#------------------------------------------------------------------------------ #$Date: 2021-09-06 14:08:47 +0300 (Mon, 06 Sep 2021) $ #$Revision: 268752 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/79/7707952.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7707952 loop_ _publ_author_name 'Fetrow, Taylor V.' 'Daly, Scott R.' _publ_section_title ; Mechanochemical synthesis and structural analysis of trivalent lanthanide and uranium diphenylphosphinodiboranates. ; _journal_issue 33 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 11472 _journal_page_last 11484 _journal_paper_doi 10.1039/d1dt01932e _journal_volume 50 _journal_year 2021 _chemical_formula_moiety 'C72 H96 B12 Ce2 P6' _chemical_formula_sum 'C72 H96 B12 Ce2 P6' _chemical_formula_weight 1557.26 _chemical_name_common Ce(Ph-PDB)3 _chemical_name_systematic Ce(BH3Ph2BH3)3 _chemical_properties_physical Air-sensitive,Moisture-sensitive,Heat-sensitive,Oxygen-sensitive _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2019-08-28 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335) ; _audit_update_record ; 2021-06-09 deposited with the CCDC. 2021-07-16 downloaded from the CCDC. ; _cell_angle_alpha 94.057(5) _cell_angle_beta 94.695(5) _cell_angle_gamma 107.346(5) _cell_formula_units_Z 2 _cell_length_a 11.4324(11) _cell_length_b 12.7542(13) _cell_length_c 28.438(3) _cell_measurement_reflns_used 9990 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.865 _cell_measurement_theta_min 2.8725 _cell_volume 3924.9(7) _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 100.15 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device_type 'D8 Ventere Duo Photon 3' _diffrn_measurement_method 'CCD Phi and Omega scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0508 _diffrn_reflns_av_unetI/netI 0.0418 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 37 _diffrn_reflns_limit_l_min -37 _diffrn_reflns_number 85558 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.987 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.865 _diffrn_reflns_theta_min 2.8725 _exptl_absorpt_coefficient_mu 1.306 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6675 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0687 before and 0.0539 after correction. The Ratio of minimum to maximum transmission is 0.8953. The \l/2 correction factor is Not present. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.318 _exptl_crystal_description plate-like _exptl_crystal_F_000 1588 _exptl_crystal_size_max 0.11 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.02 _refine_diff_density_max 2.151 _refine_diff_density_min -2.047 _refine_diff_density_rms 0.100 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 841 _refine_ls_number_reflns 18483 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0538 _refine_ls_R_factor_gt 0.0381 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0139P)^2^+8.2129P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0659 _refine_ls_wR_factor_ref 0.0704 _reflns_Friedel_coverage 0.000 _reflns_number_gt 14796 _reflns_number_total 18483 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt01932e2.cif _cod_data_source_block dal1943 _cod_depositor_comments 'Adding full bibliography for 7707952--7707958.cif.' _cod_database_code 7707952 _shelx_shelxl_version_number 2016/4 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.974 _shelx_estimated_absorpt_t_min 0.870 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All B(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C12(H12), C13(H13), C14(H14), C15(H15), C16(H16), C22(H22), C23(H23), C24(H24), C25(H25), C26(H26), C32(H32), C33(H33), C34(H34), C35(H35), C36(H36), C42(H42), C43(H43), C44(H44), C45(H45), C46(H46), C52(H52), C53(H53), C54(H54), C55(H55), C56(H56), C62(H62), C63(H63), C64(H64), C65(H65), C66(H66), C72(H72), C73(H73), C74(H74), C75(H75), C76(H76), C82(H82), C83(H83), C84(H84), C85(H85), C86(H86), C92(H92), C93(H93), C94(H94), C95(H95), C96(H96), C102(H102), C103(H103), C104(H104), C105(H105), C106(H106), C112(H112), C113(H113), C114(H114), C115(H115), C116(H116), C122(H122), C123(H123), C124(H124), C125(H125), C126(H126) 2.b Idealised Me refined as rotating group: B1(H1A,H1B,H1C), B2(H2A,H2B,H2C), B3(H3A,H3B,H3C), B4(H4A,H4B,H4C), B5(H5A, H5B,H5C), B6(H6A,H6B,H6C), B7(H7A,H7B,H7C), B8(H8A,H8B,H8C), B9(H9A,H9B,H9C), B10(H10A,H10B,H10C), B11(H11A,H11B,H11C), B12(H12A,H12B,H12C) ; _shelx_res_file ; TITL dal1943_a.res in P-1 dal1943.res created by SHELXL-2016/4 at 15:55:01 on 28-Aug-2019 REM Old TITL Dal19_43 in P-1 sample #19191 TVF_Ce(Ph-PDB) REM SHELXT solution in P-1 REM R1 0.080, Rweak 0.004, Alpha 0.104, Orientation as input REM Formula found by SHELXT: C84 P6 Ce2 CELL 0.71073 11.4324 12.7542 28.438 94.057 94.695 107.346 ZERR 2 0.0011 0.0013 0.003 0.005 0.005 0.005 LATT 1 SFAC C H B Ce P UNIT 144 192 24 4 12 EQIV $1 -1+X,+Y,+Z EQIV $2 1+X,+Y,+Z L.S. 10 PLAN 20 SIZE 0.02 0.1 0.11 TEMP -173 FREE B12 Ce2 FREE B1 Ce1 FREE B6 Ce2 FREE B2 Ce1 FREE B4 Ce1 FREE B4 Ce2_$2 FREE B3 Ce1 FREE B5 Ce1 FREE B7 Ce1 FREE B8 Ce2 FREE B9 Ce2 FREE B11 Ce2 FREE B10 Ce1_$1 BOND $H list 4 fmap 2 53 ACTA OMIT -13 11 7 OMIT 11 3 14 OMIT 12 5 3 OMIT -8 6 31 REM REM REM WGHT 0.013900 8.212900 FVAR 0.23544 B1 3 0.958717 0.408259 0.099751 11.00000 0.01856 0.01529 = 0.01256 -0.00165 -0.00128 0.00328 AFIX 137 1.2000 H1A 2 0.933884 0.476785 0.077543 11.00000 -1.50000 H1B 2 1.046205 0.451787 0.128303 11.00000 -1.50000 H1C 2 0.872249 0.362659 0.119880 11.00000 -1.50000 AFIX 0 B2 3 1.033945 0.188100 0.092145 11.00000 0.02101 0.01719 = 0.01839 0.00029 0.00479 0.00625 AFIX 137 1.2000 H2A 2 0.946347 0.143077 0.111822 11.00000 -1.50000 H2B 2 1.121050 0.230029 0.121062 11.00000 -1.50000 H2C 2 1.057145 0.121471 0.065569 11.00000 -1.50000 AFIX 0 B3 3 1.096416 0.142831 0.218826 11.00000 0.02099 0.01258 = 0.01993 0.00252 -0.00176 0.00687 AFIX 137 1.2000 H3A 2 1.188184 0.167268 0.199062 11.00000 -1.50000 H3B 2 1.094956 0.220141 0.245143 11.00000 -1.50000 H3C 2 1.007596 0.117800 0.189960 11.00000 -1.50000 AFIX 0 B4 3 1.227863 0.044322 0.303741 11.00000 0.01238 0.01283 = 0.01898 0.00039 0.00199 0.00118 AFIX 137 1.2000 H4A 2 1.202337 -0.027558 0.329657 11.00000 -1.50000 H4B 2 1.244916 0.132066 0.325984 11.00000 -1.50000 H4C 2 1.319668 0.043259 0.286314 11.00000 -1.50000 AFIX 0 B5 3 0.765806 0.184728 0.188847 11.00000 0.01269 0.01754 = 0.02197 0.00086 0.00304 0.00210 AFIX 137 1.2000 H5A 2 0.816738 0.176399 0.154150 11.00000 -1.50000 H5B 2 0.816982 0.156166 0.221824 11.00000 -1.50000 H5C 2 0.769013 0.279069 0.197504 11.00000 -1.50000 AFIX 0 B6 3 0.492356 0.088250 0.227893 11.00000 0.01672 0.02437 = 0.01962 -0.00351 0.00524 0.00235 AFIX 137 1.2000 H6A 2 0.478879 0.177344 0.235866 11.00000 -1.50000 H6B 2 0.539030 0.063639 0.263055 11.00000 -1.50000 H6C 2 0.393893 0.020913 0.215921 11.00000 -1.50000 AFIX 0 B7 3 0.987208 0.423389 0.270524 11.00000 0.01670 0.02326 = 0.02189 -0.00147 0.00788 0.00500 AFIX 137 1.2000 H7A 2 1.086242 0.490058 0.282245 11.00000 -1.50000 H7B 2 0.941157 0.447448 0.235088 11.00000 -1.50000 H7C 2 0.999336 0.333604 0.263144 11.00000 -1.50000 AFIX 0 B8 3 0.713143 0.330328 0.310534 11.00000 0.01708 0.01871 = 0.02217 -0.00140 0.00401 0.00006 AFIX 137 1.2000 H8A 2 0.709136 0.235505 0.302897 11.00000 -1.50000 H8B 2 0.661422 0.357200 0.277214 11.00000 -1.50000 H8C 2 0.663320 0.341239 0.345279 11.00000 -1.50000 AFIX 0 B9 3 0.378616 0.367159 0.281038 11.00000 0.02349 0.01560 = 0.01882 0.00023 -0.00258 0.00279 AFIX 137 1.2000 H9A 2 0.467952 0.392162 0.309654 11.00000 -1.50000 H9B 2 0.377205 0.287368 0.255690 11.00000 -1.50000 H9C 2 0.287397 0.346629 0.301172 11.00000 -1.50000 AFIX 0 B10 3 0.251425 0.464396 0.193533 11.00000 0.01623 0.01285 = 0.01555 -0.00017 0.00222 0.00333 AFIX 137 1.2000 H10A 2 0.160229 0.469879 0.210322 11.00000 -1.50000 H10B 2 0.231552 0.374909 0.172449 11.00000 -1.50000 H10C 2 0.280174 0.533962 0.166709 11.00000 -1.50000 AFIX 0 B11 3 0.529069 0.099815 0.397083 11.00000 0.02000 0.01874 = 0.01485 0.00133 0.00044 0.00337 AFIX 137 1.2000 H11A 2 0.558601 0.031751 0.418102 11.00000 -1.50000 H11B 2 0.613853 0.150775 0.377396 11.00000 -1.50000 H11C 2 0.442584 0.054934 0.368273 11.00000 -1.50000 AFIX 0 B12 3 0.437737 0.310539 0.407717 11.00000 0.02842 0.01871 = 0.01699 0.00147 0.00215 0.00668 AFIX 137 1.2000 H12A 2 0.350290 0.266230 0.379251 11.00000 -1.50000 H12B 2 0.522435 0.360030 0.387615 11.00000 -1.50000 H12C 2 0.411816 0.373750 0.435205 11.00000 -1.50000 AFIX 0 C11 1 0.870040 0.239607 0.010918 11.00000 0.02184 0.02440 = 0.01482 -0.00400 0.00439 0.00178 C12 1 0.825525 0.306798 -0.017826 11.00000 0.02386 0.02657 = 0.02295 -0.00118 0.00068 0.00467 AFIX 43 H12 2 0.861756 0.384680 -0.013432 11.00000 -1.20000 AFIX 0 C13 1 0.727939 0.259244 -0.052910 11.00000 0.03169 0.03919 = 0.02329 -0.00389 -0.00455 0.01058 AFIX 43 H13 2 0.698446 0.304484 -0.072950 11.00000 -1.20000 AFIX 0 C14 1 0.673952 0.145906 -0.058543 11.00000 0.03963 0.04477 = 0.03109 -0.01073 -0.01185 0.00034 AFIX 43 H14 2 0.606808 0.113754 -0.082314 11.00000 -1.20000 AFIX 0 C15 1 0.716330 0.079602 -0.030196 11.00000 0.05258 0.02757 = 0.03744 -0.00912 -0.00890 -0.00914 AFIX 43 H15 2 0.677374 0.002059 -0.033992 11.00000 -1.20000 AFIX 0 C16 1 0.815979 0.125228 0.004063 11.00000 0.03806 0.02300 = 0.02782 -0.00140 -0.00066 0.00172 AFIX 43 H16 2 0.847286 0.078772 0.022784 11.00000 -1.20000 AFIX 0 C21 1 1.129710 0.368186 0.026497 11.00000 0.01888 0.02092 = 0.02025 0.00472 0.00334 0.00789 C22 1 1.130874 0.348608 -0.022330 11.00000 0.02623 0.02986 = 0.02201 0.00270 0.00464 0.00775 AFIX 43 H22 2 1.061224 0.298152 -0.040812 11.00000 -1.20000 AFIX 0 C23 1 1.233574 0.402675 -0.043999 11.00000 0.03384 0.04078 = 0.02253 0.01035 0.00928 0.01736 AFIX 43 H23 2 1.233335 0.389600 -0.077316 11.00000 -1.20000 AFIX 0 C24 1 1.335026 0.474577 -0.017758 11.00000 0.02496 0.03098 = 0.04092 0.01528 0.01700 0.01114 AFIX 43 H24 2 1.404292 0.512216 -0.032938 11.00000 -1.20000 AFIX 0 C25 1 1.336833 0.492576 0.031025 11.00000 0.02136 0.02713 = 0.04492 -0.00004 0.00679 0.00296 AFIX 43 H25 2 1.408071 0.541230 0.049314 11.00000 -1.20000 AFIX 0 C26 1 1.234586 0.439522 0.053138 11.00000 0.02638 0.02744 = 0.02355 0.00013 0.00485 0.00437 AFIX 43 H26 2 1.236130 0.451901 0.086551 11.00000 -1.20000 AFIX 0 C31 1 1.086201 -0.098013 0.213506 11.00000 0.01317 0.01272 = 0.01863 -0.00277 0.00057 0.00375 C32 1 1.087262 -0.088308 0.165460 11.00000 0.03773 0.01949 = 0.01646 -0.00213 -0.00012 0.00904 AFIX 43 H32 2 1.088545 -0.020284 0.153547 11.00000 -1.20000 AFIX 0 C33 1 1.086453 -0.178093 0.134491 11.00000 0.05183 0.02847 = 0.01949 -0.00417 0.00486 0.01034 AFIX 43 H33 2 1.087106 -0.171219 0.101461 11.00000 -1.20000 AFIX 0 C34 1 1.084698 -0.277449 0.151662 11.00000 0.03693 0.01933 = 0.03142 -0.01019 0.00560 0.00628 AFIX 43 H34 2 1.083662 -0.338717 0.130410 11.00000 -1.20000 AFIX 0 C35 1 1.084458 -0.287321 0.199463 11.00000 0.03783 0.01305 = 0.03740 0.00110 0.00893 0.00652 AFIX 43 H35 2 1.083183 -0.355479 0.211239 11.00000 -1.20000 AFIX 0 C36 1 1.086077 -0.197709 0.230617 11.00000 0.03594 0.01849 = 0.02097 0.00268 0.00816 0.00760 AFIX 43 H36 2 1.087102 -0.204496 0.263689 11.00000 -1.20000 AFIX 0 C41 1 0.948682 -0.010153 0.280467 11.00000 0.01309 0.01625 = 0.01567 0.00375 0.00176 0.00584 C42 1 0.944787 0.053737 0.321921 11.00000 0.01780 0.01831 = 0.02270 -0.00160 0.00221 0.00309 AFIX 43 H42 2 1.018601 0.105084 0.337338 11.00000 -1.20000 AFIX 0 C43 1 0.834061 0.042943 0.340827 11.00000 0.02480 0.02737 = 0.02392 0.00031 0.01002 0.01034 AFIX 43 H43 2 0.831773 0.087930 0.368614 11.00000 -1.20000 AFIX 0 C44 1 0.727131 -0.033672 0.318974 11.00000 0.01714 0.02735 = 0.02992 0.00939 0.00978 0.00668 AFIX 43 H44 2 0.651410 -0.042103 0.332067 11.00000 -1.20000 AFIX 0 C45 1 0.730071 -0.097929 0.278202 11.00000 0.01429 0.02765 = 0.03120 0.00319 -0.00046 0.00088 AFIX 43 H45 2 0.656432 -0.150822 0.263498 11.00000 -1.20000 AFIX 0 C46 1 0.840246 -0.085655 0.258533 11.00000 0.01830 0.02045 = 0.02017 0.00046 0.00049 0.00369 AFIX 43 H46 2 0.841354 -0.128939 0.230075 11.00000 -1.20000 AFIX 0 C51 1 0.597352 -0.046241 0.158057 11.00000 0.01983 0.01636 = 0.01948 -0.00359 -0.00022 0.00302 C52 1 0.688795 -0.063566 0.132166 11.00000 0.03806 0.01873 = 0.11265 -0.01813 0.03903 -0.00453 AFIX 43 H52 2 0.752701 -0.001901 0.124770 11.00000 -1.20000 AFIX 0 C53 1 0.688531 -0.169746 0.116835 11.00000 0.04402 0.02834 = 0.14234 -0.02497 0.04673 0.00274 AFIX 43 H53 2 0.751673 -0.180050 0.099005 11.00000 -1.20000 AFIX 0 C54 1 0.597604 -0.259006 0.127413 11.00000 0.03877 0.02045 = 0.04728 -0.00555 0.00008 0.01300 AFIX 43 H54 2 0.596576 -0.331630 0.116803 11.00000 -1.20000 AFIX 0 C55 1 0.508822 -0.242984 0.153199 11.00000 0.05410 0.01666 = 0.03335 0.00337 0.00724 -0.00064 AFIX 43 H55 2 0.446074 -0.305189 0.160877 11.00000 -1.20000 AFIX 0 C56 1 0.507460 -0.137657 0.168668 11.00000 0.04094 0.02208 = 0.03110 -0.00018 0.01478 0.00369 AFIX 43 H56 2 0.444084 -0.128674 0.186683 11.00000 -1.20000 AFIX 0 C61 1 0.529743 0.142447 0.126889 11.00000 0.01471 0.01483 = 0.02268 -0.00285 0.00239 0.00281 C62 1 0.594326 0.168655 0.087727 11.00000 0.01971 0.04666 = 0.02706 0.00913 0.00601 0.00903 AFIX 43 H62 2 0.671381 0.155092 0.086448 11.00000 -1.20000 AFIX 0 C63 1 0.547739 0.214143 0.050704 11.00000 0.02935 0.04997 = 0.03041 0.01274 0.00584 0.00284 AFIX 43 H63 2 0.593498 0.232455 0.024426 11.00000 -1.20000 AFIX 0 C64 1 0.435788 0.233112 0.051577 11.00000 0.03900 0.02540 = 0.02981 0.00407 -0.00614 0.01064 AFIX 43 H64 2 0.404275 0.264557 0.026042 11.00000 -1.20000 AFIX 0 C65 1 0.369946 0.206535 0.089354 11.00000 0.02886 0.03751 = 0.03629 -0.00545 -0.00330 0.02307 AFIX 43 H65 2 0.292311 0.219305 0.089872 11.00000 -1.20000 AFIX 0 C66 1 0.415422 0.160996 0.127042 11.00000 0.02489 0.03144 = 0.02512 -0.00202 0.00567 0.01454 AFIX 43 H66 2 0.368514 0.142426 0.153002 11.00000 -1.20000 AFIX 0 C71 1 0.529090 0.515719 0.217517 11.00000 0.01414 0.01233 = 0.01884 0.00370 0.00292 0.00539 C72 1 0.533038 0.452582 0.175726 11.00000 0.01852 0.01821 = 0.02169 -0.00061 0.00258 0.00476 AFIX 43 H72 2 0.459259 0.401454 0.160169 11.00000 -1.20000 AFIX 0 C73 1 0.643506 0.463949 0.156840 11.00000 0.02651 0.02070 = 0.02283 0.00082 0.00781 0.01147 AFIX 43 H73 2 0.645697 0.419671 0.128821 11.00000 -1.20000 AFIX 0 C74 1 0.750846 0.540075 0.178916 11.00000 0.01769 0.03057 = 0.02904 0.00904 0.00829 0.01361 AFIX 43 H74 2 0.826600 0.548779 0.165816 11.00000 -1.20000 AFIX 0 C75 1 0.747568 0.603429 0.220083 11.00000 0.01541 0.02620 = 0.03149 0.00375 0.00400 0.00251 AFIX 43 H75 2 0.821281 0.655497 0.235196 11.00000 -1.20000 AFIX 0 C76 1 0.637040 0.591318 0.239447 11.00000 0.02122 0.02106 = 0.02122 0.00027 0.00311 0.00498 AFIX 43 H76 2 0.635511 0.634931 0.267755 11.00000 -1.20000 AFIX 0 C81 1 0.393237 0.609012 0.282838 11.00000 0.01266 0.01625 = 0.02026 -0.00094 0.00527 0.00303 C82 1 0.366655 0.698423 0.265152 11.00000 0.04325 0.01757 = 0.02608 0.00193 0.01204 0.00783 AFIX 43 H82 2 0.344988 0.696848 0.232081 11.00000 -1.20000 AFIX 0 C83 1 0.371283 0.790730 0.295263 11.00000 0.04561 0.01714 = 0.04281 0.00051 0.01741 0.00916 AFIX 43 H83 2 0.353377 0.851846 0.282577 11.00000 -1.20000 AFIX 0 C84 1 0.401262 0.794082 0.342731 11.00000 0.03163 0.02169 = 0.04479 -0.01535 0.00965 0.00223 AFIX 43 H84 2 0.403505 0.856948 0.363229 11.00000 -1.20000 AFIX 0 C85 1 0.428155 0.706381 0.360764 11.00000 0.04620 0.04263 = 0.02448 -0.01680 -0.00355 0.01656 AFIX 43 H85 2 0.450120 0.709044 0.393874 11.00000 -1.20000 AFIX 0 C86 1 0.423739 0.613404 0.331235 11.00000 0.04080 0.02998 = 0.02837 -0.00549 -0.00495 0.01656 AFIX 43 H86 2 0.441691 0.552682 0.344279 11.00000 -1.20000 AFIX 0 C91 1 0.886282 0.562848 0.339545 11.00000 0.02012 0.01888 = 0.02116 -0.00502 -0.00014 0.00258 C92 1 0.992846 0.649855 0.338890 11.00000 0.03080 0.02054 = 0.02147 -0.00006 0.00691 0.00170 AFIX 43 H92 2 1.063812 0.636174 0.328000 11.00000 -1.20000 AFIX 0 C93 1 0.996942 0.757198 0.354045 11.00000 0.04235 0.01698 = 0.02487 0.00298 0.00297 -0.00359 AFIX 43 H93 2 1.070890 0.816046 0.353658 11.00000 -1.20000 AFIX 0 C94 1 0.896426 0.778500 0.369339 11.00000 0.04720 0.02106 = 0.03817 -0.00731 -0.00947 0.01262 AFIX 43 H94 2 0.900357 0.851845 0.380067 11.00000 -1.20000 AFIX 0 C95 1 0.789391 0.694333 0.369310 11.00000 0.03801 0.03813 = 0.07533 -0.02219 0.00221 0.01773 AFIX 43 H95 2 0.718494 0.709572 0.379469 11.00000 -1.20000 AFIX 0 C96 1 0.783636 0.586568 0.354508 11.00000 0.02848 0.02882 = 0.06470 -0.01648 0.00805 0.00194 AFIX 43 H96 2 0.708767 0.528622 0.354632 11.00000 -1.20000 AFIX 0 C101 1 0.950424 0.375895 0.372054 11.00000 0.01797 0.02102 = 0.02394 -0.00003 0.00148 -0.00121 C102 1 1.049886 0.336217 0.370184 11.00000 0.03329 0.02864 = 0.02557 -0.00666 -0.00068 0.01004 AFIX 43 H102 2 1.088560 0.337485 0.341817 11.00000 -1.20000 AFIX 0 C103 1 1.094622 0.294048 0.409609 11.00000 0.03968 0.02648 = 0.04116 -0.00716 -0.01257 0.00794 AFIX 43 H103 2 1.161872 0.265202 0.407617 11.00000 -1.20000 AFIX 0 C104 1 1.041434 0.294430 0.450960 11.00000 0.03959 0.05522 = 0.04086 0.02415 -0.00686 -0.00828 AFIX 43 H104 2 1.070849 0.264862 0.477575 11.00000 -1.20000 AFIX 0 C105 1 0.944180 0.338214 0.453948 11.00000 0.03266 0.13863 = 0.03766 0.03514 0.00965 0.00939 AFIX 43 H105 2 0.909155 0.341292 0.482982 11.00000 -1.20000 AFIX 0 C106 1 0.898777 0.377082 0.414742 11.00000 0.02485 0.10067 = 0.03635 0.02150 0.00951 0.01896 AFIX 43 H106 2 0.831024 0.405221 0.416821 11.00000 -1.20000 AFIX 0 C111 1 0.355187 0.123175 0.471455 11.00000 0.02189 0.01687 = 0.01801 0.00333 0.00374 0.00638 C112 1 0.249239 0.054605 0.444428 11.00000 0.02369 0.03248 = 0.02064 -0.00304 0.00081 0.00367 AFIX 43 H112 2 0.245161 0.049152 0.410807 11.00000 -1.20000 AFIX 0 C113 1 0.150146 -0.005489 0.465937 11.00000 0.02338 0.03650 = 0.03378 -0.00300 0.00298 0.00249 AFIX 43 H113 2 0.078330 -0.051677 0.447122 11.00000 -1.20000 AFIX 0 C114 1 0.155449 0.001590 0.515172 11.00000 0.02539 0.03172 = 0.03511 0.01007 0.01292 0.00452 AFIX 43 H114 2 0.088117 -0.040848 0.530073 11.00000 -1.20000 AFIX 0 C115 1 0.258477 0.070207 0.542032 11.00000 0.03172 0.04109 = 0.02085 0.01028 0.01070 0.01380 AFIX 43 H115 2 0.261571 0.076372 0.575630 11.00000 -1.20000 AFIX 0 C116 1 0.358065 0.130600 0.520603 11.00000 0.02626 0.02936 = 0.02032 -0.00173 -0.00043 0.00531 AFIX 43 H116 2 0.429025 0.177547 0.539648 11.00000 -1.20000 AFIX 0 C121 1 0.607577 0.263818 0.488306 11.00000 0.02396 0.02116 = 0.01905 -0.00152 0.00467 -0.00087 C122 1 0.669384 0.201627 0.512515 11.00000 0.02556 0.02912 = 0.02419 -0.00601 -0.00076 0.00781 AFIX 43 H122 2 0.648938 0.124530 0.503736 11.00000 -1.20000 AFIX 0 C123 1 0.760704 0.251437 0.549401 11.00000 0.03038 0.04548 = 0.02611 -0.00275 -0.00152 0.01046 AFIX 43 H123 2 0.802327 0.208509 0.565937 11.00000 -1.20000 AFIX 0 C124 1 0.791023 0.364012 0.562053 11.00000 0.03845 0.04507 = 0.03519 -0.00962 -0.01234 -0.00076 AFIX 43 H124 2 0.853798 0.398300 0.587206 11.00000 -1.20000 AFIX 0 C125 1 0.730492 0.426243 0.538298 11.00000 0.06746 0.02649 = 0.05008 -0.00579 -0.01923 -0.00276 AFIX 43 H125 2 0.751052 0.503256 0.547303 11.00000 -1.20000 AFIX 0 C126 1 0.639491 0.376925 0.501223 11.00000 0.04930 0.02183 = 0.03576 -0.00054 -0.01430 -0.00021 AFIX 43 H126 2 0.598857 0.420471 0.484610 11.00000 -1.20000 AFIX 0 CE1 4 1.003021 0.297348 0.182168 11.00000 0.01053 0.00994 = 0.01444 0.00114 0.00186 0.00258 CE2 4 0.477310 0.212395 0.316742 11.00000 0.01137 0.01079 = 0.01381 0.00114 0.00110 0.00167 P1 5 0.997416 0.300259 0.056729 11.00000 0.01779 0.01598 = 0.01475 0.00058 0.00194 0.00279 P2 5 1.094046 0.020552 0.254394 11.00000 0.01294 0.01143 = 0.01392 0.00068 0.00156 0.00347 P3 5 0.597362 0.092840 0.177754 11.00000 0.01201 0.01428 = 0.01761 -0.00224 0.00229 0.00191 P4 5 0.882552 0.421874 0.320504 11.00000 0.01344 0.01540 = 0.02043 -0.00290 0.00345 0.00014 P5 5 0.383884 0.487632 0.243607 11.00000 0.01321 0.01052 = 0.01413 0.00038 0.00171 0.00299 P6 5 0.483910 0.200391 0.441667 11.00000 0.01993 0.01563 = 0.01364 -0.00040 0.00092 0.00275 HKLF 4 REM dal1943_a.res in P-1 REM R1 = 0.0381 for 14796 Fo > 4sig(Fo) and 0.0538 for all 18483 data REM 841 parameters refined using 0 restraints END WGHT 0.0139 8.2129 REM Highest difference peak 2.151, deepest hole -2.047, 1-sigma level 0.100 Q1 1 0.9566 0.3239 0.1800 11.00000 0.05 2.15 Q2 1 0.4346 0.2411 0.3166 11.00000 0.05 1.75 Q3 1 1.0552 0.3229 0.1941 11.00000 0.05 0.82 Q4 1 1.1022 0.2799 0.1806 11.00000 0.05 0.79 Q5 1 0.4838 0.1984 0.3356 11.00000 0.05 0.79 Q6 1 0.5463 0.1523 0.3139 11.00000 0.05 0.71 Q7 1 1.0599 0.2361 0.1932 11.00000 0.05 0.66 Q8 1 0.4596 0.1639 0.3178 11.00000 0.05 0.66 Q9 1 0.5297 0.2378 0.3202 11.00000 0.05 0.65 Q10 1 0.5817 0.2048 0.3206 11.00000 0.05 0.62 Q11 1 1.0800 0.2644 0.1681 11.00000 0.05 0.62 Q12 1 0.5166 0.2256 0.2965 11.00000 0.05 0.61 Q13 1 0.5162 0.1407 0.3084 11.00000 0.05 0.60 Q14 1 0.9833 0.2451 0.1820 11.00000 0.05 0.59 Q15 1 0.3396 0.5140 0.2402 11.00000 0.05 0.59 Q16 1 0.5562 0.1239 0.1761 11.00000 0.05 0.59 Q17 1 0.4047 0.1556 0.4599 11.00000 0.05 0.50 Q18 1 1.0460 0.0401 0.2456 11.00000 0.05 0.50 Q19 1 1.0587 0.1830 0.2201 11.00000 0.05 0.49 Q20 1 1.0280 0.2523 0.0795 11.00000 0.05 0.48 ; _shelx_res_checksum 10473 _shelx_hkl_file ; -2 0 0 4448.15 70.09 2 0 0 4477.45 69.99 2 0 0 4537.65 70.09 -3 0 0 133.19 7.40 -3 0 0 133.09 9.70 3 0 0 139.09 9.30 3 0 0 114.49 9.40 3 0 0 138.49 7.30 -4 0 0 511.85 17.90 -4 0 0 541.55 14.90 4 0 0 528.35 18.30 4 0 0 558.84 20.40 4 0 0 534.25 14.90 4 0 0 548.15 18.30 -5 0 0 21.70 5.20 -5 0 0 11.60 7.00 5 0 0 1.80 6.80 5 0 0 20.10 9.70 5 0 0 11.50 4.90 5 0 0 16.70 7.40 -6 0 0 211.28 9.50 -6 0 0 198.88 14.00 -6 0 0 213.28 11.50 6 0 0 198.38 14.70 6 0 0 234.98 17.50 6 0 0 204.28 14.50 6 0 0 203.18 11.30 -7 0 0 12.50 5.70 -7 0 0 6.70 4.20 7 0 0 17.30 5.90 7 0 0 8.30 7.20 7 0 0 8.60 7.90 -8 0 0 1573.24 36.70 -8 0 0 1550.64 32.40 -8 0 0 1522.75 43.60 8 0 0 1547.45 37.10 8 0 0 1549.84 43.60 8 0 0 1569.24 45.20 8 0 0 1575.44 48.10 -9 0 0 93.49 11.50 -9 0 0 87.19 9.40 -9 0 0 49.90 12.10 9 0 0 82.99 14.70 9 0 0 63.99 15.50 9 0 0 85.99 16.10 9 0 0 79.99 11.00 -10 0 0 483.55 21.10 -10 0 0 496.75 17.60 10 0 0 471.05 21.60 10 0 0 462.55 27.00 10 0 0 494.65 28.70 -11 0 0 147.39 14.50 -11 0 0 161.58 12.30 11 0 0 202.28 24.40 11 0 0 163.48 15.90 11 0 0 157.48 19.90 -12 0 0 163.18 18.60 -12 0 0 177.78 12.70 12 0 0 177.88 22.40 12 0 0 217.58 26.90 12 0 0 193.28 18.10 -13 0 0 222.38 14.20 -13 0 0 197.28 17.40 13 0 0 256.17 24.90 13 0 0 190.88 26.70 13 0 0 217.08 19.30 -14 0 0 12.80 9.10 -14 0 0 11.70 7.50 14 0 0 8.90 12.30 14 -1 0 57.29 15.40 -14 1 0 44.90 12.70 -14 1 0 48.90 9.90 13 -1 0 135.09 19.90 13 -1 0 101.29 19.80 13 -1 0 52.49 17.40 -13 1 0 55.99 12.60 -13 1 0 83.39 11.00 12 -1 0 4.90 11.60 12 -1 0 5.30 9.00 12 -1 0 19.20 12.10 -12 1 0 0.70 8.00 -12 1 0 6.70 6.70 11 -1 0 98.79 14.00 11 -1 0 113.99 18.60 11 -1 0 111.79 17.40 -11 1 0 97.79 11.10 -11 1 0 111.39 13.90 10 -1 0 96.19 13.10 10 -1 0 132.99 18.10 10 -1 0 85.79 16.50 10 -1 0 64.09 20.20 -10 1 0 115.09 13.40 -10 1 0 100.79 10.50 9 -1 0 141.39 17.70 9 -1 0 131.79 20.60 9 -1 0 105.49 12.40 9 -1 0 106.99 19.50 -9 1 0 113.69 16.70 -9 1 0 96.69 12.00 -9 1 0 91.39 9.60 8 -1 0 733.23 27.50 8 -1 0 678.23 31.00 8 -1 0 728.43 24.00 8 -1 0 725.43 29.30 -8 1 0 655.03 20.00 -8 1 0 732.03 23.60 -8 1 0 706.63 28.10 7 -1 0 151.68 13.50 7 -1 0 172.88 11.90 7 -1 0 167.18 14.40 7 -1 0 184.28 17.40 -7 1 0 157.48 14.50 -7 1 0 152.08 11.70 6 -1 0 282.57 18.50 6 -1 0 313.27 16.80 6 -1 0 299.67 15.90 6 -1 0 326.37 14.50 -6 1 0 311.47 16.70 -6 1 0 318.77 14.20 5 -1 0 25.60 6.30 5 -1 0 31.00 9.10 5 -1 0 23.60 7.90 -5 1 0 29.80 8.10 4 -1 0 208.88 13.10 4 -1 0 191.98 10.80 4 -1 0 228.78 10.40 -4 1 0 215.08 10.30 -4 1 0 205.28 11.50 3 -1 0 724.23 20.50 3 -1 0 733.23 19.30 3 -1 0 734.83 17.40 3 -1 0 687.23 17.30 -3 1 0 742.13 20.50 -3 1 0 713.23 17.30 -3 1 0 744.23 19.10 2 -1 0 46.90 5.00 2 -1 0 41.30 4.60 2 -1 0 46.50 5.50 2 -1 0 46.90 6.30 -2 1 0 53.19 6.50 -2 1 0 59.29 6.00 -2 1 0 46.50 5.40 -2 1 0 44.20 4.70 -1 -1 0 110.99 5.60 -1 -1 0 121.99 3.10 -1 -1 0 109.39 6.30 1 1 0 117.19 6.30 1 1 0 127.49 3.80 1 1 0 124.39 3.10 1 1 0 118.39 5.70 -2 -1 0 41.20 3.20 -2 -1 0 49.20 6.50 -2 -1 0 48.30 4.40 2 1 0 48.40 6.60 2 1 0 45.40 4.40 2 1 0 39.10 7.00 2 1 0 33.40 3.20 -3 -1 0 358.76 9.90 -3 -1 0 355.86 8.40 -3 -1 0 357.86 13.90 3 1 0 336.87 11.50 3 1 0 340.87 14.40 3 1 0 340.87 13.70 -4 -1 0 98.69 9.90 -4 -1 0 98.99 6.80 -4 -1 0 93.49 5.30 4 1 0 93.79 10.60 4 1 0 103.49 9.70 4 1 0 106.49 7.10 -5 -1 0 1102.79 23.90 -5 -1 0 1110.49 30.30 -5 -1 0 1103.59 21.40 5 1 0 1081.99 31.00 5 1 0 1074.19 30.40 5 1 0 1077.59 24.40 -6 -1 0 59.79 10.20 -6 -1 0 72.09 7.80 -6 -1 0 69.49 6.10 6 1 0 55.59 7.30 6 1 0 51.29 11.40 6 1 0 57.29 10.90 6 1 0 59.79 10.60 -7 -1 0 573.84 24.70 -7 -1 0 575.54 18.50 -7 -1 0 612.04 16.00 7 1 0 580.64 27.70 7 1 0 551.54 24.50 7 1 0 573.94 25.20 7 1 0 574.24 19.00 -8 -1 0 6.80 4.40 -8 -1 0 10.80 5.80 -8 -1 0 -4.80 8.20 8 1 0 -3.40 7.80 8 1 0 -4.80 9.40 8 1 0 1.90 8.60 8 1 0 1.90 5.10 -9 -1 0 1110.69 39.50 -9 -1 0 1134.59 26.20 -9 -1 0 1157.78 30.80 9 1 0 1156.48 53.39 9 1 0 1095.99 31.10 9 1 0 1202.18 45.90 9 1 0 1136.49 40.70 -10 -1 0 99.39 12.00 -10 -1 0 94.39 9.00 10 1 0 95.69 16.30 10 1 0 58.79 14.50 10 1 0 137.79 25.00 -11 -1 0 297.97 25.20 -11 -1 0 240.88 16.40 -11 -1 0 280.07 13.60 11 1 0 270.87 17.70 11 1 0 298.67 24.80 11 1 0 286.97 24.50 -12 -1 0 153.68 12.10 -12 -1 0 166.08 15.10 12 1 0 138.59 16.50 12 1 0 144.09 21.70 12 1 0 147.19 24.00 -13 -1 0 114.29 14.20 -13 -1 0 125.49 11.00 13 1 0 138.99 22.20 13 1 0 123.09 22.40 13 1 0 149.88 17.90 14 -2 0 233.68 23.20 14 -2 0 249.78 24.60 -14 2 0 260.87 17.80 -14 2 0 225.68 19.90 13 -2 0 50.49 14.30 13 -2 0 68.49 15.60 13 -2 0 77.89 18.10 -13 2 0 40.90 11.20 -13 2 0 76.39 11.60 12 -2 0 128.19 24.30 12 -2 0 95.49 16.90 12 -2 0 70.69 16.90 12 -2 0 107.89 15.70 -12 2 0 106.19 15.70 -12 2 0 117.99 14.10 11 -2 0 13.40 9.60 11 -2 0 13.30 11.30 -11 2 0 1.90 7.70 -11 2 0 8.80 7.60 10 -2 0 645.64 26.20 10 -2 0 633.34 28.30 10 -2 0 649.93 34.30 10 -2 0 661.83 32.20 -10 2 0 649.64 22.50 -10 2 0 623.74 25.30 -10 2 0 671.43 38.10 9 -2 0 20.10 12.50 9 -2 0 16.80 8.60 9 -2 0 17.70 10.80 9 -2 0 12.80 8.40 -9 2 0 2.60 9.00 -9 2 0 9.50 7.90 8 -2 0 497.65 20.70 8 -2 0 547.05 25.50 8 -2 0 541.25 27.30 8 -2 0 515.55 22.30 -8 2 0 527.95 24.60 -8 2 0 502.75 20.80 7 -2 0 -6.40 5.00 7 -2 0 -1.40 7.00 7 -2 0 3.30 8.00 7 -2 0 -3.40 5.90 -7 2 0 1.50 5.30 -7 2 0 -0.80 7.10 6 -2 0 2048.70 48.00 6 -2 0 1990.20 42.10 6 -2 0 2021.60 42.60 6 -2 0 2014.90 45.90 -6 2 0 2036.90 42.10 -6 2 0 1969.40 45.20 5 -2 0 19.80 6.00 5 -2 0 29.70 7.10 5 -2 0 30.80 8.30 5 -2 0 26.20 8.40 -5 2 0 36.80 6.80 -5 2 0 42.40 8.90 4 -2 0 1145.39 26.40 4 -2 0 1191.28 29.20 4 -2 0 1183.88 24.90 4 -2 0 1208.58 29.00 -4 2 0 1138.79 27.60 -4 2 0 1207.78 29.90 -4 2 0 1229.88 26.90 3 -2 0 4.40 4.50 3 -2 0 -0.50 3.30 3 -2 0 0.70 5.90 3 -2 0 -2.90 5.00 -3 2 0 -0.10 5.00 -3 2 0 2.90 4.40 -3 2 0 7.00 6.10 2 -2 0 6218.68 92.29 2 -2 0 6001.40 86.79 -2 2 0 5978.60 94.69 1 -2 0 30.50 4.00 1 -2 0 29.80 3.90 -1 2 0 21.40 2.20 -1 2 0 33.20 4.10 -1 2 0 25.70 3.70 0 2 0 2148.09 35.60 0 2 0 2166.98 33.80 0 2 0 2185.38 34.30 0 2 0 2216.18 35.20 -1 -2 0 4.40 2.10 -1 -2 0 3.20 4.40 1 2 0 2.50 5.10 1 2 0 5.00 2.00 1 2 0 4.40 4.50 -2 -2 0 3599.94 59.29 2 2 0 3452.85 61.29 2 2 0 3591.34 59.29 -3 -2 0 84.39 8.90 -3 -2 0 67.29 4.10 3 2 0 69.59 3.90 3 2 0 75.39 6.30 3 2 0 72.19 8.50 3 2 0 59.99 8.60 -4 -2 0 1759.62 31.10 -4 -2 0 1702.93 38.10 -4 -2 0 1693.83 28.60 4 2 0 1629.14 39.60 4 2 0 1719.43 38.40 4 2 0 1729.83 31.30 -5 -2 0 114.99 11.20 -5 -2 0 103.89 5.60 -5 -2 0 100.59 7.40 5 2 0 93.39 11.70 5 2 0 101.49 11.40 5 2 0 107.19 7.80 -6 -2 0 344.27 18.30 -6 -2 0 374.46 10.80 6 2 0 345.27 19.70 6 2 0 384.16 13.90 6 2 0 390.16 19.80 -7 -2 0 234.18 17.80 -7 -2 0 209.08 8.90 -7 -2 0 244.08 11.90 7 2 0 208.98 17.10 7 2 0 222.88 18.00 7 2 0 199.48 19.50 7 2 0 219.28 11.90 -8 -2 0 71.29 6.80 -8 -2 0 59.69 8.50 -8 -2 0 71.09 14.30 8 2 0 105.59 16.50 8 2 0 71.29 14.90 8 2 0 59.29 8.50 8 2 0 83.99 17.20 -9 -2 0 326.27 23.30 -9 -2 0 313.67 12.30 -9 -2 0 346.57 15.90 9 2 0 306.77 16.20 9 2 0 275.07 25.80 9 2 0 315.47 23.10 9 2 0 336.27 23.90 -10 -2 0 54.99 7.20 -10 -2 0 61.39 9.60 10 2 0 57.19 14.70 10 2 0 47.50 13.80 10 2 0 59.99 10.30 -11 -2 0 242.98 11.90 -11 -2 0 265.07 33.70 -11 -2 0 224.88 15.50 11 2 0 302.47 25.60 11 2 0 259.07 24.50 11 2 0 223.88 16.10 -12 -2 0 81.39 8.90 12 2 0 52.29 16.30 12 2 0 67.19 12.20 12 2 0 78.09 18.00 -13 -2 0 115.99 10.00 13 2 0 126.49 15.70 13 2 0 93.59 20.60 14 -3 0 534.35 39.80 14 -3 0 505.65 31.60 14 -3 0 526.25 31.30 -14 3 0 459.15 27.00 13 -3 0 25.60 12.70 13 -3 0 -21.40 13.90 13 -3 0 28.90 14.50 -13 3 0 19.50 10.30 -13 3 0 16.70 8.50 12 -3 0 346.57 31.30 12 -3 0 313.87 23.30 12 -3 0 338.87 22.70 12 -3 0 293.07 26.20 -12 3 0 300.47 18.10 -12 3 0 286.47 20.60 -12 3 0 333.47 26.60 11 -3 0 45.60 12.40 11 -3 0 21.20 12.50 11 -3 0 48.40 13.10 -11 3 0 51.39 13.60 -11 3 0 45.70 9.90 10 -3 0 288.97 19.30 10 -3 0 281.57 22.90 10 -3 0 247.48 18.60 10 -3 0 266.77 24.70 -10 3 0 261.67 18.50 -10 3 0 303.57 23.10 9 -3 0 98.49 15.90 9 -3 0 105.39 13.40 9 -3 0 74.39 16.40 9 -3 0 96.99 13.00 -9 3 0 114.89 15.80 -9 3 0 106.49 13.60 8 -3 0 98.59 11.70 8 -3 0 77.19 15.10 8 -3 0 76.09 10.80 8 -3 0 116.19 15.90 -8 3 0 96.29 12.00 -8 3 0 79.59 12.90 7 -3 0 81.29 10.20 7 -3 0 70.29 12.80 7 -3 0 90.99 13.00 7 -3 0 78.79 11.00 -7 3 0 65.19 9.70 -7 3 0 79.69 12.00 6 -3 0 132.59 13.80 6 -3 0 144.49 11.60 6 -3 0 144.99 13.30 6 -3 0 144.79 10.60 -6 3 0 165.98 15.20 -6 3 0 155.58 12.20 -6 3 0 163.08 13.20 5 -3 0 362.06 16.70 5 -3 0 342.27 12.60 5 -3 0 373.26 17.90 5 -3 0 376.16 15.60 -5 3 0 359.66 17.80 -5 3 0 356.06 16.40 -5 3 0 365.56 15.60 4 -3 0 318.27 16.90 4 -3 0 283.67 14.30 4 -3 0 293.67 13.10 4 -3 0 288.27 9.60 -4 3 0 307.77 15.10 -4 3 0 331.97 14.30 -4 3 0 312.47 13.30 3 -3 0 84.89 8.80 3 -3 0 83.69 4.00 3 -3 0 69.59 8.10 -3 3 0 91.19 8.50 -3 3 0 77.49 8.20 -3 3 0 100.79 9.20 2 -3 0 3.20 4.30 -2 3 0 0.60 4.40 -2 3 0 5.30 4.70 0 3 0 12.10 3.50 0 3 0 13.80 4.30 0 3 0 12.50 3.40 0 3 0 15.80 5.10 0 3 0 12.00 4.40 -1 -3 0 3651.13 60.39 -1 -3 0 3724.33 56.09 1 3 0 3655.83 62.89 1 3 0 3777.12 60.59 1 3 0 3751.52 55.89 -2 -3 0 11.00 2.50 -2 -3 0 15.30 5.50 2 3 0 9.80 5.20 2 3 0 13.60 6.20 2 3 0 11.70 2.40 -3 -3 0 3575.84 64.59 -3 -3 0 3694.03 54.69 3 3 0 3622.24 67.89 3 3 0 3619.44 54.49 3 3 0 3646.84 64.79 3 3 0 3649.23 57.09 -4 -3 0 8.00 2.60 -4 -3 0 16.40 7.30 4 3 0 12.00 3.90 4 3 0 13.60 7.60 4 3 0 3.00 6.60 4 3 0 6.50 2.70 -5 -3 0 1434.16 37.10 -5 -3 0 1398.86 24.50 5 3 0 1388.26 28.20 5 3 0 1397.46 38.90 5 3 0 1340.77 36.30 -6 -3 0 76.59 5.50 6 3 0 98.69 14.20 6 3 0 92.59 13.10 6 3 0 85.59 7.70 -7 -3 0 1737.93 31.60 -7 -3 0 1814.62 47.90 7 3 0 1743.43 36.70 7 3 0 1692.93 47.10 7 3 0 1787.22 49.99 -8 -3 0 17.70 10.00 -8 -3 0 5.70 4.00 8 3 0 12.20 10.70 8 3 0 1.80 11.10 8 3 0 27.40 11.30 8 3 0 5.20 5.20 -9 -3 0 398.06 13.00 -9 -3 0 440.66 26.10 9 3 0 397.46 26.50 9 3 0 423.96 30.00 9 3 0 417.76 17.60 9 3 0 389.06 25.40 -10 -3 0 4.50 4.20 -10 -3 0 4.60 9.90 10 3 0 8.80 10.40 10 3 0 -7.50 9.80 10 3 0 2.20 6.10 10 3 0 2.20 14.50 -11 -3 0 675.23 17.90 11 3 0 611.74 34.60 11 3 0 669.73 28.00 11 3 0 700.63 36.90 -12 -3 0 -4.40 3.90 12 3 0 19.70 13.00 12 3 0 23.60 13.00 12 3 0 4.30 7.60 -13 -3 0 178.48 9.40 13 3 0 195.18 18.10 14 -4 0 80.49 16.50 14 -4 0 66.49 18.50 -14 4 0 111.09 15.40 -14 4 0 83.09 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12.70 5 -4 0 141.99 11.30 5 -4 0 169.78 12.80 5 -4 0 143.09 7.50 -5 4 0 142.69 13.40 -5 4 0 143.89 11.60 -5 4 0 171.38 12.60 4 -4 0 1058.69 18.30 4 -4 0 1091.69 27.40 4 -4 0 1073.19 27.10 -4 4 0 1080.39 27.00 -4 4 0 1101.09 27.50 -4 4 0 1074.49 27.80 3 -4 0 61.19 7.70 3 -4 0 41.00 6.70 -3 4 0 73.09 8.50 -3 4 0 60.19 7.90 -3 4 0 40.40 7.70 2 -4 0 1105.49 24.60 2 -4 0 1123.59 24.10 -2 4 0 1129.49 24.20 -2 4 0 1085.99 24.80 -2 4 0 1072.79 18.10 1 -4 0 25.60 5.00 1 -4 0 34.80 5.30 -1 4 0 38.30 5.90 -1 4 0 41.60 6.10 -1 4 0 31.10 4.70 0 4 0 422.96 11.50 0 4 0 420.76 12.20 0 4 0 405.06 13.70 0 4 0 423.16 13.40 0 4 0 448.66 13.50 -1 -4 0 24.90 5.90 1 4 0 22.70 6.40 1 4 0 19.00 3.70 1 4 0 26.30 5.60 -2 -4 0 154.28 10.60 -2 -4 0 139.39 7.00 2 4 0 155.38 5.90 2 4 0 154.38 12.40 2 4 0 144.59 12.40 -3 -4 0 5.40 6.20 -3 -4 0 6.50 2.60 3 4 0 0.20 6.20 3 4 0 3.90 3.20 3 4 0 3.90 7.30 3 4 0 2.80 2.40 -4 -4 0 8.30 3.40 -4 -4 0 6.90 6.40 4 4 0 15.10 7.10 4 4 0 9.40 2.60 4 4 0 2.70 7.70 4 4 0 8.70 3.70 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26.70 -12 5 0 465.95 30.90 11 -5 0 177.38 16.10 11 -5 0 228.88 22.80 11 -5 0 226.88 24.20 11 -5 0 221.18 19.70 -11 5 0 181.68 20.10 -11 5 0 191.58 18.50 10 -5 0 476.15 27.40 10 -5 0 332.87 26.00 10 -5 0 426.46 23.60 10 -5 0 425.16 19.80 -10 5 0 456.15 26.30 -10 5 0 376.86 28.30 9 -5 0 109.19 11.50 9 -5 0 107.49 16.70 9 -5 0 109.69 14.10 9 -5 0 120.49 16.70 -9 5 0 103.49 13.70 -9 5 0 102.09 15.80 8 -5 0 206.28 18.70 8 -5 0 249.18 18.50 8 -5 0 249.68 17.10 8 -5 0 271.17 19.90 -8 5 0 251.67 17.30 -8 5 0 227.88 19.50 -8 5 0 229.88 17.60 7 -5 0 615.34 24.20 7 -5 0 631.14 17.60 7 -5 0 667.33 26.00 7 -5 0 664.03 26.50 -7 5 0 661.53 27.00 -7 5 0 637.74 24.30 -7 5 0 646.94 25.00 6 -5 0 173.88 13.00 6 -5 0 152.98 14.00 6 -5 0 163.18 7.70 -6 5 0 156.08 14.70 -6 5 0 167.18 13.30 -6 5 0 155.08 13.00 5 -5 0 939.51 27.20 5 -5 0 862.81 15.90 5 -5 0 889.41 26.30 -5 5 0 903.31 26.40 -5 5 0 906.51 26.90 -5 5 0 942.11 27.60 4 -5 0 182.18 12.10 4 -5 0 156.88 11.90 -4 5 0 170.98 11.80 -4 5 0 179.68 12.30 -4 5 0 152.28 14.10 3 -5 0 2969.80 54.49 3 -5 0 2842.82 53.19 -3 5 0 2979.80 55.19 -3 5 0 3081.29 54.09 2 -5 0 103.39 8.80 2 -5 0 102.09 8.50 -2 5 0 87.59 5.50 -2 5 0 101.89 8.60 -2 5 0 98.29 9.00 1 -5 0 553.34 15.90 -1 5 0 534.85 15.10 -1 5 0 578.14 16.70 -1 5 0 567.14 16.70 -1 5 0 553.94 15.50 0 5 0 2.80 4.60 0 5 0 3.00 4.60 0 5 0 2.50 3.70 0 5 0 -3.60 2.90 0 5 0 -0.90 4.60 -1 -5 0 1665.63 35.20 1 5 0 1623.84 37.10 1 5 0 1671.83 31.30 1 5 0 1669.53 29.90 1 5 0 1654.13 34.80 -2 -5 0 14.00 6.50 2 5 0 20.80 6.70 2 5 0 9.00 3.00 2 5 0 7.40 6.60 -3 -5 0 1674.13 29.40 -3 -5 0 1728.73 39.60 3 5 0 1696.73 42.80 3 5 0 1684.73 29.10 3 5 0 1687.43 39.20 -4 -5 0 4.30 2.70 -4 -5 0 5.50 6.70 4 5 0 5.90 3.80 4 5 0 5.10 7.10 4 5 0 1.30 6.20 4 5 0 5.00 2.40 -5 -5 0 2145.89 35.50 -5 -5 0 2005.90 51.79 5 5 0 2120.49 50.09 5 5 0 2061.19 34.20 5 5 0 2056.69 38.40 5 5 0 2078.59 53.69 -6 -5 0 54.69 12.30 -6 -5 0 51.49 5.00 6 5 0 62.69 12.20 6 5 0 58.99 13.60 6 5 0 57.89 7.20 -7 -5 0 742.13 16.40 -7 -5 0 739.33 31.10 7 5 0 753.82 34.00 7 5 0 731.63 20.60 7 5 0 735.33 40.70 -8 -5 0 -17.60 9.00 -8 -5 0 -0.60 3.50 8 5 0 8.40 5.60 8 5 0 0.80 9.70 8 5 0 14.60 11.40 9 5 0 143.39 20.80 9 5 0 127.99 20.00 9 5 0 170.78 26.70 9 5 0 161.38 11.60 10 5 0 49.99 15.20 10 5 0 68.49 16.70 10 5 0 48.00 8.40 11 5 0 238.38 24.60 11 5 0 271.27 15.60 11 5 0 291.37 27.80 12 5 0 90.39 14.00 14 -6 0 61.89 18.20 14 -6 0 59.59 14.20 13 -6 0 208.68 18.30 13 -6 0 219.88 33.50 13 -6 0 226.08 24.90 -13 6 0 188.88 21.30 12 -6 0 128.49 22.30 12 -6 0 117.09 18.80 12 -6 0 104.09 21.50 12 -6 0 125.89 15.20 -12 6 0 102.29 16.00 -12 6 0 144.19 22.20 11 -6 0 365.66 18.70 11 -6 0 386.46 27.10 11 -6 0 336.17 24.10 11 -6 0 303.17 27.00 -11 6 0 341.97 23.20 -11 6 0 387.96 26.50 10 -6 0 277.17 20.60 10 -6 0 296.17 24.50 10 -6 0 288.17 15.50 10 -6 0 281.37 22.80 -10 6 0 273.17 20.60 -10 6 0 281.37 22.50 9 -6 0 231.98 15.60 9 -6 0 191.08 19.20 9 -6 0 186.28 20.00 9 -6 0 176.58 17.10 -9 6 0 184.48 17.40 -9 6 0 209.48 19.00 8 -6 0 515.75 26.00 8 -6 0 452.95 14.80 8 -6 0 461.85 22.30 -8 6 0 424.46 22.20 -8 6 0 463.25 23.00 -8 6 0 476.95 25.30 7 -6 0 75.49 6.20 7 -6 0 108.99 13.80 7 -6 0 70.09 12.00 -7 6 0 78.39 12.80 -7 6 0 76.49 11.30 -7 6 0 103.49 13.80 6 -6 0 129.09 13.20 6 -6 0 115.89 12.10 -6 6 0 117.09 12.50 -6 6 0 140.09 13.10 -6 6 0 134.09 13.80 5 -6 0 374.06 17.20 5 -6 0 322.67 16.70 -5 6 0 319.17 17.00 -5 6 0 382.06 17.30 -5 6 0 380.06 17.90 4 -6 0 273.67 14.70 4 -6 0 294.87 14.80 -4 6 0 292.17 14.90 -4 6 0 281.17 15.20 -4 6 0 265.07 14.10 3 -6 0 407.66 16.50 3 -6 0 394.76 15.60 -3 6 0 372.56 15.50 -3 6 0 400.36 16.80 -3 6 0 384.16 8.30 2 -6 0 1.70 5.00 2 -6 0 -1.90 4.80 -2 6 0 -3.20 5.10 -2 6 0 3.90 3.50 -2 6 0 2.90 5.20 -1 6 0 136.69 10.20 -1 6 0 134.19 9.40 -1 6 0 142.49 9.90 -1 6 0 125.69 8.90 0 6 0 12.30 6.80 0 6 0 17.00 5.30 1 6 0 23.90 6.80 1 6 0 22.00 4.40 1 6 0 33.20 5.50 1 6 0 29.70 7.10 1 6 0 20.50 7.30 -2 -6 0 137.19 11.70 2 6 0 134.99 6.80 2 6 0 142.79 13.30 2 6 0 151.78 11.80 -3 -6 0 12.10 7.40 3 6 0 16.70 7.90 3 6 0 12.20 6.90 3 6 0 22.10 3.80 -4 -6 0 121.79 14.10 4 6 0 120.89 5.90 4 6 0 109.69 7.60 4 6 0 180.48 19.20 4 6 0 115.29 12.70 -5 -6 0 43.80 10.80 5 6 0 53.39 10.60 5 6 0 41.90 4.30 5 6 0 39.60 6.10 5 6 0 37.60 11.20 -6 -6 0 727.83 30.00 6 6 0 729.23 19.60 6 6 0 684.53 32.30 6 6 0 704.93 29.60 -7 -6 0 124.49 17.90 7 6 0 99.49 9.00 7 6 0 115.19 16.60 7 6 0 121.09 18.90 8 6 0 141.59 20.40 8 6 0 130.89 10.20 8 6 0 111.19 17.60 -9 -6 0 49.80 14.10 9 6 0 46.50 17.20 9 6 0 64.59 15.60 9 6 0 56.39 8.10 9 6 0 47.40 15.00 10 6 0 214.18 24.10 10 6 0 212.28 25.70 10 6 0 228.58 13.70 11 6 0 42.30 15.50 11 6 0 61.79 9.50 14 -7 0 152.88 17.80 -14 7 0 166.08 23.00 13 -7 0 136.69 15.60 -13 7 0 121.89 18.40 12 -7 0 111.89 13.10 12 -7 0 105.39 18.20 -12 7 0 111.29 19.40 -12 7 0 147.69 20.20 11 -7 0 507.15 19.70 11 -7 0 561.74 32.90 -11 7 0 517.85 27.90 -11 7 0 579.34 34.50 10 -7 0 129.99 20.00 10 -7 0 173.78 18.60 -10 7 0 106.39 15.60 -10 7 0 164.28 20.60 9 -7 0 638.94 17.60 9 -7 0 663.73 29.10 9 -7 0 687.23 31.50 -9 7 0 679.43 32.00 -9 7 0 733.03 30.50 -9 7 0 599.54 28.60 8 -7 0 46.30 5.00 8 -7 0 50.29 12.80 8 -7 0 27.40 9.70 -8 7 0 45.20 11.90 -8 7 0 43.50 11.00 -8 7 0 45.00 12.20 7 -7 0 352.66 20.20 7 -7 0 349.47 19.30 -7 7 0 369.86 20.30 -7 7 0 354.36 19.90 -7 7 0 340.77 21.00 6 -7 0 8.50 7.80 6 -7 0 8.80 6.80 -6 7 0 17.40 8.10 -6 7 0 -0.30 6.90 -6 7 0 6.30 7.10 5 -7 0 1191.78 33.30 5 -7 0 1208.68 32.70 -5 7 0 1210.38 34.20 -5 7 0 1270.97 33.20 -5 7 0 1294.57 33.90 4 -7 0 12.20 6.90 4 -7 0 12.20 6.60 -4 7 0 9.70 6.30 -4 7 0 17.50 6.90 3 -7 0 1460.35 33.50 3 -7 0 1464.25 34.90 -3 7 0 1442.16 25.80 -3 7 0 1477.75 36.10 -3 7 0 1587.14 35.20 2 -7 0 3.40 5.40 -2 7 0 4.60 5.60 -2 7 0 2.40 3.90 -2 7 0 8.20 5.90 -2 7 0 -0.30 4.40 -1 7 0 3430.06 62.19 -1 7 0 3483.75 63.59 -1 7 0 3616.04 64.59 -1 7 0 3526.65 63.69 -1 7 0 3574.04 61.79 0 7 0 10.40 5.60 0 7 0 15.20 5.00 0 7 0 15.10 4.70 0 7 0 8.10 5.90 0 7 0 20.70 6.40 1 7 0 1429.76 30.90 1 7 0 1435.86 34.30 1 7 0 1417.46 34.60 1 7 0 1402.36 36.60 1 7 0 1365.76 28.50 -2 -7 0 3.40 6.60 2 7 0 3.80 6.70 2 7 0 3.70 4.00 2 7 0 3.80 5.70 2 7 0 6.80 3.30 -3 -7 0 317.27 17.70 3 7 0 317.67 10.30 3 7 0 287.67 17.00 3 7 0 307.07 19.60 -4 -7 0 21.90 10.10 4 7 0 4.90 4.30 4 7 0 3.20 8.30 4 7 0 1.70 6.90 4 7 0 2.10 3.00 -5 -7 0 209.38 17.60 5 7 0 199.68 7.40 5 7 0 191.18 10.10 5 7 0 218.88 17.70 5 7 0 199.58 21.00 -6 -7 0 13.30 10.20 6 7 0 9.30 4.90 6 7 0 9.80 9.80 -7 -7 0 552.14 29.00 7 7 0 560.14 17.60 7 7 0 578.94 29.20 7 7 0 590.44 32.80 8 7 0 30.90 12.30 8 7 0 41.10 14.30 8 7 0 23.20 6.30 9 7 0 337.87 26.40 9 7 0 420.66 36.40 9 7 0 381.66 15.10 10 7 0 56.99 16.30 10 7 0 52.49 8.20 10 7 0 38.20 14.40 11 7 0 32.10 8.30 14 -8 0 28.50 9.70 -14 8 0 11.50 12.50 13 -8 0 148.39 13.40 -13 8 0 226.28 38.60 12 -8 0 3.50 6.30 12 -8 0 8.70 12.00 -12 8 0 14.20 12.30 -12 8 0 5.20 10.00 11 -8 0 256.17 12.20 11 -8 0 290.37 23.70 11 -8 0 265.97 25.50 -11 8 0 273.07 22.30 10 -8 0 4.20 4.30 10 -8 0 16.30 11.20 10 -8 0 5.20 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0 410.36 17.80 1 8 0 129.29 12.00 1 8 0 125.49 8.50 1 8 0 122.19 9.80 1 8 0 140.39 13.30 1 8 0 121.39 11.70 2 8 0 293.47 17.00 2 8 0 310.87 13.40 2 8 0 318.27 19.40 2 8 0 299.97 17.00 2 8 0 306.57 11.30 -3 -8 0 -3.00 7.70 3 8 0 6.40 8.00 3 8 0 -4.40 4.40 3 8 0 10.30 8.50 -4 -8 0 965.60 34.00 4 8 0 1075.99 34.80 4 8 0 1052.69 24.90 4 8 0 998.80 39.10 4 8 0 1025.00 21.40 -5 -8 0 6.90 9.50 5 8 0 1.40 7.80 5 8 0 1.10 2.80 5 8 0 2.20 4.40 5 8 0 14.10 10.20 -6 -8 0 501.45 27.20 6 8 0 504.45 16.50 6 8 0 558.14 28.20 6 8 0 551.94 31.50 7 8 0 -4.50 8.50 7 8 0 10.50 10.90 7 8 0 1.70 4.60 -8 -8 0 327.47 25.60 8 8 0 308.07 24.00 8 8 0 318.67 13.60 8 8 0 316.07 27.70 9 8 0 46.10 15.80 9 8 0 19.90 5.90 9 8 0 29.90 12.90 10 8 0 295.67 27.40 10 8 0 344.47 13.70 14 -9 0 -12.10 7.60 -14 9 0 0.70 13.40 13 -9 0 48.80 7.60 -13 9 0 42.90 15.00 12 -9 0 3.00 11.40 -12 9 0 14.70 11.50 -12 9 0 -2.90 11.90 11 -9 0 78.89 17.10 11 -9 0 55.29 17.30 -11 9 0 59.19 16.00 -11 9 0 42.80 13.90 10 -9 0 2.70 9.70 10 -9 0 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570.44 22.50 1 9 0 558.24 24.30 1 9 0 571.94 17.70 1 9 0 557.94 19.70 2 9 0 41.90 6.20 2 9 0 46.60 7.80 2 9 0 55.09 11.10 2 9 0 57.59 10.80 2 9 0 65.09 12.80 3 9 0 1000.70 34.00 3 9 0 1049.79 38.00 3 9 0 987.10 26.10 3 9 0 1035.50 23.20 3 9 0 1044.80 34.10 -4 -9 0 17.50 10.60 4 9 0 13.60 8.90 4 9 0 19.00 5.80 4 9 0 14.60 10.50 4 9 0 12.80 5.40 -5 -9 0 170.78 20.00 5 9 0 137.39 17.50 5 9 0 131.29 19.10 5 9 0 129.39 9.60 5 9 0 138.49 6.80 5 9 0 133.69 9.60 -6 -9 0 31.10 11.20 6 9 0 1.80 4.60 6 9 0 9.30 9.90 6 9 0 12.90 4.90 6 9 0 16.50 11.10 -7 -9 0 41.20 12.70 7 9 0 97.49 19.50 7 9 0 66.09 14.10 7 9 0 69.99 8.00 7 9 0 68.29 7.50 8 9 0 30.70 6.20 8 9 0 26.20 11.70 9 9 0 33.90 5.90 9 9 0 39.10 14.10 9 9 0 24.90 6.00 -13 10 0 282.97 26.00 12 -10 0 42.70 17.20 -12 10 0 22.30 13.50 11 -10 0 287.47 26.50 -11 10 0 275.37 24.40 -11 10 0 259.47 24.20 -11 10 0 235.78 23.90 10 -10 0 131.79 20.50 -10 10 0 92.09 17.10 -10 10 0 111.69 19.50 -10 10 0 89.89 17.00 9 -10 0 48.40 14.20 -9 10 0 59.29 13.30 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24.00 -8 11 0 283.87 22.00 -8 11 0 289.37 21.90 7 -11 0 109.69 16.10 7 -11 0 84.19 14.60 -7 11 0 110.19 16.80 -7 11 0 102.19 17.20 -7 11 0 76.09 14.10 6 -11 0 412.56 21.90 6 -11 0 466.05 24.50 -6 11 0 395.76 22.40 -6 11 0 419.66 22.10 -6 11 0 431.76 23.20 -6 11 0 422.36 24.70 5 -11 0 132.39 15.30 -5 11 0 121.99 14.40 -5 11 0 127.69 18.20 -5 11 0 112.39 15.90 -5 11 0 127.89 15.20 4 -11 0 96.49 13.10 -4 11 0 96.39 13.10 -4 11 0 86.59 13.50 -4 11 0 91.39 12.80 -4 11 0 81.09 6.60 -3 11 0 98.19 12.70 -3 11 0 88.39 13.00 -3 11 0 63.29 11.20 -3 11 0 74.09 12.50 -2 11 0 43.60 10.50 -2 11 0 79.09 12.20 -2 11 0 56.19 9.40 -2 11 0 66.19 11.60 -2 11 0 56.09 9.70 -1 11 0 140.19 13.20 -1 11 0 123.29 13.80 -1 11 0 121.29 14.20 -1 11 0 133.29 13.10 -1 11 0 128.59 11.70 0 11 0 77.89 9.80 0 11 0 80.09 12.50 0 11 0 91.79 12.10 0 11 0 69.59 11.70 0 11 0 101.99 13.50 1 11 0 -4.70 7.20 1 11 0 -2.70 4.40 1 11 0 4.40 8.10 1 11 0 3.70 5.50 1 11 0 -2.40 7.00 2 11 0 49.90 11.90 2 11 0 68.19 12.30 2 11 0 59.59 7.60 2 11 0 61.49 12.80 2 11 0 49.70 8.70 3 11 0 18.90 6.80 3 11 0 12.80 5.20 3 11 0 9.20 10.30 3 11 0 8.40 8.60 4 11 0 41.50 12.50 4 11 0 32.20 11.60 4 11 0 42.60 12.20 4 11 0 28.60 5.50 4 11 0 42.30 7.80 4 11 0 34.60 7.10 5 11 0 29.60 13.40 5 11 0 58.89 8.50 5 11 0 48.50 13.60 5 11 0 56.39 5.50 5 11 0 81.29 15.50 5 11 0 64.09 8.30 6 11 0 -6.40 9.40 6 11 0 6.50 9.70 6 11 0 0.30 4.60 6 11 0 23.50 13.30 6 11 0 4.80 4.90 7 11 0 10.50 15.90 7 11 0 5.10 8.60 7 11 0 7.00 4.60 12 -12 0 36.50 16.40 -12 12 0 16.40 15.00 -11 12 0 298.47 25.20 -11 12 0 244.88 25.80 -11 12 0 309.97 27.20 10 -12 0 23.20 14.10 -10 12 0 33.50 14.60 -10 12 0 38.60 13.80 9 -12 0 155.98 21.00 -9 12 0 156.58 21.10 -9 12 0 104.19 17.80 -9 12 0 130.29 22.60 8 -12 0 145.89 18.20 8 -12 0 195.78 22.90 -8 12 0 131.79 19.90 -8 12 0 105.99 16.70 -8 12 0 130.79 18.20 -8 12 0 159.18 16.90 7 -12 0 13.50 10.90 -7 12 0 7.00 9.70 -7 12 0 21.90 9.80 -7 12 0 11.90 10.10 -7 12 0 7.50 10.70 6 -12 0 488.45 24.00 -6 12 0 429.96 26.30 -6 12 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42.00 11.60 -3 13 0 31.10 9.80 -2 13 0 129.99 15.80 -2 13 0 157.48 15.80 -2 13 0 146.89 15.80 -2 13 0 140.59 13.90 -2 13 0 130.29 13.30 -1 13 0 36.90 10.30 -1 13 0 26.80 10.40 -1 13 0 37.50 10.20 0 13 0 45.30 9.70 0 13 0 79.09 14.20 0 13 0 55.39 12.30 0 13 0 61.69 9.90 0 13 0 49.99 11.90 1 13 0 51.59 13.20 1 13 0 41.60 11.30 1 13 0 63.79 14.20 1 13 0 53.09 8.70 1 13 0 40.60 9.50 2 13 0 40.20 12.60 2 13 0 40.50 11.20 2 13 0 55.19 9.90 2 13 0 44.10 12.10 2 13 0 38.10 7.60 3 13 0 104.49 17.00 3 13 0 141.69 17.80 3 13 0 100.99 17.40 3 13 0 105.29 11.70 3 13 0 99.99 9.10 4 13 0 20.80 7.30 4 13 0 15.20 5.00 4 13 0 11.20 10.20 4 13 0 20.60 15.90 4 13 0 29.20 10.80 5 13 0 195.48 7.40 5 13 0 168.48 24.80 5 13 0 171.18 11.20 5 13 0 194.38 14.10 5 13 0 265.37 37.00 5 13 0 208.78 20.00 11 -14 0 6.40 14.20 -11 14 0 3.00 10.80 10 -14 0 270.07 41.70 -10 14 0 246.18 27.40 -10 14 0 279.07 25.60 -10 14 0 274.77 24.50 -10 14 0 243.48 25.10 9 -14 0 -4.00 9.90 -9 14 0 8.10 12.20 -9 14 0 -2.60 9.70 -9 14 0 1.70 14.50 -9 14 0 -23.30 9.40 8 -14 0 190.38 19.20 -8 14 0 193.48 19.90 -8 14 0 215.08 21.90 -8 14 0 207.08 20.90 7 -14 0 5.30 9.90 -7 14 0 4.30 9.80 -7 14 0 3.60 10.30 -7 14 0 27.60 10.80 -7 14 0 20.10 12.60 6 -14 0 185.88 17.70 -6 14 0 186.68 17.80 -6 14 0 163.38 18.40 -6 14 0 166.18 21.90 -6 14 0 174.28 18.90 -5 14 0 16.10 10.90 -5 14 0 27.50 10.90 -5 14 0 29.00 9.90 -5 14 0 -0.40 9.70 -4 14 0 243.48 19.00 -4 14 0 228.08 18.90 -4 14 0 240.48 18.50 -4 14 0 191.58 15.20 -4 14 0 283.57 21.70 -3 14 0 34.10 10.40 -3 14 0 46.70 9.20 -3 14 0 47.80 11.50 -3 14 0 48.20 12.90 -3 14 0 43.20 11.90 -2 14 0 914.21 34.80 -2 14 0 836.02 29.90 -2 14 0 857.01 32.90 -2 14 0 848.62 33.20 -2 14 0 862.51 30.40 -1 14 0 15.00 9.20 -1 14 0 18.30 7.40 -1 14 0 9.30 7.80 -1 14 0 -2.90 16.50 0 14 0 310.57 17.20 0 14 0 301.27 22.70 0 14 0 345.67 20.10 0 14 0 325.97 22.80 0 14 0 313.27 21.10 1 14 0 -2.70 8.10 1 14 0 -0.80 7.50 1 14 0 1.00 5.20 1 14 0 9.10 8.80 1 14 0 -1.60 8.80 2 14 0 71.89 13.10 2 14 0 76.79 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13.20 -2 14 -21 98.19 17.30 2 -14 21 108.09 18.10 -3 14 -21 10.20 11.30 3 -14 21 -5.50 9.30 4 -14 21 151.88 18.20 5 -14 21 41.20 11.50 6 -14 21 113.59 14.20 2 13 -21 116.29 24.50 2 13 -21 204.28 11.80 1 13 -21 18.40 11.70 1 13 -21 4.30 5.90 0 13 -21 172.18 22.10 0 13 -21 204.58 22.60 0 13 -21 196.28 15.00 0 13 -21 191.78 28.20 0 -13 21 235.68 23.40 -1 13 -21 29.90 13.10 -1 13 -21 64.39 11.20 -1 13 -21 23.30 16.20 -1 13 -21 70.59 16.20 -2 13 -21 255.47 22.70 -2 13 -21 224.58 17.40 -2 13 -21 203.28 22.40 -2 13 -21 257.47 28.30 2 -13 21 245.38 21.90 -3 13 -21 26.70 12.90 -3 13 -21 37.00 15.80 -3 13 -21 29.50 13.30 -3 13 -21 51.19 11.80 3 -13 21 38.60 12.20 -4 13 -21 97.09 22.30 -4 13 -21 75.69 16.00 4 -13 21 136.89 17.80 -5 13 -21 10.80 14.20 -5 13 -21 13.10 12.10 5 -13 21 3.60 9.50 -6 13 -21 10.30 25.20 7 -13 21 32.10 8.80 8 -13 21 21.70 9.40 4 12 -21 21.40 14.80 3 12 -21 36.60 14.20 3 12 -21 25.70 5.10 3 12 -21 9.40 6.60 2 12 -21 26.20 15.20 2 12 -21 28.20 6.50 2 12 -21 36.70 14.30 1 12 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6.20 12.70 3 10 -21 435.66 29.60 3 10 -21 429.46 14.70 3 10 -21 463.35 39.10 -3 -10 21 428.76 31.10 2 10 -21 30.10 14.70 2 10 -21 20.10 11.90 2 10 -21 19.70 6.30 -2 -10 21 0.70 8.00 1 10 -21 352.56 28.50 1 10 -21 375.16 26.90 1 10 -21 376.46 16.70 0 10 -21 14.70 11.20 0 10 -21 -11.80 11.10 0 10 -21 8.20 6.70 0 -10 21 5.60 9.70 -1 10 -21 380.86 29.10 -1 10 -21 360.46 18.70 -1 10 -21 380.86 25.50 1 -10 21 335.27 24.00 -2 10 -21 -7.40 6.90 -2 10 -21 -3.70 10.20 -2 10 -21 -4.40 10.50 2 -10 21 5.50 9.60 -3 10 -21 139.39 14.50 -3 10 -21 133.99 17.60 -3 10 -21 151.98 24.10 -3 10 -21 176.48 21.10 3 -10 21 149.88 17.90 -4 10 -21 -2.80 8.70 -4 10 -21 2.70 9.60 -4 10 -21 1.90 12.30 4 -10 21 -6.80 9.10 4 -10 21 -2.30 13.10 -5 10 -21 363.56 29.30 -5 10 -21 338.77 24.70 -5 10 -21 354.06 21.40 5 -10 21 391.86 23.00 -6 10 -21 7.40 13.90 -6 10 -21 27.40 13.00 6 -10 21 16.40 10.20 -7 10 -21 312.57 25.40 -7 10 -21 290.07 14.90 7 -10 21 304.47 20.50 -8 10 -21 24.50 16.00 -8 10 -21 5.20 7.70 -8 10 -21 0.10 13.50 8 -10 21 -14.20 8.90 -9 10 -21 141.49 20.50 -9 10 -21 168.58 18.40 9 -10 21 160.68 17.60 -10 10 -21 69.99 14.00 -10 10 -21 55.39 16.20 10 -10 21 64.39 14.10 10 -10 21 46.90 12.50 -7 -9 21 9.70 8.40 6 9 -21 14.40 12.30 6 9 -21 23.10 13.90 -6 -9 21 28.30 8.10 5 9 -21 -6.10 11.00 5 9 -21 -5.40 11.10 -5 -9 21 6.70 5.70 4 9 -21 33.40 15.30 4 9 -21 18.10 4.60 4 9 -21 7.60 11.80 -4 -9 21 51.49 16.80 3 9 -21 5.70 11.80 3 9 -21 17.40 5.60 3 9 -21 17.20 12.60 -3 -9 21 12.40 12.80 2 9 -21 41.60 13.50 2 9 -21 61.49 8.90 2 9 -21 47.30 14.80 1 9 -21 47.10 14.60 1 9 -21 41.30 8.00 1 9 -21 42.20 16.40 -1 -9 21 53.79 14.50 0 9 -21 56.49 9.50 0 9 -21 38.50 14.60 -1 9 -21 80.09 17.70 -1 9 -21 63.99 10.20 1 -9 21 60.49 13.50 -2 9 -21 29.80 8.90 -2 9 -21 29.50 15.00 -2 9 -21 46.70 13.60 2 -9 21 36.00 11.90 -3 9 -21 26.30 14.30 -3 9 -21 32.70 9.70 -3 9 -21 33.60 12.00 3 -9 21 38.50 12.10 -4 9 -21 124.29 18.20 -4 9 -21 126.29 14.80 -4 9 -21 91.79 19.80 4 -9 21 86.69 14.80 -5 9 -21 188.58 17.20 -5 9 -21 137.69 21.90 -5 9 -21 195.38 19.40 5 -9 21 197.08 18.60 -6 9 -21 21.00 9.80 -6 9 -21 34.80 12.70 -6 9 -21 8.80 14.70 6 -9 21 3.00 10.20 -7 9 -21 211.58 25.90 -7 9 -21 239.58 15.50 -7 9 -21 205.08 21.80 7 -9 21 260.27 20.30 7 -9 21 249.97 16.00 -8 9 -21 15.40 11.20 -8 9 -21 1.90 13.60 8 -9 21 16.80 8.90 8 -9 21 7.50 10.80 -9 9 -21 270.87 30.40 -9 9 -21 367.26 23.90 -9 9 -21 330.97 27.10 9 -9 21 344.77 23.60 9 -9 21 342.57 22.20 -10 9 -21 52.79 14.40 -10 9 -21 64.89 16.00 10 -9 21 51.69 14.90 10 -9 21 62.69 14.40 -11 9 -21 82.09 18.70 -11 9 -21 52.69 15.60 11 -9 21 50.39 13.90 11 -9 21 35.60 14.90 -8 -8 21 20.80 9.50 7 8 -21 330.17 29.10 7 8 -21 360.16 29.80 -7 -8 21 368.56 20.90 6 8 -21 3.50 13.10 -6 -8 21 -0.90 7.30 5 8 -21 9.60 11.40 5 8 -21 27.10 11.70 5 8 -21 22.50 14.40 -5 -8 21 49.00 8.50 4 8 -21 7.40 11.30 4 8 -21 13.50 9.50 4 8 -21 6.50 4.50 4 8 -21 10.70 12.70 -4 -8 21 -1.90 11.00 -4 -8 21 15.20 5.50 3 8 -21 151.78 21.10 3 8 -21 208.78 24.00 3 8 -21 150.48 10.10 2 8 -21 2.60 10.30 2 8 -21 1.40 11.50 2 8 -21 0.40 5.50 -2 -8 21 -13.00 9.70 1 8 -21 535.75 29.70 1 8 -21 569.74 20.50 1 8 -21 535.55 31.70 -1 -8 21 522.45 29.30 0 8 -21 13.30 11.10 0 8 -21 22.60 13.00 0 8 -21 16.60 7.10 0 -8 21 15.90 10.80 -1 8 -21 674.73 34.50 -1 8 -21 701.83 24.30 -1 8 -21 692.63 31.80 1 -8 21 716.93 31.00 -2 8 -21 -3.60 7.10 -2 8 -21 -0.80 12.10 -2 8 -21 5.00 10.50 2 -8 21 6.90 9.50 -3 8 -21 393.56 25.20 -3 8 -21 458.85 21.30 -3 8 -21 386.66 28.30 3 -8 21 398.76 23.60 -4 8 -21 128.79 17.10 -4 8 -21 99.09 18.90 -4 8 -21 148.69 16.00 4 -8 21 118.69 16.50 -5 8 -21 169.68 18.70 -5 8 -21 202.58 23.70 5 -8 21 186.48 18.80 5 -8 21 187.88 11.40 -6 8 -21 124.89 17.20 -6 8 -21 120.19 21.60 -6 8 -21 118.39 12.10 -6 8 -21 131.79 15.40 6 -8 21 121.69 16.40 6 -8 21 124.89 12.40 -7 8 -21 45.30 10.40 -7 8 -21 31.70 15.90 -7 8 -21 28.60 16.70 -7 8 -21 4.10 10.00 7 -8 21 31.80 10.10 7 -8 21 52.99 13.80 -8 8 -21 111.69 22.30 -8 8 -21 191.48 17.60 -8 8 -21 185.78 20.50 8 -8 21 163.78 16.20 8 -8 21 174.58 19.70 -9 8 -21 71.29 17.20 -9 8 -21 74.19 14.80 -9 8 -21 27.30 16.10 9 -8 21 84.29 16.50 -10 8 -21 45.10 19.10 -10 8 -21 61.89 14.80 -10 8 -21 45.00 14.20 10 -8 21 25.30 14.00 10 -8 21 23.40 12.40 -11 8 -21 67.99 16.90 -11 8 -21 50.09 14.60 11 -8 21 71.39 17.00 11 -8 21 94.29 17.80 8 7 -21 110.39 20.70 8 7 -21 119.59 21.90 -8 -7 21 98.39 15.10 7 7 -21 7.50 11.70 7 7 -21 12.30 12.90 -7 -7 21 -3.20 7.40 6 7 -21 82.49 18.40 6 7 -21 84.89 16.50 6 7 -21 90.79 18.60 -6 -7 21 88.19 11.90 5 7 -21 24.20 10.90 5 7 -21 11.40 4.30 5 7 -21 8.10 10.70 5 7 -21 -2.70 10.20 -5 -7 21 5.10 12.00 -5 -7 21 9.60 6.40 4 7 -21 6.50 12.40 4 7 -21 32.10 14.20 4 7 -21 8.60 4.90 4 7 -21 30.90 11.10 -4 -7 21 27.00 6.50 3 7 -21 -3.80 9.70 3 7 -21 0.70 10.00 3 7 -21 18.10 12.20 3 7 -21 4.90 5.20 -3 -7 21 9.70 11.80 -3 -7 21 7.30 4.40 2 7 -21 43.10 13.10 2 7 -21 73.39 16.40 2 7 -21 68.89 8.90 -2 -7 21 58.29 14.20 1 7 -21 -3.10 9.90 1 7 -21 7.10 10.90 1 7 -21 15.60 12.10 -1 -7 21 7.30 10.00 0 7 -21 171.08 22.70 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33.70 12.80 -9 7 -21 10.40 14.90 9 -7 21 30.80 12.40 9 -7 21 48.30 15.20 -10 7 -21 64.39 14.40 -10 7 -21 75.19 21.60 10 -7 21 67.59 18.00 10 -7 21 70.19 16.20 -11 7 -21 38.50 20.70 -11 7 -21 8.30 11.30 11 -7 21 20.20 12.50 -10 -6 21 -6.50 10.30 9 6 -21 291.87 27.70 -9 -6 21 322.67 27.70 8 6 -21 4.30 13.20 8 6 -21 0.10 10.10 -8 -6 21 7.80 9.90 7 6 -21 313.47 25.80 7 6 -21 271.47 26.20 7 6 -21 286.17 25.60 -7 -6 21 298.07 19.90 6 6 -21 10.10 10.10 6 6 -21 7.80 10.80 6 6 -21 4.60 11.40 -6 -6 21 10.40 13.70 -6 -6 21 0.00 8.00 5 6 -21 350.16 26.70 5 6 -21 375.16 24.30 5 6 -21 334.27 12.50 5 6 -21 360.06 25.90 -5 -6 21 354.56 17.60 4 6 -21 17.30 10.80 4 6 -21 17.50 11.60 4 6 -21 1.40 4.70 4 6 -21 4.70 10.50 -4 -6 21 2.00 6.20 3 6 -21 352.96 14.60 3 6 -21 347.47 25.00 3 6 -21 295.37 23.60 3 6 -21 335.47 21.20 -3 -6 21 331.57 13.20 -3 -6 21 339.37 24.90 2 6 -21 3.30 10.20 2 6 -21 1.90 5.40 2 6 -21 -2.50 9.50 -2 -6 21 -0.40 4.30 -2 -6 21 6.90 10.30 1 6 -21 720.13 37.30 1 6 -21 741.83 33.70 -1 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327.37 23.10 -8 6 -21 300.67 22.30 8 -6 21 306.37 25.10 8 -6 21 305.77 21.80 -9 6 -21 0.70 10.50 -9 6 -21 10.70 10.70 -9 6 -21 22.30 19.90 9 -6 21 24.10 14.20 9 -6 21 6.20 11.20 -10 6 -21 407.66 29.10 -10 6 -21 380.96 25.30 -10 6 -21 304.47 32.20 10 -6 21 398.96 27.10 -11 6 -21 25.00 10.80 11 -6 21 15.70 11.60 11 -6 21 -6.60 15.30 -10 -5 21 46.70 13.20 9 5 -21 22.80 12.80 9 5 -21 15.30 13.80 -9 -5 21 43.50 12.80 8 5 -21 167.08 23.40 8 5 -21 164.78 25.10 -8 -5 21 212.18 19.20 7 5 -21 -6.40 11.10 7 5 -21 5.30 9.70 7 5 -21 11.80 11.70 -7 -5 21 1.30 9.10 6 5 -21 182.38 9.60 6 5 -21 163.68 19.90 6 5 -21 222.38 25.40 6 5 -21 185.08 19.50 -6 -5 21 214.88 28.10 5 5 -21 4.10 10.70 5 5 -21 -5.10 9.90 5 5 -21 -0.60 8.60 5 5 -21 -1.20 4.30 -5 -5 21 -7.30 6.60 4 5 -21 36.10 12.60 4 5 -21 28.10 6.50 4 5 -21 47.00 11.70 4 5 -21 31.50 13.50 -4 -5 21 31.60 14.10 -4 -5 21 35.70 8.60 -4 -5 21 31.40 6.90 3 5 -21 3.10 7.70 3 5 -21 3.50 9.80 3 5 -21 6.70 10.70 3 5 -21 3.40 5.30 -3 -5 21 5.60 5.50 -3 -5 21 7.50 6.20 -3 -5 21 10.40 11.40 2 5 -21 201.88 12.50 2 5 -21 231.08 38.40 -2 -5 21 212.58 11.50 -2 -5 21 197.78 12.80 -2 -5 21 216.08 20.20 1 5 -21 -1.50 10.30 1 5 -21 5.10 10.50 1 5 -21 -3.00 10.20 -1 -5 21 -1.80 9.20 -1 -5 21 11.10 5.20 -1 -5 21 6.60 4.80 -1 -5 21 1.70 6.20 -1 -5 21 9.00 9.80 0 5 -21 39.20 12.90 0 5 -21 43.90 14.10 0 5 -21 38.10 8.30 0 -5 21 43.10 6.30 0 -5 21 28.90 8.60 0 -5 21 39.60 12.40 0 -5 21 45.00 13.20 -1 5 -21 9.00 11.30 -1 5 -21 15.10 11.50 -1 5 -21 6.60 6.80 1 -5 21 -8.00 5.80 1 -5 21 16.80 10.80 1 -5 21 7.00 10.60 1 -5 21 11.50 5.20 -2 5 -21 607.24 23.00 -2 5 -21 601.04 29.90 -2 5 -21 665.33 31.80 2 -5 21 621.34 18.60 2 -5 21 645.94 30.40 2 -5 21 577.94 28.30 -3 5 -21 23.40 8.20 -3 5 -21 26.20 14.30 3 -5 21 33.60 7.80 3 -5 21 62.79 14.00 3 -5 21 24.00 12.20 -4 5 -21 731.13 34.80 -4 5 -21 661.63 25.40 4 -5 21 705.33 33.60 4 -5 21 643.84 30.30 4 -5 21 696.73 23.30 -5 5 -21 16.10 12.70 -5 5 -21 22.50 9.90 -5 5 -21 17.10 8.80 -5 5 -21 29.30 9.20 5 -5 21 33.70 13.30 5 -5 21 20.30 13.00 5 -5 21 28.10 9.30 -6 5 -21 393.66 21.50 -6 5 -21 379.56 28.70 -6 5 -21 344.57 27.90 6 -5 21 379.16 20.70 6 -5 21 398.46 28.50 6 -5 21 379.66 25.60 -7 5 -21 17.20 10.80 -7 5 -21 6.60 14.00 -7 5 -21 21.20 10.00 7 -5 21 15.20 12.40 7 -5 21 -9.20 14.40 7 -5 21 16.60 10.10 -8 5 -21 135.49 17.60 -8 5 -21 159.28 19.40 -8 5 -21 150.88 24.30 -8 5 -21 125.69 17.80 8 -5 21 147.29 21.30 8 -5 21 126.39 17.60 8 -5 21 121.19 22.30 -9 5 -21 13.50 10.10 -9 5 -21 -6.90 15.30 -9 5 -21 24.90 12.90 9 -5 21 14.70 11.80 9 -5 21 21.60 15.60 -10 5 -21 303.27 31.30 -10 5 -21 325.57 26.40 -10 5 -21 272.27 22.30 10 -5 21 257.27 24.30 -11 5 -21 16.90 11.40 11 -5 21 0.30 17.30 11 -5 21 29.90 13.30 10 4 -21 5.80 13.40 10 4 -21 8.40 11.80 -10 -4 21 10.10 11.40 9 4 -21 89.59 19.50 9 4 -21 132.09 22.10 -9 -4 21 148.49 19.20 8 4 -21 14.10 11.50 8 4 -21 3.90 11.90 8 4 -21 0.90 10.70 -8 -4 21 9.80 10.60 7 4 -21 231.68 24.00 7 4 -21 231.48 21.40 7 4 -21 230.28 21.80 -7 -4 21 241.08 19.40 -7 -4 21 246.08 15.10 6 4 -21 26.30 11.90 6 4 -21 17.00 5.50 6 4 -21 49.10 14.10 6 4 -21 44.50 13.90 -6 -4 21 48.50 12.10 -6 -4 21 39.80 6.50 5 4 -21 357.26 14.50 5 4 -21 345.27 24.20 5 4 -21 339.07 25.10 5 4 -21 367.26 23.00 -5 -4 21 362.96 19.20 -5 -4 21 348.07 14.10 4 4 -21 4.50 8.70 4 4 -21 5.10 5.40 4 4 -21 6.40 10.60 4 4 -21 0.70 9.90 -4 -4 21 -15.60 8.70 -4 -4 21 -0.90 5.20 -4 -4 21 -11.70 6.50 3 4 -21 241.18 13.20 3 4 -21 279.87 21.50 3 4 -21 264.57 22.60 3 4 -21 261.57 17.90 -3 -4 21 258.17 14.80 -3 -4 21 259.57 13.80 -3 -4 21 253.67 21.40 2 4 -21 5.40 10.00 2 4 -21 5.10 5.80 2 4 -21 0.80 10.00 2 4 -21 6.90 9.10 -2 -4 21 0.90 6.20 -2 -4 21 5.20 6.20 -2 -4 21 -5.80 9.30 1 4 -21 75.79 17.60 1 4 -21 53.39 14.50 1 4 -21 45.10 12.30 -1 -4 21 86.19 15.70 -1 -4 21 65.79 9.70 -1 -4 21 84.29 15.00 -1 -4 21 69.49 11.40 0 4 -21 3.50 6.00 0 4 -21 15.80 10.90 0 4 -21 -5.70 8.60 0 -4 21 9.00 5.80 0 -4 21 9.90 6.70 0 -4 21 2.30 9.00 0 -4 21 2.30 9.30 -1 4 -21 55.09 9.40 -1 4 -21 61.29 13.30 -1 4 -21 62.29 14.50 1 -4 21 71.29 14.50 1 -4 21 50.89 9.50 1 -4 21 57.29 13.60 1 -4 21 70.39 10.00 -2 4 -21 161.08 13.40 -2 4 -21 147.79 18.40 2 -4 21 155.68 14.20 2 -4 21 142.39 17.50 2 -4 21 142.69 17.10 2 -4 21 176.88 12.50 -3 4 -21 62.89 10.60 -3 4 -21 39.60 13.50 3 -4 21 50.79 13.80 3 -4 21 41.70 13.10 3 -4 21 40.10 9.80 3 -4 21 30.60 8.50 -4 4 -21 162.28 23.20 -4 4 -21 210.28 15.80 4 -4 21 220.78 21.80 4 -4 21 233.88 15.90 4 -4 21 216.78 20.70 -5 4 -21 35.70 10.10 -5 4 -21 43.00 15.10 -5 4 -21 44.10 11.10 5 -4 21 52.89 11.00 5 -4 21 57.69 16.30 5 -4 21 46.90 13.90 -6 4 -21 160.78 17.50 -6 4 -21 129.99 21.00 -6 4 -21 132.39 15.00 6 -4 21 150.28 16.60 6 -4 21 138.79 21.30 6 -4 21 199.48 22.70 -7 4 -21 124.19 15.40 -7 4 -21 139.79 18.00 -7 4 -21 125.29 22.60 7 -4 21 133.29 22.80 7 -4 21 135.29 20.90 7 -4 21 154.98 18.30 -8 4 -21 72.29 13.40 -8 4 -21 68.39 14.80 -8 4 -21 50.99 18.50 -8 4 -21 60.09 16.20 8 -4 21 43.10 17.20 8 -4 21 80.39 18.80 8 -4 21 33.80 12.70 -9 4 -21 43.60 17.80 -9 4 -21 37.20 11.20 -9 4 -21 33.90 17.70 9 -4 21 26.70 12.30 -10 4 -21 54.39 18.90 -10 4 -21 79.79 14.40 -10 4 -21 98.09 21.90 10 -4 21 106.19 23.80 10 -4 21 73.99 16.20 -11 4 -21 31.90 11.30 11 -4 21 32.20 15.40 11 3 -21 6.20 12.70 10 3 -21 38.30 16.40 10 3 -21 32.30 18.60 -10 -3 21 61.29 17.20 9 3 -21 -16.50 10.60 9 3 -21 11.80 11.50 -9 -3 21 11.60 10.70 -9 -3 21 -4.30 5.60 8 3 -21 33.20 12.10 8 3 -21 32.60 13.30 8 3 -21 11.70 12.80 -8 -3 21 38.40 6.10 -8 -3 21 19.80 14.80 -8 -3 21 44.80 12.60 7 3 -21 7.50 11.50 7 3 -21 10.40 10.70 7 3 -21 10.80 10.10 -7 -3 21 21.30 11.20 -7 -3 21 -21.60 12.40 -7 -3 21 16.90 5.70 6 3 -21 491.55 17.20 6 3 -21 478.35 27.20 6 3 -21 491.05 29.50 6 3 -21 487.85 26.10 -6 -3 21 468.45 16.30 -6 -3 21 507.95 24.20 5 3 -21 8.00 13.30 5 3 -21 11.50 5.70 5 3 -21 -7.80 9.60 5 3 -21 8.70 9.40 -5 -3 21 0.10 8.10 -5 -3 21 -2.40 5.10 4 3 -21 1532.55 45.70 4 3 -21 1465.55 42.50 4 3 -21 1482.35 47.70 4 3 -21 1487.95 34.20 -4 -3 21 1463.25 46.60 -4 -3 21 1505.55 33.70 -4 -3 21 1487.65 38.20 3 3 -21 7.30 9.50 3 3 -21 11.80 11.60 3 3 -21 10.10 7.50 3 3 -21 9.10 5.80 -3 -3 21 2.40 7.30 -3 -3 21 -1.40 5.70 -3 -3 21 8.80 9.60 2 3 -21 775.52 31.00 2 3 -21 848.22 24.40 2 3 -21 770.82 28.30 2 3 -21 800.52 33.60 -2 -3 21 797.62 24.80 -2 -3 21 788.22 23.90 -2 -3 21 817.22 32.80 1 3 -21 2.80 5.90 1 3 -21 7.20 8.90 1 3 -21 11.70 10.00 -1 -3 21 11.50 6.70 -1 -3 21 -8.30 8.50 -1 -3 21 5.10 9.10 -1 -3 21 4.60 6.50 0 3 -21 187.48 17.70 0 3 -21 184.58 13.00 0 3 -21 191.68 20.30 0 -3 21 174.08 12.40 0 -3 21 183.98 13.40 0 -3 21 175.38 18.00 0 -3 21 185.68 17.00 -1 3 -21 -9.40 9.40 -1 3 -21 -4.90 6.10 -1 3 -21 -6.10 8.90 1 -3 21 -7.00 8.30 1 -3 21 -6.30 6.30 1 -3 21 9.00 8.90 1 -3 21 -9.60 5.90 -2 3 -21 121.09 12.20 -2 3 -21 116.49 16.40 2 -3 21 113.49 15.70 2 -3 21 124.49 13.30 2 -3 21 125.09 14.00 2 -3 21 131.99 18.10 -3 3 -21 8.80 10.80 -3 3 -21 6.90 7.60 3 -3 21 10.10 10.40 3 -3 21 25.50 12.30 3 -3 21 8.40 7.50 3 -3 21 27.90 9.00 -4 3 -21 1123.39 41.30 -4 3 -21 1087.89 32.40 4 -3 21 1057.39 33.00 4 -3 21 1072.79 39.10 4 -3 21 1104.79 39.90 4 -3 21 1054.09 33.70 -5 3 -21 -2.50 7.10 -5 3 -21 5.60 9.30 -5 3 -21 0.70 11.70 5 -3 21 15.90 10.10 5 -3 21 1.60 7.70 5 -3 21 8.50 11.60 5 -3 21 12.60 13.00 -6 3 -21 447.86 21.70 -6 3 -21 422.36 30.00 -6 3 -21 458.55 24.80 6 -3 21 464.45 29.80 6 -3 21 440.76 24.30 6 -3 21 471.25 29.90 -7 3 -21 0.10 6.50 -7 3 -21 -9.00 9.70 -7 3 -21 3.80 7.90 -7 3 -21 16.10 14.60 7 -3 21 -3.40 12.50 7 -3 21 3.40 10.60 -8 3 -21 141.19 17.20 -8 3 -21 136.59 24.30 -8 3 -21 140.39 15.30 -8 3 -21 147.69 20.10 8 -3 21 138.59 19.30 8 -3 21 121.49 22.00 -9 3 -21 56.99 18.00 -9 3 -21 82.19 13.40 -9 3 -21 66.69 17.10 9 -3 21 63.29 15.80 9 -3 21 36.20 16.10 -10 3 -21 -6.70 13.60 -10 3 -21 18.90 10.00 10 -3 21 -3.60 17.70 10 -3 21 21.50 12.30 -11 3 -21 189.58 17.80 11 -3 21 132.89 21.20 11 2 -21 182.18 25.70 10 2 -21 74.59 17.00 -10 -2 21 84.79 17.60 -10 -2 21 70.69 7.50 9 2 -21 117.29 21.40 9 2 -21 83.79 16.40 -9 -2 21 85.99 8.50 -9 -2 21 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34.90 1 10 -22 11.10 12.70 1 10 -22 2.50 11.30 1 10 -22 24.50 7.40 0 10 -22 291.17 16.30 0 10 -22 233.88 23.10 0 10 -22 256.87 26.50 0 -10 22 280.47 23.60 -1 10 -22 6.90 12.30 -1 10 -22 -3.80 9.90 -1 10 -22 5.50 7.20 1 -10 22 13.80 14.60 1 -10 22 2.30 10.30 -2 10 -22 112.59 14.30 -2 10 -22 91.49 19.50 -2 10 -22 82.69 16.20 2 -10 22 61.89 19.50 2 -10 22 84.59 15.20 -3 10 -22 51.19 11.50 -3 10 -22 60.39 15.40 -3 10 -22 56.59 13.50 -3 10 -22 25.50 14.90 3 -10 22 53.39 13.10 3 -10 22 33.90 23.00 -4 10 -22 107.29 14.60 -4 10 -22 68.79 18.10 -4 10 -22 86.99 16.20 4 -10 22 95.99 15.80 -5 10 -22 218.88 26.00 -5 10 -22 255.87 19.20 -5 10 -22 240.78 22.00 5 -10 22 239.48 20.30 -6 10 -22 56.19 13.90 -6 10 -22 70.49 27.30 6 -10 22 89.29 14.80 -7 10 -22 390.66 32.90 -7 10 -22 464.45 43.00 7 -10 22 433.06 24.00 -8 10 -22 8.50 8.50 -8 10 -22 26.30 17.40 -8 10 -22 13.30 10.90 8 -10 22 7.50 11.10 -9 10 -22 349.37 22.60 -9 10 -22 323.97 27.90 9 -10 22 261.07 20.40 -10 10 -22 10.30 10.70 -10 10 -22 -5.50 13.30 10 -10 22 -9.90 9.60 10 -10 22 -17.10 11.20 -7 -9 22 12.90 8.70 6 9 -22 5.80 13.60 6 9 -22 -3.30 12.40 -6 -9 22 11.90 6.90 5 9 -22 21.60 14.00 5 9 -22 31.10 22.10 -5 -9 22 17.50 6.10 4 9 -22 7.60 4.50 4 9 -22 35.70 20.90 4 9 -22 15.60 11.90 3 9 -22 308.47 27.60 3 9 -22 329.67 13.90 3 9 -22 294.17 25.50 -3 -9 22 345.97 27.80 2 9 -22 13.60 12.40 2 9 -22 26.60 13.60 2 9 -22 36.40 7.40 1 9 -22 536.95 20.10 1 9 -22 513.95 30.20 1 9 -22 567.54 33.70 -1 -9 22 529.85 31.40 0 9 -22 37.90 14.00 0 9 -22 18.30 13.80 0 9 -22 9.70 7.20 0 -9 22 24.90 12.20 -1 9 -22 844.52 40.20 -1 9 -22 855.41 36.80 -1 9 -22 885.11 28.50 1 -9 22 905.11 36.00 -2 9 -22 10.60 14.00 -2 9 -22 18.10 8.30 2 -9 22 38.00 12.20 -3 9 -22 287.57 18.30 -3 9 -22 263.57 25.60 -3 9 -22 268.97 22.50 3 -9 22 260.17 21.10 -4 9 -22 15.30 13.40 -4 9 -22 4.70 9.30 4 -9 22 12.40 10.00 -5 9 -22 215.08 25.00 -5 9 -22 172.68 19.40 -5 9 -22 161.78 16.80 5 -9 22 165.58 18.40 -6 9 -22 4.30 13.00 -6 9 -22 5.50 9.70 -6 9 -22 -8.90 12.60 6 -9 22 0.20 10.20 -7 9 -22 241.08 22.50 -7 9 -22 284.67 16.80 -7 9 -22 305.77 33.70 7 -9 22 281.87 16.70 7 -9 22 309.07 22.10 -8 9 -22 31.70 13.30 -8 9 -22 -0.70 13.20 8 -9 22 21.70 12.10 8 -9 22 13.10 9.30 -9 9 -22 369.66 35.70 -9 9 -22 433.26 24.60 -9 9 -22 459.75 36.80 9 -9 22 400.16 23.60 9 -9 22 430.06 26.20 -10 9 -22 0.80 11.40 -10 9 -22 4.10 11.60 10 -9 22 6.90 12.20 10 -9 22 -3.00 10.20 -8 -8 22 373.26 22.40 7 8 -22 -4.60 12.50 7 8 -22 3.50 12.50 -7 -8 22 -0.70 7.90 6 8 -22 84.29 18.50 6 8 -22 60.69 16.80 -6 -8 22 109.69 12.30 5 8 -22 1.50 11.60 5 8 -22 1.80 3.90 5 8 -22 -19.70 10.60 -5 -8 22 6.90 5.80 4 8 -22 116.09 19.80 4 8 -22 59.29 16.40 4 8 -22 74.69 8.00 4 8 -22 98.49 15.70 -4 -8 22 80.09 7.70 -4 -8 22 72.79 17.00 3 8 -22 5.70 10.90 3 8 -22 -0.10 5.10 3 8 -22 -5.60 8.90 3 8 -22 8.30 12.40 2 8 -22 286.67 14.40 2 8 -22 307.87 25.60 2 8 -22 288.87 24.60 1 8 -22 30.40 14.40 1 8 -22 11.20 12.10 1 8 -22 32.90 8.00 -1 -8 22 23.10 11.80 0 8 -22 374.76 26.00 0 8 -22 365.16 17.60 0 8 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23.00 8 7 -22 3.00 12.00 8 7 -22 6.30 14.50 -8 -7 22 15.40 9.90 7 7 -22 377.86 29.60 7 7 -22 332.77 29.00 -7 -7 22 364.46 20.70 6 7 -22 9.60 11.20 6 7 -22 -13.30 10.10 -6 -7 22 6.10 7.60 5 7 -22 780.82 18.80 5 7 -22 790.02 34.30 5 7 -22 727.03 38.10 5 7 -22 751.32 38.70 -5 -7 22 761.62 24.00 -5 -7 22 725.33 38.60 4 7 -22 1.20 10.30 4 7 -22 4.80 8.90 4 7 -22 1.90 4.60 4 7 -22 1.70 10.40 -4 -7 22 0.70 9.90 -4 -7 22 0.60 5.10 3 7 -22 396.36 24.60 3 7 -22 419.76 28.20 3 7 -22 433.46 28.30 3 7 -22 421.96 16.20 -3 -7 22 418.16 13.10 2 7 -22 2.00 11.70 2 7 -22 22.20 12.10 2 7 -22 2.10 5.70 -2 -7 22 -4.80 10.40 1 7 -22 474.25 28.40 1 7 -22 467.85 18.90 1 7 -22 458.15 29.30 -1 -7 22 430.26 26.50 0 7 -22 7.80 11.80 0 7 -22 2.90 6.70 0 7 -22 -3.10 9.50 0 -7 22 -6.40 8.60 0 -7 22 2.80 11.00 -1 7 -22 368.76 18.40 -1 7 -22 379.06 26.40 -1 7 -22 333.87 25.90 1 -7 22 367.66 25.80 1 -7 22 377.36 24.10 -2 7 -22 11.20 7.60 -2 7 -22 17.00 10.40 -2 7 -22 2.20 12.80 2 -7 22 23.10 11.00 2 -7 22 4.30 12.00 -3 7 -22 766.02 36.90 -3 7 -22 759.22 27.30 3 -7 22 774.72 36.40 3 -7 22 719.03 16.00 3 -7 22 730.73 31.40 -4 7 -22 8.60 8.00 -4 7 -22 -0.80 12.10 4 -7 22 -9.00 9.20 4 -7 22 -0.60 13.00 4 -7 22 6.80 5.30 -5 7 -22 399.46 29.50 -5 7 -22 426.66 29.20 -5 7 -22 441.76 25.20 5 -7 22 419.86 25.30 5 -7 22 321.67 27.30 5 -7 22 436.86 17.80 -6 7 -22 125.99 17.40 -6 7 -22 112.79 14.90 -6 7 -22 99.59 20.40 -6 7 -22 143.49 14.40 6 -7 22 124.99 17.40 6 -7 22 136.79 13.60 6 -7 22 85.49 20.60 -7 7 -22 333.57 29.40 -7 7 -22 311.57 19.80 -7 7 -22 325.17 23.60 7 -7 22 410.76 44.90 7 -7 22 323.07 20.00 7 -7 22 330.07 24.70 -8 7 -22 312.07 21.60 -8 7 -22 322.77 24.30 -8 7 -22 270.47 28.80 8 -7 22 290.57 21.10 8 -7 22 313.37 24.90 -9 7 -22 171.58 21.80 -9 7 -22 141.69 19.70 -9 7 -22 92.39 21.20 9 -7 22 121.69 19.60 9 -7 22 123.69 18.20 -10 7 -22 104.39 17.90 -10 7 -22 111.39 18.90 -10 7 -22 101.19 34.20 10 -7 22 94.49 17.20 -11 7 -22 31.60 13.10 11 -7 22 62.29 15.50 11 -7 22 4.30 13.40 -9 -6 22 32.60 13.40 8 6 -22 17.80 12.50 8 6 -22 6.90 13.20 -8 -6 22 40.60 11.60 7 6 -22 27.70 15.10 7 6 -22 12.40 12.20 -7 -6 22 23.00 10.40 6 6 -22 10.30 11.10 6 6 -22 19.50 4.60 6 6 -22 9.60 12.40 6 6 -22 1.10 12.00 -6 -6 22 17.40 9.10 5 6 -22 4.50 4.80 5 6 -22 -6.60 10.50 5 6 -22 11.90 11.70 5 6 -22 10.00 10.40 -5 -6 22 3.20 6.80 -5 -6 22 0.70 10.90 4 6 -22 63.19 15.00 4 6 -22 94.39 9.40 4 6 -22 144.89 22.10 4 6 -22 76.19 23.80 -4 -6 22 91.19 10.20 3 6 -22 28.60 6.80 3 6 -22 17.90 10.10 3 6 -22 10.50 11.20 3 6 -22 30.10 12.50 -3 -6 22 8.60 11.30 -3 -6 22 16.40 5.90 2 6 -22 70.59 9.40 2 6 -22 75.99 16.70 2 6 -22 66.89 15.30 -2 -6 22 78.99 16.10 -2 -6 22 60.49 6.60 1 6 -22 41.40 13.40 1 6 -22 30.10 12.50 1 6 -22 30.40 7.80 -1 -6 22 31.60 13.10 -1 -6 22 36.90 4.50 -1 -6 22 39.60 4.40 0 6 -22 265.57 15.50 0 6 -22 237.38 26.70 0 6 -22 239.18 22.00 0 -6 22 265.47 21.20 0 -6 22 272.77 22.80 -1 6 -22 89.79 16.10 -1 6 -22 120.19 18.40 -1 6 -22 112.59 12.70 1 -6 22 87.29 5.50 1 -6 22 89.59 17.40 1 -6 22 93.99 6.00 1 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25.70 -10 6 -22 176.08 19.90 10 -6 22 144.79 19.50 -11 6 -22 25.30 11.20 11 -6 22 39.00 19.20 11 -6 22 39.20 14.50 -10 -5 22 4.50 10.70 9 5 -22 240.08 25.00 9 5 -22 266.67 27.40 -9 -5 22 259.47 25.80 8 5 -22 -11.30 11.70 8 5 -22 -9.70 10.40 -8 -5 22 12.60 10.00 7 5 -22 368.16 26.00 7 5 -22 392.56 29.80 7 5 -22 374.06 27.30 -7 -5 22 379.66 22.40 6 5 -22 -0.50 9.70 6 5 -22 -6.50 10.30 6 5 -22 3.40 4.80 6 5 -22 -1.70 10.10 5 5 -22 540.85 30.50 5 5 -22 584.14 32.10 5 5 -22 548.15 17.80 5 5 -22 557.74 38.90 -5 -5 22 558.84 22.40 -5 -5 22 543.55 17.40 4 5 -22 3.30 5.60 4 5 -22 6.50 10.70 4 5 -22 -6.90 9.20 4 5 -22 4.60 8.60 -4 -5 22 1.80 5.10 -4 -5 22 6.60 11.90 -4 -5 22 0.50 6.50 3 5 -22 700.23 33.80 3 5 -22 634.44 31.60 3 5 -22 709.83 21.70 -3 -5 22 699.53 33.30 -3 -5 22 758.02 22.20 -3 -5 22 689.63 21.80 2 5 -22 -0.30 6.30 2 5 -22 -3.50 9.60 2 5 -22 4.60 10.60 -2 -5 22 13.20 11.80 -2 -5 22 0.20 6.00 -2 -5 22 -2.00 5.30 1 5 -22 696.63 22.80 1 5 -22 646.94 36.20 -1 -5 22 631.44 30.10 -1 -5 22 684.53 18.70 -1 -5 22 705.83 31.70 -1 -5 22 673.03 18.50 -1 -5 22 652.63 22.90 0 5 -22 5.40 11.00 0 5 -22 4.30 7.00 0 -5 22 -2.20 9.80 0 -5 22 -3.70 6.20 0 -5 22 -2.90 10.80 0 -5 22 -4.80 4.40 -1 5 -22 243.88 15.50 -1 5 -22 251.97 22.50 1 -5 22 254.07 21.00 1 -5 22 243.58 11.60 1 -5 22 235.48 20.60 1 -5 22 244.48 16.20 -2 5 -22 103.79 18.10 -2 5 -22 50.69 14.40 -2 5 -22 75.19 11.30 2 -5 22 54.39 13.30 2 -5 22 98.89 17.50 -3 5 -22 162.28 20.00 -3 5 -22 157.78 14.10 3 -5 22 158.18 12.20 3 -5 22 161.68 19.60 3 -5 22 178.98 20.10 -4 5 -22 104.69 18.20 -4 5 -22 88.89 12.50 4 -5 22 117.19 12.60 4 -5 22 108.99 17.00 4 -5 22 109.49 19.40 -5 5 -22 181.08 17.30 -5 5 -22 180.78 23.50 -5 5 -22 212.28 16.70 5 -5 22 197.48 15.60 5 -5 22 184.58 20.80 5 -5 22 180.68 21.80 -6 5 -22 81.39 13.80 -6 5 -22 60.79 17.00 -6 5 -22 60.89 12.70 6 -5 22 80.29 16.00 6 -5 22 50.69 11.20 6 -5 22 32.80 24.80 -7 5 -22 57.69 13.80 -7 5 -22 29.80 10.60 -7 5 -22 61.39 18.70 7 -5 22 49.99 15.20 7 -5 22 41.60 11.90 7 -5 22 46.70 17.50 -8 5 -22 135.89 17.70 -8 5 -22 132.89 19.50 -8 5 -22 120.99 23.10 8 -5 22 140.39 22.40 8 -5 22 126.29 18.50 -9 5 -22 7.60 13.10 -9 5 -22 -6.30 8.40 9 -5 22 7.20 10.10 -10 5 -22 348.77 24.00 -10 5 -22 428.06 30.40 -10 5 -22 366.96 33.90 10 -5 22 382.46 33.10 10 -5 22 408.16 27.70 -11 5 -22 13.90 10.60 10 4 -22 1.70 12.10 10 4 -22 16.50 16.00 -10 -4 22 40.20 13.30 9 4 -22 9.20 13.40 -9 -4 22 79.49 18.20 8 4 -22 10.40 12.50 8 4 -22 18.60 12.30 -8 -4 22 -2.20 10.50 -8 -4 22 20.80 4.40 7 4 -22 27.50 13.20 7 4 -22 6.20 9.80 7 4 -22 31.10 13.00 -7 -4 22 41.70 12.20 -7 -4 22 25.90 5.60 6 4 -22 417.66 25.60 6 4 -22 452.15 27.40 6 4 -22 440.06 29.10 6 4 -22 403.86 15.40 -6 -4 22 426.86 15.20 -6 -4 22 433.46 22.90 5 4 -22 5.10 10.00 5 4 -22 -1.70 10.70 5 4 -22 -1.70 9.80 5 4 -22 4.30 5.50 -5 -4 22 7.30 8.50 -5 -4 22 4.00 5.30 4 4 -22 175.78 21.00 4 4 -22 153.28 11.50 4 4 -22 138.59 18.50 -4 -4 22 162.48 14.30 -4 -4 22 159.58 11.40 3 4 -22 13.30 11.20 3 4 -22 3.20 5.80 -3 -4 22 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31.50 14.20 5 -12 23 0.20 10.50 -6 12 -23 150.18 28.80 6 -12 23 206.98 18.50 7 -12 23 16.80 10.30 8 -12 23 150.98 16.40 4 11 -23 369.56 31.50 3 11 -23 7.20 14.90 3 11 -23 10.50 15.10 3 11 -23 3.00 5.00 2 11 -23 470.45 34.20 2 11 -23 466.55 32.40 2 11 -23 564.14 21.30 1 11 -23 9.10 12.50 1 11 -23 11.60 14.50 1 11 -23 22.30 7.30 -1 -11 23 20.20 11.90 0 11 -23 226.58 26.20 0 11 -23 284.17 25.10 0 11 -23 301.27 17.20 -1 11 -23 32.20 22.00 -1 11 -23 13.80 8.20 -1 11 -23 36.60 13.90 1 -11 23 11.00 13.20 -2 11 -23 551.64 31.60 -2 11 -23 537.55 25.00 2 -11 23 558.14 30.20 -3 11 -23 0.50 19.90 -3 11 -23 18.40 13.90 -3 11 -23 -3.70 10.60 -3 11 -23 6.60 8.60 3 -11 23 23.00 11.30 -4 11 -23 225.88 22.60 -4 11 -23 214.78 18.10 -4 11 -23 170.58 24.90 4 -11 23 238.88 20.90 -5 11 -23 77.19 19.50 -5 11 -23 97.59 16.70 5 -11 23 119.49 16.50 -6 11 -23 138.19 24.90 -6 11 -23 140.89 20.20 6 -11 23 174.08 18.90 -7 11 -23 57.99 20.40 -7 11 -23 48.20 15.30 7 -11 23 91.79 14.50 -8 11 -23 54.99 17.30 8 -11 23 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9 -23 17.60 13.20 -5 9 -23 18.40 10.50 5 -9 23 2.60 10.90 -6 9 -23 157.48 20.70 -6 9 -23 66.79 19.20 6 -9 23 116.99 17.40 -7 9 -23 155.18 20.50 -7 9 -23 146.39 24.00 7 -9 23 212.38 15.00 7 -9 23 187.18 20.10 -8 9 -23 151.08 18.20 -8 9 -23 98.29 21.30 -8 9 -23 79.49 21.00 8 -9 23 122.29 14.80 8 -9 23 114.09 17.30 -9 9 -23 327.07 27.50 -9 9 -23 381.96 23.40 9 -9 23 354.56 25.00 9 -9 23 368.16 23.10 -10 9 -23 10.40 11.60 -10 9 -23 36.70 13.20 10 -9 23 36.00 12.60 10 -9 23 37.70 13.90 -8 -8 23 13.80 10.10 7 8 -23 150.48 29.80 -7 -8 23 128.29 14.30 6 8 -23 -7.50 12.10 6 8 -23 -2.20 11.70 -6 -8 23 0.50 6.80 5 8 -23 68.19 17.00 5 8 -23 76.89 6.70 -5 -8 23 85.99 9.70 4 8 -23 5.60 5.00 4 8 -23 1.90 12.50 4 8 -23 0.50 12.30 -4 -8 23 -3.80 12.00 -4 -8 23 4.50 4.50 3 8 -23 12.00 6.40 3 8 -23 12.10 12.80 3 8 -23 -1.10 9.80 3 8 -23 11.10 12.50 -3 -8 23 17.70 12.60 2 8 -23 65.79 16.70 2 8 -23 31.80 13.70 2 8 -23 36.80 8.20 1 8 -23 106.49 19.00 1 8 -23 144.79 23.10 1 8 -23 126.09 13.00 -1 -8 23 106.99 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6.60 11.60 10 -8 23 -11.50 15.00 -8 -7 23 497.45 25.00 7 7 -23 4.30 12.50 7 7 -23 11.40 13.00 -7 -7 23 -2.30 8.40 6 7 -23 524.25 46.00 6 7 -23 500.55 41.80 -6 -7 23 447.16 20.80 5 7 -23 -5.20 10.50 5 7 -23 -2.30 11.00 5 7 -23 6.90 4.80 -5 -7 23 5.90 6.40 4 7 -23 457.15 16.40 4 7 -23 473.85 27.00 4 7 -23 448.46 29.90 4 7 -23 462.45 30.60 -4 -7 23 477.65 16.40 -4 -7 23 500.15 32.10 3 7 -23 10.50 11.50 3 7 -23 8.50 12.70 3 7 -23 15.50 6.60 3 7 -23 14.90 10.60 -3 -7 23 18.50 5.90 2 7 -23 46.70 8.60 2 7 -23 49.80 15.50 2 7 -23 60.59 15.10 -2 -7 23 52.69 17.50 1 7 -23 18.90 13.00 1 7 -23 32.80 14.10 1 7 -23 37.30 9.20 -1 -7 23 20.80 11.40 0 7 -23 140.79 12.80 0 7 -23 140.69 20.30 0 7 -23 139.89 19.80 0 -7 23 125.09 18.60 0 -7 23 80.59 16.90 -1 7 -23 25.70 8.20 -1 7 -23 50.89 14.80 -1 7 -23 49.99 16.10 1 -7 23 68.29 15.80 1 -7 23 52.69 15.30 -2 7 -23 195.48 15.40 -2 7 -23 163.48 34.20 -2 7 -23 200.78 22.90 2 -7 23 189.28 19.80 2 -7 23 190.48 22.40 -3 7 -23 199.48 22.50 -3 7 -23 224.88 17.10 3 -7 23 209.08 20.90 3 -7 23 252.57 35.20 3 -7 23 204.68 8.60 -4 7 -23 102.59 13.80 -4 7 -23 80.39 17.80 4 -7 23 109.89 21.00 4 -7 23 112.49 17.50 4 -7 23 111.29 9.80 -5 7 -23 235.48 18.40 -5 7 -23 214.28 25.00 -5 7 -23 202.98 19.50 5 -7 23 219.18 25.30 5 -7 23 213.78 21.40 5 -7 23 233.28 14.30 -6 7 -23 11.20 9.30 -6 7 -23 6.20 10.00 -6 7 -23 23.70 14.20 6 -7 23 0.20 7.50 6 -7 23 7.20 15.90 6 -7 23 5.00 11.40 -7 7 -23 220.28 21.10 -7 7 -23 150.38 23.80 -7 7 -23 232.28 18.80 7 -7 23 205.18 22.60 7 -7 23 228.08 17.90 -8 7 -23 5.00 22.20 -8 7 -23 -0.80 10.70 -8 7 -23 7.40 10.90 8 -7 23 -2.70 9.20 8 -7 23 -7.70 11.10 -9 7 -23 209.78 21.80 -9 7 -23 153.48 25.90 -9 7 -23 221.18 21.10 9 -7 23 192.98 20.20 9 -7 23 216.38 24.00 -10 7 -23 22.00 11.50 -10 7 -23 26.00 13.80 10 -7 23 30.20 13.60 8 6 -23 -14.80 10.70 8 6 -23 -21.10 11.10 -8 -6 23 13.80 9.50 7 6 -23 166.48 23.80 7 6 -23 272.37 40.70 -7 -6 23 218.88 17.60 6 6 -23 15.90 12.10 6 6 -23 17.50 4.90 6 6 -23 15.40 13.30 -6 -6 23 12.60 8.50 5 6 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7.30 4 8 -28 7.50 12.40 4 8 -28 22.90 16.00 3 8 -28 43.50 17.50 3 8 -28 14.20 7.50 3 8 -28 33.60 16.10 2 8 -28 16.40 14.10 2 8 -28 33.60 9.00 2 8 -28 40.50 18.30 1 8 -28 41.10 15.50 1 8 -28 38.30 24.40 1 8 -28 59.39 10.60 0 8 -28 82.69 20.10 0 8 -28 104.19 14.10 0 8 -28 74.19 18.60 0 -8 28 59.69 16.20 -1 8 -28 35.30 11.20 -1 8 -28 18.70 14.20 -1 8 -28 21.10 15.10 1 -8 28 3.40 12.40 -2 8 -28 21.70 15.50 -2 8 -28 22.20 10.40 -2 8 -28 13.50 13.30 2 -8 28 11.50 12.40 -3 8 -28 12.40 17.10 3 -8 28 -3.10 10.00 -4 8 -28 3.80 10.20 -4 8 -28 -11.30 11.00 4 -8 28 -11.90 8.10 -5 8 -28 25.60 14.70 -5 8 -28 79.89 25.30 5 -8 28 -0.90 9.60 -6 8 -28 38.90 16.20 -6 8 -28 33.80 16.30 6 -8 28 71.39 16.10 6 -8 28 56.69 10.00 -7 8 -28 115.19 19.40 7 -8 28 198.18 16.40 7 -8 28 158.88 22.70 -8 8 -28 70.79 17.40 8 -8 28 92.59 13.70 8 -8 28 113.59 20.20 -7 -7 28 200.58 17.40 6 7 -28 12.80 16.40 6 7 -28 10.70 6.00 -6 -7 28 5.30 7.30 5 7 -28 65.09 18.70 5 7 -28 91.89 21.00 -5 -7 28 90.29 10.20 4 7 -28 13.20 12.30 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33.20 9.50 5 6 -28 5.50 6.60 5 6 -28 7.90 15.00 -5 -6 28 9.80 7.50 4 6 -28 33.30 9.10 4 6 -28 30.10 14.70 4 6 -28 35.20 15.40 -4 -6 28 22.50 7.50 3 6 -28 -2.30 11.30 3 6 -28 -1.30 12.40 3 6 -28 -3.60 7.20 -3 -6 28 2.90 5.90 -3 -6 28 0.80 6.10 2 6 -28 27.70 14.80 2 6 -28 38.30 9.90 2 6 -28 18.40 15.00 -2 -6 28 27.20 6.70 -2 -6 28 34.60 15.50 -2 -6 28 41.30 6.90 1 6 -28 2.20 11.70 1 6 -28 2.50 12.00 1 6 -28 -5.30 13.30 1 6 -28 -4.90 7.00 -1 -6 28 2.40 4.80 -1 -6 28 -2.50 5.10 -1 -6 28 -7.90 11.50 0 6 -28 184.58 16.00 0 6 -28 219.78 27.80 0 6 -28 162.48 22.70 0 -6 28 207.58 23.80 0 -6 28 186.88 23.90 0 -6 28 180.28 9.90 0 -6 28 199.08 10.70 -1 6 -28 39.10 16.30 -1 6 -28 51.99 15.90 1 -6 28 40.20 16.00 1 -6 28 36.40 6.80 -2 6 -28 230.78 18.80 -2 6 -28 212.68 24.10 2 -6 28 260.57 14.20 2 -6 28 190.68 23.60 -3 6 -28 75.29 14.10 -3 6 -28 45.00 15.80 3 -6 28 59.69 9.40 3 -6 28 8.80 15.80 3 -6 28 61.39 17.30 -4 6 -28 113.19 20.40 4 -6 28 146.69 13.40 -5 6 -28 -12.80 11.30 -5 6 -28 5.40 9.80 5 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13.10 7.10 -1 -5 28 -3.30 6.20 -1 -5 28 3.30 13.00 -1 -5 28 17.40 8.10 0 5 -28 19.00 14.10 0 5 -28 35.10 10.30 0 5 -28 20.00 14.60 0 -5 28 13.50 7.10 0 -5 28 11.70 8.30 0 -5 28 16.20 13.50 0 -5 28 5.70 9.70 -1 5 -28 12.30 12.20 -1 5 -28 8.50 12.40 1 -5 28 1.90 13.00 1 -5 28 13.90 7.20 1 -5 28 4.20 8.90 -2 5 -28 123.79 20.70 -2 5 -28 122.69 15.30 2 -5 28 136.59 16.00 2 -5 28 116.59 12.90 2 -5 28 135.19 21.30 -3 5 -28 89.89 14.60 -3 5 -28 104.39 19.70 3 -5 28 90.89 12.70 3 -5 28 86.79 19.40 -4 5 -28 53.19 16.80 4 -5 28 52.19 18.90 4 -5 28 25.30 12.10 4 -5 28 40.90 10.90 -5 5 -28 32.90 15.60 -5 5 -28 39.60 12.50 5 -5 28 28.80 16.30 5 -5 28 40.60 11.80 -6 5 -28 85.89 20.30 -6 5 -28 119.09 17.20 6 -5 28 138.89 20.60 6 -5 28 118.49 20.90 -7 5 -28 -1.50 9.40 -7 5 -28 5.30 14.30 7 -5 28 0.40 9.80 -8 5 -28 82.19 21.50 -8 5 -28 67.89 15.00 8 -5 28 58.29 15.60 9 -5 28 29.60 12.70 -9 -4 28 26.90 13.20 8 4 -28 75.59 18.00 -8 -4 28 87.89 9.80 7 4 -28 3.80 6.90 7 4 -28 0.10 13.30 7 4 -28 1.30 12.40 -7 -4 28 2.50 6.10 -7 -4 28 13.90 11.00 6 4 -28 156.78 23.00 6 4 -28 135.29 13.30 6 4 -28 111.69 21.40 -6 -4 28 154.68 13.10 -6 -4 28 190.88 18.80 5 4 -28 6.60 7.30 5 4 -28 21.00 14.20 5 4 -28 0.60 11.80 -5 -4 28 13.00 7.80 -5 -4 28 12.20 9.70 4 4 -28 227.78 16.50 4 4 -28 191.08 24.30 4 4 -28 189.78 22.40 -4 -4 28 229.88 15.90 -4 -4 28 242.58 19.10 3 4 -28 -2.80 7.00 3 4 -28 3.50 12.40 3 4 -28 -6.60 9.40 3 4 -28 4.80 12.30 -3 -4 28 15.50 9.40 -3 -4 28 11.20 13.40 -3 -4 28 -7.60 7.10 2 4 -28 334.87 26.70 2 4 -28 357.16 29.90 2 4 -28 364.56 23.90 2 4 -28 378.86 19.60 -2 -4 28 368.46 18.70 -2 -4 28 356.86 19.30 -2 -4 28 379.86 20.10 -2 -4 28 312.77 26.70 1 4 -28 -8.20 12.10 1 4 -28 -4.30 7.10 1 4 -28 7.50 9.10 1 4 -28 -3.70 10.50 -1 -4 28 9.20 11.10 -1 -4 28 -5.80 7.70 -1 -4 28 6.70 7.60 0 4 -28 234.88 23.30 0 4 -28 237.28 25.70 0 4 -28 245.88 17.80 0 -4 28 251.37 16.20 0 -4 28 264.07 18.80 0 -4 28 243.78 23.30 -1 4 -28 1.30 12.20 -1 4 -28 18.30 13.10 1 -4 28 8.00 8.00 1 -4 28 9.10 12.50 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15.30 -5 2 -28 136.99 22.40 5 -2 28 150.78 23.40 5 -2 28 155.48 19.00 5 -2 28 234.78 40.70 5 -2 28 143.39 19.30 -6 2 -28 316.47 29.70 -6 2 -28 300.07 24.10 6 -2 28 360.56 39.50 6 -2 28 305.17 22.80 6 -2 28 265.07 24.10 -7 2 -28 51.89 18.50 7 -2 28 50.79 16.20 -8 2 -28 45.30 18.70 8 -2 28 20.40 14.50 10 1 -28 65.29 17.20 9 1 -28 0.70 15.60 9 1 -28 -3.40 10.50 -9 -1 28 1.50 7.10 -9 -1 28 16.60 14.30 8 1 -28 19.10 8.60 8 1 -28 15.30 12.70 8 1 -28 26.40 15.40 -8 -1 28 10.40 7.80 -8 -1 28 23.40 11.10 7 1 -28 61.89 11.80 7 1 -28 61.49 18.50 7 1 -28 40.60 14.40 -7 -1 28 56.99 10.60 -7 -1 28 73.49 17.70 6 1 -28 7.00 13.70 6 1 -28 21.70 9.00 6 1 -28 15.90 11.20 -6 -1 28 8.50 11.50 -6 -1 28 13.60 8.30 5 1 -28 -7.90 7.90 5 1 -28 3.20 14.10 5 1 -28 17.70 12.40 5 1 -28 12.60 10.90 -5 -1 28 13.90 14.40 -5 -1 28 11.20 12.40 -5 -1 28 5.70 7.40 4 1 -28 2.90 12.30 4 1 -28 2.60 11.80 4 1 -28 8.20 9.70 4 1 -28 -1.80 8.00 -4 -1 28 9.90 7.80 -4 -1 28 6.40 10.40 3 1 -28 88.69 18.70 3 1 -28 121.09 18.00 3 1 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3 28 -8.60 14.30 0 3 28 16.40 12.40 0 3 28 5.60 8.20 0 3 28 -2.60 7.40 -1 -3 -28 263.67 20.30 -1 -3 -28 263.37 17.60 1 3 28 291.37 27.00 1 3 28 279.37 31.40 1 3 28 231.08 23.40 1 3 28 248.28 19.00 -2 -3 -28 -3.00 9.80 2 3 28 14.70 13.40 2 3 28 9.80 9.20 2 3 28 -8.70 8.50 -3 -3 -28 154.68 19.30 -3 -3 -28 157.38 13.00 3 3 28 166.38 19.60 3 3 28 179.88 24.20 3 3 28 125.69 16.40 -4 -3 -28 10.40 6.40 -4 -3 -28 17.10 6.20 4 3 28 0.70 8.70 4 3 28 7.60 13.00 4 3 28 -1.40 11.20 -5 -3 -28 185.98 9.70 -5 -3 -28 179.58 9.10 5 3 28 201.18 18.90 5 3 28 215.98 23.00 5 3 28 152.38 23.30 6 3 28 3.90 9.10 6 3 28 1.80 13.60 6 3 28 -8.40 11.80 10 -4 -28 43.20 14.00 10 -4 -28 24.00 11.90 10 -4 -28 -3.40 13.40 -10 4 28 32.40 10.70 9 -4 -28 48.60 12.60 9 -4 -28 53.49 19.90 -9 4 28 35.70 11.20 8 -4 -28 3.30 8.90 8 -4 -28 -22.40 10.50 -8 4 28 15.10 9.80 7 -4 -28 49.99 15.90 7 -4 -28 53.79 11.30 7 -4 -28 45.90 15.20 -7 4 28 53.69 25.10 -7 4 28 86.19 13.90 6 -4 -28 25.90 13.20 6 -4 -28 42.40 13.00 6 -4 -28 16.00 8.40 6 -4 -28 20.70 14.70 -6 4 28 7.00 8.70 -6 4 28 30.20 16.50 5 -4 -28 37.00 11.30 5 -4 -28 52.59 13.40 5 -4 -28 84.39 11.30 -5 4 28 62.19 17.10 -5 4 28 57.89 12.20 4 -4 -28 64.99 14.30 4 -4 -28 59.29 10.10 -4 4 28 74.39 20.00 -4 4 28 53.79 12.80 3 -4 -28 32.10 11.50 3 -4 -28 40.50 11.80 3 -4 -28 23.70 7.70 -3 4 28 29.00 16.00 -3 4 28 23.80 9.70 2 -4 -28 86.39 11.10 2 -4 -28 93.39 14.20 2 -4 -28 99.19 16.00 -2 4 28 122.49 22.90 -2 4 28 85.79 13.80 -2 4 28 74.69 16.80 1 -4 -28 6.80 9.10 1 -4 -28 4.80 7.30 1 -4 -28 13.70 8.70 -1 4 28 1.50 14.30 -1 4 28 0.80 12.30 -1 4 28 3.90 8.30 0 -4 -28 30.90 10.20 0 -4 -28 42.70 10.90 0 4 28 44.20 9.30 0 4 28 47.10 15.60 0 4 28 71.29 22.50 0 4 28 15.80 9.90 -1 -4 -28 10.10 7.50 -1 -4 -28 5.40 8.30 1 4 28 -2.70 7.90 1 4 28 6.60 13.40 1 4 28 12.40 8.60 -2 -4 -28 169.68 13.60 2 4 28 149.29 16.60 2 4 28 129.39 16.20 2 4 28 134.79 21.50 -3 -4 -28 13.00 6.60 3 4 28 30.60 12.00 3 4 28 7.10 11.10 3 4 28 17.70 13.80 -4 -4 -28 80.49 6.90 -4 -4 -28 80.89 7.00 4 4 28 100.59 16.00 4 4 28 108.49 18.20 4 4 28 95.99 20.00 5 4 28 20.10 13.00 5 4 28 31.70 13.70 5 4 28 30.90 11.20 6 4 28 -20.20 11.30 10 -5 -28 89.59 15.80 10 -5 -28 35.10 16.90 10 -5 -28 69.29 13.90 -10 5 28 64.69 13.40 9 -5 -28 96.39 13.90 9 -5 -28 104.49 20.80 -9 5 28 73.19 16.90 8 -5 -28 0.20 7.50 8 -5 -28 -2.50 12.70 8 -5 -28 1.20 8.50 -8 5 28 -2.40 8.60 -8 5 28 9.40 12.10 7 -5 -28 196.88 13.70 -7 5 28 195.78 17.90 -7 5 28 136.19 33.50 6 -5 -28 37.10 15.10 -6 5 28 26.00 10.60 -6 5 28 26.40 15.80 5 -5 -28 477.15 15.60 -5 5 28 470.95 32.20 -5 5 28 455.85 24.70 4 -5 -28 5.50 4.80 -4 5 28 -10.10 13.90 -4 5 28 -9.80 8.30 3 -5 -28 201.98 19.40 3 -5 -28 219.58 10.20 -3 5 28 239.68 27.40 -3 5 28 231.18 19.10 -3 5 28 277.17 25.10 2 -5 -28 3.10 9.90 -2 5 28 12.60 13.00 -2 5 28 -0.70 15.20 -2 5 28 5.10 8.80 1 -5 -28 129.09 15.60 -1 5 28 101.59 19.50 -1 5 28 124.99 15.80 0 -5 -28 -10.50 7.00 0 5 28 -0.50 6.30 0 5 28 -11.10 11.80 0 5 28 12.10 9.60 -1 -5 -28 88.79 11.90 1 5 28 102.89 17.30 1 5 28 107.59 21.20 1 5 28 102.39 12.00 -2 -5 -28 5.50 6.30 2 5 28 0.50 8.90 2 5 28 2.40 9.30 -3 -5 -28 212.58 10.00 3 5 28 199.98 26.40 3 5 28 209.98 19.10 3 5 28 195.48 19.10 4 5 28 11.20 12.00 4 5 28 16.60 9.30 4 5 28 28.20 16.00 5 5 28 80.89 17.20 10 -6 -28 -2.10 14.70 10 -6 -28 4.30 8.60 -10 6 28 -0.60 8.30 9 -6 -28 44.10 10.30 9 -6 -28 65.69 18.10 9 -6 -28 21.80 8.40 -9 6 28 10.80 13.30 -9 6 28 31.40 12.40 8 -6 -28 9.90 6.20 -8 6 28 2.20 8.60 -8 6 28 4.30 10.20 -7 6 28 48.00 13.80 -7 6 28 24.90 11.90 6 -6 -28 16.10 14.70 -6 6 28 -7.50 11.10 -6 6 28 5.20 15.10 5 -6 -28 73.19 15.90 -5 6 28 50.49 11.80 -5 6 28 44.90 16.20 -4 6 28 63.19 18.90 -4 6 28 48.90 12.50 3 -6 -28 26.50 11.10 -3 6 28 9.90 13.90 -3 6 28 3.30 17.10 -3 6 28 24.00 9.50 2 -6 -28 215.18 19.00 -2 6 28 167.48 17.80 -2 6 28 142.79 23.10 1 -6 -28 24.70 9.90 -1 6 28 13.40 13.50 -1 6 28 2.20 14.60 0 -6 -28 39.30 9.60 0 6 28 26.20 10.80 0 6 28 25.30 18.90 -1 -6 -28 0.90 6.50 1 6 28 9.30 14.20 1 6 28 6.50 7.00 1 6 28 -8.70 8.10 -2 -6 -28 14.40 5.40 2 6 28 -1.20 12.20 2 6 28 0.30 8.60 2 6 28 17.40 9.00 3 6 28 3.90 10.70 3 6 28 9.80 9.70 3 6 28 4.30 12.70 4 6 28 198.48 20.60 -9 7 28 83.99 14.40 -8 7 28 -0.70 8.80 -8 7 28 9.50 11.00 -7 7 28 57.49 13.40 -6 7 28 -0.40 9.60 -6 7 28 -5.70 8.50 5 -7 -28 30.90 13.10 -5 7 28 22.10 11.20 -4 7 28 5.70 9.30 3 -7 -28 394.26 24.30 -3 7 28 407.36 24.40 -3 7 28 388.56 34.20 2 -7 -28 28.90 10.50 -2 7 28 9.50 13.90 -2 7 28 37.50 12.00 1 -7 -28 265.77 18.40 -1 7 28 240.48 26.50 -1 7 28 235.28 19.90 0 7 28 13.90 9.80 0 7 28 -3.20 13.70 -1 -7 -28 21.20 6.30 1 7 28 33.50 12.20 1 7 28 55.39 16.40 1 7 28 27.60 7.20 2 7 28 15.30 10.10 2 7 28 6.30 7.30 3 7 28 35.10 17.50 -8 8 28 42.50 13.80 -7 8 28 16.30 10.80 -7 8 28 19.30 12.90 -6 8 28 46.90 12.40 -6 8 28 41.30 12.00 5 -8 -28 1.50 11.50 -5 8 28 -0.20 8.70 -5 8 28 7.10 9.30 -4 8 28 54.99 17.40 -4 8 28 37.60 11.60 3 -8 -28 4.00 10.20 -3 8 28 7.20 10.40 -3 8 28 8.10 13.70 2 -8 -28 98.89 14.60 -2 8 28 54.79 19.10 -2 8 28 50.39 12.80 1 -8 -28 5.70 7.90 -1 8 28 -5.10 8.10 -1 8 28 -3.20 13.50 0 -8 -28 89.29 11.20 0 8 28 100.59 16.90 -1 -8 -28 0.00 4.80 2 8 28 210.28 10.70 -7 9 28 118.39 18.20 -6 9 28 13.80 9.30 5 -9 -28 27.80 13.30 -5 9 28 45.20 12.60 4 -9 -28 20.10 9.60 3 -9 -28 11.90 9.80 2 -9 -28 32.10 10.10 1 -9 -28 10.20 8.20 0 -9 -28 6.00 6.40 -5 10 28 18.30 10.90 4 -10 -28 161.18 18.60 3 -10 -28 21.50 10.50 0 11 -29 71.39 18.50 0 11 -29 84.79 13.40 -2 11 -29 22.70 14.10 4 -11 29 17.00 14.50 3 10 -29 119.79 12.20 2 10 -29 10.80 14.10 2 10 -29 33.60 8.70 1 10 -29 101.99 13.10 1 10 -29 58.89 18.70 0 10 -29 71.79 13.10 -1 10 -29 161.58 25.70 -1 10 -29 135.99 17.10 -2 10 -29 31.80 15.40 3 -10 29 134.49 22.10 4 -10 29 -13.50 13.00 5 -10 29 258.57 26.00 6 -10 29 10.60 14.50 4 9 -29 34.20 8.10 3 9 -29 1.00 6.90 3 9 -29 1.80 14.50 2 9 -29 -2.10 12.10 2 9 -29 10.90 7.80 2 9 -29 10.70 14.20 1 9 -29 42.20 18.40 1 9 -29 23.30 9.30 0 9 -29 23.00 15.70 0 9 -29 57.09 12.80 0 9 -29 65.89 19.60 -1 9 -29 45.40 16.40 -1 9 -29 46.80 17.40 -1 9 -29 48.60 12.30 -2 9 -29 56.49 16.50 -2 9 -29 50.99 17.90 2 -9 29 41.90 16.70 -3 9 -29 4.60 13.90 3 -9 29 48.40 15.90 -4 9 -29 -0.20 11.80 -4 9 -29 4.40 14.60 4 -9 29 -1.20 13.10 -5 9 -29 135.49 20.20 5 -9 29 159.88 21.60 -6 9 -29 54.89 15.40 6 -9 29 53.39 18.00 7 -9 29 75.59 18.00 7 -9 29 91.79 11.50 5 8 -29 220.88 19.80 -5 -8 29 199.28 11.50 4 8 -29 14.90 14.40 4 8 -29 8.00 6.90 4 8 -29 10.50 15.60 3 8 -29 330.27 30.60 3 8 -29 361.46 18.50 3 8 -29 303.27 29.80 2 8 -29 -1.60 12.90 2 8 -29 -2.10 7.70 1 8 -29 353.46 30.40 1 8 -29 361.16 20.10 1 8 -29 403.66 32.70 0 8 -29 7.20 14.20 0 8 -29 10.80 15.60 0 8 -29 -9.50 8.40 -1 8 -29 232.18 19.10 -1 8 -29 279.17 27.60 1 -8 29 265.67 26.50 -2 8 -29 10.60 9.90 -2 8 -29 5.00 15.10 2 -8 29 -2.00 12.90 -3 8 -29 115.79 20.40 3 -8 29 140.69 21.40 -4 8 -29 -15.20 10.40 -4 8 -29 10.70 13.90 4 -8 29 -5.70 12.50 -5 8 -29 124.59 24.40 -5 8 -29 99.19 17.30 5 -8 29 99.89 19.60 -6 8 -29 28.90 23.70 -6 8 -29 10.20 12.10 6 -8 29 17.20 7.40 6 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-7 -6 29 480.85 24.50 6 6 -29 -4.50 12.80 6 6 -29 13.60 7.10 -6 -6 29 0.70 7.50 5 6 -29 448.26 33.20 5 6 -29 439.66 19.50 -5 -6 29 444.56 19.90 4 6 -29 5.80 12.90 4 6 -29 8.30 8.10 4 6 -29 8.10 12.90 -4 -6 29 0.00 6.30 3 6 -29 193.58 15.30 3 6 -29 203.48 26.90 3 6 -29 180.58 25.20 -3 -6 29 227.68 13.10 -3 -6 29 177.88 11.90 2 6 -29 4.10 12.90 2 6 -29 12.30 13.60 2 6 -29 -2.40 8.00 -2 -6 29 18.40 6.20 -2 -6 29 8.70 8.90 1 6 -29 182.88 25.30 1 6 -29 167.58 15.80 1 6 -29 177.48 24.50 -1 -6 29 200.08 25.80 -1 -6 29 177.98 10.20 -1 -6 29 197.48 10.80 0 6 -29 -0.20 12.70 0 6 -29 20.20 14.20 0 6 -29 10.80 14.70 0 -6 29 14.50 5.50 0 -6 29 20.80 15.30 0 -6 29 -2.80 14.50 0 -6 29 20.90 6.10 -1 6 -29 429.36 23.10 -1 6 -29 437.56 31.90 -1 6 -29 423.06 30.70 1 -6 29 379.96 30.10 1 -6 29 408.96 30.00 -2 6 -29 10.40 13.80 -2 6 -29 3.10 9.20 2 -6 29 3.70 17.20 2 -6 29 11.50 6.60 2 -6 29 2.40 14.80 -3 6 -29 345.97 29.20 3 -6 29 351.76 28.10 3 -6 29 327.87 16.50 -4 6 -29 23.90 15.30 4 -6 29 46.60 9.90 4 -6 29 33.50 15.20 -5 6 -29 76.79 15.20 5 -6 29 71.89 12.10 5 -6 29 89.59 20.20 -6 6 -29 44.70 13.30 -6 6 -29 30.50 15.70 6 -6 29 36.20 23.20 6 -6 29 30.40 11.00 -7 6 -29 7.40 16.00 -7 6 -29 0.20 9.00 7 -6 29 6.90 10.80 -8 6 -29 84.99 16.50 8 -6 29 91.59 15.50 -8 -5 29 20.40 11.70 7 5 -29 42.20 13.90 7 5 -29 13.10 14.60 -7 -5 29 45.10 11.40 6 5 -29 29.70 17.40 6 5 -29 71.89 10.60 6 5 -29 54.79 18.00 -6 -5 29 69.49 13.20 -6 -5 29 69.49 9.80 5 5 -29 10.70 14.40 5 5 -29 4.60 12.00 5 5 -29 2.30 7.30 -5 -5 29 15.00 6.70 4 5 -29 13.90 14.80 4 5 -29 -0.20 13.10 4 5 -29 -0.90 7.70 -4 -5 29 -3.80 7.30 3 5 -29 2.50 12.40 3 5 -29 13.70 8.10 3 5 -29 3.00 11.30 -3 -5 29 10.40 7.90 -3 -5 29 -4.70 5.90 -3 -5 29 5.00 7.20 2 5 -29 47.10 16.20 2 5 -29 77.39 12.00 2 5 -29 79.99 18.80 -2 -5 29 69.09 20.00 -2 -5 29 77.19 10.30 -2 -5 29 75.79 11.00 -2 -5 29 76.59 12.10 1 5 -29 20.60 13.10 1 5 -29 -14.40 10.00 1 5 -29 -1.20 7.30 1 5 -29 10.40 14.60 -1 -5 29 -5.80 13.20 -1 -5 29 0.80 7.30 -1 -5 29 0.30 6.40 -1 -5 29 -3.30 6.90 0 5 -29 80.19 18.10 0 5 -29 70.19 17.80 0 5 -29 108.59 17.90 0 5 -29 91.29 20.00 0 -5 29 56.49 11.30 0 -5 29 72.89 17.30 0 -5 29 58.69 17.20 0 -5 29 75.59 10.20 -1 5 -29 11.40 12.60 -1 5 -29 28.60 11.10 1 -5 29 11.80 7.40 1 -5 29 29.60 11.10 1 -5 29 20.70 14.10 1 -5 29 8.10 14.00 -2 5 -29 496.05 31.80 -2 5 -29 460.05 24.80 2 -5 29 500.65 31.50 2 -5 29 469.35 31.60 2 -5 29 498.35 21.00 2 -5 29 465.85 24.90 -3 5 -29 113.49 20.20 3 -5 29 88.89 19.30 3 -5 29 90.99 12.50 3 -5 29 81.89 18.70 -4 5 -29 147.99 23.80 4 -5 29 151.68 15.80 4 -5 29 224.68 24.50 -5 5 -29 87.19 15.90 -5 5 -29 76.59 20.10 5 -5 29 67.99 18.30 5 -5 29 68.49 12.90 -6 5 -29 220.88 29.70 -6 5 -29 202.78 20.20 6 -5 29 237.88 20.30 -7 5 -29 17.10 10.90 -7 5 -29 17.40 14.70 7 -5 29 18.50 11.30 -8 5 -29 84.09 15.30 8 -5 29 74.09 15.40 8 4 -29 -3.10 11.80 -8 -4 29 9.90 6.20 7 4 -29 35.80 17.60 7 4 -29 50.59 9.90 7 4 -29 71.19 24.90 -7 -4 29 60.49 9.30 -7 -4 29 61.49 14.30 6 4 -29 -13.20 10.90 6 4 -29 16.20 15.00 6 4 -29 2.00 6.90 -6 -4 29 14.40 10.40 -6 -4 29 1.30 6.30 5 4 -29 296.67 18.00 5 4 -29 263.47 25.40 -5 -4 29 303.17 20.90 -5 -4 29 296.07 20.70 4 4 -29 7.00 11.60 4 4 -29 4.80 8.30 4 4 -29 -3.30 12.80 -4 -4 29 1.10 7.30 -4 -4 29 8.40 14.10 3 4 -29 433.16 32.60 3 4 -29 448.86 29.90 3 4 -29 449.76 21.70 -3 -4 29 434.46 21.70 -3 -4 29 400.26 21.00 2 4 -29 -1.80 13.30 2 4 -29 -5.80 7.50 2 4 -29 -2.70 8.90 2 4 -29 -2.70 11.10 -2 -4 29 -2.00 7.80 -2 -4 29 17.30 13.30 -2 -4 29 2.70 7.80 -2 -4 29 1.10 7.80 1 4 -29 136.29 15.40 1 4 -29 144.59 23.50 1 4 -29 144.29 18.30 1 4 -29 150.28 22.60 -1 -4 29 106.19 20.80 -1 -4 29 119.89 15.20 -1 -4 29 139.39 14.00 0 4 -29 1.80 11.90 0 4 -29 0.50 11.90 0 4 -29 19.50 14.80 0 4 -29 9.50 8.40 0 -4 29 8.90 8.90 0 -4 29 9.70 19.00 0 -4 29 20.00 8.90 0 -4 29 13.50 13.40 -1 4 -29 -13.80 11.20 -1 4 -29 -7.00 8.70 1 -4 29 -1.50 8.20 1 -4 29 8.30 13.20 1 -4 29 8.50 8.60 -2 4 -29 34.70 10.70 -2 4 -29 38.20 15.40 2 -4 29 50.69 11.00 2 -4 29 45.10 15.70 2 -4 29 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14.00 2 -3 36 14.70 11.50 -4 -2 36 153.28 19.60 -4 -2 36 122.99 15.90 3 2 -36 3.50 13.00 -3 -2 36 -3.30 8.80 -3 -2 36 20.40 11.70 2 2 -36 373.76 29.30 -2 -2 36 437.46 26.70 1 2 -36 12.20 13.00 -1 -2 36 17.70 12.20 -1 -2 36 -0.50 9.10 0 2 -36 193.38 23.70 0 -2 36 221.28 21.50 -1 2 -36 -4.20 12.60 1 -2 36 2.00 11.30 -2 2 -36 82.19 18.00 2 -2 36 94.99 16.70 5 1 -36 39.20 14.70 -5 -1 36 40.80 15.70 -5 -1 36 2.50 9.20 4 1 -36 22.40 13.40 -4 -1 36 4.90 9.40 -4 -1 36 9.00 13.00 -4 -1 36 35.70 16.60 3 1 -36 -17.80 10.90 -3 -1 36 1.90 12.90 -3 -1 36 -4.00 8.30 2 1 -36 19.30 13.20 -2 -1 36 10.80 10.20 -2 -1 36 4.90 11.50 1 1 -36 5.10 12.70 -1 -1 36 20.40 12.60 -1 -1 36 -5.30 10.10 0 1 -36 4.20 12.10 0 -1 36 45.50 14.40 0 -1 36 44.40 14.80 -1 1 -36 7.40 11.70 1 -1 36 13.10 13.40 1 -1 36 -3.20 10.30 -2 1 -36 13.70 13.10 2 -1 36 38.40 14.40 5 0 -36 9.70 12.80 -5 0 36 12.80 10.90 4 0 -36 48.10 15.40 -4 0 36 51.89 13.00 -4 0 36 37.10 15.10 3 0 -36 -1.50 10.80 -3 0 36 3.40 11.90 -3 0 36 7.10 10.00 2 0 -36 155.68 21.10 -2 0 36 122.49 18.90 -2 0 36 169.88 20.10 -1 0 36 31.90 14.40 -1 0 36 29.00 12.50 0 0 -36 144.49 21.50 0 0 36 152.68 20.60 -1 0 -36 15.20 13.70 1 0 36 20.70 12.80 1 0 36 7.80 12.70 -2 0 -36 151.58 18.70 -2 0 -36 112.49 19.80 2 0 36 147.19 22.50 2 0 36 156.48 22.90 5 -1 -36 16.10 12.10 -5 1 36 10.00 10.40 4 -1 -36 14.00 12.00 -4 1 36 0.40 13.50 -4 1 36 14.30 10.80 3 -1 -36 74.59 15.90 -3 1 36 43.50 16.40 -3 1 36 59.59 12.90 2 -1 -36 10.80 12.10 -2 1 36 -5.80 12.20 1 -1 -36 135.99 19.90 -1 1 36 122.69 20.90 0 -1 -36 11.10 12.50 0 1 36 -10.90 12.10 -1 -1 -36 137.59 18.90 -1 -1 -36 130.49 20.10 1 1 36 171.48 31.50 1 1 36 112.19 22.60 -4 2 36 105.59 20.80 3 -2 -36 20.60 18.20 -3 2 36 -20.90 11.70 -2 2 36 18.20 14.50 1 -2 -36 2.00 11.70 -1 2 36 17.50 12.40 0 -2 -36 48.40 13.00 0 -2 -36 38.20 13.20 0 2 36 68.69 17.00 3 -3 -36 4.40 8.70 -3 3 36 -1.00 14.50 2 -3 -36 14.40 9.20 -2 3 36 19.60 14.70 1 -3 -36 30.10 11.10 -1 3 36 17.30 13.80 2 3 -37 169.88 27.80 -2 -3 37 193.58 18.90 -2 -3 37 220.88 20.40 -2 -3 37 210.68 22.90 1 3 -37 -2.30 18.50 -1 -3 37 1.40 9.80 -1 -3 37 23.10 10.90 0 3 -37 23.20 14.40 0 -3 37 41.40 12.10 -3 -2 37 76.19 14.60 2 2 -37 18.70 13.30 -2 -2 37 24.20 10.90 -2 -2 37 10.20 12.00 1 2 -37 124.29 19.80 -1 -2 37 178.88 21.40 0 2 -37 22.10 13.10 0 -2 37 38.50 13.70 3 1 -37 -5.90 11.80 -3 -1 37 1.30 9.60 -3 -1 37 5.90 12.10 2 1 -37 273.07 25.10 -2 -1 37 307.97 25.20 -2 -1 37 296.17 35.10 1 1 -37 14.10 12.60 -1 -1 37 -5.70 11.80 0 1 -37 262.97 25.90 0 -1 37 276.27 24.20 3 0 -37 15.70 12.50 -3 0 37 5.50 12.80 2 0 -37 18.90 12.80 -2 0 37 16.50 13.20 1 0 -37 55.69 16.40 -1 0 37 20.00 13.90 0 0 -37 20.00 13.10 0 0 37 -5.90 12.50 2 -1 -37 141.89 19.30 1 -1 -37 -2.00 10.40 -1 1 37 6.90 16.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 23515 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group B1 B 0.9587(3) 0.4083(3) 0.09975(12) 0.0162(7) Uani 1 1 d . . . . . H1A H 0.933884 0.476785 0.077543 0.024 Uiso 1 1 calc GR . . . . H1B H 1.046205 0.451787 0.128303 0.024 Uiso 1 1 calc GR . . . . H1C H 0.872249 0.362659 0.119880 0.024 Uiso 1 1 calc GR . . . . B2 B 1.0339(3) 0.1881(3) 0.09215(13) 0.0187(7) Uani 1 1 d . . . . . H2A H 0.946347 0.143077 0.111822 0.028 Uiso 1 1 calc GR . . . . H2B H 1.121050 0.230029 0.121062 0.028 Uiso 1 1 calc GR . . . . H2C H 1.057145 0.121471 0.065569 0.028 Uiso 1 1 calc GR . . . . B3 B 1.0964(3) 0.1428(3) 0.21883(13) 0.0176(7) Uani 1 1 d . . . . . H3A H 1.188184 0.167268 0.199062 0.026 Uiso 1 1 calc GR . . . . H3B H 1.094956 0.220141 0.245143 0.026 Uiso 1 1 calc GR . . . . H3C H 1.007596 0.117800 0.189960 0.026 Uiso 1 1 calc GR . . . . B4 B 1.2279(3) 0.0443(3) 0.30374(13) 0.0154(7) Uani 1 1 d . . . . . H4A H 1.202337 -0.027558 0.329657 0.023 Uiso 1 1 calc GR . . . . H4B H 1.244916 0.132066 0.325984 0.023 Uiso 1 1 calc GR . . . . H4C H 1.319668 0.043259 0.286314 0.023 Uiso 1 1 calc GR . . . . B5 B 0.7658(3) 0.1847(3) 0.18885(13) 0.0179(7) Uani 1 1 d . . . . . H5A H 0.816738 0.176399 0.154150 0.027 Uiso 1 1 calc GR . . . . H5B H 0.816982 0.156166 0.221824 0.027 Uiso 1 1 calc GR . . . . H5C H 0.769013 0.279069 0.197504 0.027 Uiso 1 1 calc GR . . . . B6 B 0.4924(3) 0.0882(3) 0.22789(14) 0.0212(8) Uani 1 1 d . . . . . H6A H 0.478879 0.177344 0.235866 0.032 Uiso 1 1 calc GR . . . . H6B H 0.539030 0.063639 0.263055 0.032 Uiso 1 1 calc GR . . . . H6C H 0.393893 0.020913 0.215921 0.032 Uiso 1 1 calc GR . . . . B7 B 0.9872(3) 0.4234(3) 0.27052(14) 0.0207(8) Uani 1 1 d . . . . . H7A H 1.086242 0.490058 0.282245 0.031 Uiso 1 1 calc GR . . . . H7B H 0.941157 0.447448 0.235088 0.031 Uiso 1 1 calc GR . . . . H7C H 0.999336 0.333604 0.263144 0.031 Uiso 1 1 calc GR . . . . B8 B 0.7131(3) 0.3303(3) 0.31053(14) 0.0206(8) Uani 1 1 d . . . . . H8A H 0.709136 0.235505 0.302897 0.031 Uiso 1 1 calc GR . . . . H8B H 0.661422 0.357200 0.277214 0.031 Uiso 1 1 calc GR . . . . H8C H 0.663320 0.341239 0.345279 0.031 Uiso 1 1 calc GR . . . . B9 B 0.3786(3) 0.3672(3) 0.28104(13) 0.0204(7) Uani 1 1 d . . . . . H9A H 0.467952 0.392162 0.309654 0.031 Uiso 1 1 calc GR . . . . H9B H 0.377205 0.287368 0.255690 0.031 Uiso 1 1 calc GR . . . . H9C H 0.287397 0.346629 0.301172 0.031 Uiso 1 1 calc GR . . . . B10 B 0.2514(3) 0.4644(3) 0.19353(12) 0.0152(7) Uani 1 1 d . . . . . H10A H 0.160229 0.469879 0.210322 0.023 Uiso 1 1 calc GR . . . . H10B H 0.231552 0.374909 0.172449 0.023 Uiso 1 1 calc GR . . . . H10C H 0.280174 0.533962 0.166709 0.023 Uiso 1 1 calc GR . . . . B11 B 0.5291(3) 0.0998(3) 0.39708(13) 0.0185(7) Uani 1 1 d . . . . . H11A H 0.558601 0.031751 0.418102 0.028 Uiso 1 1 calc GR . . . . H11B H 0.613853 0.150775 0.377396 0.028 Uiso 1 1 calc GR . . . . H11C H 0.442584 0.054934 0.368273 0.028 Uiso 1 1 calc GR . . . . B12 B 0.4377(4) 0.3105(3) 0.40772(14) 0.0215(8) Uani 1 1 d . . . . . H12A H 0.350290 0.266230 0.379251 0.032 Uiso 1 1 calc GR . . . . H12B H 0.522435 0.360030 0.387615 0.032 Uiso 1 1 calc GR . . . . H12C H 0.411816 0.373750 0.435205 0.032 Uiso 1 1 calc GR . . . . C11 C 0.8700(3) 0.2396(3) 0.01092(12) 0.0217(7) Uani 1 1 d . . . . . C12 C 0.8255(3) 0.3068(3) -0.01783(13) 0.0254(7) Uani 1 1 d . . . . . H12 H 0.861756 0.384680 -0.013432 0.031 Uiso 1 1 calc R . . . . C13 C 0.7279(3) 0.2592(3) -0.05291(13) 0.0322(8) Uani 1 1 d . . . . . H13 H 0.698446 0.304484 -0.072950 0.039 Uiso 1 1 calc R . . . . C14 C 0.6740(4) 0.1459(4) -0.05854(15) 0.0429(10) Uani 1 1 d . . . . . H14 H 0.606808 0.113754 -0.082314 0.051 Uiso 1 1 calc R . . . . C15 C 0.7163(4) 0.0796(3) -0.03020(15) 0.0453(11) Uani 1 1 d . . . . . H15 H 0.677374 0.002059 -0.033992 0.054 Uiso 1 1 calc R . . . . C16 C 0.8160(3) 0.1252(3) 0.00406(14) 0.0317(8) Uani 1 1 d . . . . . H16 H 0.847286 0.078772 0.022784 0.038 Uiso 1 1 calc R . . . . C21 C 1.1297(3) 0.3682(3) 0.02650(12) 0.0194(7) Uani 1 1 d . . . . . C22 C 1.1309(3) 0.3486(3) -0.02233(13) 0.0261(7) Uani 1 1 d . . . . . H22 H 1.061224 0.298152 -0.040812 0.031 Uiso 1 1 calc R . . . . C23 C 1.2336(3) 0.4027(3) -0.04400(13) 0.0303(8) Uani 1 1 d . . . . . H23 H 1.233335 0.389600 -0.077316 0.036 Uiso 1 1 calc R . . . . C24 C 1.3350(3) 0.4746(3) -0.01776(14) 0.0304(8) Uani 1 1 d . . . . . H24 H 1.404292 0.512216 -0.032938 0.036 Uiso 1 1 calc R . . . . C25 C 1.3368(3) 0.4926(3) 0.03103(15) 0.0321(9) Uani 1 1 d . . . . . H25 H 1.408071 0.541230 0.049314 0.039 Uiso 1 1 calc R . . . . C26 C 1.2346(3) 0.4395(3) 0.05314(13) 0.0266(8) Uani 1 1 d . . . . . H26 H 1.236130 0.451901 0.086551 0.032 Uiso 1 1 calc R . . . . C31 C 1.0862(3) -0.0980(2) 0.21351(11) 0.0152(6) Uani 1 1 d . . . . . C32 C 1.0873(3) -0.0883(3) 0.16546(12) 0.0249(7) Uani 1 1 d . . . . . H32 H 1.088545 -0.020284 0.153547 0.030 Uiso 1 1 calc R . . . . C33 C 1.0865(4) -0.1781(3) 0.13449(14) 0.0340(9) Uani 1 1 d . . . . . H33 H 1.087106 -0.171219 0.101461 0.041 Uiso 1 1 calc R . . . . C34 C 1.0847(3) -0.2774(3) 0.15166(14) 0.0303(8) Uani 1 1 d . . . . . H34 H 1.083662 -0.338717 0.130410 0.036 Uiso 1 1 calc R . . . . C35 C 1.0845(3) -0.2873(3) 0.19946(14) 0.0295(8) Uani 1 1 d . . . . . H35 H 1.083183 -0.355479 0.211239 0.035 Uiso 1 1 calc R . . . . C36 C 1.0861(3) -0.1977(3) 0.23062(13) 0.0250(7) Uani 1 1 d . . . . . H36 H 1.087102 -0.204496 0.263689 0.030 Uiso 1 1 calc R . . . . C41 C 0.9487(3) -0.0102(2) 0.28047(11) 0.0146(6) Uani 1 1 d . . . . . C42 C 0.9448(3) 0.0537(3) 0.32192(12) 0.0203(7) Uani 1 1 d . . . . . H42 H 1.018601 0.105084 0.337338 0.024 Uiso 1 1 calc R . . . . C43 C 0.8341(3) 0.0429(3) 0.34083(13) 0.0245(7) Uani 1 1 d . . . . . H43 H 0.831773 0.087930 0.368614 0.029 Uiso 1 1 calc R . . . . C44 C 0.7271(3) -0.0337(3) 0.31897(13) 0.0241(7) Uani 1 1 d . . . . . H44 H 0.651410 -0.042103 0.332067 0.029 Uiso 1 1 calc R . . . . C45 C 0.7301(3) -0.0979(3) 0.27820(13) 0.0258(8) Uani 1 1 d . . . . . H45 H 0.656432 -0.150822 0.263498 0.031 Uiso 1 1 calc R . . . . C46 C 0.8402(3) -0.0857(3) 0.25853(12) 0.0203(7) Uani 1 1 d . . . . . H46 H 0.841354 -0.128939 0.230075 0.024 Uiso 1 1 calc R . . . . C51 C 0.5974(3) -0.0462(3) 0.15806(12) 0.0195(7) Uani 1 1 d . . . . . C52 C 0.6888(4) -0.0636(3) 0.1322(2) 0.0588(16) Uani 1 1 d . . . . . H52 H 0.752701 -0.001901 0.124770 0.071 Uiso 1 1 calc R . . . . C53 C 0.6885(4) -0.1697(4) 0.1168(2) 0.073(2) Uani 1 1 d . . . . . H53 H 0.751673 -0.180050 0.099005 0.088 Uiso 1 1 calc R . . . . C54 C 0.5976(4) -0.2590(3) 0.12741(15) 0.0353(9) Uani 1 1 d . . . . . H54 H 0.596576 -0.331630 0.116803 0.042 Uiso 1 1 calc R . . . . C55 C 0.5088(4) -0.2430(3) 0.15320(15) 0.0370(9) Uani 1 1 d . . . . . H55 H 0.446074 -0.305189 0.160877 0.044 Uiso 1 1 calc R . . . . C56 C 0.5075(4) -0.1377(3) 0.16867(14) 0.0322(9) Uani 1 1 d . . . . . H56 H 0.444084 -0.128674 0.186683 0.039 Uiso 1 1 calc R . . . . C61 C 0.5297(3) 0.1424(2) 0.12689(12) 0.0180(6) Uani 1 1 d . . . . . C62 C 0.5943(3) 0.1687(3) 0.08773(13) 0.0309(8) Uani 1 1 d . . . . . H62 H 0.671381 0.155092 0.086448 0.037 Uiso 1 1 calc R . . . . C63 C 0.5477(3) 0.2141(4) 0.05070(15) 0.0380(9) Uani 1 1 d . . . . . H63 H 0.593498 0.232455 0.024426 0.046 Uiso 1 1 calc R . . . . C64 C 0.4358(4) 0.2331(3) 0.05158(14) 0.0317(8) Uani 1 1 d . . . . . H64 H 0.404275 0.264557 0.026042 0.038 Uiso 1 1 calc R . . . . C65 C 0.3699(3) 0.2065(3) 0.08935(14) 0.0322(9) Uani 1 1 d . . . . . H65 H 0.292311 0.219305 0.089872 0.039 Uiso 1 1 calc R . . . . C66 C 0.4154(3) 0.1610(3) 0.12704(13) 0.0259(7) Uani 1 1 d . . . . . H66 H 0.368514 0.142426 0.153002 0.031 Uiso 1 1 calc R . . . . C71 C 0.5291(3) 0.5157(2) 0.21752(11) 0.0146(6) Uani 1 1 d . . . . . C72 C 0.5330(3) 0.4526(3) 0.17573(12) 0.0198(7) Uani 1 1 d . . . . . H72 H 0.459259 0.401454 0.160169 0.024 Uiso 1 1 calc R . . . . C73 C 0.6435(3) 0.4639(3) 0.15684(12) 0.0222(7) Uani 1 1 d . . . . . H73 H 0.645697 0.419671 0.128821 0.027 Uiso 1 1 calc R . . . . C74 C 0.7508(3) 0.5401(3) 0.17892(12) 0.0238(7) Uani 1 1 d . . . . . H74 H 0.826600 0.548779 0.165816 0.029 Uiso 1 1 calc R . . . . C75 C 0.7476(3) 0.6034(3) 0.22008(13) 0.0251(7) Uani 1 1 d . . . . . H75 H 0.821281 0.655497 0.235196 0.030 Uiso 1 1 calc R . . . . C76 C 0.6370(3) 0.5913(3) 0.23945(12) 0.0215(7) Uani 1 1 d . . . . . H76 H 0.635511 0.634931 0.267755 0.026 Uiso 1 1 calc R . . . . C81 C 0.3932(3) 0.6090(2) 0.28284(11) 0.0166(6) Uani 1 1 d . . . . . C82 C 0.3667(3) 0.6984(3) 0.26515(13) 0.0288(8) Uani 1 1 d . . . . . H82 H 0.344988 0.696848 0.232081 0.035 Uiso 1 1 calc R . . . . C83 C 0.3713(4) 0.7907(3) 0.29526(15) 0.0347(9) Uani 1 1 d . . . . . H83 H 0.353377 0.851846 0.282577 0.042 Uiso 1 1 calc R . . . . C84 C 0.4013(3) 0.7941(3) 0.34273(15) 0.0346(9) Uani 1 1 d . . . . . H84 H 0.403505 0.856948 0.363229 0.042 Uiso 1 1 calc R . . . . C85 C 0.4282(4) 0.7064(3) 0.36076(14) 0.0385(10) Uani 1 1 d . . . . . H85 H 0.450120 0.709044 0.393874 0.046 Uiso 1 1 calc R . . . . C86 C 0.4237(4) 0.6134(3) 0.33123(14) 0.0327(9) Uani 1 1 d . . . . . H86 H 0.441691 0.552682 0.344279 0.039 Uiso 1 1 calc R . . . . C91 C 0.8863(3) 0.5628(3) 0.33955(12) 0.0213(7) Uani 1 1 d . . . . . C92 C 0.9928(3) 0.6499(3) 0.33889(12) 0.0255(7) Uani 1 1 d . . . . . H92 H 1.063812 0.636174 0.328000 0.031 Uiso 1 1 calc R . . . . C93 C 0.9969(4) 0.7572(3) 0.35404(13) 0.0308(8) Uani 1 1 d . . . . . H93 H 1.070890 0.816046 0.353658 0.037 Uiso 1 1 calc R . . . . C94 C 0.8964(4) 0.7785(3) 0.36934(15) 0.0363(9) Uani 1 1 d . . . . . H94 H 0.900357 0.851845 0.380067 0.044 Uiso 1 1 calc R . . . . C95 C 0.7894(4) 0.6943(4) 0.36931(18) 0.0508(12) Uani 1 1 d . . . . . H95 H 0.718494 0.709572 0.379469 0.061 Uiso 1 1 calc R . . . . C96 C 0.7836(4) 0.5866(3) 0.35451(17) 0.0431(11) Uani 1 1 d . . . . . H96 H 0.708767 0.528622 0.354632 0.052 Uiso 1 1 calc R . . . . C101 C 0.9504(3) 0.3759(3) 0.37205(12) 0.0227(7) Uani 1 1 d . . . . . C102 C 1.0499(3) 0.3362(3) 0.37018(14) 0.0297(8) Uani 1 1 d . . . . . H102 H 1.088560 0.337485 0.341817 0.036 Uiso 1 1 calc R . . . . C103 C 1.0946(4) 0.2940(3) 0.40961(15) 0.0378(10) Uani 1 1 d . . . . . H103 H 1.161872 0.265202 0.407617 0.045 Uiso 1 1 calc R . . . . C104 C 1.0414(4) 0.2944(4) 0.45096(17) 0.0499(12) Uani 1 1 d . . . . . H104 H 1.070849 0.264862 0.477575 0.060 Uiso 1 1 calc R . . . . C105 C 0.9442(4) 0.3382(6) 0.45395(18) 0.0717(19) Uani 1 1 d . . . . . H105 H 0.909155 0.341292 0.482982 0.086 Uiso 1 1 calc R . . . . C106 C 0.8988(4) 0.3771(5) 0.41474(16) 0.0529(13) Uani 1 1 d . . . . . H106 H 0.831024 0.405221 0.416821 0.063 Uiso 1 1 calc R . . . . C111 C 0.3552(3) 0.1232(3) 0.47145(11) 0.0187(6) Uani 1 1 d . . . . . C112 C 0.2492(3) 0.0546(3) 0.44443(13) 0.0271(8) Uani 1 1 d . . . . . H112 H 0.245161 0.049152 0.410807 0.032 Uiso 1 1 calc R . . . . C113 C 0.1501(3) -0.0055(3) 0.46594(14) 0.0330(9) Uani 1 1 d . . . . . H113 H 0.078330 -0.051677 0.447122 0.040 Uiso 1 1 calc R . . . . C114 C 0.1554(3) 0.0016(3) 0.51517(14) 0.0308(8) Uani 1 1 d . . . . . H114 H 0.088117 -0.040848 0.530073 0.037 Uiso 1 1 calc R . . . . C115 C 0.2585(3) 0.0702(3) 0.54203(13) 0.0298(8) Uani 1 1 d . . . . . H115 H 0.261571 0.076372 0.575630 0.036 Uiso 1 1 calc R . . . . C116 C 0.3581(3) 0.1306(3) 0.52060(12) 0.0264(8) Uani 1 1 d . . . . . H116 H 0.429025 0.177547 0.539648 0.032 Uiso 1 1 calc R . . . . C121 C 0.6076(3) 0.2638(3) 0.48831(12) 0.0231(7) Uani 1 1 d . . . . . C122 C 0.6694(3) 0.2016(3) 0.51252(13) 0.0270(8) Uani 1 1 d . . . . . H122 H 0.648938 0.124530 0.503736 0.032 Uiso 1 1 calc R . . . . C123 C 0.7607(3) 0.2514(3) 0.54940(14) 0.0348(9) Uani 1 1 d . . . . . H123 H 0.802327 0.208509 0.565937 0.042 Uiso 1 1 calc R . . . . C124 C 0.7910(4) 0.3640(4) 0.56205(16) 0.0442(11) Uani 1 1 d . . . . . H124 H 0.853798 0.398300 0.587206 0.053 Uiso 1 1 calc R . . . . C125 C 0.7305(5) 0.4262(4) 0.53830(17) 0.0538(13) Uani 1 1 d . . . . . H125 H 0.751052 0.503256 0.547303 0.065 Uiso 1 1 calc R . . . . C126 C 0.6395(4) 0.3769(3) 0.50122(15) 0.0393(10) Uani 1 1 d . . . . . H126 H 0.598857 0.420471 0.484610 0.047 Uiso 1 1 calc R . . . . Ce1 Ce 1.00302(2) 0.29735(2) 0.18217(2) 0.01173(4) Uani 1 1 d . . . . . Ce2 Ce 0.47731(2) 0.21240(2) 0.31674(2) 0.01239(4) Uani 1 1 d . . . . . P1 P 0.99742(7) 0.30026(7) 0.05673(3) 0.01673(16) Uani 1 1 d . . . . . P2 P 1.09405(7) 0.02055(6) 0.25439(3) 0.01284(15) Uani 1 1 d . . . . . P3 P 0.59736(7) 0.09284(6) 0.17775(3) 0.01525(16) Uani 1 1 d . . . . . P4 P 0.88255(7) 0.42187(7) 0.32050(3) 0.01750(17) Uani 1 1 d . . . . . P5 P 0.38388(7) 0.48763(6) 0.24361(3) 0.01279(15) Uani 1 1 d . . . . . P6 P 0.48391(7) 0.20039(7) 0.44167(3) 0.01714(16) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 B1 0.0186(16) 0.0153(15) 0.0126(17) -0.0016(13) -0.0013(13) 0.0033(14) B2 0.0210(17) 0.0172(16) 0.0184(19) 0.0003(14) 0.0048(14) 0.0062(15) B3 0.0210(17) 0.0126(15) 0.0199(19) 0.0025(14) -0.0018(14) 0.0069(14) B4 0.0124(15) 0.0128(15) 0.0190(19) 0.0004(14) 0.0020(13) 0.0012(13) B5 0.0127(15) 0.0175(16) 0.022(2) 0.0009(15) 0.0030(14) 0.0021(14) B6 0.0167(17) 0.0244(18) 0.020(2) -0.0035(16) 0.0052(14) 0.0023(15) B7 0.0167(17) 0.0233(18) 0.022(2) -0.0015(16) 0.0079(14) 0.0050(15) B8 0.0171(17) 0.0187(17) 0.022(2) -0.0014(15) 0.0040(14) 0.0001(15) B9 0.0235(18) 0.0156(16) 0.0188(19) 0.0002(14) -0.0026(14) 0.0028(15) B10 0.0162(16) 0.0129(15) 0.0156(18) -0.0002(13) 0.0022(13) 0.0033(13) B11 0.0200(17) 0.0187(17) 0.0148(18) 0.0013(14) 0.0004(14) 0.0034(15) B12 0.0284(19) 0.0187(17) 0.0170(19) 0.0015(15) 0.0022(15) 0.0067(16) C11 0.0218(16) 0.0244(16) 0.0148(17) -0.0040(14) 0.0044(13) 0.0018(14) C12 0.0239(17) 0.0266(17) 0.0229(19) -0.0012(15) 0.0007(14) 0.0047(15) C13 0.0317(19) 0.039(2) 0.023(2) -0.0039(17) -0.0045(15) 0.0106(17) C14 0.040(2) 0.045(2) 0.031(2) -0.0107(19) -0.0119(18) 0.000(2) C15 0.053(3) 0.028(2) 0.037(2) -0.0091(18) -0.009(2) -0.0091(19) C16 0.038(2) 0.0230(17) 0.028(2) -0.0014(15) -0.0007(16) 0.0017(16) C21 0.0189(15) 0.0209(15) 0.0202(17) 0.0047(13) 0.0033(13) 0.0079(13) C22 0.0262(17) 0.0299(18) 0.0220(19) 0.0027(15) 0.0046(14) 0.0077(15) C23 0.034(2) 0.041(2) 0.0225(19) 0.0103(16) 0.0093(15) 0.0174(18) C24 0.0250(18) 0.0310(19) 0.041(2) 0.0153(17) 0.0170(16) 0.0111(16) C25 0.0214(17) 0.0271(18) 0.045(2) 0.0000(17) 0.0068(16) 0.0030(15) C26 0.0264(17) 0.0274(18) 0.024(2) 0.0001(15) 0.0048(15) 0.0044(15) C31 0.0132(14) 0.0127(13) 0.0186(16) -0.0028(12) 0.0006(12) 0.0037(12) C32 0.0377(19) 0.0195(15) 0.0165(17) -0.0021(13) -0.0001(14) 0.0090(15) C33 0.052(2) 0.0285(19) 0.0195(19) -0.0042(15) 0.0049(17) 0.0103(18) C34 0.037(2) 0.0193(16) 0.031(2) -0.0102(15) 0.0056(16) 0.0063(16) C35 0.038(2) 0.0131(15) 0.037(2) 0.0011(15) 0.0089(17) 0.0065(15) C36 0.0359(19) 0.0185(15) 0.0210(18) 0.0027(14) 0.0082(14) 0.0076(15) C41 0.0131(14) 0.0162(14) 0.0157(16) 0.0038(12) 0.0018(11) 0.0058(12) C42 0.0178(15) 0.0183(15) 0.0227(18) -0.0016(13) 0.0022(13) 0.0031(13) C43 0.0248(17) 0.0274(17) 0.0239(19) 0.0003(15) 0.0100(14) 0.0103(15) C44 0.0171(15) 0.0273(17) 0.030(2) 0.0094(15) 0.0098(14) 0.0067(14) C45 0.0143(15) 0.0276(18) 0.031(2) 0.0032(15) -0.0005(14) 0.0009(14) C46 0.0183(15) 0.0204(15) 0.0202(18) 0.0005(13) 0.0005(13) 0.0037(13) C51 0.0198(15) 0.0164(14) 0.0195(17) -0.0036(13) -0.0002(13) 0.0030(13) C52 0.038(2) 0.0187(18) 0.113(5) -0.018(2) 0.039(3) -0.0045(18) C53 0.044(3) 0.028(2) 0.142(6) -0.025(3) 0.047(3) 0.003(2) C54 0.039(2) 0.0204(17) 0.047(3) -0.0055(17) 0.0001(18) 0.0130(17) C55 0.054(3) 0.0167(16) 0.033(2) 0.0034(16) 0.0072(19) -0.0006(17) C56 0.041(2) 0.0221(17) 0.031(2) -0.0002(16) 0.0148(17) 0.0037(16) C61 0.0147(14) 0.0148(14) 0.0227(18) -0.0029(13) 0.0024(12) 0.0028(12) C62 0.0197(16) 0.047(2) 0.027(2) 0.0091(17) 0.0060(14) 0.0090(16) C63 0.029(2) 0.050(2) 0.030(2) 0.0127(19) 0.0058(16) 0.0028(18) C64 0.039(2) 0.0254(18) 0.030(2) 0.0041(16) -0.0061(16) 0.0106(17) C65 0.0289(19) 0.038(2) 0.036(2) -0.0054(17) -0.0033(16) 0.0231(17) C66 0.0249(17) 0.0314(18) 0.0251(19) -0.0020(15) 0.0057(14) 0.0145(15) C71 0.0141(14) 0.0123(13) 0.0188(16) 0.0037(12) 0.0029(12) 0.0054(12) C72 0.0185(15) 0.0182(15) 0.0217(18) -0.0006(13) 0.0026(13) 0.0048(13) C73 0.0265(17) 0.0207(16) 0.0228(18) 0.0008(14) 0.0078(14) 0.0115(14) C74 0.0177(15) 0.0306(18) 0.029(2) 0.0090(15) 0.0083(14) 0.0136(14) C75 0.0154(15) 0.0262(17) 0.031(2) 0.0038(15) 0.0040(14) 0.0025(14) C76 0.0212(16) 0.0211(16) 0.0212(18) 0.0003(14) 0.0031(13) 0.0050(14) C81 0.0127(14) 0.0163(14) 0.0203(17) -0.0009(13) 0.0053(12) 0.0030(12) C82 0.043(2) 0.0176(15) 0.026(2) 0.0019(14) 0.0120(16) 0.0078(16) C83 0.046(2) 0.0171(16) 0.043(2) 0.0005(16) 0.0174(19) 0.0092(16) C84 0.032(2) 0.0217(17) 0.045(3) -0.0153(17) 0.0096(17) 0.0022(16) C85 0.046(2) 0.043(2) 0.024(2) -0.0168(18) -0.0036(17) 0.017(2) C86 0.041(2) 0.0300(19) 0.028(2) -0.0055(16) -0.0049(16) 0.0166(17) C91 0.0201(15) 0.0189(15) 0.0212(18) -0.0050(13) -0.0001(13) 0.0026(13) C92 0.0308(18) 0.0205(16) 0.0215(18) -0.0001(14) 0.0069(14) 0.0017(15) C93 0.042(2) 0.0170(16) 0.025(2) 0.0030(14) 0.0030(16) -0.0036(16) C94 0.047(2) 0.0211(17) 0.038(2) -0.0073(16) -0.0095(19) 0.0126(18) C95 0.038(2) 0.038(2) 0.075(3) -0.022(2) 0.002(2) 0.018(2) C96 0.028(2) 0.029(2) 0.065(3) -0.016(2) 0.0080(19) 0.0019(17) C101 0.0180(15) 0.0210(16) 0.0239(19) 0.0000(14) 0.0015(13) -0.0012(13) C102 0.0333(19) 0.0286(18) 0.026(2) -0.0067(15) -0.0007(15) 0.0100(16) C103 0.040(2) 0.0265(19) 0.041(3) -0.0072(18) -0.0126(18) 0.0079(17) C104 0.040(2) 0.055(3) 0.041(3) 0.024(2) -0.007(2) -0.008(2) C105 0.033(2) 0.139(6) 0.038(3) 0.035(3) 0.010(2) 0.009(3) C106 0.025(2) 0.101(4) 0.036(3) 0.022(3) 0.0095(18) 0.019(2) C111 0.0219(16) 0.0169(14) 0.0180(17) 0.0033(13) 0.0037(13) 0.0064(13) C112 0.0237(17) 0.0325(19) 0.0206(19) -0.0030(15) 0.0008(14) 0.0037(15) C113 0.0234(18) 0.036(2) 0.034(2) -0.0030(17) 0.0030(15) 0.0025(16) C114 0.0254(18) 0.0317(19) 0.035(2) 0.0101(17) 0.0129(16) 0.0045(16) C115 0.0317(19) 0.041(2) 0.0208(19) 0.0103(16) 0.0107(15) 0.0138(17) C116 0.0263(17) 0.0294(18) 0.0203(18) -0.0017(15) -0.0004(14) 0.0053(15) C121 0.0240(16) 0.0212(16) 0.0190(18) -0.0015(14) 0.0047(13) -0.0009(14) C122 0.0256(17) 0.0291(18) 0.0242(19) -0.0060(15) -0.0008(14) 0.0078(15) C123 0.0304(19) 0.045(2) 0.026(2) -0.0027(18) -0.0015(16) 0.0105(18) C124 0.038(2) 0.045(2) 0.035(2) -0.010(2) -0.0123(18) -0.001(2) C125 0.067(3) 0.026(2) 0.050(3) -0.006(2) -0.019(2) -0.003(2) C126 0.049(2) 0.0218(18) 0.036(2) -0.0005(16) -0.0143(19) -0.0002(17) Ce1 0.01053(8) 0.00994(8) 0.01444(9) 0.00114(7) 0.00186(6) 0.00258(6) Ce2 0.01137(8) 0.01079(8) 0.01381(9) 0.00114(7) 0.00110(6) 0.00167(6) P1 0.0178(4) 0.0160(4) 0.0148(4) 0.0006(3) 0.0019(3) 0.0028(3) P2 0.0129(3) 0.0114(3) 0.0139(4) 0.0007(3) 0.0016(3) 0.0035(3) P3 0.0120(3) 0.0143(4) 0.0176(4) -0.0022(3) 0.0023(3) 0.0019(3) P4 0.0134(4) 0.0154(4) 0.0204(4) -0.0029(3) 0.0035(3) 0.0001(3) P5 0.0132(3) 0.0105(3) 0.0141(4) 0.0004(3) 0.0017(3) 0.0030(3) P6 0.0199(4) 0.0156(4) 0.0136(4) -0.0004(3) 0.0009(3) 0.0028(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ce Ce -0.2486 2.6331 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag H1A B1 H1B 109.5 . . ? H1A B1 H1C 109.5 . . ? H1B B1 H1C 109.5 . . ? P1 B1 H1A 109.5 . . ? P1 B1 H1B 109.5 . . ? P1 B1 H1C 109.5 . . ? H2A B2 H2B 109.5 . . ? H2A B2 H2C 109.5 . . ? H2B B2 H2C 109.5 . . ? P1 B2 H2A 109.5 . . ? P1 B2 H2B 109.5 . . ? P1 B2 H2C 109.5 . . ? H3A B3 H3B 109.5 . . ? H3A B3 H3C 109.5 . . ? H3B B3 H3C 109.5 . . ? P2 B3 H3A 109.5 . . ? P2 B3 H3B 109.5 . . ? P2 B3 H3C 109.5 . . ? H4A B4 H4B 109.5 . . ? H4A B4 H4C 109.5 . . ? H4B B4 H4C 109.5 . . ? P2 B4 H4A 109.5 . . ? P2 B4 H4B 109.5 . . ? P2 B4 H4C 109.5 . . ? H5A B5 H5B 109.5 . . ? H5A B5 H5C 109.5 . . ? H5B B5 H5C 109.5 . . ? P3 B5 H5A 109.5 . . ? P3 B5 H5B 109.5 . . ? P3 B5 H5C 109.5 . . ? H6A B6 H6B 109.5 . . ? H6A B6 H6C 109.5 . . ? H6B B6 H6C 109.5 . . ? P3 B6 H6A 109.5 . . ? P3 B6 H6B 109.5 . . ? P3 B6 H6C 109.5 . . ? H7A B7 H7B 109.5 . . ? H7A B7 H7C 109.5 . . ? H7B B7 H7C 109.5 . . ? P4 B7 H7A 109.5 . . ? P4 B7 H7B 109.5 . . ? P4 B7 H7C 109.5 . . ? H8A B8 H8B 109.5 . . ? H8A B8 H8C 109.5 . . ? H8B B8 H8C 109.5 . . ? P4 B8 H8A 109.5 . . ? P4 B8 H8B 109.5 . . ? P4 B8 H8C 109.5 . . ? H9A B9 H9B 109.5 . . ? H9A B9 H9C 109.5 . . ? H9B B9 H9C 109.5 . . ? P5 B9 H9A 109.5 . . ? P5 B9 H9B 109.5 . . ? P5 B9 H9C 109.5 . . ? H10A B10 H10B 109.5 . . ? H10A B10 H10C 109.5 . . ? H10B B10 H10C 109.5 . . ? P5 B10 H10A 109.5 . . ? P5 B10 H10B 109.5 . . ? P5 B10 H10C 109.5 . . ? H11A B11 H11B 109.5 . . ? H11A B11 H11C 109.5 . . ? H11B B11 H11C 109.5 . . ? P6 B11 H11A 109.5 . . ? P6 B11 H11B 109.5 . . ? P6 B11 H11C 109.5 . . ? H12A B12 H12B 109.5 . . ? H12A B12 H12C 109.5 . . ? H12B B12 H12C 109.5 . . ? P6 B12 H12A 109.5 . . ? P6 B12 H12B 109.5 . . ? P6 B12 H12C 109.5 . . ? C12 C11 P1 120.3(3) . . ? C16 C11 C12 119.5(3) . . ? C16 C11 P1 120.1(3) . . ? C11 C12 H12 120.1 . . ? C13 C12 C11 119.8(3) . . ? C13 C12 H12 120.1 . . ? C12 C13 H13 120.1 . . ? C14 C13 C12 119.9(4) . . ? C14 C13 H13 120.1 . . ? C13 C14 H14 119.7 . . ? C15 C14 C13 120.7(4) . . ? C15 C14 H14 119.7 . . ? C14 C15 H15 119.9 . . ? C14 C15 C16 120.3(4) . . ? C16 C15 H15 119.9 . . ? C11 C16 H16 120.1 . . ? C15 C16 C11 119.8(4) . . ? C15 C16 H16 120.1 . . ? C22 C21 P1 122.1(3) . . ? C26 C21 C22 118.9(3) . . ? C26 C21 P1 119.0(3) . . ? C21 C22 H22 119.9 . . ? C23 C22 C21 120.2(3) . . ? C23 C22 H22 119.9 . . ? C22 C23 H23 119.7 . . ? C24 C23 C22 120.5(4) . . ? C24 C23 H23 119.7 . . ? C23 C24 H24 120.0 . . ? C23 C24 C25 120.0(3) . . ? C25 C24 H24 120.0 . . ? C24 C25 H25 120.0 . . ? C24 C25 C26 120.1(4) . . ? C26 C25 H25 120.0 . . ? C21 C26 H26 119.9 . . ? C25 C26 C21 120.3(3) . . ? C25 C26 H26 119.9 . . ? C32 C31 C36 119.4(3) . . ? C32 C31 P2 120.3(2) . . ? C36 C31 P2 120.2(2) . . ? C31 C32 H32 120.0 . . ? C31 C32 C33 120.1(3) . . ? C33 C32 H32 120.0 . . ? C32 C33 H33 119.9 . . ? C34 C33 C32 120.2(4) . . ? C34 C33 H33 119.9 . . ? C33 C34 H34 120.0 . . ? C35 C34 C33 119.9(3) . . ? C35 C34 H34 120.0 . . ? C34 C35 H35 120.0 . . ? C34 C35 C36 120.1(3) . . ? C36 C35 H35 120.0 . . ? C31 C36 H36 119.9 . . ? C35 C36 C31 120.2(3) . . ? C35 C36 H36 119.9 . . ? C42 C41 P2 117.6(2) . . ? C46 C41 C42 119.1(3) . . ? C46 C41 P2 122.9(2) . . ? C41 C42 H42 119.7 . . ? C43 C42 C41 120.6(3) . . ? C43 C42 H42 119.7 . . ? C42 C43 H43 120.2 . . ? C44 C43 C42 119.6(3) . . ? C44 C43 H43 120.2 . . ? C43 C44 H44 119.9 . . ? C45 C44 C43 120.2(3) . . ? C45 C44 H44 119.9 . . ? C44 C45 H45 119.8 . . ? C44 C45 C46 120.4(3) . . ? C46 C45 H45 119.8 . . ? C41 C46 C45 120.1(3) . . ? C41 C46 H46 120.0 . . ? C45 C46 H46 120.0 . . ? C52 C51 P3 121.1(3) . . ? C56 C51 C52 117.7(3) . . ? C56 C51 P3 121.2(3) . . ? C51 C52 H52 119.4 . . ? C51 C52 C53 121.1(4) . . ? C53 C52 H52 119.4 . . ? C52 C53 H53 120.0 . . ? C54 C53 C52 120.0(4) . . ? C54 C53 H53 120.0 . . ? C53 C54 H54 120.4 . . ? C55 C54 C53 119.3(3) . . ? C55 C54 H54 120.4 . . ? C54 C55 H55 119.3 . . ? C54 C55 C56 121.5(4) . . ? C56 C55 H55 119.3 . . ? C51 C56 C55 120.4(4) . . ? C51 C56 H56 119.8 . . ? C55 C56 H56 119.8 . . ? C62 C61 C66 118.0(3) . . ? C62 C61 P3 120.5(2) . . ? C66 C61 P3 121.3(3) . . ? C61 C62 H62 119.6 . . ? C63 C62 C61 120.8(3) . . ? C63 C62 H62 119.6 . . ? C62 C63 H63 119.7 . . ? C64 C63 C62 120.5(4) . . ? C64 C63 H63 119.7 . . ? C63 C64 H64 120.2 . . ? C65 C64 C63 119.7(3) . . ? C65 C64 H64 120.2 . . ? C64 C65 H65 119.7 . . ? C64 C65 C66 120.7(3) . . ? C66 C65 H65 119.7 . . ? C61 C66 H66 119.9 . . ? C65 C66 C61 120.3(3) . . ? C65 C66 H66 119.9 . . ? C72 C71 P5 118.4(2) . . ? C76 C71 C72 119.1(3) . . ? C76 C71 P5 122.2(2) . . ? C71 C72 H72 119.7 . . ? C73 C72 C71 120.6(3) . . ? C73 C72 H72 119.7 . . ? C72 C73 H73 120.1 . . ? C72 C73 C74 119.8(3) . . ? C74 C73 H73 120.1 . . ? C73 C74 H74 120.0 . . ? C75 C74 C73 119.9(3) . . ? C75 C74 H74 120.0 . . ? C74 C75 H75 119.8 . . ? C74 C75 C76 120.4(3) . . ? C76 C75 H75 119.8 . . ? C71 C76 C75 120.1(3) . . ? C71 C76 H76 119.9 . . ? C75 C76 H76 119.9 . . ? C82 C81 C86 118.3(3) . . ? C82 C81 P5 120.5(3) . . ? C86 C81 P5 121.1(2) . . ? C81 C82 H82 119.7 . . ? C81 C82 C83 120.7(4) . . ? C83 C82 H82 119.7 . . ? C82 C83 H83 119.8 . . ? C84 C83 C82 120.4(4) . . ? C84 C83 H83 119.8 . . ? C83 C84 H84 120.2 . . ? C83 C84 C85 119.6(3) . . ? C85 C84 H84 120.2 . . ? C84 C85 H85 119.6 . . ? C84 C85 C86 120.8(4) . . ? C86 C85 H85 119.6 . . ? C81 C86 C85 120.2(4) . . ? C81 C86 H86 119.9 . . ? C85 C86 H86 119.9 . . ? C92 C91 C96 118.0(3) . . ? C92 C91 P4 120.3(2) . . ? C96 C91 P4 121.7(3) . . ? C91 C92 H92 119.7 . . ? C91 C92 C93 120.6(3) . . ? C93 C92 H92 119.7 . . ? C92 C93 H93 119.7 . . ? C94 C93 C92 120.6(3) . . ? C94 C93 H93 119.7 . . ? C93 C94 H94 120.1 . . ? C93 C94 C95 119.9(3) . . ? C95 C94 H94 120.1 . . ? C94 C95 H95 119.8 . . ? C94 C95 C96 120.4(4) . . ? C96 C95 H95 119.8 . . ? C91 C96 C95 120.6(4) . . ? C91 C96 H96 119.7 . . ? C95 C96 H96 119.7 . . ? C102 C101 C106 118.3(3) . . ? C102 C101 P4 122.2(3) . . ? C106 C101 P4 119.5(3) . . ? C101 C102 H102 119.6 . . ? C101 C102 C103 120.8(4) . . ? C103 C102 H102 119.6 . . ? C102 C103 H103 120.0 . . ? C104 C103 C102 120.0(4) . . ? C104 C103 H103 120.0 . . ? C103 C104 H104 120.1 . . ? C103 C104 C105 119.8(4) . . ? C105 C104 H104 120.1 . . ? C104 C105 H105 120.1 . . ? C106 C105 C104 119.9(5) . . ? C106 C105 H105 120.1 . . ? C101 C106 H106 119.4 . . ? C105 C106 C101 121.2(4) . . ? C105 C106 H106 119.4 . . ? C112 C111 P6 119.4(3) . . ? C116 C111 C112 118.4(3) . . ? C116 C111 P6 122.3(3) . . ? C111 C112 H112 119.6 . . ? C113 C112 C111 120.8(3) . . ? C113 C112 H112 119.6 . . ? C112 C113 H113 120.0 . . ? C112 C113 C114 120.0(3) . . ? C114 C113 H113 120.0 . . ? C113 C114 H114 120.2 . . ? C115 C114 C113 119.6(3) . . ? C115 C114 H114 120.2 . . ? C114 C115 H115 119.7 . . ? C114 C115 C116 120.6(3) . . ? C116 C115 H115 119.7 . . ? C111 C116 H116 119.7 . . ? C115 C116 C111 120.6(3) . . ? C115 C116 H116 119.7 . . ? C122 C121 C126 119.1(3) . . ? C122 C121 P6 121.5(3) . . ? C126 C121 P6 119.4(3) . . ? C121 C122 H122 119.8 . . ? C123 C122 C121 120.4(3) . . ? C123 C122 H122 119.8 . . ? C122 C123 H123 120.1 . . ? C124 C123 C122 119.8(4) . . ? C124 C123 H123 120.1 . . ? C123 C124 H124 119.9 . . ? C125 C124 C123 120.2(4) . . ? C125 C124 H124 119.9 . . ? C124 C125 H125 119.9 . . ? C124 C125 C126 120.2(4) . . ? C126 C125 H125 119.9 . . ? C121 C126 H126 119.9 . . ? C125 C126 C121 120.2(4) . . ? C125 C126 H126 119.9 . . ? B2 P1 B1 109.60(15) . . ? C11 P1 B1 110.28(15) . . ? C11 P1 B2 110.92(16) . . ? C11 P1 C21 106.46(15) . . ? C21 P1 B1 109.90(15) . . ? C21 P1 B2 109.63(15) . . ? B3 P2 B4 116.22(15) . . ? C31 P2 B3 108.73(15) . . ? C31 P2 B4 110.02(14) . . ? C31 P2 C41 107.34(14) . . ? C41 P2 B3 104.61(14) . . ? C41 P2 B4 109.48(14) . . ? B5 P3 B6 118.85(16) . . ? C51 P3 B5 107.70(15) . . ? C51 P3 B6 110.08(16) . . ? C51 P3 C61 105.94(15) . . ? C61 P3 B5 105.62(15) . . ? C61 P3 B6 107.86(15) . . ? B8 P4 B7 119.40(17) . . ? C91 P4 B7 109.79(16) . . ? C91 P4 B8 108.46(15) . . ? C101 P4 B7 107.88(16) . . ? C101 P4 B8 105.62(16) . . ? C101 P4 C91 104.64(15) . . ? B9 P5 B10 116.88(15) . . ? C71 P5 B9 105.41(15) . . ? C71 P5 B10 108.79(15) . . ? C81 P5 B9 108.76(15) . . ? C81 P5 B10 109.53(14) . . ? C81 P5 C71 106.99(14) . . ? B12 P6 B11 109.31(16) . . ? C111 P6 B11 109.48(15) . . ? C111 P6 B12 109.85(16) . . ? C121 P6 B11 111.48(15) . . ? C121 P6 B12 111.18(16) . . ? C121 P6 C111 105.47(15) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag B1 H1A 1.2000 . ? B1 H1B 1.2000 . ? B1 H1C 1.2000 . ? B1 P1 1.950(3) . ? B2 H2A 1.2000 . ? B2 H2B 1.2000 . ? B2 H2C 1.2000 . ? B2 P1 1.930(4) . ? B3 H3A 1.2000 . ? B3 H3B 1.2000 . ? B3 H3C 1.2000 . ? B3 P2 1.913(3) . ? B4 H4A 1.2000 . ? B4 H4B 1.2000 . ? B4 H4C 1.2000 . ? B4 P2 1.927(3) . ? B5 H5A 1.2000 . ? B5 H5B 1.2000 . ? B5 H5C 1.2000 . ? B5 P3 1.919(3) . ? B6 H6A 1.2000 . ? B6 H6B 1.2000 . ? B6 H6C 1.2000 . ? B6 P3 1.931(4) . ? B7 H7A 1.2000 . ? B7 H7B 1.2000 . ? B7 H7C 1.2000 . ? B7 P4 1.929(4) . ? B8 H8A 1.2000 . ? B8 H8B 1.2000 . ? B8 H8C 1.2000 . ? B8 P4 1.926(4) . ? B9 H9A 1.2000 . ? B9 H9B 1.2000 . ? B9 H9C 1.2000 . ? B9 P5 1.919(4) . ? B10 H10A 1.2000 . ? B10 H10B 1.2000 . ? B10 H10C 1.2000 . ? B10 P5 1.931(3) . ? B11 H11A 1.2000 . ? B11 H11B 1.2000 . ? B11 H11C 1.2000 . ? B11 P6 1.947(4) . ? B12 H12A 1.2000 . ? B12 H12B 1.2000 . ? B12 H12C 1.2000 . ? B12 P6 1.933(4) . ? C11 C12 1.397(5) . ? C11 C16 1.397(5) . ? C11 P1 1.814(3) . ? C12 H12 0.9500 . ? C12 C13 1.392(5) . ? C13 H13 0.9500 . ? C13 C14 1.384(6) . ? C14 H14 0.9500 . ? C14 C15 1.370(6) . ? C15 H15 0.9500 . ? C15 C16 1.389(5) . ? C16 H16 0.9500 . ? C21 C22 1.395(5) . ? C21 C26 1.394(5) . ? C21 P1 1.820(3) . ? C22 H22 0.9500 . ? C22 C23 1.389(5) . ? C23 H23 0.9500 . ? C23 C24 1.368(5) . ? C24 H24 0.9500 . ? C24 C25 1.388(5) . ? C25 H25 0.9500 . ? C25 C26 1.389(5) . ? C26 H26 0.9500 . ? C31 C32 1.381(5) . ? C31 C36 1.393(4) . ? C31 P2 1.817(3) . ? C32 H32 0.9500 . ? C32 C33 1.392(5) . ? C33 H33 0.9500 . ? C33 C34 1.385(5) . ? C34 H34 0.9500 . ? C34 C35 1.374(5) . ? C35 H35 0.9500 . ? C35 C36 1.390(5) . ? C36 H36 0.9500 . ? C41 C42 1.396(4) . ? C41 C46 1.389(4) . ? C41 P2 1.822(3) . ? C42 H42 0.9500 . ? C42 C43 1.389(4) . ? C43 H43 0.9500 . ? C43 C44 1.383(5) . ? C44 H44 0.9500 . ? C44 C45 1.380(5) . ? C45 H45 0.9500 . ? C45 C46 1.391(4) . ? C46 H46 0.9500 . ? C51 C52 1.387(5) . ? C51 C56 1.376(5) . ? C51 P3 1.822(3) . ? C52 H52 0.9500 . ? C52 C53 1.392(5) . ? C53 H53 0.9500 . ? C53 C54 1.364(6) . ? C54 H54 0.9500 . ? C54 C55 1.354(6) . ? C55 H55 0.9500 . ? C55 C56 1.389(5) . ? C56 H56 0.9500 . ? C61 C62 1.392(5) . ? C61 C66 1.396(4) . ? C61 P3 1.824(3) . ? C62 H62 0.9500 . ? C62 C63 1.381(5) . ? C63 H63 0.9500 . ? C63 C64 1.373(5) . ? C64 H64 0.9500 . ? C64 C65 1.367(5) . ? C65 H65 0.9500 . ? C65 C66 1.390(5) . ? C66 H66 0.9500 . ? C71 C72 1.399(4) . ? C71 C76 1.386(4) . ? C71 P5 1.822(3) . ? C72 H72 0.9500 . ? C72 C73 1.385(4) . ? C73 H73 0.9500 . ? C73 C74 1.386(5) . ? C74 H74 0.9500 . ? C74 C75 1.384(5) . ? C75 H75 0.9500 . ? C75 C76 1.390(4) . ? C76 H76 0.9500 . ? C81 C82 1.381(5) . ? C81 C86 1.385(5) . ? C81 P5 1.814(3) . ? C82 H82 0.9500 . ? C82 C83 1.391(5) . ? C83 H83 0.9500 . ? C83 C84 1.360(6) . ? C84 H84 0.9500 . ? C84 C85 1.367(6) . ? C85 H85 0.9500 . ? C85 C86 1.389(5) . ? C86 H86 0.9500 . ? C91 C92 1.384(5) . ? C91 C96 1.387(5) . ? C91 P4 1.828(3) . ? C92 H92 0.9500 . ? C92 C93 1.392(5) . ? C93 H93 0.9500 . ? C93 C94 1.355(6) . ? C94 H94 0.9500 . ? C94 C95 1.366(6) . ? C95 H95 0.9500 . ? C95 C96 1.389(5) . ? C96 H96 0.9500 . ? C101 C102 1.379(5) . ? C101 C106 1.394(5) . ? C101 P4 1.817(4) . ? C102 H102 0.9500 . ? C102 C103 1.401(5) . ? C103 H103 0.9500 . ? C103 C104 1.368(6) . ? C104 H104 0.9500 . ? C104 C105 1.391(7) . ? C105 H105 0.9500 . ? C105 C106 1.377(6) . ? C106 H106 0.9500 . ? C111 C112 1.394(5) . ? C111 C116 1.391(5) . ? C111 P6 1.820(3) . ? C112 H112 0.9500 . ? C112 C113 1.381(5) . ? C113 H113 0.9500 . ? C113 C114 1.392(5) . ? C114 H114 0.9500 . ? C114 C115 1.371(5) . ? C115 H115 0.9500 . ? C115 C116 1.385(5) . ? C116 H116 0.9500 . ? C121 C122 1.391(5) . ? C121 C126 1.392(5) . ? C121 P6 1.809(3) . ? C122 H122 0.9500 . ? C122 C123 1.387(5) . ? C123 H123 0.9500 . ? C123 C124 1.386(6) . ? C124 H124 0.9500 . ? C124 C125 1.376(6) . ? C125 H125 0.9500 . ? C125 C126 1.388(6) . ? C126 H126 0.9500 . ? Ce1 B10 2.975(3) 1_655 ? Ce2 B4 2.989(3) 1_455 ?