) -0.0054(5) -0.0037(6) C24 0.0328(9) 0.0406(10) 0.0260(8) 0.0098(7) -0.0065(6) -0.0071(7) C25 0.0344(9) 0.0509(11) 0.0231(7) 0.0075(7) 0.0002(6) -0.0146(8) C26 0.0272(8) 0.0495(11) 0.0285(8) -0.0007(7) 0.0063(6) -0.0039(7) C27 0.0280(8) 0.0348(9) 0.0290(8) -0.0004(6) 0.0039(6) -0.0017(7) C28 0.0245(7) 0.0247(7) 0.0231(7) -0.0012(5) 0.0015(5) -0.0063(6) C29 0.0303(8) 0.0270(8) 0.0240(7) -0.0009(6) 0.0021(6) -0.0080(6) C30 0.0412(9) 0.0318(9) 0.0253(7) -0.0070(6) 0.0075(6) -0.0153(7) C31 0.0329(9) 0.0283(8) 0.0415(9) -0.0111(7) 0.0133(7) -0.0109(7) C32 0.0280(8) 0.0324(9) 0.0428(10) -0.0064(7) 0.0037(7) -0.0014(7) C33 0.0261(8) 0.0327(9) 0.0285(8) -0.0037(6) -0.0007(6) -0.0017(6) C34 0.0220(7) 0.0296(8) 0.0207(6) -0.0008(5) 0.0010(5) -0.0010(6) C35 0.0263(8) 0.0339(9) 0.0287(8) 0.0025(6) -0.0040(6) -0.0053(6) C36 0.0236(8) 0.0460(10) 0.0279(8) -0.0013(7) -0.0025(6) 0.0011(7) C37 0.0285(8) 0.0413(10) 0.0236(7) 0.0021(6) 0.0026(6) 0.0128(7) C38 0.0315(8) 0.0300(8) 0.0308(8) 0.0037(6) 0.0052(6) 0.0047(7) C39 0.0249(7) 0.0292(8) 0.0263(7) -0.0006(6) 0.0023(6) -0.0010(6) C40 0.0202(6) 0.0234(7) 0.0221(6) -0.0002(5) -0.0019(5) 0.0009(5) C41 0.0254(7) 0.0318(8) 0.0271(7) -0.0024(6) 0.0026(6) -0.0039(6) C42 0.0220(7) 0.0298(8) 0.0392(9) 0.0008(7) 0.0003(6) -0.0045(6) C43 0.0278(8) 0.0237(8) 0.0358(8) -0.0019(6) -0.0106(6) -0.0009(6) C44 0.0319(8) 0.0255(8) 0.0248(7) -0.0034(6) -0.0056(6) 0.0039(6) C45 0.0243(7) 0.0251(7) 0.0219(6) -0.0002(5) 0.0000(5) 0.0007(6) C46 0.0193(6) 0.0207(7) 0.0218(6) -0.0011(5) 0.0048(5) -0.0016(5) C47 0.0265(7) 0.0231(7) 0.0272(7) 0.0010(6) 0.0039(6) 0.0010(6) C48 0.0274(8) 0.0221(8) 0.0422(9) -0.0009(6) 0.0072(7) 0.0028(6) C49 0.0336(9) 0.0266(8) 0.0398(9) -0.0099(7) 0.0145(7) -0.0026(7) C50 0.0360(9) 0.0306(8) 0.0247(7) -0.0060(6) 0.0068(6) -0.0039(7) C51 0.0246(7) 0.0247(7) 0.0227(7) -0.0016(5) 0.0031(5) -0.0009(6) C52 0.0271(7) 0.0242(7) 0.0192(6) 0.0016(5) 0.0053(5) -0.0048(6) C53 0.0312(8) 0.0265(8) 0.0286(8) -0.0037(6) 0.0080(6) -0.0069(6) C54 0.0451(10) 0.0340(9) 0.0307(8) -0.0070(7) 0.0074(7) -0.0134(8) C55 0.0464(11) 0.0457(11) 0.0290(8) -0.0027(7) -0.0034(7) -0.0182(9) C56 0.0332(9) 0.0465(11) 0.0357(9) 0.0033(8) -0.0074(7) -0.0061(8) C57 0.0317(8) 0.0307(8) 0.0270(7) 0.0014(6) -0.0013(6) -0.0014(7) C58 0.0230(7) 0.0168(6) 0.0213(6) 0.0005(5) 0.0047(5) 0.0031(5) C59 0.0263(7) 0.0200(7) 0.0221(6) 0.0021(5) 0.0034(5) 0.0022(5) C60 0.0408(9) 0.0233(7) 0.0231(7) 0.0040(6) 0.0079(6) 0.0023(7) C61 0.0379(9) 0.0238(8) 0.0374(9) 0.0074(6) 0.0152(7) -0.0015(7) C62 0.0301(8) 0.0243(8) 0.0432(9) 0.0044(7) 0.0024(7) -0.0058(6) C63 0.0307(8) 0.0231(7) 0.0265(7) 0.0007(6) 0.0001(6) -0.0025(6) C64 0.0270(7) 0.0193(7) 0.0183(6) -0.0010(5) 0.0038(5) 0.0013(5) C65 0.0285(7) 0.0232(7) 0.0223(7) 0.0018(5) 0.0014(5) -0.0006(6) C66 0.0294(8) 0.0291(8) 0.0321(8) 0.0011(6) -0.0037(6) 0.0022(6) C67 0.0431(10) 0.0262(8) 0.0270(8) 0.0032(6) -0.0029(7) 0.0060(7) C68 0.0466(10) 0.0237(8) 0.0294(8) 0.0075(6) 0.0096(7) 0.0038(7) C69 0.0319(8) 0.0244(8) 0.0301(8) 0.0045(6) 0.0102(6) 0.0034(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 Co1 N4 122.42(5) . . ? N2 Co1 N3 118.06(5) . . ? N4 Co1 N3 117.83(5) . . ? N2 Co1 N1 85.71(5) . . ? N4 Co1 N1 84.81(5) . . ? N3 Co1 N1 86.56(5) . . ? C3 N1 C5 112.11(12) . . ? C3 N1 C1 113.68(12) . . ? C5 N1 C1 112.30(12) . . ? C3 N1 Co1 104.97(9) . . ? C5 N1 Co1 106.63(9) . . ? C1 N1 Co1 106.45(8) . . ? C7 N2 C2 118.39(11) . . ? C7 N2 Co1 131.70(10) . . ? C2 N2 Co1 109.81(8) . . ? C12 N3 C4 118.67(12) . . ? C12 N3 Co1 131.87(10) . . ? C4 N3 Co1 109.07(9) . . ? C17 N4 C6 118.44(12) . . ? C17 N4 Co1 128.81(10) . . ? C6 N4 Co1 111.52(10) . . ? C7 N5 C9 122.66(12) . . ? C7 N5 C8 120.58(14) . . ? C9 N5 C8 115.03(14) . . ? C7 N6 C11 122.28(13) . . ? C7 N6 C10 122.21(13) . . ? C11 N6 C10 115.41(13) . . ? C12 N7 C15 121.79(13) . . ? C12 N7 C16 122.37(12) . . ? C15 N7 C16 115.62(13) . . ? C12 N8 C14 121.70(13) . . ? C12 N8 C13 121.58(13) . . ? C14 N8 C13 114.58(13) . . ? C17 N9 C21 122.10(14) . . ? C17 N9 C20 123.44(15) . . ? C21 N9 C20 114.44(14) . . ? C17 N10 C19 121.27(14) . . ? C17 N10 C18 121.85(14) . . ? C19 N10 C18 115.31(14) . . ? C40 B1 C34 108.31(13) . . ? C40 B1 C28 109.04(12) . . ? C34 B1 C28 108.54(12) . . ? C40 B1 C22 110.43(12) . . ? C34 B1 C22 109.52(12) . . ? C28 B1 C22 110.95(13) . . ? C58 B2 C46 106.15(12) . . ? C58 B2 C64 111.57(12) . . ? C46 B2 C64 110.39(11) . . ? C58 B2 C52 108.66(11) . . ? C46 B2 C52 111.81(12) . . ? C64 B2 C52 108.27(12) . . ? N1 C1 C2 109.10(12) . . ? N1 C1 H1A 109.9 . . ? C2 C1 H1A 109.9 . . ? N1 C1 H1B 109.9 . . ? C2 C1 H1B 109.9 . . ? H1A C1 H1B 108.3 . . ? N2 C2 C1 108.40(11) . . ? N2 C2 H2A 110.0 . . ? C1 C2 H2A 110.0 . . ? N2 C2 H2B 110.0 . . ? C1 C2 H2B 110.0 . . ? H2A C2 H2B 108.4 . . ? N1 C3 C4 110.30(11) . . ? N1 C3 H3A 109.6 . . ? C4 C3 H3A 109.6 . . ? N1 C3 H3B 109.6 . . ? C4 C3 H3B 109.6 . . ? H3A C3 H3B 108.1 . . ? N3 C4 C3 108.80(12) . . ? N3 C4 H4A 109.9 . . ? C3 C4 H4A 109.9 . . ? N3 C4 H4B 109.9 . . ? C3 C4 H4B 109.9 . . ? H4A C4 H4B 108.3 . . ? N1 C5 C6 109.35(13) . . ? N1 C5 H5A 109.8 . . ? C6 C5 H5A 109.8 . . ? N1 C5 H5B 109.8 . . ? C6 C5 H5B 109.8 . . ? H5A C5 H5B 108.3 . . ? N4 C6 C5 107.97(12) . . ? N4 C6 H6A 110.1 . . ? C5 C6 H6A 110.1 . . ? N4 C6 H6B 110.1 . . ? C5 C6 H6B 110.1 . . ? H6A C6 H6B 108.4 . . ? N2 C7 N5 120.26(13) . . ? N2 C7 N6 123.04(13) . . ? N5 C7 N6 116.70(13) . . ? N5 C8 H8A 109.5 . . ? N5 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? N5 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? N5 C9 H9A 109.5 . . ? N5 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? N5 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? N6 C10 H10A 109.5 . . ? N6 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? N6 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? N6 C11 H11A 109.5 . . ? N6 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? N6 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? N3 C12 N7 123.74(13) . . ? N3 C12 N8 119.92(13) . . ? N7 C12 N8 116.32(13) . . ? N8 C13 H13A 109.5 . . ? N8 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? N8 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? N8 C14 H14A 109.5 . . ? N8 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? N8 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? N7 C15 H15A 109.5 . . ? N7 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? N7 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? N7 C16 H16A 109.5 . . ? N7 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? N7 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? N4 C17 N10 119.52(13) . . ? N4 C17 N9 123.15(14) . . ? N10 C17 N9 117.32(14) . . ? N10 C18 H18A 109.5 . . ? N10 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? N10 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? N10 C19 H19A 109.5 . . ? N10 C19 H19B 109.5 . . ? H19A C19 H19B 109.5 . . ? N10 C19 H19C 109.5 . . ? H19A C19 H19C 109.5 . . ? H19B C19 H19C 109.5 . . ? N9 C20 H20A 109.5 . . ? N9 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? N9 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? N9 C21 H21A 109.5 . . ? N9 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? N9 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C23 C22 C27 114.82(15) . . ? C23 C22 B1 123.65(14) . . ? C27 C22 B1 121.52(14) . . ? C24 C23 C22 123.00(16) . . ? C24 C23 H23 118.5 . . ? C22 C23 H23 118.5 . . ? C25 C24 C23 120.12(17) . . ? C25 C24 H24 119.9 . . ? C23 C24 H24 119.9 . . ? C26 C25 C24 118.79(16) . . ? C26 C25 H25 120.6 . . ? C24 C25 H25 120.6 . . ? C25 C26 C27 120.39(17) . . ? C25 C26 H26 119.8 . . ? C27 C26 H26 119.8 . . ? C26 C27 C22 122.84(17) . . ? C26 C27 H27 118.6 . . ? C22 C27 H27 118.6 . . ? C29 C28 C33 114.37(15) . . ? C29 C28 B1 123.73(14) . . ? C33 C28 B1 121.88(13) . . ? C30 C29 C28 123.01(16) . . ? C30 C29 H29 118.5 . . ? C28 C29 H29 118.5 . . ? C31 C30 C29 120.61(16) . . ? C31 C30 H30 119.7 . . ? C29 C30 H30 119.7 . . ? C30 C31 C32 118.55(16) . . ? C30 C31 H31 120.7 . . ? C32 C31 H31 120.7 . . ? C31 C32 C33 120.33(17) . . ? C31 C32 H32 119.8 . . ? C33 C32 H32 119.8 . . ? C32 C33 C28 123.08(15) . . ? C32 C33 H33 118.5 . . ? C28 C33 H33 118.5 . . ? C39 C34 C35 114.70(14) . . ? C39 C34 B1 124.40(13) . . ? C35 C34 B1 120.80(14) . . ? C36 C35 C34 122.89(16) . . ? C36 C35 H35 118.6 . . ? C34 C35 H35 118.6 . . ? C37 C36 C35 120.27(16) . . ? C37 C36 H36 119.9 . . ? C35 C36 H36 119.9 . . ? C36 C37 C38 119.06(15) . . ? C36 C37 H37 120.5 . . ? C38 C37 H37 120.5 . . ? C37 C38 C39 119.99(16) . . ? C37 C38 H38 120.0 . . ? C39 C38 H38 120.0 . . ? C38 C39 C34 123.06(15) . . ? C38 C39 H39 118.5 . . ? C34 C39 H39 118.5 . . ? C45 C40 C41 114.97(14) . . ? C45 C40 B1 124.20(13) . . ? C41 C40 B1 120.53(13) . . ? C42 C41 C40 123.05(15) . . ? C42 C41 H41 118.5 . . ? C40 C41 H41 118.5 . . ? C43 C42 C41 120.10(16) . . ? C43 C42 H42 119.9 . . ? C41 C42 H42 119.9 . . ? C44 C43 C42 118.71(15) . . ? C44 C43 H43 120.6 . . ? C42 C43 H43 120.6 . . ? C43 C44 C45 120.63(15) . . ? C43 C44 H44 119.7 . . ? C45 C44 H44 119.7 . . ? C40 C45 C44 122.49(15) . . ? C40 C45 H45 118.8 . . ? C44 C45 H45 118.8 . . ? C51 C46 C47 114.66(13) . . ? C51 C46 B2 124.71(13) . . ? C47 C46 B2 120.62(13) . . ? C48 C47 C46 122.98(15) . . ? C48 C47 H47 118.5 . . ? C46 C47 H47 118.5 . . ? C49 C48 C47 120.07(16) . . ? C49 C48 H48 120.0 . . ? C47 C48 H48 120.0 . . ? C50 C49 C48 119.08(15) . . ? C50 C49 H49 120.5 . . ? C48 C49 H49 120.5 . . ? C49 C50 C51 120.14(15) . . ? C49 C50 H50 119.9 . . ? C51 C50 H50 119.9 . . ? C50 C51 C46 122.93(15) . . ? C50 C51 H51 118.5 . . ? C46 C51 H51 118.5 . . ? C57 C52 C53 114.63(14) . . ? C57 C52 B2 124.45(14) . . ? C53 C52 B2 120.73(14) . . ? C54 C53 C52 123.39(17) . . ? C54 C53 H53 118.3 . . ? C52 C53 H53 118.3 . . ? C55 C54 C53 119.95(18) . . ? C55 C54 H54 120.0 . . ? C53 C54 H54 120.0 . . ? C54 C55 C56 118.99(17) . . ? C54 C55 H55 120.5 . . ? C56 C55 H55 120.5 . . ? C55 C56 C57 120.27(18) . . ? C55 C56 H56 119.9 . . ? C57 C56 H56 119.9 . . ? C56 C57 C52 122.76(17) . . ? C56 C57 H57 118.6 . . ? C52 C57 H57 118.6 . . ? C59 C58 C63 114.83(13) . . ? C59 C58 B2 124.53(13) . . ? C63 C58 B2 120.64(13) . . ? C60 C59 C58 122.82(15) . . ? C60 C59 H59 118.6 . . ? C58 C59 H59 118.6 . . ? C61 C60 C59 120.43(15) . . ? C61 C60 H60 119.8 . . ? C59 C60 H60 119.8 . . ? C60 C61 C62 118.80(15) . . ? C60 C61 H61 120.6 . . ? C62 C61 H61 120.6 . . ? C63 C62 C61 119.93(16) . . ? C63 C62 H62 120.0 . . ? C61 C62 H62 120.0 . . ? C62 C63 C58 123.07(15) . . ? C62 C63 H63 118.5 . . ? C58 C63 H63 118.5 . . ? C65 C64 C69 114.59(14) . . ? C65 C64 B2 125.48(13) . . ? C69 C64 B2 119.93(13) . . ? C66 C65 C64 122.91(15) . . ? C66 C65 H65 118.5 . . ? C64 C65 H65 118.5 . . ? C67 C66 C65 120.30(16) . . ? C67 C66 H66 119.8 . . ? C65 C66 H66 119.8 . . ? C68 C67 C66 118.80(15) . . ? C68 C67 H67 120.6 . . ? C66 C67 H67 120.6 . . ? C67 C68 C69 120.26(16) . . ? C67 C68 H68 119.9 . . ? C69 C68 H68 119.9 . . ? C68 C69 C64 123.10(16) . . ? C68 C69 H69 118.4 . . ? C64 C69 H69 118.4 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Co1 N2 1.9779(11) . ? Co1 N4 1.9798(12) . ? Co1 N3 1.9886(12) . ? Co1 N1 2.0639(12) . ? N1 C3 1.4810(19) . ? N1 C5 1.485(2) . ? N1 C1 1.4881(18) . ? N2 C7 1.3301(17) . ? N2 C2 1.4769(18) . ? N3 C12 1.3246(18) . ? N3 C4 1.4799(18) . ? N4 C17 1.3257(19) . ? N4 C6 1.4767(19) . ? N5 C7 1.3491(19) . ? N5 C9 1.449(2) . ? N5 C8 1.456(2) . ? N6 C7 1.3587(18) . ? N6 C11 1.457(2) . ? N6 C10 1.461(2) . ? N7 C12 1.3590(19) . ? N7 C15 1.4621(19) . ? N7 C16 1.463(2) . ? N8 C12 1.3637(19) . ? N8 C14 1.446(2) . ? N8 C13 1.465(2) . ? N9 C17 1.3615(18) . ? N9 C21 1.456(2) . ? N9 C20 1.459(2) . ? N10 C17 1.3511(19) . ? N10 C19 1.454(2) . ? N10 C18 1.462(2) . ? B1 C40 1.647(2) . ? B1 C34 1.651(2) . ? B1 C28 1.652(2) . ? B1 C22 1.653(2) . ? B2 C58 1.639(2) . ? B2 C46 1.649(2) . ? B2 C64 1.652(2) . ? B2 C52 1.662(2) . ? C1 C2 1.522(2) . ? C1 H1A 0.9900 . ? C1 H1B 0.9900 . ? C2 H2A 0.9900 . ? C2 H2B 0.9900 . ? C3 C4 1.517(2) . ? C3 H3A 0.9900 . ? C3 H3B 0.9900 . ? C4 H4A 0.9900 . ? C4 H4B 0.9900 . ? C5 C6 1.518(2) . ? C5 H5A 0.9900 . ? C5 H5B 0.9900 . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C8 H8A 0.9800 . ? C8 H8B 0.9800 . ? C8 H8C 0.9800 . ? C9 H9A 0.9800 . ? C9 H9B 0.9800 . ? C9 H9C 0.9800 . ? C10 H10A 0.9800 . ? C10 H10B 0.9800 . ? C10 H10C 0.9800 . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C13 H13A 0.9800 . ? C13 H13B 0.9800 . ? C13 H13C 0.9800 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C18 H18A 0.9800 . ? C18 H18B 0.9800 . ? C18 H18C 0.9800 . ? C19 H19A 0.9800 . ? C19 H19B 0.9800 . ? C19 H19C 0.9800 . ? C20 H20A 0.9800 . ? C20 H20B 0.9800 . ? C20 H20C 0.9800 . ? C21 H21A 0.9800 . ? C21 H21B 0.9800 . ? C21 H21C 0.9800 . ? C22 C23 1.403(2) . ? C22 C27 1.406(2) . ? C23 C24 1.395(2) . ? C23 H23 0.9500 . ? C24 C25 1.386(3) . ? C24 H24 0.9500 . ? C25 C26 1.383(3) . ? C25 H25 0.9500 . ? C26 C27 1.393(2) . ? C26 H26 0.9500 . ? C27 H27 0.9500 . ? C28 C29 1.405(2) . ? C28 C33 1.411(2) . ? C29 C30 1.394(2) . ? C29 H29 0.9500 . ? C30 C31 1.378(3) . ? C30 H30 0.9500 . ? C31 C32 1.389(3) . ? C31 H31 0.9500 . ? C32 C33 1.390(2) . ? C32 H32 0.9500 . ? C33 H33 0.9500 . ? C34 C39 1.404(2) . ? C34 C35 1.409(2) . ? C35 C36 1.393(2) . ? C35 H35 0.9500 . ? C36 C37 1.380(3) . ? C36 H36 0.9500 . ? C37 C38 1.387(2) . ? C37 H37 0.9500 . ? C38 C39 1.394(2) . ? C38 H38 0.9500 . ? C39 H39 0.9500 . ? C40 C45 1.399(2) . ? C40 C41 1.408(2) . ? C41 C42 1.392(2) . ? C41 H41 0.9500 . ? C42 C43 1.386(2) . ? C42 H42 0.9500 . ? C43 C44 1.381(2) . ? C43 H43 0.9500 . ? C44 C45 1.400(2) . ? C44 H44 0.9500 . ? C45 H45 0.9500 . ? C46 C51 1.403(2) . ? C46 C47 1.412(2) . ? C47 C48 1.391(2) . ? C47 H47 0.9500 . ? C48 C49 1.385(3) . ? C48 H48 0.9500 . ? C49 C50 1.383(3) . ? C49 H49 0.9500 . ? C50 C51 1.397(2) . ? C50 H50 0.9500 . ? C51 H51 0.9500 . ? C52 C57 1.403(2) . ? C52 C53 1.406(2) . ? C53 C54 1.392(2) . ? C53 H53 0.9500 . ? C54 C55 1.381(3) . ? C54 H54 0.9500 . ? C55 C56 1.384(3) . ? C55 H55 0.9500 . ? C56 C57 1.399(2) . ? C56 H56 0.9500 . ? C57 H57 0.9500 . ? C58 C59 1.397(2) . ? C58 C63 1.410(2) . ? C59 C60 1.395(2) . ? C59 H59 0.9500 . ? C60 C61 1.378(3) . ? C60 H60 0.9500 . ? C61 C62 1.392(3) . ? C61 H61 0.9500 . ? C62 C63 1.386(2) . ? C62 H62 0.9500 . ? C63 H63 0.9500 . ? C64 C65 1.401(2) . ? C64 C69 1.410(2) . ? C65 C66 1.398(2) . ? C65 H65 0.9500 . ? C66 C67 1.385(2) . ? C66 H66 0.9500 . ? C67 C68 1.381(3) . ? C67 H67 0.9500 . ? C68 C69 1.392(2) . ? C68 H68 0.9500 . ? C69 H69 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C3 N1 C1 C2 152.53(12) . . . . ? C5 N1 C1 C2 -78.86(15) . . . . ? Co1 N1 C1 C2 37.47(13) . . . . ? C7 N2 C2 C1 -145.20(13) . . . . ? Co1 N2 C2 C1 37.92(13) . . . . ? N1 C1 C2 N2 -50.54(15) . . . . ? C5 N1 C3 C4 154.74(12) . . . . ? C1 N1 C3 C4 -76.55(15) . . . . ? Co1 N1 C3 C4 39.37(13) . . . . ? C12 N3 C4 C3 -151.26(12) . . . . ? Co1 N3 C4 C3 35.04(13) . . . . ? N1 C3 C4 N3 -50.81(15) . . . . ? C3 N1 C5 C6 -74.75(16) . . . . ? C1 N1 C5 C6 155.82(13) . . . . ? Co1 N1 C5 C6 39.60(15) . . . . ? C17 N4 C6 C5 -157.28(14) . . . . ? Co1 N4 C6 C5 34.28(17) . . . . ? N1 C5 C6 N4 -49.13(18) . . . . ? C2 N2 C7 N5 154.97(13) . . . . ? Co1 N2 C7 N5 -29.0(2) . . . . ? C2 N2 C7 N6 -24.2(2) . . . . ? Co1 N2 C7 N6 151.83(12) . . . . ? C9 N5 C7 N2 -22.9(2) . . . . ? C8 N5 C7 N2 141.39(18) . . . . ? C9 N5 C7 N6 156.38(15) . . . . ? C8 N5 C7 N6 -39.4(2) . . . . ? C11 N6 C7 N2 -38.0(2) . . . . ? C10 N6 C7 N2 145.89(16) . . . . ? C11 N6 C7 N5 142.79(16) . . . . ? C10 N6 C7 N5 -33.3(2) . . . . ? C4 N3 C12 N7 -17.2(2) . . . . ? Co1 N3 C12 N7 154.79(11) . . . . ? C4 N3 C12 N8 161.42(13) . . . . ? Co1 N3 C12 N8 -26.6(2) . . . . ? C15 N7 C12 N3 141.82(15) . . . . ? C16 N7 C12 N3 -43.7(2) . . . . ? C15 N7 C12 N8 -36.9(2) . . . . ? C16 N7 C12 N8 137.60(15) . . . . ? C14 N8 C12 N3 -17.9(2) . . . . ? C13 N8 C12 N3 144.58(14) . . . . ? C14 N8 C12 N7 160.83(14) . . . . ? C13 N8 C12 N7 -36.7(2) . . . . ? C6 N4 C17 N10 149.27(15) . . . . ? Co1 N4 C17 N10 -44.6(2) . . . . ? C6 N4 C17 N9 -30.5(2) . . . . ? Co1 N4 C17 N9 135.63(14) . . . . ? C19 N10 C17 N4 -22.0(2) . . . . ? C18 N10 C17 N4 143.03(16) . . . . ? C19 N10 C17 N9 157.84(16) . . . . ? C18 N10 C17 N9 -37.2(2) . . . . ? C21 N9 C17 N4 -34.5(2) . . . . ? C20 N9 C17 N4 147.20(19) . . . . ? C21 N9 C17 N10 145.70(17) . . . . ? C20 N9 C17 N10 -32.6(3) . . . . ? C40 B1 C22 C23 -91.72(17) . . . . ? C34 B1 C22 C23 149.09(14) . . . . ? C28 B1 C22 C23 29.30(18) . . . . ? C40 B1 C22 C27 87.54(17) . . . . ? C34 B1 C22 C27 -31.65(18) . . . . ? C28 B1 C22 C27 -151.45(14) . . . . ? C27 C22 C23 C24 -0.7(2) . . . . ? B1 C22 C23 C24 178.62(14) . . . . ? C22 C23 C24 C25 1.7(2) . . . . ? C23 C24 C25 C26 -0.6(2) . . . . ? C24 C25 C26 C27 -1.2(3) . . . . ? C25 C26 C27 C22 2.3(3) . . . . ? C23 C22 C27 C26 -1.3(2) . . . . ? B1 C22 C27 C26 179.41(15) . . . . ? C40 B1 C28 C29 -130.50(15) . . . . ? C34 B1 C28 C29 -12.7(2) . . . . ? C22 B1 C28 C29 107.67(16) . . . . ? C40 B1 C28 C33 47.83(19) . . . . ? C34 B1 C28 C33 165.61(14) . . . . ? C22 B1 C28 C33 -74.01(17) . . . . ? C33 C28 C29 C30 0.3(2) . . . . ? B1 C28 C29 C30 178.78(15) . . . . ? C28 C29 C30 C31 1.4(2) . . . . ? C29 C30 C31 C32 -1.7(2) . . . . ? C30 C31 C32 C33 0.2(3) . . . . ? C31 C32 C33 C28 1.6(3) . . . . ? C29 C28 C33 C32 -1.8(2) . . . . ? B1 C28 C33 C32 179.69(16) . . . . ? C40 B1 C34 C39 20.4(2) . . . . ? C28 B1 C34 C39 -97.87(17) . . . . ? C22 B1 C34 C39 140.87(15) . . . . ? C40 B1 C34 C35 -163.57(14) . . . . ? C28 B1 C34 C35 78.19(17) . . . . ? C22 B1 C34 C35 -43.07(19) . . . . ? C39 C34 C35 C36 0.9(2) . . . . ? B1 C34 C35 C36 -175.49(16) . . . . ? C34 C35 C36 C37 0.7(3) . . . . ? C35 C36 C37 C38 -1.3(3) . . . . ? C36 C37 C38 C39 0.3(2) . . . . ? C37 C38 C39 C34 1.5(3) . . . . ? C35 C34 C39 C38 -2.0(2) . . . . ? B1 C34 C39 C38 174.29(15) . . . . ? C34 B1 C40 C45 95.79(17) . . . . ? C28 B1 C40 C45 -146.29(14) . . . . ? C22 B1 C40 C45 -24.1(2) . . . . ? C34 B1 C40 C41 -77.61(17) . . . . ? C28 B1 C40 C41 40.32(19) . . . . ? C22 B1 C40 C41 162.47(14) . . . . ? C45 C40 C41 C42 -2.3(2) . . . . ? B1 C40 C41 C42 171.72(15) . . . . ? C40 C41 C42 C43 0.8(3) . . . . ? C41 C42 C43 C44 1.0(2) . . . . ? C42 C43 C44 C45 -1.2(2) . . . . ? C41 C40 C45 C44 2.0(2) . . . . ? B1 C40 C45 C44 -171.72(14) . . . . ? C43 C44 C45 C40 -0.3(2) . . . . ? C58 B2 C46 C51 -128.80(15) . . . . ? C64 B2 C46 C51 -7.7(2) . . . . ? C52 B2 C46 C51 112.85(16) . . . . ? C58 B2 C46 C47 50.86(17) . . . . ? C64 B2 C46 C47 171.92(13) . . . . ? C52 B2 C46 C47 -67.48(17) . . . . ? C51 C46 C47 C48 -4.0(2) . . . . ? B2 C46 C47 C48 176.31(14) . . . . ? C46 C47 C48 C49 2.2(3) . . . . ? C47 C48 C49 C50 1.1(3) . . . . ? C48 C49 C50 C51 -2.2(3) . . . . ? C49 C50 C51 C46 0.2(3) . . . . ? C47 C46 C51 C50 2.8(2) . . . . ? B2 C46 C51 C50 -177.50(14) . . . . ? C58 B2 C52 C57 -86.03(17) . . . . ? C46 B2 C52 C57 30.81(19) . . . . ? C64 B2 C52 C57 152.63(14) . . . . ? C58 B2 C52 C53 88.62(16) . . . . ? C46 B2 C52 C53 -154.54(13) . . . . ? C64 B2 C52 C53 -32.71(18) . . . . ? C57 C52 C53 C54 0.6(2) . . . . ? B2 C52 C53 C54 -174.58(15) . . . . ? C52 C53 C54 C55 -0.3(3) . . . . ? C53 C54 C55 C56 -0.3(3) . . . . ? C54 C55 C56 C57 0.4(3) . . . . ? C55 C56 C57 C52 -0.1(3) . . . . ? C53 C52 C57 C56 -0.4(2) . . . . ? B2 C52 C57 C56 174.54(15) . . . . ? C46 B2 C58 C59 -117.49(15) . . . . ? C64 B2 C58 C59 122.21(15) . . . . ? C52 B2 C58 C59 2.91(19) . . . . ? C46 B2 C58 C63 62.14(17) . . . . ? C64 B2 C58 C63 -58.17(18) . . . . ? C52 B2 C58 C63 -177.46(13) . . . . ? C63 C58 C59 C60 1.1(2) . . . . ? B2 C58 C59 C60 -179.24(14) . . . . ? C58 C59 C60 C61 2.0(2) . . . . ? C59 C60 C61 C62 -2.8(3) . . . . ? C60 C61 C62 C63 0.6(3) . . . . ? C61 C62 C63 C58 2.7(3) . . . . ? C59 C58 C63 C62 -3.4(2) . . . . ? B2 C58 C63 C62 176.89(15) . . . . ? C58 B2 C64 C65 8.4(2) . . . . ? C46 B2 C64 C65 -109.35(16) . . . . ? C52 B2 C64 C65 127.96(15) . . . . ? C58 B2 C64 C69 -171.68(13) . . . . ? C46 B2 C64 C69 70.54(17) . . . . ? C52 B2 C64 C69 -52.15(17) . . . . ? C69 C64 C65 C66 -1.5(2) . . . . ? B2 C64 C65 C66 178.34(14) . . . . ? C64 C65 C66 C67 0.9(3) . . . . ? C65 C66 C67 C68 0.7(3) . . . . ? C66 C67 C68 C69 -1.5(3) . . . . ? C67 C68 C69 C64 0.7(3) . . . . ? C65 C64 C69 C68 0.7(2) . . . . ? B2 C64 C69 C68 -179.15(15) . . . . ?