#------------------------------------------------------------------------------ #$Date: 2021-10-06 18:34:01 +0300 (Wed, 06 Oct 2021) $ #$Revision: 269711 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/81/7708162.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708162 loop_ _publ_author_name 'Yang, Feng' 'Xu, Yuangang' 'Wang, Pengcheng' 'Lin, Qiuhan' 'Lu, Ming' _publ_section_title ; Novel metal-organic frameworks assembled from the combination of polynitro-pyrazole and 5-nitroamine-1,2,4-oxadiazole: synthesis, structure and thermal properties. ; _journal_issue 37 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 12906 _journal_page_last 12912 _journal_paper_doi 10.1039/d1dt02093e _journal_volume 50 _journal_year 2021 _chemical_formula_moiety 'C6 H5 N9 O7, H2 O' _chemical_formula_sum 'C6 H7 N9 O8' _chemical_formula_weight 333.21 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-06-10 deposited with the CCDC. 2021-08-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 108.117(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 7.8296(8) _cell_length_b 22.796(3) _cell_length_c 7.4593(7) _cell_measurement_reflns_used 2568 _cell_measurement_temperature 296(2) _cell_measurement_theta_max 22.88 _cell_measurement_theta_min 2.74 _cell_volume 1265.4(2) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX3' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296(2) _diffrn_detector_area_resol_mean 10.42 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.990 _diffrn_measurement_device_type 'Bruker D8 QUEST PHOTON 100' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0749 _diffrn_reflns_av_unetI/netI 0.0947 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.990 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 12417 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.990 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.465 _diffrn_reflns_theta_min 2.737 _diffrn_source.source 'Ius 2.0' _diffrn_source.type microfocus _exptl_absorpt_coefficient_mu 0.161 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6969 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.749 _exptl_crystal_description plate _exptl_crystal_F_000 680 _exptl_crystal_size_max 0.120 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.010 _refine_diff_density_max 0.360 _refine_diff_density_min -0.573 _refine_diff_density_rms 0.059 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.030 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 246 _refine_ls_number_reflns 2867 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.030 _refine_ls_R_factor_all 0.1695 _refine_ls_R_factor_gt 0.0689 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0805P)^2^+0.8965P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1590 _refine_ls_wR_factor_ref 0.1960 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1434 _reflns_number_total 2867 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt02093e2.cif _cod_data_source_block YF_052_a _cod_depositor_comments 'Adding full bibliography for 7708161--7708163.cif.' _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7708162 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.981 _shelx_estimated_absorpt_t_max 0.998 _shelx_res_file ; TITL YF_052_a.res in P2(1)/c YF_052_a.res created by SHELXL-2018/3 at 15:48:11 on 24-Mar-2021 CELL 0.71073 7.8296 22.7963 7.4593 90 108.117 90 ZERR 4 0.0008 0.0025 0.0007 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O UNIT 24 28 36 32 L.S. 10 omit 0 2 0 ACTA BOND $H FMAP 2 PLAN -5 SIZE 0.12 0.1 0.01 TEMP 23 EQIV $1 x, y, z-1 HTAB C4 N5_$1 HTAB N4 O8 EQIV $2 x-1, y, z-1 HTAB N9 N6_$2 HTAB N9 O6_$2 HTAB N9 O7_$2 HTAB N9 O4A HTAB N9 O4B EQIV $3 x-1, y, z HTAB N9 O1A_$3 HTAB N9 O1B_$3 EQIV $4 x-1, -y+1/2, z-1/2 HTAB N9 O1B_$4 HTAB O8 O7_$1 EQIV $5 x+1, -y+1/2, z+1/2 HTAB O8 O4A_$5 HTAB O8 O4B_$5 WGHT 0.080500 0.896500 FVAR 0.59922 0.54682 0.59366 C1 1 0.318070 0.280992 0.001775 11.00000 0.05455 0.03934 = 0.04667 -0.00207 0.01423 0.01669 C2 1 0.138870 0.267336 -0.041651 11.00000 0.06206 0.03002 = 0.04922 -0.00929 0.01536 -0.00255 C3 1 0.052390 0.321386 -0.057449 11.00000 0.04610 0.03623 = 0.05489 -0.00989 0.00844 -0.00212 C4 1 0.169383 0.424993 -0.003411 11.00000 0.05374 0.02691 = 0.03985 0.00287 0.00634 0.00305 AFIX 23 H4A 2 0.053426 0.438577 -0.083744 11.00000 -1.20000 H4B 2 0.262061 0.445120 -0.040826 11.00000 -1.20000 AFIX 0 C5 1 0.188845 0.438943 0.197292 11.00000 0.03567 0.02023 = 0.04383 0.00146 0.01323 0.00216 C6 1 0.305179 0.447375 0.489197 11.00000 0.03561 0.02325 = 0.04657 -0.00005 0.01782 -0.00183 N1 3 0.184542 0.361721 -0.027013 11.00000 0.03785 0.02951 = 0.03596 -0.00296 0.00261 0.00305 N2 3 0.349721 0.337309 0.012520 11.00000 0.04294 0.04481 = 0.05586 -0.00469 0.01244 0.00516 N3 3 0.053536 0.455460 0.249442 11.00000 0.03574 0.04559 = 0.05583 -0.00467 0.01079 0.00609 N4 3 0.347060 0.433196 0.339235 11.00000 0.02588 0.03042 = 0.03592 -0.00160 0.01443 0.00301 AFIX 43 H4 2 0.450036 0.422698 0.331496 11.00000 -1.20000 AFIX 0 N5 3 0.388956 0.452238 0.676497 11.00000 0.05283 0.04565 = 0.03729 -0.00375 0.02128 -0.00594 N6 3 0.561947 0.439618 0.734906 11.00000 0.05627 0.03738 = 0.03806 0.00117 0.01110 -0.01011 N8 3 0.053764 0.212774 -0.061698 11.00000 0.09817 0.04025 = 0.08395 -0.01631 0.03951 -0.01117 N9 3 -0.119585 0.334807 -0.093251 11.00000 0.04110 0.05946 = 0.17176 -0.02934 0.01410 -0.00915 AFIX 93 H9A 2 -0.152235 0.370946 -0.098109 11.00000 -1.20000 H9B 2 -0.198597 0.307382 -0.111639 11.00000 -1.20000 PART 1 31.00 AFIX 0 O3A 4 0.120406 0.171219 -0.104997 31.00000 0.11436 0.03805 = 0.12895 -0.02438 0.02544 0.00851 O4A 4 -0.096738 0.208591 -0.048811 31.00000 0.08855 0.05985 = 0.15954 -0.02657 0.05573 -0.02546 PART 2 -31.00 O3B 4 0.155436 0.172183 0.025106 -31.00000 0.16855 0.03368 = 0.10626 -0.00632 0.06425 -0.00894 O4B 4 -0.115096 0.215380 -0.153718 -31.00000 0.16446 0.07031 = 0.12735 -0.03359 0.03870 -0.06930 PART 0 O5 4 0.130275 0.461761 0.447033 11.00000 0.04076 0.05371 = 0.05612 -0.00725 0.02526 0.00507 O6 4 0.651811 0.425825 0.631662 11.00000 0.04618 0.06226 = 0.04552 -0.00274 0.01027 0.00508 O7 4 0.638421 0.443154 0.909241 11.00000 0.08673 0.08889 = 0.03066 -0.00050 0.00375 -0.02669 O8 4 0.688498 0.403389 0.279714 11.00000 0.06188 0.09164 = 0.06520 0.00933 0.02155 0.01256 AFIX 3 H8A 2 0.709240 0.404844 0.174509 11.00000 -1.50000 H8B 2 0.775744 0.383821 0.350950 11.00000 -1.50000 AFIX 0 N7 3 0.470829 0.241680 0.035777 11.00000 0.07658 0.08555 = 0.11186 -0.01729 0.01015 0.04058 PART 1 21.00 O1A 4 0.584610 0.251855 -0.012736 21.00000 0.11341 0.23702 = 0.37150 0.10979 0.15861 0.09366 O2A 4 0.467392 0.199084 0.146215 21.00000 0.12169 0.08298 = 0.17611 0.05683 0.04086 0.07338 PART 2 -21.00 O1B 4 0.630080 0.266399 0.119077 -21.00000 0.10872 0.11220 = 0.14054 -0.04794 -0.03276 0.07170 O2B 4 0.467596 0.202157 -0.062326 -21.00000 0.11565 0.04112 = 0.12802 -0.02649 0.05381 0.02815 PART 0 HKLF 4 REM YF_052_a.res in P2(1)/c REM wR2 = 0.1960, GooF = S = 1.030, Restrained GooF = 1.030 for all data REM R1 = 0.0689 for 1434 Fo > 4sig(Fo) and 0.1695 for all 2867 data REM 246 parameters refined using 0 restraints END WGHT 0.0795 0.9443 REM Highest difference peak 0.360, deepest hole -0.573, 1-sigma level 0.059 Q1 1 0.5880 0.4180 0.3327 11.00000 0.05 0.36 Q2 1 0.7939 0.4500 0.3075 11.00000 0.05 0.28 Q3 1 0.5499 0.2447 0.2324 11.00000 0.05 0.26 Q4 1 -0.1920 0.3011 -0.2028 11.00000 0.05 0.23 Q5 1 0.6234 0.4220 1.1131 11.00000 0.05 0.21 ; _shelx_res_checksum 78056 _shelx_hkl_file ; 0 0 1 0.30 0.40 0 0 1 -0.50 0.50 0 0 1 -0.10 0.30 0 0 -1 0.10 0.40 0 0 2 4493.35 140.39 0 0 2 4482.05 139.89 0 0 2 4561.84 140.29 0 0 3 4.10 1.60 0 0 3 1.40 1.10 0 0 3 1.60 1.80 0 0 4 574.64 19.90 0 0 4 557.14 19.10 0 0 4 569.24 20.50 0 0 5 5.90 3.50 0 0 5 1.80 1.80 0 0 5 0.20 2.20 0 0 6 21.90 3.00 0 0 6 30.30 5.40 0 0 6 25.60 3.90 0 0 7 -1.70 6.40 0 0 7 -4.00 4.30 0 0 8 15.60 6.20 0 1 0 -0.50 0.20 0 -1 0 -0.10 0.20 0 -1 0 -0.20 0.20 0 1 -1 66.09 2.90 0 1 1 64.09 2.80 0 1 1 68.59 2.70 0 -1 1 70.19 3.00 0 -1 -1 68.39 2.70 0 -1 -1 68.19 2.90 0 1 2 1130.79 39.10 0 1 -2 1227.08 38.80 0 1 2 1237.68 38.60 0 -1 2 1219.58 39.00 0 -1 -2 1244.48 38.60 0 1 3 943.61 30.60 0 1 3 948.31 30.80 0 1 3 940.51 30.90 0 -1 3 940.21 30.90 0 -1 3 933.01 31.20 0 -1 3 923.91 29.90 0 1 4 492.15 17.30 0 1 4 487.75 17.90 0 1 4 505.25 17.60 0 -1 4 494.45 18.40 0 -1 4 499.45 17.80 0 -1 4 477.75 16.50 0 1 5 25.00 4.40 0 1 5 24.60 3.30 0 1 5 28.70 3.50 0 -1 5 22.50 2.80 0 -1 5 18.80 4.30 0 -1 5 30.50 3.70 0 1 6 36.70 5.40 0 1 6 36.70 4.60 0 1 6 48.80 5.80 0 -1 6 41.80 6.00 0 -1 6 38.40 4.90 0 1 7 9.90 3.20 0 1 7 6.20 4.50 0 1 7 7.20 3.70 0 1 7 4.30 6.30 0 -1 7 -2.20 4.10 0 -1 7 -2.40 6.50 0 1 8 6.90 6.00 0 -1 8 -0.60 5.90 0 -2 0 2.10 0.60 0 2 -1 35.20 1.60 0 2 -1 31.50 2.20 0 2 1 36.20 2.20 0 2 1 35.90 1.90 0 2 -1 35.50 1.60 0 -2 1 30.50 2.30 0 -2 1 36.00 1.60 0 -2 -1 39.10 2.30 0 -2 -1 37.20 1.90 0 2 2 4644.44 149.59 0 2 -2 4762.72 148.89 0 2 2 4693.53 148.29 0 -2 -2 4866.11 148.69 0 -2 -2 4715.43 148.29 0 -2 2 4955.80 148.99 0 2 3 490.85 17.10 0 2 3 478.95 17.30 0 2 -3 491.15 17.60 0 -2 -3 497.55 17.00 0 -2 3 512.15 17.90 0 2 4 1.60 2.10 0 2 4 6.70 2.00 0 2 4 3.40 2.40 0 -2 4 3.60 2.00 0 -2 4 4.70 2.70 0 2 5 1.50 3.00 0 2 5 3.80 2.40 0 2 5 0.50 2.00 0 -2 5 -2.50 2.40 0 -2 5 -0.60 3.50 0 2 6 -0.30 4.50 0 2 6 1.90 2.50 0 2 6 5.60 3.20 0 -2 6 6.40 3.00 0 -2 6 2.00 5.10 0 2 7 9.10 6.40 0 2 7 3.80 4.30 0 2 7 6.30 3.50 0 2 7 8.60 4.60 0 -2 7 5.00 4.30 0 -2 7 -0.60 7.30 0 2 8 4.40 6.10 0 -2 8 6.30 5.70 0 3 0 -0.20 0.60 0 3 0 0.90 0.90 0 3 0 -0.20 0.70 0 -3 0 2.40 1.00 0 -3 0 0.90 0.70 0 3 -1 1122.19 36.00 0 3 -1 1154.38 36.20 0 3 -1 1153.88 36.90 0 3 1 1134.99 36.40 0 3 1 1137.19 36.90 0 -3 -1 1169.88 36.90 0 -3 1 1125.69 36.10 0 -3 1 1127.79 36.90 0 -3 -1 1167.88 36.40 0 3 -2 2.80 1.70 0 3 2 1.10 1.30 0 3 2 0.60 1.20 0 -3 -2 3.00 1.20 0 -3 -2 3.30 1.50 0 -3 2 4.20 1.80 0 3 -3 320.47 14.30 0 3 3 357.56 12.80 0 3 3 360.36 13.30 0 -3 3 346.17 14.90 0 -3 -3 357.06 12.70 0 3 4 94.89 5.50 0 3 4 103.39 5.80 0 -3 -4 102.49 5.80 0 -3 4 101.99 7.00 0 -3 4 95.79 5.70 0 3 5 109.59 7.40 0 3 5 109.09 6.60 0 3 5 116.99 6.70 0 -3 5 105.79 6.70 0 -3 5 120.79 8.60 0 3 6 -0.50 2.60 0 3 6 -2.00 4.10 0 3 6 6.70 3.30 0 -3 6 2.40 5.10 0 -3 6 7.70 3.20 0 3 7 13.10 6.40 0 3 7 14.40 4.80 0 3 7 11.90 4.60 0 3 7 6.20 4.20 0 -3 7 13.80 4.70 0 -3 7 20.80 8.40 0 3 8 -11.00 5.90 0 3 8 1.40 4.50 0 3 8 0.20 5.50 0 -3 8 -3.10 5.50 0 4 0 1157.08 37.70 0 4 0 1154.18 37.80 0 -4 0 1186.38 37.70 0 -4 0 1187.98 37.80 0 4 1 44.60 3.80 0 4 -1 31.30 2.40 0 4 -1 29.80 2.80 0 4 1 31.70 2.50 0 4 -1 31.80 2.10 0 -4 1 30.30 3.00 0 -4 -1 34.10 2.50 0 -4 -1 29.50 2.80 0 -4 1 31.30 2.10 0 4 2 297.57 11.60 0 4 -2 300.67 10.10 0 4 -2 288.17 11.60 0 4 2 298.07 11.00 0 -4 2 304.77 10.30 0 -4 2 297.07 11.80 0 -4 -2 306.97 10.90 0 -4 -2 304.57 11.70 0 4 3 278.57 11.20 0 4 3 273.67 10.70 0 4 -3 277.67 11.50 0 -4 -3 280.77 10.50 0 -4 3 262.67 11.70 0 4 4 -2.10 1.70 0 4 4 0.30 1.80 0 4 -4 2.10 2.80 0 -4 -4 1.70 2.30 0 -4 4 0.80 2.90 0 4 5 49.99 5.70 0 4 5 46.60 5.30 0 4 5 46.20 4.80 0 -4 -5 45.40 5.10 0 -4 5 50.29 5.10 0 -4 5 56.99 6.50 0 4 6 9.10 3.50 0 4 6 8.20 3.60 0 4 6 7.30 4.40 0 -4 6 7.40 5.60 0 -4 6 9.40 3.70 0 4 7 42.40 6.60 0 4 7 43.60 7.40 0 4 7 52.09 6.30 0 4 7 47.90 6.80 0 -4 7 49.70 9.40 0 -4 7 55.29 6.10 0 4 8 -0.70 6.40 0 4 8 14.60 6.60 0 4 8 7.80 5.40 0 -4 8 -2.40 6.00 0 4 9 4.90 5.90 0 5 0 0.90 1.30 0 5 0 1.70 1.80 0 5 0 4.30 2.60 0 -5 0 -1.40 1.50 0 -5 0 1.00 1.20 0 5 -1 238.38 9.90 0 5 -1 264.87 9.30 0 5 1 239.08 10.10 0 5 -1 263.37 9.50 0 5 1 252.47 9.70 0 -5 1 236.98 9.20 0 -5 -1 251.27 9.60 0 -5 -1 247.58 10.20 0 -5 1 264.97 10.20 0 5 2 63.49 4.20 0 5 2 57.19 4.40 0 5 -2 55.79 6.00 0 5 -2 67.19 3.40 0 5 -2 71.19 3.50 0 -5 2 69.99 3.50 0 -5 -2 67.39 4.00 0 -5 2 61.69 5.00 0 5 3 130.39 6.90 0 5 -3 135.29 7.40 0 5 3 114.79 7.50 0 -5 3 129.69 5.20 0 -5 -3 136.39 6.30 0 -5 3 141.99 7.90 0 5 4 309.17 12.30 0 5 4 295.37 12.90 0 5 -4 305.87 13.20 0 -5 -4 308.57 12.20 0 -5 4 322.47 14.20 0 5 -5 20.00 4.30 0 5 5 18.80 3.80 0 5 5 20.30 3.30 0 -5 -5 17.50 3.70 0 -5 5 12.30 5.20 0 -5 5 15.80 3.40 0 5 6 5.40 3.40 0 5 6 4.90 4.30 0 5 6 0.40 3.60 0 -5 6 -2.90 5.90 0 -5 6 0.10 3.60 0 5 7 4.70 5.10 0 5 7 6.40 6.10 0 5 7 0.30 4.20 0 5 7 6.80 4.80 0 -5 7 2.80 4.60 0 -5 7 1.80 8.50 0 5 8 5.00 6.80 0 5 8 0.50 5.70 0 5 8 -1.70 6.90 0 -5 8 3.30 6.00 0 5 9 5.60 6.30 0 6 0 3463.25 115.89 0 6 0 3459.05 115.69 0 6 0 4145.08 116.49 0 -6 0 3657.03 115.89 0 6 1 11.60 2.10 0 6 -1 6.40 1.70 0 6 -1 8.00 2.30 0 6 -1 9.70 2.00 0 6 1 7.00 2.30 0 -6 -1 10.90 2.50 0 -6 1 10.60 2.60 0 -6 -1 7.70 2.20 0 6 2 634.64 21.80 0 6 -2 627.34 21.00 0 6 2 591.14 22.30 0 6 -2 617.04 22.40 0 6 -2 629.34 20.80 0 -6 2 624.74 21.10 0 -6 2 646.54 22.60 0 -6 -2 641.34 21.50 0 6 3 117.09 6.40 0 6 3 119.89 6.90 0 6 -3 112.89 7.10 0 -6 3 108.49 7.60 0 -6 3 111.99 5.00 0 6 4 3.60 2.20 0 6 4 2.50 2.10 0 6 -4 3.50 3.30 0 -6 -4 3.40 2.40 0 -6 4 7.00 3.90 0 6 -5 62.89 6.90 0 6 5 56.49 5.50 0 6 5 44.00 5.60 0 -6 -5 49.50 5.60 0 -6 5 57.59 7.30 0 6 6 12.10 4.00 0 6 6 11.20 4.50 0 6 6 11.20 4.40 0 -6 6 6.90 3.70 0 -6 6 6.80 6.30 0 6 7 23.10 5.60 0 6 7 9.00 5.50 0 6 7 20.50 6.50 0 6 7 30.30 6.10 0 -6 7 18.10 5.40 0 6 8 3.50 5.90 0 6 8 4.20 7.80 0 6 8 10.30 7.30 0 -6 8 5.30 6.10 0 7 0 4.50 2.00 0 7 0 0.70 1.50 0 7 0 2.80 2.20 0 -7 0 4.60 2.40 0 7 1 1318.37 42.90 0 7 -1 1249.38 41.90 0 7 -1 1266.77 42.40 0 7 1 1274.87 42.10 0 7 -1 1281.77 41.70 0 -7 -1 1271.17 41.90 0 7 -2 369.36 13.80 0 7 2 371.46 15.30 0 7 -2 400.76 15.40 0 7 -2 393.76 13.70 0 -7 2 420.76 15.70 0 -7 -2 375.56 14.40 0 -7 2 354.96 13.70 0 7 3 215.08 9.70 0 7 -3 209.48 10.40 0 7 3 223.58 10.60 0 7 -3 225.68 8.00 0 7 -3 205.98 8.60 0 -7 3 216.68 8.60 0 -7 3 230.88 11.10 0 -7 -3 217.68 9.40 0 7 4 533.15 21.50 0 7 -4 542.55 21.60 0 7 4 586.44 20.60 0 -7 4 556.44 22.30 0 -7 4 557.44 18.80 0 -7 -4 566.44 20.20 0 7 -5 14.40 4.70 0 7 5 12.70 4.10 0 7 5 20.90 3.70 0 -7 5 27.40 6.00 0 -7 -5 13.20 3.60 0 7 6 14.80 5.10 0 7 6 8.20 4.10 0 -7 6 -0.70 7.20 0 -7 6 15.40 4.30 0 -7 -6 5.40 4.20 0 7 7 7.70 6.00 0 7 7 5.80 5.20 0 7 7 14.70 6.70 0 7 7 9.70 6.20 0 -7 7 15.20 5.40 0 7 8 -5.50 6.20 0 7 8 -7.90 7.50 0 7 8 -2.10 7.90 0 -7 8 4.50 6.60 0 8 0 9999.00 308.77 0 8 0 9804.82 308.27 0 8 0 9832.32 308.57 0 -8 0 9991.10 308.57 0 8 1 276.17 11.40 0 8 1 265.87 11.90 0 8 -1 254.67 11.50 0 8 -1 276.07 11.70 0 -8 1 267.67 11.90 0 -8 -1 248.78 11.20 0 8 -2 27.20 3.80 0 8 -2 46.00 3.90 0 8 2 45.70 4.70 0 8 2 36.60 4.60 0 8 -2 38.40 3.70 0 -8 -2 45.00 4.30 0 -8 2 42.60 3.70 0 -8 2 47.50 5.40 0 8 3 15.80 3.60 0 8 -3 10.50 3.30 0 8 -3 14.90 2.30 0 8 -3 14.80 2.60 0 8 3 16.80 3.10 0 -8 -3 17.30 2.90 0 -8 3 15.80 2.40 0 -8 3 21.00 4.40 0 8 4 5.80 2.80 0 8 -4 6.10 3.50 0 8 4 5.70 2.90 0 -8 -4 5.70 2.80 0 -8 4 2.90 4.40 0 8 5 8.50 3.50 0 8 -5 5.00 4.30 0 8 5 8.70 3.60 0 -8 5 3.60 5.90 0 -8 -5 3.00 3.20 0 8 6 0.30 4.10 0 8 -6 -5.90 5.30 0 8 6 5.10 5.30 0 -8 6 2.10 7.40 0 -8 -6 -2.10 4.50 0 8 7 4.30 6.20 0 8 7 -4.10 5.30 0 8 7 -0.70 6.00 0 -8 7 -7.80 5.30 0 8 8 -0.80 8.50 0 8 8 3.00 6.60 0 -8 8 -5.60 6.90 0 9 0 1.50 2.00 0 9 0 -0.30 2.00 0 9 0 1.00 2.20 0 -9 0 1.70 2.90 0 9 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74.49 6.60 0 10 -2 74.59 5.30 0 10 2 69.79 5.80 0 10 -2 68.29 5.40 0 10 -2 69.29 6.40 0 -10 2 66.29 7.50 0 -10 -2 75.59 6.10 0 10 -3 174.78 10.50 0 10 3 169.78 10.30 0 10 -3 175.78 8.00 0 10 3 181.58 9.20 0 10 -3 175.18 8.40 0 -10 -3 170.68 9.00 0 -10 3 161.48 10.70 0 10 -4 81.89 8.60 0 10 4 79.59 6.70 0 10 4 81.89 8.10 0 -10 -4 85.59 6.60 0 -10 4 80.19 9.00 0 10 -5 47.60 6.90 0 10 5 32.10 5.60 0 10 5 27.90 6.10 0 10 5 25.40 4.90 0 -10 5 24.10 7.00 0 -10 -5 34.90 5.10 0 10 -6 4.20 6.20 0 10 6 0.00 5.90 0 10 6 10.50 4.90 0 -10 -6 -7.00 5.00 0 10 7 41.50 7.70 0 10 7 43.80 7.40 0 10 7 30.90 8.00 0 -10 7 33.50 6.90 0 10 8 -7.80 7.30 0 -10 8 8.70 7.50 0 11 0 6.70 2.70 0 11 0 7.00 2.90 0 11 0 8.30 6.30 0 -11 0 8.10 3.70 0 11 1 2.70 3.20 0 11 1 5.00 4.30 0 11 -1 4.10 2.90 0 11 1 1.30 2.70 0 11 -1 8.80 3.00 0 -11 1 6.50 4.20 0 -11 -1 5.50 3.50 0 11 2 20.30 4.20 0 11 2 32.10 4.60 0 11 -2 25.00 4.50 0 11 -2 28.60 3.90 0 11 -2 28.40 3.80 0 11 2 43.50 8.50 0 -11 -2 27.70 4.60 0 -11 2 25.70 5.90 0 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6.30 2.50 0 12 3 14.60 3.70 0 12 3 12.80 4.70 0 -12 3 19.20 5.50 0 -12 -3 5.50 4.00 0 12 -4 21.30 3.30 0 12 4 20.00 5.80 0 12 -4 16.30 3.10 0 12 -4 24.90 5.50 0 12 4 14.80 5.30 0 12 4 29.80 4.90 0 -12 4 14.30 6.50 0 -12 -4 17.20 4.80 0 12 5 76.69 9.90 0 12 -5 66.69 8.50 0 12 5 55.39 6.80 0 12 5 57.79 8.60 0 -12 -5 55.39 6.60 0 12 6 11.20 5.80 0 12 -6 4.30 7.00 0 12 6 15.50 6.70 0 -12 -6 4.90 6.40 0 12 7 21.90 7.40 0 12 7 3.60 7.50 0 12 8 -2.90 8.00 0 -12 8 21.90 8.50 0 13 0 5.70 3.00 0 13 0 3.00 3.10 0 13 0 -0.40 3.10 0 -13 0 0.90 4.50 0 13 -1 673.83 25.70 0 13 -1 649.93 25.80 0 13 1 778.92 28.10 0 13 -1 640.04 26.20 0 13 1 646.94 26.10 0 13 1 794.62 29.00 0 -13 -1 666.73 26.10 0 -13 1 656.23 26.90 0 13 2 15.90 4.20 0 13 -2 9.90 3.60 0 13 2 11.50 7.50 0 13 2 23.60 7.10 0 13 -2 9.90 3.70 0 13 -2 7.70 3.80 0 -13 -2 11.80 4.10 0 -13 2 7.70 5.10 0 13 -3 305.77 13.60 0 13 3 310.57 16.10 0 13 3 298.87 15.70 0 13 3 313.07 14.40 0 13 -3 316.57 15.80 0 13 -3 293.27 12.80 0 -13 -3 299.57 14.00 0 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14 -4 9.20 4.00 0 14 4 7.00 6.10 0 -14 -4 -8.10 4.80 0 14 -5 2.90 7.40 0 14 5 9.00 6.30 0 14 5 -1.30 5.40 0 14 5 -3.80 5.60 0 -14 -5 9.70 5.70 0 14 6 47.50 8.20 0 14 -6 42.90 9.50 0 14 6 35.80 8.40 0 14 6 29.30 8.30 0 -14 -6 24.50 7.20 0 14 7 6.00 8.40 0 14 -7 27.60 10.50 0 14 7 18.90 8.50 0 14 8 -11.90 8.50 0 -14 8 11.80 9.40 0 15 0 6.50 3.70 0 15 0 4.40 4.20 0 15 0 6.80 4.80 0 -15 0 -4.30 4.40 0 15 1 50.09 9.90 0 15 -1 36.20 5.30 0 15 -1 37.60 6.30 0 15 1 27.00 5.80 0 15 -1 22.60 5.60 0 15 1 20.60 4.70 0 -15 1 36.00 7.20 0 -15 -1 40.10 6.60 0 15 2 16.60 5.00 0 15 2 4.70 5.30 0 15 -2 10.10 4.90 0 15 -2 13.40 4.50 0 15 -2 8.00 4.00 0 15 2 9.70 4.50 0 -15 -2 15.50 5.50 0 -15 2 14.90 6.10 0 15 -3 17.60 5.00 0 15 -3 7.80 5.40 0 15 3 16.40 5.10 0 15 3 24.30 7.00 0 15 3 23.10 6.10 0 -15 -3 22.80 5.50 0 15 -4 32.60 5.50 0 15 -4 38.40 7.00 0 15 4 53.29 8.80 0 15 4 42.20 6.40 0 15 4 46.30 8.70 0 -15 -4 32.70 6.60 0 15 5 -0.60 7.00 0 15 -5 8.00 7.90 0 15 5 3.30 8.10 0 15 5 9.70 5.70 0 -15 -5 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17.80 7.50 2 -4 5 19.50 4.50 2 4 6 -2.90 3.70 2 4 6 0.30 5.20 2 4 6 -0.10 3.80 2 -4 6 2.90 5.00 2 4 7 12.50 4.70 2 4 7 3.00 4.70 2 4 7 -4.90 6.90 2 -4 7 2.60 6.40 2 4 8 11.50 9.20 2 -4 8 13.50 8.70 -2 5 9 -10.20 6.70 -2 5 8 5.90 5.70 -2 -5 8 4.80 4.40 -2 -5 8 -0.10 4.30 -2 5 7 -2.20 2.80 -2 5 7 2.50 3.30 -2 -5 7 5.80 6.00 -2 -5 7 -1.60 3.40 -2 -5 7 5.20 3.60 -2 5 6 284.37 13.90 2 5 -6 266.77 12.30 -2 5 6 283.27 10.30 -2 5 6 270.17 10.40 -2 -5 6 274.87 13.20 -2 -5 6 275.57 13.70 -2 5 5 24.10 2.80 2 5 -5 29.00 4.50 -2 5 5 27.30 4.60 2 5 -5 31.00 3.60 -2 5 5 26.40 2.60 -2 -5 5 24.40 3.60 -2 -5 5 27.40 4.60 2 -5 -5 21.40 4.60 -2 5 4 2.80 1.30 -2 5 4 -0.10 2.00 2 5 -4 4.70 2.40 2 5 -4 1.30 3.50 -2 -5 4 -1.10 4.70 -2 -5 4 2.90 1.90 2 -5 -4 -5.60 2.30 2 -5 -4 1.70 1.00 2 5 -3 315.57 12.70 2 5 -3 320.57 12.40 -2 5 3 311.57 10.80 -2 5 3 281.27 13.00 -2 -5 3 316.67 12.60 2 -5 -3 307.27 13.40 -2 -5 3 312.37 12.40 2 -5 -3 323.77 10.70 -2 5 2 24.30 2.50 2 5 -2 19.70 3.10 2 5 -2 31.60 3.80 2 -5 -2 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28.50 4.50 -4 -3 -2 28.30 5.40 4 3 3 12.00 4.30 -4 3 -3 12.60 3.30 4 3 3 8.90 4.30 4 -3 3 5.20 3.80 4 -3 3 7.10 2.90 -4 -3 -3 2.90 4.70 4 3 4 13.90 3.90 4 3 4 5.40 5.10 4 -3 4 5.20 3.00 4 -3 4 5.60 4.70 4 3 5 12.80 4.20 4 3 5 16.50 6.30 4 -3 5 16.20 5.70 4 3 6 12.20 5.70 4 3 6 8.50 5.10 4 3 6 6.20 8.50 4 -3 6 23.00 8.40 4 3 7 13.00 11.30 4 -3 7 5.30 10.90 -4 4 9 2.90 7.10 -4 -4 9 8.70 7.20 -4 4 8 9.30 7.30 -4 -4 8 5.30 5.70 -4 -4 7 -1.50 2.40 -4 -4 7 3.60 2.10 -4 4 6 15.60 5.70 4 4 -6 11.20 3.40 -4 -4 6 12.60 4.00 -4 -4 6 7.40 2.70 4 4 -5 36.40 4.60 4 4 -5 29.00 4.90 -4 4 5 41.50 6.50 -4 -4 5 25.40 5.00 -4 -4 5 33.50 3.60 4 -4 -5 29.70 6.10 4 4 -4 5.00 3.60 -4 4 4 3.50 3.90 -4 -4 4 2.80 2.30 4 -4 -4 0.60 4.00 -4 -4 4 5.40 3.50 4 4 -3 89.29 6.80 4 4 -3 94.39 7.30 -4 4 3 93.99 8.30 4 -4 -3 99.59 5.20 4 -4 -3 103.19 5.90 -4 -4 3 107.99 8.10 -4 -4 3 109.79 6.10 4 -4 -3 109.79 8.40 4 4 -2 22.50 3.90 -4 4 2 28.20 6.50 4 4 -2 25.40 4.70 4 -4 -2 17.30 2.90 -4 -4 2 22.40 4.50 -4 -4 2 16.90 3.00 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6 5 1.40 5.00 4 6 5 1.60 6.30 4 -6 5 1.70 6.40 4 6 6 12.20 6.80 4 6 6 -10.50 8.40 4 6 6 8.10 6.90 4 -6 6 -10.30 7.70 4 6 7 7.30 12.60 4 6 7 -0.90 7.10 4 -6 7 24.40 11.80 -4 7 9 6.70 9.10 -4 -7 9 10.50 7.60 -4 7 8 34.10 9.60 -4 -7 8 30.60 7.80 4 7 -7 15.40 5.30 -4 -7 7 12.90 5.10 -4 7 6 1.70 5.60 4 7 -6 -2.80 4.70 -4 -7 6 -2.80 4.30 -4 -7 6 5.50 4.20 4 7 -5 5.90 4.50 -4 7 5 1.10 4.90 4 -7 -5 18.10 5.30 -4 -7 5 13.90 4.20 -4 -7 5 13.30 4.40 4 7 -4 48.00 5.80 -4 7 4 38.20 5.60 4 7 -4 52.09 6.90 4 -7 -4 49.99 4.50 4 -7 -4 44.50 3.40 -4 -7 4 53.89 6.70 -4 -7 4 48.30 5.40 4 -7 -4 50.89 7.10 4 7 -3 4.40 3.70 4 7 -3 5.30 3.50 -4 7 3 8.30 4.00 4 -7 -3 8.90 3.30 -4 -7 3 16.50 7.30 4 -7 -3 9.80 3.10 -4 -7 3 3.60 3.20 4 -7 -3 8.00 4.50 -4 7 2 95.99 6.10 -4 7 2 107.39 11.10 4 7 -2 112.99 7.90 4 -7 -2 107.19 6.10 4 -7 -2 100.29 7.30 -4 -7 2 99.39 8.50 4 -7 -2 98.69 8.50 -4 -7 2 95.99 7.20 4 7 -1 -0.80 3.30 -4 7 1 7.90 3.90 -4 7 1 6.20 2.60 4 7 -1 3.00 3.50 4 -7 -1 5.60 3.50 4 -7 -1 -0.40 2.20 -4 -7 1 5.60 3.50 4 -7 -1 -0.90 3.00 -4 -7 1 2.60 4.00 4 7 0 267.67 13.30 4 7 0 291.67 13.80 -4 -7 0 280.67 13.20 4 -7 0 279.77 12.70 4 -7 0 292.57 13.50 4 -7 0 275.27 13.90 4 7 1 4.10 3.70 -4 7 -1 6.30 3.10 4 7 1 4.80 3.60 4 -7 1 9.20 4.50 -4 -7 -1 -1.40 3.20 4 -7 1 3.50 2.80 4 -7 1 2.70 3.00 -4 -7 -1 9.40 4.60 4 7 2 33.30 5.10 4 7 2 40.90 6.00 -4 7 -2 37.80 6.20 4 -7 2 44.90 5.80 4 -7 2 41.80 8.20 -4 -7 -2 49.90 6.60 4 -7 2 36.20 5.20 -4 -7 -2 41.20 6.40 -4 7 -3 178.08 8.80 4 7 3 192.28 11.60 4 7 3 187.38 11.60 4 -7 3 174.28 11.80 -4 -7 -3 169.68 12.20 4 -7 3 173.58 9.40 4 7 4 110.09 11.30 4 7 4 112.89 11.60 4 -7 4 110.19 7.40 4 -7 4 114.39 12.10 4 7 5 32.90 8.40 4 7 5 24.30 6.40 4 -7 5 21.20 6.70 4 7 6 -11.10 8.90 4 7 6 11.50 7.60 4 -7 6 7.80 8.20 -4 8 9 2.00 8.90 -4 -8 9 4.90 7.50 -4 8 8 28.40 12.00 -4 -8 8 9.50 7.10 -4 8 7 2.40 11.00 4 8 -7 5.40 9.00 -4 -8 7 1.40 5.40 -4 -8 7 0.60 5.70 4 8 -6 36.40 6.20 -4 8 6 44.80 8.50 -4 -8 6 66.79 8.00 -4 8 5 12.30 5.00 4 8 -5 7.40 4.50 -4 -8 5 2.10 4.20 4 -8 -5 9.10 5.60 -4 -8 5 6.30 4.60 -4 8 4 93.49 9.50 4 8 -4 101.29 8.50 4 8 -4 115.39 8.80 -4 -8 4 105.09 8.80 4 -8 -4 107.59 6.40 -4 -8 4 104.39 7.90 4 -8 -4 106.19 5.40 4 -8 -4 107.89 9.60 4 8 -3 61.89 7.10 -4 8 3 60.79 7.40 4 8 -3 62.69 7.20 -4 8 3 50.59 4.80 4 -8 -3 55.59 6.00 -4 -8 3 54.39 7.00 -4 -8 3 51.69 6.30 4 -8 -3 58.59 8.10 -4 8 2 261.97 11.10 4 8 -2 266.27 13.20 -4 8 2 242.48 13.70 4 8 -2 254.37 13.00 -4 -8 2 238.58 11.70 -4 -8 2 241.68 13.30 4 -8 -2 252.67 13.50 4 -8 -2 262.77 12.20 4 8 -1 47.30 6.00 -4 8 1 42.80 5.10 -4 8 1 60.69 7.10 4 8 -1 32.50 4.90 -4 -8 1 39.70 5.20 -4 -8 1 49.99 7.00 4 -8 -1 38.90 5.40 4 -8 -1 42.60 5.70 -4 8 0 402.66 16.80 4 8 0 376.96 17.10 4 8 0 407.56 17.80 4 -8 0 396.36 17.90 -4 -8 0 400.56 17.10 -4 -8 0 420.66 18.60 4 -8 0 407.36 17.50 4 8 1 4.10 3.70 -4 8 -1 3.00 3.80 4 8 1 6.30 4.00 -4 8 -1 5.00 3.60 -4 -8 -1 4.40 4.40 4 -8 1 1.70 3.30 -4 -8 -1 2.70 4.60 4 -8 1 4.00 3.30 4 -8 1 8.10 5.10 4 8 2 40.20 6.40 4 8 2 33.00 5.70 4 -8 2 37.10 5.30 4 -8 2 44.40 5.90 -4 -8 -2 36.10 6.20 -4 8 -3 6.30 3.40 4 8 3 14.90 5.40 4 8 3 9.80 4.90 4 -8 3 0.50 4.90 4 -8 3 10.70 3.60 -4 -8 -3 6.50 5.90 4 8 4 -2.40 6.20 4 8 4 7.00 5.80 4 -8 4 9.80 6.30 4 -8 4 9.60 3.60 4 8 5 39.40 7.10 4 8 5 24.30 8.10 4 -8 5 44.40 8.80 4 8 6 -0.70 7.20 4 8 6 6.20 9.70 4 -8 6 -2.80 9.00 -4 9 9 -13.80 9.50 -4 -9 9 6.80 7.80 -4 9 8 13.80 9.00 -4 -9 8 13.00 7.50 4 9 -7 -11.40 6.50 -4 9 7 14.70 8.90 -4 -9 7 1.50 5.50 -4 -9 7 0.60 8.20 4 9 -6 15.10 6.30 -4 9 6 14.30 7.20 -4 -9 6 23.90 6.10 -4 -9 6 14.30 5.70 4 9 -5 11.50 5.20 -4 9 5 22.90 6.90 -4 -9 5 -2.80 4.50 -4 -9 5 3.70 4.60 4 -9 -5 -2.20 5.50 -4 9 4 98.49 9.90 -4 9 4 92.99 6.00 4 9 -4 100.89 8.80 4 9 -4 82.29 8.40 -4 -9 4 93.59 8.90 -4 -9 4 84.89 8.10 4 -9 -4 83.19 9.40 4 -9 -4 89.29 6.70 -4 9 3 102.89 10.30 4 9 -3 72.29 8.00 -4 9 3 76.49 5.70 4 9 -3 73.19 7.60 -4 -9 3 71.39 8.40 -4 -9 3 77.89 7.40 4 -9 -3 87.89 8.50 4 -9 -3 79.79 7.00 -4 9 2 125.19 7.50 4 9 -2 139.39 9.80 -4 9 2 169.28 11.70 4 9 -2 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4.90 4 -11 -3 -7.90 4.60 4 11 -2 34.20 5.60 -4 11 2 49.70 5.40 4 11 -2 43.00 6.70 -4 11 2 59.19 8.20 -4 -11 2 50.09 6.30 -4 -11 2 87.79 11.50 4 -11 -2 51.29 6.50 4 11 -1 17.20 4.50 -4 11 1 19.20 4.40 4 11 -1 17.90 5.50 -4 11 1 19.80 5.30 -4 -11 1 14.10 4.70 -4 -11 1 20.20 5.50 4 -11 -1 18.30 5.30 4 -11 -1 12.60 4.50 4 11 0 2.80 4.70 -4 11 0 4.10 3.60 -4 11 0 1.50 3.90 4 -11 0 2.50 3.40 4 -11 0 -4.30 5.70 -4 -11 0 8.60 9.50 -4 -11 0 8.60 5.00 -4 11 -1 60.69 7.40 4 11 1 68.89 8.30 4 11 1 61.49 7.90 -4 11 -1 58.09 7.80 -4 -11 -1 70.49 9.40 4 -11 1 68.19 7.40 -4 11 -2 8.20 5.30 4 11 2 5.90 5.40 4 11 2 -4.00 4.80 -4 11 -2 2.80 4.50 4 -11 2 10.50 4.80 -4 -11 -2 6.30 6.10 4 11 3 12.10 5.70 4 11 3 1.50 6.10 -4 11 -3 7.60 3.90 4 -11 3 5.90 4.30 4 11 4 1.90 6.50 4 11 4 3.40 6.10 4 -11 4 6.60 4.40 4 -11 4 -11.10 6.20 4 11 5 3.40 8.60 4 11 5 2.70 8.40 4 -11 5 11.80 7.80 4 11 6 12.00 9.30 4 11 6 -10.60 12.30 4 -11 6 -0.30 9.90 -4 12 8 22.50 10.20 -4 -12 8 12.10 8.40 -4 12 7 14.90 10.70 4 12 -7 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6.00 5.70 -4 12 -2 -4.80 4.80 4 12 2 3.60 5.20 -4 12 -2 0.40 5.20 4 -12 2 -3.10 5.20 -4 -12 -2 3.00 5.80 4 12 3 22.30 7.30 -4 12 -3 19.10 4.60 4 12 3 20.00 6.40 4 -12 3 14.10 4.80 4 12 4 6.50 6.40 4 12 4 9.40 8.10 4 -12 4 11.00 6.60 4 -12 4 2.00 4.20 4 12 5 6.30 9.00 4 12 5 15.70 10.30 4 -12 5 6.20 8.00 4 12 6 5.80 9.00 4 12 6 17.80 12.70 4 -12 6 13.50 10.50 -4 13 8 8.40 11.20 -4 -13 8 18.00 8.60 4 13 -7 24.70 10.10 -4 13 7 36.90 11.30 -4 -13 7 24.10 8.30 4 13 -6 -1.30 7.70 -4 13 6 -0.40 2.90 -4 -13 6 14.90 9.10 -4 -13 6 -1.90 5.80 -4 13 5 9.60 3.70 -4 13 5 3.70 7.30 4 13 -5 11.20 7.30 -4 -13 5 11.60 8.20 4 -13 -5 7.30 5.30 -4 -13 5 6.40 7.60 -4 13 4 50.89 8.50 -4 13 4 64.09 6.60 4 13 -4 73.99 9.20 4 -13 -4 73.29 9.00 4 -13 -4 70.89 10.50 -4 -13 4 71.99 9.70 -4 -13 4 62.49 8.00 4 13 -3 8.70 4.50 4 13 -3 12.90 6.70 -4 13 3 5.40 3.70 -4 13 3 0.30 5.20 4 -13 -3 -2.60 5.40 -4 -13 3 -6.10 5.50 -4 -13 3 8.00 5.50 4 -13 -3 28.50 10.80 -4 13 2 26.90 6.90 -4 13 2 27.10 5.00 4 13 -2 30.10 5.80 4 13 -2 29.10 6.00 -4 -13 2 30.60 6.40 -4 -13 2 38.00 6.70 4 -13 -2 31.40 6.90 4 -13 -2 34.20 6.40 -4 13 1 96.09 8.50 4 13 -1 98.29 9.20 -4 13 1 109.99 10.60 4 13 -1 108.39 10.80 -4 -13 1 104.99 9.30 4 -13 -1 98.69 10.20 -4 -13 1 104.59 10.70 4 -13 -1 90.69 9.60 -4 13 0 10.70 4.40 4 13 0 4.70 4.80 -4 13 0 -3.60 4.30 4 13 0 5.90 4.80 4 -13 0 14.60 4.90 4 -13 0 3.30 6.30 -4 -13 0 5.40 8.80 -4 13 -1 70.59 8.10 4 13 1 61.19 8.20 -4 13 -1 67.89 8.00 -4 -13 -1 56.09 9.60 4 -13 1 69.69 8.80 4 13 2 24.40 7.60 -4 13 -2 11.40 5.70 -4 13 -2 8.70 6.00 4 13 2 20.20 6.30 -4 -13 -2 3.30 6.70 4 -13 2 7.70 6.00 -4 13 -3 160.48 10.30 4 13 3 157.98 14.20 4 -13 3 179.08 11.30 4 13 4 14.50 8.00 4 13 4 11.00 8.20 4 -13 4 18.20 5.00 4 -13 4 21.50 7.90 4 13 5 14.20 9.50 4 13 5 12.10 10.30 4 -13 5 3.00 8.70 4 13 6 -10.20 8.40 4 13 6 -14.70 12.70 4 -13 6 -13.10 11.00 -4 14 8 18.40 12.30 -4 -14 8 17.60 8.80 -4 14 7 3.90 10.60 4 14 -7 2.70 10.70 -4 -14 7 1.50 7.50 -4 14 6 2.60 9.10 4 14 -6 -3.80 8.30 -4 -14 6 -4.90 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14 -4 3.20 7.90 4 14 4 25.30 9.50 4 14 4 9.00 7.10 4 -14 4 10.80 5.40 4 -14 4 22.00 7.60 4 14 5 4.50 10.50 4 14 5 5.50 10.70 4 -14 5 15.90 9.90 4 14 6 -17.70 9.60 4 14 6 12.10 13.50 4 -14 6 14.40 11.50 -4 15 8 5.20 12.40 -4 -15 8 9.80 8.20 -4 15 7 19.50 11.40 4 15 -7 11.50 12.00 -4 -15 7 10.40 8.60 4 15 -6 -5.00 9.20 -4 15 6 3.10 4.60 -4 -15 6 -3.20 7.00 -4 15 5 -7.30 7.20 -4 15 5 7.60 4.30 4 15 -5 1.60 8.10 4 -15 -5 3.40 6.10 -4 15 4 -2.50 7.80 -4 15 4 7.20 4.40 4 15 -4 -5.50 6.70 4 -15 -4 3.90 6.60 4 -15 -4 -2.00 7.20 -4 -15 4 -5.40 6.40 -4 15 3 8.90 4.40 -4 15 3 1.40 7.50 4 15 -3 11.50 7.30 -4 -15 3 0.00 5.90 4 -15 -3 14.00 6.90 4 -15 -3 -0.70 6.70 -4 15 2 -6.00 6.00 4 15 -2 -4.40 6.00 4 15 -2 2.80 4.80 -4 15 2 3.60 4.40 4 -15 -2 3.80 6.70 -4 -15 2 0.90 6.40 4 -15 -2 -2.40 6.40 4 15 -1 -2.10 5.20 -4 15 1 -7.50 4.30 4 15 -1 8.10 6.10 -4 15 1 4.90 5.60 4 -15 -1 7.00 7.60 4 -15 -1 0.40 6.30 -4 -15 1 2.60 6.80 4 15 0 52.59 8.30 -4 15 0 54.39 7.80 4 15 0 55.09 8.30 -4 -15 0 40.30 7.90 4 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5 -4 -3 17.20 5.10 -5 -4 3 14.10 3.00 -5 4 2 130.09 10.30 5 4 -2 134.39 10.00 5 4 -2 150.98 9.40 5 -4 -2 151.48 7.90 -5 -4 2 137.99 8.20 5 -4 -2 137.19 8.40 -5 -4 2 138.59 10.20 -5 4 1 254.87 13.90 5 4 -1 266.77 13.80 5 4 -1 263.27 12.70 5 -4 -1 257.57 12.80 -5 -4 1 260.97 12.20 5 -4 -1 266.67 13.70 5 -4 -1 262.17 12.00 -5 -4 1 264.37 14.80 5 4 0 47.90 7.10 5 4 0 37.00 5.20 5 -4 0 35.80 5.40 5 -4 0 37.60 4.80 5 -4 0 25.80 5.00 -5 -4 0 34.60 5.40 -5 -4 0 40.60 6.70 5 4 1 6.40 3.90 5 4 1 4.70 3.80 -5 4 -1 -0.80 3.00 5 -4 1 1.60 3.60 5 -4 1 -0.20 3.60 -5 -4 -1 6.00 4.90 5 -4 1 2.80 4.80 -5 -4 -1 4.80 5.00 -5 4 -2 115.99 9.30 5 4 2 108.19 9.30 5 4 2 127.89 9.60 -5 -4 -2 124.09 10.30 5 -4 2 133.09 9.80 5 -4 2 125.09 9.80 5 4 3 14.20 5.70 -5 4 -3 20.50 5.20 5 4 3 10.50 5.70 5 -4 3 12.20 4.30 5 -4 3 18.50 5.70 5 4 4 44.30 6.40 5 4 4 38.30 8.60 5 -4 4 41.50 5.40 5 -4 4 43.60 8.00 5 4 5 13.80 8.10 5 4 5 -3.10 6.10 5 -4 5 -10.50 4.40 5 -4 5 -2.30 7.60 5 4 6 23.10 7.90 5 4 6 10.10 10.90 5 -4 6 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1 33.10 5.40 5 -5 1 29.70 4.80 5 -5 1 30.60 7.50 5 -5 1 27.90 5.30 5 5 2 23.40 5.10 5 5 2 18.70 5.00 5 -5 2 22.40 5.00 5 -5 2 25.50 5.50 -5 -5 -2 24.00 6.50 -5 5 -3 11.30 5.20 5 5 3 3.00 5.00 5 5 3 17.30 5.60 -5 -5 -3 3.50 7.10 5 -5 3 3.30 4.10 5 5 4 20.60 7.60 5 5 4 14.20 5.60 5 -5 4 -3.10 5.80 5 -5 4 7.80 4.40 5 5 5 0.30 6.40 5 5 5 6.70 7.90 5 -5 5 2.00 8.10 5 -5 5 1.60 4.60 5 5 6 3.20 10.70 5 5 6 -1.60 7.70 5 -5 6 -1.00 9.70 -5 6 9 -6.20 9.50 -5 -6 9 -4.70 8.70 -5 6 8 14.50 9.90 -5 -6 8 7.30 7.40 5 6 -7 -6.80 6.50 -5 -6 7 10.40 6.90 5 6 -6 1.20 5.00 -5 6 6 -5.00 6.70 -5 -6 6 8.20 8.30 -5 -6 6 5.80 3.60 -5 6 5 11.10 6.40 5 6 -5 -4.10 4.20 5 -6 -5 5.90 5.90 -5 -6 5 3.80 3.60 -5 -6 5 0.80 4.70 5 6 -4 1.10 4.20 -5 6 4 -3.40 4.20 5 6 -4 9.90 4.30 -5 -6 4 7.10 3.40 5 -6 -4 12.10 5.60 5 -6 -4 1.50 2.50 5 -6 -4 -1.90 3.30 -5 -6 4 3.90 4.50 5 6 -3 25.20 4.70 5 6 -3 47.30 10.30 -5 6 3 39.50 7.20 5 -6 -3 22.10 5.40 5 -6 -3 23.10 3.50 -5 -6 3 26.20 5.80 5 -6 -3 28.10 4.60 -5 -6 3 26.20 4.10 5 6 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8.90 5 7 -7 11.60 5.50 -5 -7 7 8.90 6.70 -5 7 6 41.30 8.40 5 7 -6 58.49 7.40 -5 -7 6 35.90 9.70 -5 -7 6 52.99 5.60 -5 7 5 109.79 11.80 5 7 -5 83.09 9.00 5 -7 -5 75.49 10.10 -5 -7 5 88.49 7.50 -5 -7 5 85.09 10.20 5 7 -4 15.10 4.80 5 7 -4 25.30 5.80 -5 7 4 14.80 5.20 -5 -7 4 11.70 4.90 5 -7 -4 23.60 3.50 -5 -7 4 26.50 4.30 5 -7 -4 30.30 7.20 5 -7 -4 18.00 4.10 5 7 -3 71.89 7.80 -5 7 3 66.59 8.30 5 7 -3 64.89 8.60 -5 -7 3 64.89 8.60 -5 -7 3 61.49 7.00 5 -7 -3 66.99 7.10 5 -7 -3 107.89 13.50 5 -7 -3 71.49 5.40 5 7 -2 107.89 8.60 5 7 -2 87.39 8.80 -5 7 2 96.39 10.00 5 -7 -2 99.69 8.50 -5 -7 2 101.69 9.70 5 -7 -2 93.29 8.90 5 -7 -2 88.89 6.50 -5 -7 2 102.59 7.70 5 7 -1 16.10 8.70 -5 7 1 8.00 5.20 5 7 -1 4.90 4.40 5 -7 -1 8.30 4.60 -5 -7 1 18.60 9.50 5 -7 -1 9.20 4.70 5 -7 -1 5.80 3.40 -5 -7 1 11.10 3.90 -5 7 0 1.90 3.60 5 7 0 18.30 4.50 5 7 0 12.00 4.40 -5 -7 0 19.50 5.80 -5 -7 0 8.00 4.70 5 -7 0 12.00 5.20 5 -7 0 10.80 3.90 5 -7 0 17.00 5.00 -5 7 -1 19.40 5.10 5 7 1 20.60 5.70 5 7 1 19.50 5.20 5 -7 1 24.00 5.30 5 -7 1 25.60 5.20 -5 -7 -1 14.90 5.50 -5 7 -2 18.80 4.80 5 7 2 11.00 5.30 5 7 2 12.80 5.70 -5 -7 -2 5.10 6.00 5 -7 2 17.90 6.20 5 -7 2 17.00 4.90 5 7 3 0.10 9.70 -5 7 -3 7.90 4.90 5 7 3 -4.80 5.20 5 -7 3 8.80 4.30 -5 -7 -3 1.40 8.00 5 7 4 2.30 6.80 5 7 4 15.00 6.40 5 -7 4 9.10 6.60 5 -7 4 9.70 4.60 5 7 5 5.80 9.30 5 -7 5 12.60 8.80 5 -7 5 18.00 4.80 5 7 6 12.90 11.50 5 7 6 -8.40 7.80 5 -7 6 -0.70 10.70 -5 8 9 5.10 10.10 -5 -8 9 1.10 8.00 -5 8 8 -8.40 10.50 -5 -8 8 7.70 8.60 -5 8 7 4.30 8.10 5 8 -7 -3.00 5.70 -5 -8 7 1.00 6.40 5 8 -6 45.40 7.10 -5 8 6 49.20 10.00 -5 -8 6 60.89 13.20 -5 -8 6 45.20 5.90 5 8 -5 -2.90 5.20 -5 8 5 -1.40 4.90 -5 -8 5 1.90 4.70 -5 -8 5 -0.20 4.10 5 -8 -5 9.90 6.30 5 8 -4 94.09 9.60 -5 8 4 99.69 10.30 5 8 -4 85.19 9.60 -5 -8 4 79.99 7.70 -5 -8 4 90.59 10.10 5 -8 -4 88.29 10.40 5 8 -3 32.40 6.00 5 8 -3 17.90 5.00 -5 8 3 38.60 6.90 5 -8 -3 29.30 4.00 -5 -8 3 34.40 4.90 5 -8 -3 33.20 5.20 5 -8 -3 30.20 5.70 -5 -8 3 22.00 5.30 5 8 -2 170.68 11.30 -5 8 2 185.38 13.00 5 8 -2 183.08 11.90 5 -8 -2 145.49 13.50 5 -8 -2 169.98 11.00 5 -8 -2 170.68 9.20 -5 -8 2 179.08 10.20 -5 -8 2 164.78 11.80 5 8 -1 157.88 11.00 -5 8 1 150.88 11.30 5 8 -1 150.28 10.80 5 -8 -1 158.78 11.20 -5 -8 1 151.78 11.70 5 -8 -1 145.79 10.80 5 -8 -1 164.68 9.50 -5 -8 1 156.68 10.30 5 8 0 0.60 3.50 -5 8 0 -0.70 4.40 5 8 0 0.60 4.50 5 -8 0 4.00 4.00 5 -8 0 10.00 5.60 -5 -8 0 3.30 5.50 5 -8 0 5.00 3.90 -5 -8 0 8.60 4.40 5 8 1 121.69 9.70 5 8 1 129.19 10.70 -5 8 -1 102.79 9.00 5 -8 1 105.39 9.10 -5 -8 -1 108.89 10.80 5 -8 1 118.69 9.40 5 8 2 47.10 7.00 -5 8 -2 51.19 6.50 5 8 2 62.99 8.70 5 -8 2 65.49 7.90 5 -8 2 51.69 7.00 -5 -8 -2 52.49 8.40 -5 8 -3 11.80 5.30 5 8 3 2.40 5.60 5 8 3 18.90 7.60 -5 -8 -3 6.50 8.40 5 -8 3 11.20 4.50 5 8 4 32.80 7.90 5 8 4 11.90 8.20 5 -8 4 22.60 7.70 5 -8 4 18.30 5.00 5 8 5 0.80 9.50 5 -8 5 -1.40 8.80 5 -8 5 -6.30 4.60 5 8 6 33.90 13.00 5 8 6 16.50 8.90 5 -8 6 5.50 10.50 -5 9 8 13.60 11.20 -5 -9 8 9.90 8.50 5 9 -7 11.60 7.10 -5 9 7 8.00 7.90 -5 -9 7 -1.80 6.60 -5 9 6 35.50 8.70 5 9 -6 24.50 7.10 -5 -9 6 14.20 5.70 -5 9 5 4.00 6.30 5 9 -5 7.50 6.10 -5 -9 5 14.90 5.10 5 -9 -5 14.40 2.30 5 -9 -5 10.80 3.10 5 -9 -5 14.60 9.20 -5 -9 5 17.10 6.40 5 9 -4 25.30 5.70 -5 9 4 8.20 5.50 5 9 -4 18.70 5.80 -5 -9 4 14.90 5.30 5 -9 -4 17.60 3.40 -5 -9 4 17.00 4.80 5 -9 -4 -2.60 7.50 5 -9 -4 25.10 4.90 5 9 -3 94.39 9.40 -5 9 3 82.29 10.00 5 9 -3 89.89 9.10 -5 -9 3 91.09 10.00 5 -9 -3 77.49 8.60 -5 -9 3 107.19 8.20 5 -9 -3 99.19 6.70 5 9 -2 52.79 7.20 -5 9 2 48.60 8.30 5 9 -2 41.50 5.70 -5 -9 2 49.40 7.50 -5 -9 2 49.90 6.30 5 -9 -2 36.10 6.20 5 -9 -2 46.40 5.30 5 9 -1 14.30 7.50 5 9 -1 12.00 5.20 -5 9 1 10.50 5.40 5 -9 -1 11.20 5.60 5 -9 -1 11.40 4.90 5 -9 -1 8.50 4.10 -5 -9 1 9.70 4.90 -5 -9 1 11.20 5.10 5 9 0 38.70 7.00 5 9 0 41.70 7.10 -5 9 0 20.60 5.50 5 -9 0 51.69 7.30 5 -9 0 29.10 5.10 -5 -9 0 46.80 8.40 5 -9 0 31.80 6.90 -5 9 -1 79.19 8.90 5 9 1 90.49 9.90 5 9 1 66.99 8.40 5 -9 1 78.89 8.70 -5 -9 -1 87.49 11.00 5 -9 1 83.69 9.00 -5 9 -2 37.60 6.10 5 9 2 30.50 6.50 5 9 2 27.70 7.00 5 -9 2 47.70 8.10 -5 -9 -2 51.99 8.80 5 9 3 238.68 15.30 5 9 3 226.48 16.10 -5 9 -3 263.67 14.70 5 -9 3 249.97 13.20 -5 -9 -3 237.98 18.40 5 9 4 12.30 8.30 5 -9 4 -9.00 6.60 5 -9 4 5.00 4.50 5 9 5 5.10 10.30 5 -9 5 5.70 8.60 5 -9 5 1.90 5.30 -5 10 8 -1.50 11.10 -5 -10 8 -4.30 8.20 -5 10 7 10.90 10.10 5 10 -7 10.80 8.30 -5 -10 7 2.50 7.80 5 10 -6 8.50 6.90 -5 10 6 5.30 7.80 -5 -10 6 4.80 6.10 -5 10 5 -2.50 6.00 5 10 -5 1.90 6.50 5 -10 -5 1.50 3.80 -5 -10 5 -1.20 5.20 -5 -10 5 13.70 6.00 5 -10 -5 2.20 2.60 5 10 -4 23.60 6.90 -5 10 4 28.80 7.20 -5 -10 4 38.80 5.90 5 -10 -4 31.40 4.20 5 -10 -4 28.00 5.50 -5 -10 4 28.50 6.90 5 10 -3 5.50 5.70 -5 10 3 20.00 6.40 5 10 -3 6.80 5.90 5 -10 -3 15.30 5.50 5 -10 -3 13.90 3.40 5 -10 -3 24.60 8.50 -5 -10 3 4.90 4.80 -5 -10 3 9.70 4.90 -5 10 2 52.49 6.00 -5 10 2 39.60 6.50 5 10 -2 55.79 8.30 5 10 -2 52.49 7.30 5 -10 -2 41.50 5.20 5 -10 -2 41.70 6.90 -5 -10 2 58.69 8.30 -5 -10 2 51.59 6.90 5 10 -1 6.10 4.60 -5 10 1 10.30 5.40 5 10 -1 2.00 4.80 -5 10 1 4.00 3.60 -5 -10 1 3.30 5.10 5 -10 -1 4.20 3.60 5 -10 -1 -1.40 5.90 5 -10 -1 11.00 5.20 -5 -10 1 0.80 5.10 -5 10 0 50.19 7.70 5 10 0 75.39 9.00 5 10 0 100.59 14.70 5 -10 0 82.69 9.10 5 -10 0 80.69 15.00 5 -10 0 77.59 7.80 5 10 1 22.70 6.10 5 10 1 24.10 6.70 -5 10 -1 32.70 6.50 5 -10 1 26.40 5.50 -5 -10 -1 19.40 7.00 5 -10 1 29.80 6.20 -5 10 -2 29.10 6.00 5 10 2 25.30 6.70 5 10 2 37.30 7.30 5 -10 2 44.20 7.80 5 -10 2 32.20 8.40 5 10 3 8.60 6.50 -5 10 -3 5.80 5.20 5 10 3 8.10 7.40 -5 -10 -3 -1.40 8.30 5 -10 3 11.70 4.70 5 10 4 -3.80 8.10 5 -10 4 4.60 5.00 5 -10 4 8.40 7.30 5 10 5 -0.30 10.90 5 -10 5 -1.60 8.60 -5 11 8 4.80 9.90 -5 -11 8 8.80 9.20 -5 11 7 -9.20 9.10 5 11 -7 16.50 9.00 -5 -11 7 6.30 6.80 -5 11 6 12.20 8.00 5 11 -6 22.90 8.70 -5 -11 6 16.80 7.10 -5 -11 6 9.40 7.90 5 11 -5 -0.40 6.80 -5 11 5 -15.30 13.50 -5 -11 5 -1.80 5.90 5 -11 -5 -0.70 3.20 5 -11 -5 -5.90 4.60 -5 -11 5 6.60 6.00 -5 11 4 9.00 6.00 5 11 -4 22.40 7.00 5 -11 -4 22.30 12.30 5 -11 -4 7.70 3.40 5 -11 -4 6.30 5.90 -5 -11 4 15.50 6.80 -5 -11 4 4.30 5.80 5 11 -3 30.20 6.80 -5 11 3 34.00 4.60 -5 11 3 47.90 8.20 5 11 -3 35.10 7.10 5 -11 -3 21.40 6.30 -5 -11 3 33.00 6.90 5 -11 -3 36.90 6.50 -5 -11 3 34.20 6.10 5 11 -2 -9.30 5.40 5 11 -2 5.70 6.00 -5 11 2 2.40 5.60 -5 11 2 -2.90 3.60 -5 -11 2 5.50 5.60 -5 -11 2 -4.10 4.80 5 -11 -2 8.80 5.70 5 -11 -2 4.90 6.10 -5 11 1 220.18 14.20 5 11 -1 218.98 13.60 -5 11 1 214.88 12.00 5 11 -1 211.48 14.10 5 -11 -1 206.78 14.50 -5 -11 1 215.58 14.60 5 -11 -1 201.98 13.50 -5 11 0 52.19 6.90 -5 11 0 40.00 6.90 5 11 0 53.09 8.00 5 11 0 50.69 8.50 5 -11 0 32.30 6.30 5 -11 0 62.69 7.40 -5 -11 0 44.60 8.80 -5 11 -1 -0.10 5.90 5 11 1 2.20 6.00 5 11 1 4.30 5.80 5 -11 1 6.40 4.90 5 -11 1 10.80 5.30 -5 -11 -1 3.80 7.20 5 11 2 21.70 7.30 -5 11 -2 14.10 5.90 5 -11 2 17.40 7.80 -5 -11 -2 15.20 8.40 5 11 3 15.70 7.30 -5 11 -3 8.40 5.10 5 11 3 21.20 8.60 -5 -11 -3 0.50 12.20 5 -11 3 12.30 5.10 5 11 4 62.39 11.60 5 -11 4 47.80 7.00 5 -11 4 48.60 9.30 5 11 5 6.30 9.90 5 11 5 3.60 10.60 5 -11 5 -4.30 10.30 -5 12 8 -3.60 12.70 -5 -12 8 -2.30 8.30 -5 12 7 -6.10 10.50 5 12 -7 -3.70 9.60 -5 -12 7 -1.10 7.80 5 12 -6 5.00 8.00 -5 12 6 13.80 10.20 -5 -12 6 7.00 6.60 -5 -12 6 7.90 8.00 5 12 -5 2.70 6.90 -5 12 5 9.50 11.50 -5 -12 5 4.10 7.00 -5 -12 5 3.80 7.30 5 -12 -5 0.90 4.20 5 -12 -5 0.10 7.60 5 12 -4 3.70 6.20 -5 12 4 -4.20 3.40 -5 12 4 -10.00 6.80 -5 -12 4 -5.80 5.90 5 -12 -4 -3.40 6.20 5 -12 -4 -3.70 6.40 -5 -12 4 0.80 6.10 -5 12 3 54.59 9.30 5 12 -3 45.20 7.90 -5 12 3 58.99 6.60 5 12 -3 52.19 8.20 -5 -12 3 34.70 6.40 5 -12 -3 49.20 7.70 -5 -12 3 35.40 7.40 5 -12 -3 56.99 7.80 5 12 -2 92.59 10.30 -5 12 2 70.89 9.00 5 12 -2 82.69 10.20 -5 12 2 79.69 7.70 5 -12 -2 77.49 9.20 5 -12 -2 83.89 12.30 -5 -12 2 113.79 12.80 5 12 -1 99.49 10.60 -5 12 1 96.89 10.90 5 12 -1 94.19 10.40 -5 12 1 91.69 8.50 -5 -12 1 143.19 16.30 5 -12 -1 80.99 10.20 5 -12 -1 69.89 9.60 -5 12 0 -0.30 4.80 -5 12 0 2.70 5.80 5 12 0 0.60 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47.30 6.50 5 15 -4 54.29 10.30 -5 15 4 73.99 11.50 -5 -15 4 53.69 9.40 5 -15 -4 62.89 9.90 5 -15 -4 44.10 11.50 5 15 -3 21.10 8.30 -5 15 3 28.00 9.70 -5 15 3 20.90 5.50 -5 -15 3 21.10 8.10 5 -15 -3 27.30 9.30 5 -15 -3 30.00 9.70 -5 15 2 -1.20 5.10 5 15 -2 6.30 7.40 -5 15 2 7.70 7.40 5 15 -2 -6.00 5.80 -5 -15 2 7.70 13.00 5 -15 -2 -2.20 6.50 5 15 -1 2.00 7.20 -5 15 1 1.50 7.70 5 15 -1 -1.20 6.00 -5 15 1 1.70 5.60 5 -15 -1 9.20 6.90 -5 -15 1 11.80 8.30 -5 15 0 -1.00 5.90 -5 15 0 0.00 7.00 5 15 0 -0.90 5.80 5 -15 0 1.00 6.70 -5 -15 0 0.00 7.80 5 15 1 94.19 12.90 -5 15 -1 105.49 14.10 -5 15 -1 102.39 11.40 5 -15 1 119.19 12.60 -5 -15 -1 112.59 14.40 -5 15 -2 27.30 7.90 5 15 2 10.40 8.60 -5 -15 -2 20.90 13.00 5 15 3 -2.60 9.90 5 -15 3 -2.20 7.90 5 -15 3 -2.90 7.10 5 15 4 19.10 9.30 5 15 4 18.00 11.60 5 -15 4 14.40 8.90 5 15 5 -5.00 14.00 5 16 -7 4.40 13.70 -5 16 7 -13.10 11.20 -5 -16 7 5.20 9.50 5 16 -6 9.00 11.40 -5 -16 6 2.10 9.70 5 16 -5 29.20 10.70 -5 16 5 31.40 10.70 -5 -16 5 7.60 8.50 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41.60 12.70 -5 17 3 25.20 10.40 -5 17 3 47.10 7.40 5 -17 -3 34.30 11.60 -5 -17 3 39.60 11.00 -5 17 2 133.29 14.70 -5 17 2 105.09 11.30 -5 -17 2 98.19 13.10 5 -17 -2 121.89 14.20 5 17 -1 15.60 7.80 -5 17 1 19.80 9.80 -5 17 1 11.00 6.70 5 -17 -1 -0.30 8.20 -5 -17 1 14.30 9.50 5 17 0 -0.90 8.20 5 17 0 0.10 12.30 -5 17 0 -2.60 7.50 -5 17 0 18.20 7.20 -5 -17 0 11.40 10.20 5 -17 0 -0.40 7.80 -5 17 -1 -6.30 7.40 5 17 1 4.70 8.30 5 -17 1 21.50 7.90 -5 -17 -1 -0.10 9.40 5 17 2 2.50 9.60 -5 17 -2 10.70 9.10 -5 17 -3 15.30 10.50 5 17 3 3.20 11.60 5 -17 3 5.00 8.90 5 17 4 -8.00 13.10 5 17 4 2.50 11.00 5 -17 4 -13.20 10.40 5 18 -7 8.70 18.60 -5 18 7 25.80 19.40 -5 -18 7 -5.90 10.40 -5 18 6 12.60 16.90 5 18 -6 13.70 14.20 -5 -18 6 12.40 11.60 -5 18 5 27.00 12.70 -5 18 5 12.50 6.40 -5 -18 5 2.30 9.50 -5 18 4 18.60 6.90 -5 18 4 14.20 12.00 5 -18 -4 19.80 12.10 -5 18 3 -1.20 9.40 -5 18 3 11.70 6.60 5 -18 -3 43.20 11.70 -5 -18 3 19.10 10.40 -5 18 2 148.59 13.30 -5 18 2 132.49 15.20 5 -18 -2 190.68 17.80 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33.90 7.40 -6 -7 -1 56.89 9.90 6 -7 1 47.60 7.40 6 -7 1 45.10 6.20 6 7 2 -4.60 5.40 -6 7 -2 2.80 6.70 -6 -7 -2 -1.70 8.50 6 -7 2 -0.40 6.30 -6 7 -3 1.20 10.70 6 7 3 12.30 7.90 6 -7 3 -1.60 5.50 6 7 4 3.00 9.70 6 -7 4 4.10 6.90 6 -7 4 2.00 8.30 6 7 5 1.40 11.80 6 -7 5 -26.50 9.60 -6 8 8 3.20 12.30 -6 -8 8 10.60 9.30 -6 8 7 22.40 10.50 -6 -8 7 16.60 8.40 6 8 -6 63.69 9.00 -6 8 6 85.59 13.00 -6 -8 6 71.99 8.90 6 8 -5 11.10 6.60 -6 8 5 12.40 7.60 -6 -8 5 2.20 6.40 6 -8 -5 9.00 4.90 -6 -8 5 15.40 5.30 6 -8 -5 7.50 3.20 6 8 -4 8.80 7.70 6 8 -4 26.20 7.30 -6 8 4 19.10 7.40 6 -8 -4 18.90 4.00 6 -8 -4 30.90 6.30 6 -8 -4 22.60 7.90 -6 -8 4 11.10 5.10 -6 -8 4 20.20 7.80 -6 8 3 27.10 6.80 6 8 -3 19.30 6.30 6 8 -3 5.70 5.90 6 -8 -3 13.60 4.20 6 -8 -3 20.50 6.00 6 -8 -3 12.40 6.60 -6 -8 3 19.10 6.90 -6 -8 3 7.60 5.00 6 8 -2 16.70 6.20 -6 8 2 10.80 10.10 6 8 -2 -1.10 5.50 6 -8 -2 18.00 6.80 -6 -8 2 16.30 5.50 6 -8 -2 19.90 4.70 -6 -8 2 16.80 7.30 6 -8 -2 20.60 8.20 6 8 -1 188.78 13.40 -6 8 1 182.28 13.80 6 8 -1 186.98 13.30 6 -8 -1 185.58 11.40 -6 -8 1 177.98 14.70 6 -8 -1 193.28 14.10 6 -8 -1 165.28 13.90 -6 8 0 4.40 5.20 6 8 0 6.60 5.90 6 8 0 9.10 6.20 -6 -8 0 5.10 7.60 6 -8 0 12.20 5.20 6 -8 0 2.00 5.60 6 8 1 90.89 10.50 6 8 1 85.39 12.80 -6 8 -1 80.69 11.10 6 -8 1 80.39 10.60 -6 -8 -1 92.89 11.60 6 -8 1 91.69 9.90 6 8 2 17.10 7.70 -6 8 -2 8.60 6.20 -6 -8 -2 1.00 9.00 6 -8 2 0.40 9.10 6 8 3 29.20 8.80 6 -8 3 46.40 9.50 6 -8 3 52.99 7.90 6 8 4 11.50 10.80 6 -8 4 -1.90 8.20 6 -8 4 10.60 7.70 6 8 5 29.00 11.70 6 -8 5 -12.40 11.40 -6 9 8 24.70 14.00 -6 -9 8 18.30 9.60 -6 9 7 37.60 11.80 -6 -9 7 34.80 9.90 6 9 -6 2.70 7.70 -6 9 6 -1.60 9.10 -6 -9 6 -0.90 5.80 -6 -9 6 6.90 12.20 6 9 -5 9.20 7.00 -6 9 5 25.00 8.60 6 -9 -5 11.10 3.60 -6 -9 5 16.00 6.70 6 -9 -5 8.10 5.60 -6 -9 5 5.00 5.90 6 9 -4 0.40 6.20 -6 9 4 -10.80 6.90 -6 -9 4 5.30 5.50 6 -9 -4 -0.90 3.30 6 -9 -4 14.20 7.20 6 -9 -4 0.50 5.80 -6 -9 4 -0.90 6.30 -6 9 3 90.29 11.70 6 9 -3 90.19 10.40 6 9 -3 78.19 9.70 -6 -9 3 70.69 7.70 6 -9 -3 74.19 8.80 -6 -9 3 93.29 11.30 6 -9 -3 78.69 10.70 6 -9 -3 76.99 7.90 6 9 -2 2.50 5.90 6 9 -2 2.60 6.10 -6 9 2 -4.90 6.20 6 -9 -2 3.80 4.30 6 -9 -2 6.10 6.90 6 -9 -2 3.30 6.50 -6 -9 2 -4.40 5.80 6 9 -1 44.90 8.00 6 9 -1 28.30 7.60 -6 9 1 29.60 7.60 -6 -9 1 40.40 9.90 6 -9 -1 28.00 5.70 6 -9 -1 25.50 7.00 6 9 0 17.30 6.80 -6 9 0 7.50 5.80 6 9 0 10.30 7.80 -6 -9 0 17.90 9.40 6 -9 0 16.30 6.50 6 -9 0 11.40 5.60 6 9 1 0.50 6.40 -6 9 -1 2.60 5.90 6 -9 1 3.40 5.90 6 -9 1 6.00 5.60 -6 -9 -1 0.60 7.90 -6 9 -2 19.70 6.60 6 9 2 9.70 6.80 -6 -9 -2 13.60 10.00 6 -9 2 26.20 7.20 6 9 3 -12.50 8.40 6 -9 3 14.70 7.70 6 -9 3 11.80 6.80 6 9 4 20.20 11.30 6 -9 4 7.40 7.40 6 -9 4 22.00 10.40 6 9 5 -19.00 13.50 6 -9 5 17.70 11.80 -6 10 8 -3.70 11.90 -6 -10 8 11.10 10.00 6 10 -7 6.20 14.70 -6 10 7 6.60 11.20 -6 -10 7 -3.40 8.70 6 10 -6 80.39 10.80 -6 10 6 99.29 14.90 -6 -10 6 66.19 10.40 -6 10 5 5.10 6.70 6 10 -5 12.20 7.30 -6 -10 5 17.80 6.60 -6 -10 5 8.60 7.30 6 10 -4 5.70 6.60 -6 10 4 -5.00 7.00 6 -10 -4 -0.80 3.70 -6 -10 4 6.10 6.00 6 -10 -4 -4.40 6.60 6 -10 -4 -6.60 7.70 -6 -10 4 -4.60 6.20 -6 10 3 17.40 7.30 6 10 -3 15.30 7.20 6 10 -3 18.50 6.50 -6 -10 3 7.00 6.40 6 -10 -3 15.50 4.90 6 -10 -3 22.50 7.20 6 -10 -3 17.50 7.90 -6 10 2 202.28 15.70 6 10 -2 201.78 14.50 6 10 -2 214.48 14.50 6 -10 -2 202.28 11.80 6 -10 -2 174.58 15.00 6 -10 -2 190.58 15.20 -6 -10 2 170.18 15.60 6 10 -1 12.20 6.70 -6 10 1 10.40 7.00 6 10 -1 4.10 5.10 6 -10 -1 20.40 7.50 -6 -10 1 13.50 7.20 6 -10 -1 4.20 4.80 6 10 0 23.50 7.50 6 10 0 0.20 7.20 -6 10 0 8.80 7.30 6 -10 0 3.40 6.20 6 -10 0 16.70 5.80 -6 10 -1 70.39 8.80 6 10 1 82.19 11.40 -6 -10 -1 60.19 11.00 6 -10 1 54.59 8.80 -6 10 -2 18.50 8.30 6 10 2 11.30 7.90 6 -10 2 15.10 8.50 6 -10 2 0.40 6.30 6 10 3 21.50 9.90 6 -10 3 -10.40 6.10 6 -10 3 2.00 7.50 6 10 4 8.50 12.30 6 -10 4 -4.00 9.70 -6 11 8 0.10 14.00 -6 -11 8 -6.20 10.00 -6 11 7 1.30 10.20 6 11 -7 25.80 13.20 -6 -11 7 21.30 9.10 -6 11 6 -12.70 13.30 6 11 -6 7.30 9.00 -6 -11 6 0.20 8.50 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7.60 7 5 3 18.50 10.30 7 -5 3 13.40 8.30 7 5 4 -9.00 11.40 7 -5 4 -20.40 10.50 -7 6 8 -15.80 12.90 -7 -6 8 2.30 11.00 -7 6 7 3.10 11.40 -7 -6 7 -2.60 9.50 7 6 -6 14.20 7.90 -7 6 6 6.70 10.70 -7 6 5 -2.30 8.20 7 6 -5 -11.00 6.50 7 -6 -5 11.10 4.60 -7 -6 5 10.60 5.30 7 -6 -5 -1.40 8.80 -7 -6 5 12.40 8.10 7 6 -4 144.99 13.00 -7 6 4 133.19 14.90 -7 -6 4 128.39 16.00 7 -6 -4 111.09 14.50 7 -6 -4 111.69 12.50 -7 -6 4 157.18 10.80 7 -6 -4 137.19 9.90 7 6 -3 81.99 10.50 -7 6 3 66.29 10.30 7 6 -3 75.49 9.60 7 -6 -3 102.09 11.60 -7 -6 3 93.19 11.20 7 -6 -3 73.39 9.60 -7 -6 3 98.09 13.30 7 -6 -3 106.29 9.50 -7 6 2 40.20 9.80 7 6 -2 24.60 7.40 7 6 -2 38.00 7.90 7 -6 -2 39.40 8.50 -7 -6 2 41.60 13.80 7 -6 -2 45.20 6.60 -7 6 1 -1.50 7.00 7 6 -1 7.40 6.90 7 6 -1 18.60 8.00 -7 -6 1 19.80 9.80 7 -6 -1 2.80 7.20 7 -6 -1 10.50 5.60 -7 6 0 -3.60 7.00 7 6 0 -6.30 6.90 7 -6 0 -2.40 6.70 7 -6 0 -5.90 6.20 -7 -6 0 -9.70 8.40 7 6 1 9.20 7.60 7 6 1 8.60 8.00 7 -6 1 12.30 7.20 -7 -6 -1 2.90 10.20 7 -6 1 4.70 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11.50 -7 9 7 -1.10 11.60 -7 -9 7 20.40 12.20 -7 9 6 -3.30 18.60 7 9 -6 0.60 9.20 -7 -9 6 1.70 9.40 7 9 -5 17.60 9.10 -7 9 5 29.50 18.20 7 -9 -5 14.90 4.90 -7 -9 5 22.50 7.10 7 9 -4 32.80 8.90 -7 9 4 28.70 10.20 7 -9 -4 32.20 8.30 -7 -9 4 39.30 11.00 7 -9 -4 58.19 19.60 7 -9 -4 24.40 5.80 7 9 -3 221.28 16.70 7 9 -3 212.48 18.00 -7 9 3 234.08 18.90 7 -9 -3 232.78 17.30 7 -9 -3 242.48 13.30 7 -9 -3 230.98 18.50 -7 -9 3 249.38 19.10 7 9 -2 2.00 8.60 -7 9 2 -1.50 8.90 7 9 -2 1.00 7.40 -7 -9 2 8.30 7.90 7 -9 -2 8.70 5.30 7 -9 -2 2.60 8.30 7 9 -1 4.90 9.30 -7 9 1 5.40 9.00 7 -9 -1 6.80 5.70 7 -9 -1 9.80 8.20 -7 -9 1 6.40 9.50 -7 9 0 -17.20 6.90 7 9 0 0.10 6.80 7 9 0 0.70 8.00 7 -9 0 -6.20 7.10 -7 -9 0 3.10 9.90 7 9 1 52.09 10.50 7 -9 1 71.89 9.90 7 9 2 -12.70 9.50 7 -9 2 6.40 8.10 7 9 3 32.80 12.30 7 -9 3 3.10 10.70 -7 10 7 -7.10 13.80 -7 -10 7 1.20 11.50 7 10 -6 1.20 9.90 -7 10 6 -5.80 12.20 -7 -10 6 8.70 10.70 -7 10 5 -0.40 10.20 7 10 -5 -5.10 8.90 -7 -10 5 5.00 9.60 7 -10 -5 3.70 4.60 -7 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17 -6 21.70 20.00 -7 17 6 3.30 20.90 -7 17 5 1.10 22.20 7 17 -5 6.90 15.80 -7 -17 5 5.90 15.10 7 17 -4 -10.70 13.00 7 -17 -4 12.70 8.70 -7 -17 4 14.60 16.60 7 17 -3 26.60 13.90 7 -17 -3 14.90 9.70 -7 -17 3 8.80 19.30 7 17 -2 22.20 13.50 -7 -17 2 12.30 13.60 7 -17 -2 27.10 10.10 7 17 -1 23.70 13.50 7 -17 -1 13.10 9.80 7 17 0 22.70 13.80 7 -17 0 -15.70 10.30 7 17 1 23.00 12.70 7 -17 1 25.90 11.50 7 18 -5 -24.10 16.70 -7 -18 5 14.70 17.30 7 18 -4 33.00 16.00 -7 -18 4 7.90 15.40 7 -18 -4 2.10 9.60 7 18 -3 -17.60 14.40 -7 -18 3 -16.80 17.20 7 18 -2 1.10 14.50 -7 -18 2 7.70 17.60 7 -18 -2 -5.40 9.20 7 18 -1 -2.90 13.10 7 -18 -1 6.90 10.30 7 18 0 -1.50 13.60 7 -18 0 -9.00 10.70 7 18 1 35.80 15.60 7 -18 1 -4.50 11.00 7 19 -5 -4.50 18.90 7 19 -4 0.50 16.40 -7 -19 4 13.30 18.00 7 -19 -4 2.80 12.50 7 19 -3 6.80 16.00 7 -19 -3 8.60 12.20 7 19 -2 32.70 16.00 -7 -19 2 -4.40 17.10 7 -19 -2 -10.50 10.00 7 19 -1 -6.90 15.00 7 -19 -1 -5.90 10.80 7 19 0 -0.40 15.60 7 -19 0 8.60 12.10 7 19 1 -14.40 13.60 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8 1 -3 14.70 6.50 8 1 -3 0.60 10.10 -8 1 3 -0.10 6.00 8 -1 -3 7.40 6.60 8 -1 -3 -1.40 10.00 -8 -1 3 7.20 10.40 -8 1 2 2.20 7.60 8 1 -2 -2.30 6.50 8 1 -2 3.40 9.20 -8 -1 2 -1.50 8.80 8 -1 -2 -5.60 8.90 8 -1 -2 3.20 6.80 -8 1 1 46.20 10.90 -8 -1 1 23.80 11.20 8 1 0 6.50 8.30 8 -1 0 -13.20 8.00 8 1 1 25.90 9.70 8 -1 1 -5.20 8.00 8 1 2 -12.40 9.40 8 -1 2 5.30 9.90 8 1 3 -4.30 11.40 8 -1 3 11.30 11.70 -8 2 7 2.40 11.70 -8 -2 7 -0.90 12.80 -8 2 5 6.70 10.70 8 2 -5 8.70 8.10 8 -2 -5 -2.10 6.30 -8 -2 5 5.70 10.00 -8 2 4 18.30 9.80 8 2 -4 31.80 8.10 8 -2 -4 20.70 11.70 8 -2 -4 29.60 9.10 -8 -2 4 19.10 6.80 8 -2 -4 31.50 7.30 -8 -2 4 19.60 9.30 -8 2 3 26.80 11.20 8 2 -3 23.80 7.80 8 2 -3 27.70 17.70 -8 -2 3 44.20 12.30 8 -2 -3 29.00 10.10 8 -2 -3 35.90 7.40 8 2 -2 72.29 11.30 8 2 -2 64.59 9.70 -8 -2 2 86.19 18.40 8 -2 -2 98.89 12.80 8 -2 -2 73.39 9.70 -8 2 1 20.80 9.50 -8 -2 1 -4.80 11.30 8 2 0 -6.60 7.80 8 -2 0 23.30 8.80 8 2 1 3.30 9.10 8 -2 1 -2.80 9.10 8 2 2 11.90 10.90 8 -2 2 -3.50 10.60 8 2 3 3.60 10.20 8 -2 3 8.90 11.30 -8 3 7 19.40 13.20 -8 -3 7 2.50 12.60 8 3 -5 17.10 8.30 -8 3 5 8.20 10.30 8 -3 -5 18.60 6.70 -8 -3 5 16.10 9.70 -8 3 4 11.30 10.20 8 3 -4 0.90 7.70 8 -3 -4 -8.70 11.90 -8 -3 4 11.00 6.90 8 -3 -4 0.10 9.30 8 -3 -4 14.50 6.60 -8 -3 4 14.90 9.40 8 3 -3 -0.60 7.60 -8 3 3 11.10 8.90 8 3 -3 4.00 9.60 8 -3 -3 -0.90 10.50 8 -3 -3 11.20 6.50 -8 -3 3 10.60 16.40 8 3 -2 3.80 8.80 -8 3 2 2.70 9.70 8 3 -2 9.00 7.00 -8 -3 2 16.30 9.50 8 -3 -2 12.50 6.70 8 -3 -2 10.30 8.90 -8 3 1 0.80 11.30 8 3 0 15.90 8.60 8 -3 0 2.80 8.00 8 3 1 -8.00 8.80 8 -3 1 21.50 9.00 8 3 2 -20.00 9.00 8 -3 2 -8.00 10.10 8 3 3 -7.00 11.50 8 -3 3 2.70 11.50 -8 4 7 8.60 12.20 -8 -4 7 -3.90 13.00 -8 -4 6 -7.00 11.20 -8 4 5 13.70 11.60 8 4 -5 6.90 8.30 -8 -4 5 12.20 10.20 8 -4 -5 3.80 6.30 -8 4 4 3.50 10.10 8 4 -4 10.50 7.80 8 -4 -4 13.00 11.40 -8 -4 4 10.90 9.10 8 -4 -4 -5.40 16.30 8 -4 -4 6.00 6.50 -8 4 3 8.60 10.10 8 4 -3 -3.10 7.90 8 4 -3 1.40 7.80 8 -4 -3 -2.50 10.40 -8 -4 3 -0.10 9.10 8 -4 -3 -1.40 6.10 -8 4 2 1.60 7.00 8 4 -2 6.50 17.40 8 4 -2 1.20 7.40 8 -4 -2 -4.70 6.40 -8 -4 2 -14.40 8.80 8 -4 -2 -19.40 9.30 -8 -4 1 19.80 12.00 8 4 0 8.10 9.10 8 -4 0 -1.50 7.10 8 4 1 4.90 9.80 8 -4 1 9.50 9.10 8 4 2 21.60 11.40 8 -4 2 -14.80 9.80 8 4 3 23.50 11.80 8 -4 3 -16.70 11.00 -8 5 7 -5.10 11.80 -8 -5 7 -3.30 13.30 -8 -5 6 21.60 12.50 8 5 -5 8.10 8.90 -8 5 5 4.50 11.30 8 -5 -5 8.60 6.30 -8 -5 5 2.70 9.50 8 5 -4 16.10 8.80 -8 5 4 15.00 9.10 8 -5 -4 10.40 7.10 -8 -5 4 38.40 20.40 8 -5 -4 26.20 12.30 8 5 -3 -3.70 8.10 8 5 -3 6.70 11.20 -8 5 3 14.20 7.60 8 -5 -3 -2.90 6.10 8 -5 -3 -6.10 10.50 -8 -5 3 -4.30 9.70 -8 5 2 5.30 10.80 8 5 -2 8.60 8.70 8 5 -2 11.40 8.20 -8 -5 2 15.80 9.90 8 -5 -2 17.10 7.60 8 5 -1 4.30 9.10 -8 -5 1 13.70 11.30 8 5 0 13.70 9.30 8 -5 0 9.10 8.30 8 5 1 12.30 10.30 8 -5 1 -3.80 8.70 8 5 2 21.80 11.50 8 -5 2 5.60 10.10 8 5 3 15.70 11.80 8 -5 3 3.20 11.10 -8 6 7 10.50 13.30 -8 -6 7 7.00 13.50 -8 -6 6 12.80 12.20 8 6 -5 -3.80 9.30 -8 6 5 -5.20 13.20 8 -6 -5 3.70 6.90 -8 -6 5 20.10 13.80 -8 6 4 33.00 11.50 8 6 -4 29.70 8.90 8 -6 -4 37.40 7.80 -8 -6 4 30.60 12.00 8 -6 -4 51.99 11.90 -8 6 3 12.90 9.60 8 6 -3 -18.90 9.50 8 6 -3 17.10 8.70 -8 -6 3 3.70 10.70 8 -6 -3 7.20 11.70 8 -6 -3 2.90 6.30 8 6 -2 29.80 10.40 -8 6 2 32.80 12.50 -8 -6 2 27.60 11.80 8 -6 -2 45.40 8.60 8 6 -1 9.70 8.70 -8 -6 1 -7.00 11.00 8 6 0 20.70 10.00 8 -6 0 16.50 8.10 8 6 1 -3.60 9.90 8 -6 1 -4.30 8.40 8 6 2 14.20 12.10 8 -6 2 11.10 10.10 -8 7 7 6.30 15.40 -8 -7 7 23.90 15.10 -8 -7 6 3.20 12.00 8 7 -5 12.20 10.50 -8 7 5 28.60 13.40 -8 -7 5 -13.70 10.90 -8 7 4 21.40 10.90 8 7 -4 13.20 8.80 8 -7 -4 -8.10 6.90 -8 -7 4 -3.80 10.60 8 -7 -4 -5.40 12.80 -8 7 3 16.00 10.60 8 7 -3 7.30 8.80 8 7 -3 20.40 10.30 8 -7 -3 10.20 6.70 -8 -7 3 12.20 11.50 -8 7 2 -19.10 9.90 -8 -7 2 12.40 11.30 8 -7 -2 -3.80 7.00 8 7 -1 10.20 9.50 -8 -7 1 5.60 12.20 8 7 0 -5.50 9.50 8 -7 0 13.20 9.20 8 7 1 15.20 10.30 8 -7 1 14.30 10.00 8 7 2 2.10 11.70 8 -7 2 -20.80 9.80 -8 8 7 19.20 17.30 -8 -8 7 10.30 14.50 -8 -8 6 10.60 12.70 8 8 -5 34.30 11.90 -8 8 5 40.00 14.40 -8 -8 5 43.80 15.90 8 8 -4 42.50 10.60 -8 8 4 89.29 24.00 -8 -8 4 59.89 14.60 8 -8 -4 58.39 8.40 8 8 -3 17.00 9.60 8 8 -3 23.30 12.40 -8 8 3 -1.70 10.00 -8 -8 3 43.60 20.70 8 -8 -3 10.80 6.90 -8 8 2 16.60 19.00 8 -8 -2 23.90 7.90 -8 -8 2 37.60 13.10 8 8 -1 6.10 9.70 8 -8 -1 4.10 12.90 8 8 0 19.70 10.80 8 -8 0 4.70 8.50 8 8 1 6.80 11.20 8 -8 1 -0.70 9.30 8 8 2 7.30 11.30 8 -8 2 -8.00 10.50 -8 9 7 8.30 18.50 -8 -9 7 -32.10 13.90 -8 -9 6 21.90 13.60 -8 9 5 18.90 13.10 8 9 -5 15.10 11.50 -8 9 4 -13.20 11.80 8 9 -4 -4.40 9.80 -8 -9 4 7.30 12.70 8 -9 -4 17.30 7.10 -8 9 3 -5.60 10.40 -8 -9 3 7.60 12.20 8 -9 -3 -3.90 6.90 8 9 -2 -4.50 10.30 8 -9 -2 10.60 7.70 -8 -9 2 15.80 11.60 8 9 -1 -3.50 10.20 8 -9 -1 22.30 8.60 8 9 0 4.50 10.20 8 -9 0 11.60 9.10 8 9 1 -3.50 12.20 8 -9 1 -24.50 8.50 8 9 2 -2.10 13.00 8 -9 2 20.20 10.80 -8 10 7 14.60 20.00 -8 -10 6 7.90 13.90 -8 10 5 -8.20 13.00 8 10 -5 -9.50 12.00 -8 10 4 26.50 13.30 8 10 -4 44.00 11.30 -8 -10 4 34.90 13.80 8 -10 -4 29.70 7.70 -8 10 3 -8.80 12.20 8 -10 -3 1.70 7.80 -8 -10 3 9.90 12.80 8 10 -2 1.10 10.70 -8 -10 2 4.90 12.80 8 10 -1 13.90 10.50 8 -10 -1 8.20 8.10 8 10 0 11.80 11.20 8 -10 0 -6.30 8.70 8 10 1 -2.20 12.10 8 -10 1 0.70 10.50 8 10 2 -0.90 13.70 8 -10 2 -9.60 11.20 -8 -11 6 46.20 15.60 -8 11 5 4.00 13.90 8 11 -5 7.50 13.10 -8 -11 5 15.60 13.80 -8 11 4 18.70 13.90 8 -11 -4 12.40 7.90 -8 -11 4 22.70 14.40 8 11 -3 7.60 11.10 -8 -11 3 23.70 13.40 8 -11 -3 5.60 8.60 8 11 -2 6.20 11.40 -8 -11 2 14.60 12.90 8 11 -1 -7.70 10.00 8 -11 -1 8.40 8.70 8 11 0 5.60 12.30 8 -11 0 5.10 9.60 8 11 1 14.00 11.70 8 -11 1 -0.30 10.60 8 11 2 -17.00 13.20 8 -11 2 -8.50 10.70 -8 -12 6 15.60 14.80 -8 12 5 -2.50 15.20 -8 -12 5 -13.90 14.90 8 -12 -4 8.80 8.20 8 12 -3 9.40 12.20 8 -12 -3 7.40 8.30 -8 -12 3 -7.70 12.40 8 12 -2 12.00 11.00 -8 -12 2 -4.90 14.50 8 12 -1 -3.90 11.50 8 -12 -1 10.80 9.00 8 12 0 11.10 12.70 8 -12 0 13.60 10.00 8 12 1 11.90 13.90 8 -12 1 7.80 10.60 -8 -13 6 -9.80 15.10 -8 13 5 -32.00 20.30 -8 -13 5 -6.90 16.70 8 13 -4 16.00 13.40 8 -13 -4 6.10 8.30 -8 -13 4 -6.30 15.50 8 13 -3 -15.10 11.50 8 -13 -3 -2.90 8.90 -8 -13 3 46.60 27.60 8 13 -2 -1.40 12.60 -8 -13 2 25.00 29.60 8 -13 -2 -1.60 8.60 8 13 -1 8.90 12.90 8 -13 -1 10.80 9.20 8 13 0 25.80 13.00 8 -13 0 3.80 10.40 8 13 1 -11.20 13.60 8 -13 1 17.50 10.70 8 14 -5 11.00 16.80 -8 -14 5 8.80 15.80 8 14 -4 0.80 13.60 8 -14 -4 3.20 8.40 8 14 -3 -18.30 13.20 -8 -14 3 4.80 15.40 8 14 -2 11.50 13.60 8 -14 -2 -13.20 9.00 8 14 -1 -4.90 12.10 8 -14 -1 -3.20 9.60 8 14 0 -25.40 13.50 8 -14 0 13.90 11.10 8 14 1 7.60 14.10 8 -14 1 20.00 11.70 8 15 -5 -15.50 17.50 -8 -15 5 -3.20 18.80 8 15 -4 16.20 14.90 -8 -15 4 2.60 22.90 8 -15 -4 -0.10 12.40 8 15 -3 -6.20 14.20 -8 -15 3 10.50 16.30 8 15 -2 -19.10 14.10 8 -15 -2 7.20 10.50 8 15 -1 36.50 14.80 8 -15 -1 19.30 11.20 8 15 0 21.00 14.60 8 -15 0 -4.40 11.80 8 16 -5 25.30 19.00 -8 -16 4 17.10 21.40 8 16 -3 2.00 15.70 8 -16 -3 9.60 12.30 8 16 -2 8.20 14.50 8 -16 -2 -7.60 11.40 8 16 -1 13.90 14.20 8 -16 -1 -1.20 12.30 8 16 0 10.60 15.10 8 -16 0 26.30 13.60 8 17 -4 13.30 17.20 8 17 -3 8.10 17.50 8 -17 -3 -15.60 13.50 8 17 -2 -17.30 15.50 8 -17 -2 14.50 13.00 8 17 -1 5.80 14.70 8 -17 -1 22.80 12.40 8 18 -3 21.40 18.70 8 18 -2 -4.50 16.40 8 -18 -2 -5.30 13.90 -9 0 6 32.90 20.00 -9 0 5 2.00 12.40 -9 0 4 -12.20 11.30 9 0 -4 -10.90 9.80 9 0 -3 1.70 9.80 9 0 -2 21.40 9.90 9 0 -1 15.30 10.10 9 0 0 -1.60 11.20 9 0 1 18.80 12.20 -9 1 6 26.70 17.80 -9 -1 6 4.30 18.00 -9 1 5 6.00 13.40 -9 -1 5 -4.10 15.20 9 1 -4 2.80 10.20 -9 1 4 4.60 12.00 -9 -1 4 23.90 22.90 9 -1 -4 7.40 9.90 9 -1 -3 7.60 9.50 9 -1 -2 -11.30 9.20 9 1 -1 -16.60 9.80 9 -1 -1 -14.20 9.60 9 1 0 2.90 11.40 9 -1 0 22.80 11.20 9 1 1 17.70 11.70 9 -1 1 11.80 11.50 -9 2 6 -22.90 15.70 -9 -2 6 -7.20 16.10 9 2 -5 -8.00 14.70 -9 2 5 6.00 14.10 -9 -2 5 11.50 14.70 9 2 -4 3.80 10.10 -9 2 4 4.00 15.50 9 -2 -4 -4.30 9.00 -9 -2 4 -47.80 24.10 9 -2 -3 4.30 9.60 9 2 -2 12.50 10.30 9 -2 -2 -14.90 9.30 9 2 -1 3.90 10.30 9 -2 -1 0.60 9.80 9 2 0 -12.00 10.80 9 -2 0 2.40 10.60 9 2 1 -3.70 11.60 9 -2 1 -0.50 12.70 -9 3 6 -3.50 18.60 -9 -3 6 -23.80 16.40 9 3 -5 20.00 12.80 -9 3 5 -25.30 14.90 -9 3 4 -7.30 19.60 9 3 -4 -7.10 10.50 -9 -3 4 20.40 22.70 9 -3 -4 14.50 10.00 9 -3 -3 -0.80 9.70 -9 -3 3 35.00 26.00 9 3 -2 4.70 10.60 9 -3 -2 -0.20 9.10 9 3 -1 4.20 10.50 9 -3 -1 11.60 9.60 9 3 0 13.60 12.50 9 -3 0 -17.60 10.80 9 3 1 -2.20 12.30 9 -3 1 -2.20 12.50 -9 4 6 -0.10 18.90 -9 -4 6 10.80 18.20 -9 4 5 9.90 16.30 9 4 -5 -8.50 11.90 -9 -4 5 -1.60 14.20 -9 4 4 7.90 16.30 9 4 -4 16.10 12.10 9 -4 -4 6.30 9.80 -9 -4 4 -12.90 13.30 9 -4 -3 4.10 9.30 9 4 -2 21.20 11.80 9 -4 -2 3.60 9.00 9 4 -1 -2.80 10.60 9 -4 -1 -7.50 9.60 9 4 0 -9.40 11.40 9 -4 0 -16.50 11.30 9 4 1 1.70 12.00 9 -4 1 3.70 12.10 -9 5 6 -4.90 18.90 -9 -5 6 -19.60 17.60 9 5 -5 -4.50 11.20 -9 5 5 9.10 15.80 9 5 -4 15.50 12.40 -9 -5 4 -22.90 13.30 9 -5 -4 -17.40 8.90 9 5 -3 -15.30 17.30 9 -5 -3 10.20 9.70 9 5 -2 -16.10 10.40 9 -5 -2 29.20 9.70 9 5 -1 8.00 11.90 9 -5 -1 22.50 10.80 9 5 0 -0.80 12.10 9 -5 0 -14.50 11.10 9 5 1 17.00 12.30 9 -5 1 16.60 11.50 -9 6 6 -14.20 20.60 -9 -6 6 -8.80 18.30 -9 6 5 12.80 16.40 9 6 -5 16.00 12.70 -9 -6 4 39.20 27.30 9 6 -3 7.90 11.20 9 -6 -3 -0.30 10.90 9 6 -2 17.20 12.40 9 -6 -2 21.90 10.20 9 6 -1 6.40 12.60 9 -6 -1 13.40 11.10 9 6 0 19.20 12.10 9 -6 0 13.50 11.80 9 6 1 12.00 13.40 9 -6 1 -1.80 12.00 -9 7 6 6.20 20.10 -9 -7 6 12.40 19.20 9 7 -5 -4.60 12.80 9 -7 -4 9.20 9.40 -9 -7 4 -2.10 15.80 9 7 -3 -10.20 11.30 9 7 -2 19.20 13.10 9 -7 -2 0.20 10.00 9 7 -1 4.80 12.90 9 -7 -1 17.10 11.00 9 7 0 4.90 13.30 9 -7 0 15.60 11.50 9 8 -5 9.60 14.30 -9 -8 5 0.60 19.20 9 -8 -4 -11.30 9.50 -9 -8 4 -5.00 14.90 9 8 -3 14.00 13.10 9 8 -2 -5.30 12.50 9 -8 -2 6.80 10.20 9 8 -1 1.00 13.60 9 -8 -1 17.80 10.50 9 8 0 17.60 13.60 9 -8 0 6.00 11.70 -9 -9 5 2.70 20.50 9 9 -4 2.30 15.00 -9 -9 4 1.80 17.80 9 -9 -4 -21.30 10.40 9 9 -3 -9.70 12.50 9 9 -2 17.40 13.90 9 -9 -2 15.00 11.10 9 9 -1 19.30 13.70 9 -9 -1 -16.70 10.60 9 9 0 -9.60 13.30 9 -9 0 -15.40 11.10 -9 -10 5 36.10 22.30 9 10 -4 -4.20 15.30 9 10 -3 24.20 13.50 9 10 -2 -4.80 14.30 9 -10 -2 14.30 11.40 9 10 -1 20.30 14.20 9 -10 -1 3.10 11.60 9 10 0 5.90 13.90 9 -10 0 11.00 13.20 9 11 -5 11.30 18.40 9 11 -4 2.80 16.40 9 11 -3 -13.40 13.50 9 -11 -3 -16.70 11.60 9 11 -2 -0.30 15.20 9 -11 -2 -2.90 11.80 9 11 -1 19.90 15.00 9 -11 -1 -7.80 11.70 9 12 -4 5.20 18.10 9 12 -3 11.30 15.30 9 -12 -3 7.10 13.50 9 12 -2 16.90 16.10 9 -12 -2 36.90 13.00 9 12 -1 -35.70 14.70 9 -12 -1 13.90 12.20 9 13 -4 17.70 19.80 9 13 -3 -32.90 15.20 9 -13 -3 10.30 13.90 9 13 -2 18.80 16.50 9 -13 -2 -1.70 13.80 10 0 -3 14.50 15.20 10 0 -2 13.30 14.90 10 1 -4 11.60 17.30 10 1 -3 -6.20 15.90 10 -1 -3 -15.90 14.20 10 1 -2 -40.60 14.00 10 -1 -2 16.30 14.70 10 2 -4 -24.40 16.50 10 2 -3 9.90 16.30 10 -2 -3 -9.90 14.70 10 2 -2 -20.30 13.90 10 -2 -2 4.20 14.00 10 3 -4 -11.90 16.60 10 3 -3 -0.30 16.70 10 -3 -3 -14.50 14.20 10 3 -2 27.30 15.40 10 -3 -2 6.50 14.60 10 4 -4 -3.40 17.30 10 4 -3 -3.50 16.30 10 -4 -3 3.80 15.70 10 4 -2 -5.70 14.60 10 5 -3 -11.80 16.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 784 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.3181(5) 0.28099(17) 0.0018(5) 0.0472(10) Uani 1 1 d . . . . . C2 C 0.1389(5) 0.26734(16) -0.0417(5) 0.0475(10) Uani 1 1 d . . . . . C3 C 0.0524(5) 0.32139(16) -0.0574(5) 0.0474(10) Uani 1 1 d . . . . . C4 C 0.1694(5) 0.42499(15) -0.0034(5) 0.0421(9) Uani 1 1 d . . . . . H4A H 0.053426 0.438577 -0.083744 0.050 Uiso 1 1 calc R U . . . H4B H 0.262061 0.445120 -0.040826 0.050 Uiso 1 1 calc R U . . . C5 C 0.1888(4) 0.43894(14) 0.1973(5) 0.0330(8) Uani 1 1 d . . . . . C6 C 0.3052(4) 0.44738(14) 0.4892(5) 0.0340(8) Uani 1 1 d . . . . . N1 N 0.1845(4) 0.36172(12) -0.0270(4) 0.0365(7) Uani 1 1 d . . . . . N2 N 0.3497(4) 0.33731(15) 0.0125(4) 0.0485(8) Uani 1 1 d . . . . . N3 N 0.0535(4) 0.45546(14) 0.2494(4) 0.0465(8) Uani 1 1 d . . . . . N4 N 0.3471(3) 0.43320(11) 0.3392(3) 0.0296(6) Uani 1 1 d . . . . . H4 H 0.450036 0.422698 0.331496 0.036 Uiso 1 1 calc R U . . . N5 N 0.3890(4) 0.45224(13) 0.6765(4) 0.0436(8) Uani 1 1 d . . . . . N6 N 0.5619(5) 0.43962(13) 0.7349(4) 0.0447(8) Uani 1 1 d . . . . . N8 N 0.0538(8) 0.21277(18) -0.0617(7) 0.0716(12) Uani 1 1 d . . . . . N9 N -0.1196(5) 0.33481(18) -0.0933(7) 0.0951(16) Uani 1 1 d . . . . . H9A H -0.152235 0.370946 -0.098109 0.114 Uiso 1 1 calc R U . . . H9B H -0.198597 0.307382 -0.111639 0.114 Uiso 1 1 calc R U . . . O3A O 0.1204(12) 0.1712(3) -0.105(4) 0.097(6) Uani 0.59(4) 1 d . . P A 1 O4A O -0.097(2) 0.2086(6) -0.049(4) 0.099(5) Uani 0.59(4) 1 d . . P A 1 O3B O 0.155(3) 0.1722(5) 0.025(5) 0.098(7) Uani 0.41(4) 1 d . . P A 2 O4B O -0.115(4) 0.2154(10) -0.154(5) 0.122(7) Uani 0.41(4) 1 d . . P A 2 O5 O 0.1303(3) 0.46176(11) 0.4470(3) 0.0479(7) Uani 1 1 d . . . . . O6 O 0.6518(3) 0.42583(12) 0.6317(4) 0.0522(7) Uani 1 1 d . . . . . O7 O 0.6384(4) 0.44315(14) 0.9092(4) 0.0721(9) Uani 1 1 d . . . . . O8 O 0.6885(4) 0.40339(14) 0.2797(4) 0.0725(9) Uani 1 1 d . . . . . H8A H 0.709240 0.404844 0.174509 0.109 Uiso 1 1 d R U . . . H8B H 0.775744 0.383821 0.350950 0.109 Uiso 1 1 d R U . . . N7 N 0.4708(7) 0.2417(3) 0.0358(9) 0.0957(16) Uani 1 1 d . . . . . O1A O 0.585(2) 0.2519(9) -0.013(3) 0.222(12) Uani 0.547(13) 1 d . . P B 1 O2A O 0.4674(11) 0.1991(4) 0.1462(16) 0.128(5) Uani 0.547(13) 1 d . . P B 1 O1B O 0.630(2) 0.2664(7) 0.1191(19) 0.137(7) Uani 0.453(13) 1 d . . P B 2 O2B O 0.4676(14) 0.2022(4) -0.0623(14) 0.091(4) Uani 0.453(13) 1 d . . P B 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.055(3) 0.039(3) 0.047(2) -0.0021(18) 0.0142(18) 0.017(2) C2 0.062(3) 0.030(2) 0.049(2) -0.0093(17) 0.0154(19) -0.0025(19) C3 0.046(2) 0.036(2) 0.055(2) -0.0099(18) 0.0084(18) -0.0021(19) C4 0.054(2) 0.027(2) 0.0399(19) 0.0029(15) 0.0063(16) 0.0030(17) C5 0.036(2) 0.0202(18) 0.0438(19) 0.0015(15) 0.0132(16) 0.0022(15) C6 0.036(2) 0.0232(18) 0.047(2) -0.0001(15) 0.0178(16) -0.0018(15) N1 0.0378(17) 0.0295(17) 0.0360(15) -0.0030(12) 0.0026(12) 0.0030(14) N2 0.0429(19) 0.045(2) 0.056(2) -0.0047(15) 0.0124(15) 0.0052(15) N3 0.0357(17) 0.046(2) 0.056(2) -0.0047(15) 0.0108(15) 0.0061(14) N4 0.0259(14) 0.0304(16) 0.0359(15) -0.0016(12) 0.0144(12) 0.0030(11) N5 0.053(2) 0.046(2) 0.0373(17) -0.0038(13) 0.0213(15) -0.0059(15) N6 0.056(2) 0.0374(19) 0.0381(18) 0.0012(14) 0.0111(16) -0.0101(16) N8 0.098(3) 0.040(3) 0.084(3) -0.016(2) 0.040(3) -0.011(3) N9 0.041(2) 0.059(3) 0.172(5) -0.029(3) 0.014(2) -0.0092(19) O3A 0.114(6) 0.038(4) 0.129(14) -0.024(5) 0.025(6) 0.009(3) O4A 0.089(7) 0.060(5) 0.160(13) -0.027(7) 0.056(8) -0.025(4) O3B 0.169(12) 0.034(6) 0.106(17) -0.006(7) 0.064(12) -0.009(7) O4B 0.164(17) 0.070(9) 0.127(16) -0.034(10) 0.039(13) -0.069(9) O5 0.0408(15) 0.0537(17) 0.0561(17) -0.0073(12) 0.0253(13) 0.0051(12) O6 0.0462(16) 0.0623(19) 0.0455(15) -0.0027(13) 0.0103(13) 0.0051(13) O7 0.087(2) 0.089(2) 0.0307(15) -0.0005(14) 0.0038(14) -0.0267(18) O8 0.0619(18) 0.092(2) 0.0652(19) 0.0093(16) 0.0215(15) 0.0126(17) N7 0.077(4) 0.086(4) 0.112(4) -0.017(4) 0.010(3) 0.041(3) O1A 0.113(12) 0.24(2) 0.37(3) 0.11(2) 0.159(17) 0.094(15) O2A 0.122(7) 0.083(6) 0.176(11) 0.057(6) 0.041(6) 0.073(5) O1B 0.109(10) 0.112(10) 0.141(10) -0.048(8) -0.033(7) 0.072(8) O2B 0.116(8) 0.041(5) 0.128(9) -0.026(5) 0.054(6) 0.028(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 C1 C2 113.4(3) . . ? N2 C1 N7 117.8(4) . . ? C2 C1 N7 128.8(4) . . ? C1 C2 C3 104.7(3) . . ? C1 C2 N8 130.2(4) . . ? C3 C2 N8 125.1(4) . . ? N9 C3 N1 123.7(4) . . ? N9 C3 C2 131.2(4) . . ? N1 C3 C2 105.1(3) . . ? N1 C4 C5 110.1(3) . . ? N1 C4 H4A 109.6 . . ? C5 C4 H4A 109.6 . . ? N1 C4 H4B 109.6 . . ? C5 C4 H4B 109.6 . . ? H4A C4 H4B 108.1 . . ? N3 C5 N4 115.2(3) . . ? N3 C5 C4 121.8(3) . . ? N4 C5 C4 123.0(3) . . ? N4 C6 O5 111.7(3) . . ? N4 C6 N5 137.6(3) . . ? O5 C6 N5 110.7(3) . . ? C3 N1 N2 112.8(3) . . ? C3 N1 C4 127.3(3) . . ? N2 N1 C4 119.2(3) . . ? C1 N2 N1 103.9(3) . . ? C5 N3 O5 102.7(3) . . ? C6 N4 C5 103.5(3) . . ? C6 N4 H4 128.3 . . ? C5 N4 H4 128.3 . . ? N6 N5 C6 116.2(3) . . ? O6 N6 O7 118.8(3) . . ? O6 N6 N5 125.1(3) . . ? O7 N6 N5 116.0(3) . . ? O3A N8 O4A 118.9(9) . . ? O3B N8 O4B 133.4(18) . . ? O3A N8 C2 120.6(7) . . ? O4A N8 C2 120.2(7) . . ? O3B N8 C2 113.2(12) . . ? O4B N8 C2 113.1(11) . . ? C3 N9 H9A 120.0 . . ? C3 N9 H9B 120.0 . . ? H9A N9 H9B 120.0 . . ? C6 O5 N3 106.9(2) . . ? H8A O8 H8B 104.5 . . ? O1A N7 O2A 124.1(10) . . ? O2B N7 O1B 117.2(9) . . ? O1A N7 C1 121.8(11) . . ? O2B N7 C1 121.0(7) . . ? O2A N7 C1 113.6(6) . . ? O1B N7 C1 114.9(7) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N2 1.305(5) . ? C1 C2 1.374(5) . ? C1 N7 1.452(6) . ? C2 C3 1.393(5) . ? C2 N8 1.397(6) . ? C3 N9 1.325(5) . ? C3 N1 1.350(5) . ? C4 N1 1.462(4) . ? C4 C5 1.491(5) . ? C4 H4A 0.9700 . ? C4 H4B 0.9700 . ? C5 N3 1.293(4) . ? C5 N4 1.363(4) . ? C6 N4 1.301(4) . ? C6 O5 1.347(4) . ? C6 N5 1.351(4) . ? N1 N2 1.354(4) . ? N3 O5 1.415(4) . ? N4 H4 0.8600 . ? N5 N6 1.319(4) . ? N6 O6 1.235(4) . ? N6 O7 1.254(4) . ? N8 O3A 1.174(12) . ? N8 O4A 1.215(14) . ? N8 O3B 1.26(2) . ? N8 O4B 1.29(3) . ? N9 H9A 0.8600 . ? N9 H9B 0.8600 . ? O8 H8A 0.8500 . ? O8 H8B 0.8498 . ? N7 O1A 1.086(13) . ? N7 O2B 1.156(9) . ? N7 O2A 1.279(10) . ? N7 O1B 1.333(17) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag C4 H4B N5 0.97 2.60 3.405(5) 140.5 1_554 yes N4 H4 O8 0.86 2.07 2.923(4) 172.5 . yes N9 H9A N6 0.86 2.70 3.403(5) 140.2 1_454 yes N9 H9A O6 0.86 2.46 3.072(5) 128.5 1_454 yes N9 H9A O7 0.86 2.34 3.117(5) 151.1 1_454 yes N9 H9B O4A^a 0.86 2.39 2.895(14) 118.3 . yes N9 H9B O4B^b 0.86 2.25 2.76(2) 118.3 . yes N9 H9B O1A^a 0.86 2.41 3.188(18) 150.8 1_455 yes N9 H9B O1B^b 0.86 2.66 3.27(2) 129.4 1_455 yes N9 H9B O1B^b 0.86 2.64 3.340(14) 138.9 4_465 yes O8 H8A O7 0.85 2.07 2.818(4) 145.7 1_554 yes O8 H8B O4A^a 0.85 2.35 3.105(14) 148.0 4_666 yes O8 H8B O4B^b 0.85 2.42 3.08(2) 134.4 4_666 yes