#------------------------------------------------------------------------------ #$Date: 2021-10-06 18:40:04 +0300 (Wed, 06 Oct 2021) $ #$Revision: 269722 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/82/7708234.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708234 loop_ _publ_author_name 'Shmelev, Nikita Y.' 'Okubazghi, Tesfu H.' 'Abramov, Pavel A.' 'Komarov, Vladislav Y.' 'Rakhmanova, Mariana I.' 'Novikov, Alexander S.' 'Gushchin, Artem L.' _publ_section_title ; Intramolecular aurophilic interactions in dinuclear gold(I) complexes with twisted bridging 2,2'-bipyridine ligands. ; _journal_issue 36 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 12448 _journal_page_last 12456 _journal_paper_doi 10.1039/d1dt02164h _journal_volume 50 _journal_year 2021 _chemical_formula_sum 'C52 H42 Au2 F6 N2 O10 P2 S2' _chemical_formula_weight 1488.87 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2017/1 _audit_update_record ; 2021-05-24 deposited with the CCDC. 2021-08-17 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.878(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.0607(5) _cell_length_b 21.8487(10) _cell_length_c 22.2046(11) _cell_measurement_reflns_used 9855 _cell_measurement_temperature 150(2) _cell_measurement_theta_max 29.3790 _cell_measurement_theta_min 2.3343 _cell_volume 5209.4(4) _computing_cell_refinement 'SAINT (Bruker-AXS, 2004)' _computing_data_collection 'APEX2 (Bruker-AXS, 2004)' _computing_data_reduction 'SAINT (Bruker-AXS, 2004)' _computing_molecular_graphics 'ShelXle (H\"ubschle, 2011)' _computing_publication_material 'CIFTAB-2014 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-2014 (Sheldrick, 2014)' _diffrn_ambient_temperature 150(2) _diffrn_detector_area_resol_mean 25 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0535 _diffrn_reflns_av_unetI/netI 0.0405 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 68561 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.500 _diffrn_reflns_theta_max 28.700 _diffrn_reflns_theta_min 1.864 _diffrn_source 'sealed X-ray tube' _exptl_absorpt_coefficient_mu 5.850 _exptl_absorpt_correction_T_max 0.7466 _exptl_absorpt_correction_T_min 0.6202 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (Bruker-AXS, 2004)' _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.898 _exptl_crystal_description block _exptl_crystal_F_000 2888 _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.100 _refine_diff_density_max 1.241 _refine_diff_density_min -1.216 _refine_diff_density_rms 0.129 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.056 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 678 _refine_ls_number_reflns 13432 _refine_ls_number_restraints 36 _refine_ls_restrained_S_all 1.061 _refine_ls_R_factor_all 0.0437 _refine_ls_R_factor_gt 0.0334 _refine_ls_shift/su_max 0.004 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0300P)^2^+9.1876P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0750 _refine_ls_wR_factor_ref 0.0788 _reflns_Friedel_coverage 0.000 _reflns_number_gt 11267 _reflns_number_total 13432 _reflns_threshold_expression >2\s(I) _cod_data_source_file d1dt02164h2.cif _cod_data_source_block ns237 _cod_depositor_comments 'Adding full bibliography for 7708233--7708237.cif.' _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7708234 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.474 _shelx_estimated_absorpt_t_max 0.592 _shelx_res_file ; TITL ns-327_150k_a.res in P2(1)/c 1_a.res created by SHELXL-2017/1 at 17:50:25 on 19-Apr-2021 REM Old TITL NS-327_150K in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.106, Rweak 0.006, Alpha 0.064, Orientation as input REM Formula found by SHELXT: C56 N6 O11 S4 Au2 CELL 0.71073 11.0607 21.8487 22.2046 90 103.878 90 ZERR 4 0.0005 0.001 0.0011 0 0.002 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Au F N O P S UNIT 208 168 8 24 8 40 8 8 L.S. 10 PLAN 10 TEMP -123.15 BOND $H list 4 fmap 2 ACTA 51 OMIT 0 SHEL 0.74 15 SIMU 0.01 0.01 c33 c34 c35 c36 c37 c38 SIZE 0.15 0.10 0.10 WGHT 0.030000 9.187600 FVAR 0.13371 C1 1 0.426464 0.405040 0.895841 11.00000 0.02537 0.02126 = 0.02923 0.00027 0.00953 -0.00275 C00G 1 0.859195 0.262526 0.743617 11.00000 0.03205 0.03106 = 0.03260 -0.00303 0.00656 -0.00218 AFIX 43 H00G 2 0.851220 0.221320 0.729560 11.00000 -1.20000 AFIX 0 C00H 1 0.801473 0.368630 0.730220 11.00000 0.02856 0.02826 = 0.03906 -0.00406 0.01650 -0.00213 AFIX 43 H00H 2 0.753627 0.400272 0.706456 11.00000 -1.20000 AFIX 0 C00I 1 0.786197 0.308160 0.708971 11.00000 0.02581 0.02642 = 0.02727 -0.00359 0.01115 -0.00313 C2 1 0.310722 0.423622 0.860066 11.00000 0.02722 0.03356 = 0.03518 -0.00242 0.00554 -0.00388 AFIX 43 H2 2 0.294559 0.422355 0.816089 11.00000 -1.20000 AFIX 0 C01F 1 0.944572 0.277550 0.799347 11.00000 0.03435 0.04445 = 0.03940 0.00004 0.00159 -0.00425 AFIX 43 H01F 2 0.994943 0.246413 0.822641 11.00000 -1.20000 AFIX 0 C01G 1 0.956063 0.337240 0.820669 11.00000 0.03875 0.05030 = 0.03432 -0.01256 0.00601 -0.01240 AFIX 43 H01G 2 1.011912 0.346836 0.859152 11.00000 -1.20000 AFIX 0 C3 1 0.219236 0.443915 0.888358 11.00000 0.02405 0.03399 = 0.05535 -0.00167 0.00693 -0.00210 AFIX 43 H3 2 0.140463 0.456358 0.863800 11.00000 -1.20000 AFIX 0 C4 1 0.242474 0.446025 0.951833 11.00000 0.03485 0.04599 = 0.05751 -0.00959 0.02523 -0.00090 AFIX 43 H4 2 0.179687 0.460176 0.971065 11.00000 -1.20000 AFIX 0 C5 1 0.356051 0.427802 0.987914 11.00000 0.05206 0.07798 = 0.03508 -0.00630 0.02073 0.00961 AFIX 43 H5 2 0.371482 0.429301 1.031860 11.00000 -1.20000 AFIX 0 C6 1 0.448926 0.407010 0.959546 11.00000 0.03512 0.05726 = 0.02697 0.00025 0.00866 0.00993 AFIX 43 H6 2 0.527318 0.394289 0.984296 11.00000 -1.20000 AFIX 0 C7 1 0.693159 0.382364 0.909649 11.00000 0.02227 0.02744 = 0.02011 -0.00082 0.00574 -0.00277 C8 1 0.763974 0.435089 0.912668 11.00000 0.02935 0.02510 = 0.03000 -0.00465 0.00475 -0.00209 AFIX 43 H8 2 0.731022 0.469768 0.888429 11.00000 -1.20000 AFIX 0 C9 1 0.882322 0.437219 0.950874 11.00000 0.03144 0.03693 = 0.03393 -0.00940 0.00495 -0.00517 AFIX 43 H9 2 0.930246 0.473619 0.953354 11.00000 -1.20000 AFIX 0 C10 1 0.931616 0.386477 0.985660 11.00000 0.02532 0.05523 = 0.02610 -0.00087 -0.00172 0.00290 AFIX 43 H10 2 1.013622 0.387948 1.011449 11.00000 -1.20000 AFIX 0 C11 1 0.861891 0.334043 0.982850 11.00000 0.03662 0.04668 = 0.03680 0.01459 0.00040 0.00480 AFIX 43 H11 2 0.895777 0.299371 1.006848 11.00000 -1.20000 AFIX 0 C12 1 0.742001 0.331502 0.945054 11.00000 0.03492 0.03225 = 0.03144 0.00959 0.00507 -0.00200 AFIX 43 H12 2 0.693677 0.295319 0.943374 11.00000 -1.20000 AFIX 0 C13 1 0.511933 0.300556 0.835728 11.00000 0.03673 0.02719 = 0.01804 0.00201 0.00535 -0.00594 C14 1 0.603185 0.268299 0.814142 11.00000 0.04288 0.03158 = 0.03174 -0.00123 0.01456 -0.00277 AFIX 43 H14 2 0.678072 0.288160 0.811380 11.00000 -1.20000 AFIX 0 C014 1 0.885704 0.382973 0.785616 11.00000 0.03552 0.03722 = 0.04340 -0.01640 0.01779 -0.01254 AFIX 43 H014 2 0.895081 0.424220 0.799492 11.00000 -1.20000 AFIX 0 C15 1 0.583690 0.207764 0.796992 11.00000 0.07009 0.03029 = 0.02762 -0.00210 0.01752 -0.00026 AFIX 43 H15 2 0.645558 0.186124 0.782430 11.00000 -1.20000 AFIX 0 C16 1 0.475827 0.178321 0.800701 11.00000 0.08348 0.02569 = 0.03565 -0.00190 0.01587 -0.01387 AFIX 43 H16 2 0.463141 0.136703 0.788420 11.00000 -1.20000 AFIX 0 C17 1 0.385778 0.209455 0.822367 11.00000 0.05833 0.03821 = 0.05241 -0.00455 0.01972 -0.02802 AFIX 43 H17 2 0.311354 0.189074 0.825007 11.00000 -1.20000 AFIX 0 C18 1 0.403781 0.270684 0.840366 11.00000 0.04601 0.03383 = 0.03745 -0.00102 0.01625 -0.01125 AFIX 43 H18 2 0.342288 0.291787 0.855711 11.00000 -1.20000 AFIX 0 C19 1 0.245639 0.336750 0.680844 11.00000 0.02891 0.02945 = 0.06615 0.00340 -0.00059 -0.00747 AFIX 43 H19 2 0.262319 0.294081 0.681224 11.00000 -1.20000 AFIX 0 C20 1 0.142912 0.356676 0.699252 11.00000 0.02543 0.05205 = 0.06243 0.00808 0.00503 -0.01560 AFIX 43 H20 2 0.088376 0.328181 0.711413 11.00000 -1.20000 AFIX 0 C21 1 0.119579 0.418277 0.699944 11.00000 0.01966 0.04844 = 0.03670 0.00688 0.00378 -0.00304 AFIX 43 H21 2 0.048763 0.432893 0.712716 11.00000 -1.20000 AFIX 0 C22 1 0.200286 0.459096 0.681827 11.00000 0.02356 0.03255 = 0.01990 0.00076 0.00301 0.00278 C23 1 0.301164 0.435923 0.662376 11.00000 0.02200 0.02365 = 0.02284 0.00002 0.00003 0.00061 C24 1 0.182785 0.526518 0.685552 11.00000 0.03284 0.03972 = 0.02329 -0.00436 0.00433 0.01391 C25 1 0.040430 0.603642 0.694646 11.00000 0.06648 0.07265 = 0.08212 -0.03231 0.00919 0.03769 AFIX 137 H01R 2 0.057910 0.627011 0.660023 11.00000 -1.50000 H01S 2 0.093389 0.618592 0.733770 11.00000 -1.50000 H25 2 -0.047301 0.608760 0.695236 11.00000 -1.50000 AFIX 0 C26 1 0.395390 0.475535 0.642685 11.00000 0.02378 0.01965 = 0.02344 -0.00537 0.00595 0.00482 C27 1 0.596810 0.515074 0.669985 11.00000 0.02947 0.02590 = 0.02704 -0.00079 0.00891 -0.00182 AFIX 43 H27 2 0.672981 0.520346 0.700222 11.00000 -1.20000 AFIX 0 C28 1 0.583024 0.542075 0.612781 11.00000 0.03035 0.02668 = 0.03117 -0.00033 0.01322 -0.00190 AFIX 43 H28 2 0.649031 0.565241 0.603579 11.00000 -1.20000 AFIX 0 C29 1 0.471781 0.535062 0.568811 11.00000 0.03562 0.03003 = 0.02214 0.00496 0.01041 0.00843 AFIX 43 H29 2 0.461265 0.552529 0.528707 11.00000 -1.20000 AFIX 0 C30 1 0.375435 0.502148 0.583948 11.00000 0.02858 0.03169 = 0.01983 -0.00215 0.00741 0.00595 C31 1 0.249103 0.499040 0.540063 11.00000 0.03305 0.03964 = 0.02381 0.00364 0.00343 0.01055 C32 1 0.138074 0.502662 0.435636 11.00000 0.03710 0.06098 = 0.02215 0.00182 -0.00650 0.00823 AFIX 137 H01C 2 0.150858 0.512532 0.394556 11.00000 -1.50000 H01H 2 0.080669 0.532419 0.446663 11.00000 -1.50000 H01N 2 0.102714 0.461466 0.434929 11.00000 -1.50000 AFIX 0 C33 1 0.726000 0.314337 0.574466 11.00000 0.05962 0.02256 = 0.02990 -0.00305 0.01411 0.00063 C34 1 0.642464 0.320596 0.516788 11.00000 0.09741 0.03289 = 0.03022 -0.00160 0.00824 0.01356 AFIX 43 H34 2 0.555436 0.315947 0.512582 11.00000 -1.20000 AFIX 0 C35 1 0.689795 0.333839 0.465467 11.00000 0.15728 0.03129 = 0.03238 0.00177 0.02113 0.01919 AFIX 43 H35 2 0.634533 0.337159 0.425614 11.00000 -1.20000 AFIX 0 C36 1 0.814756 0.342115 0.471741 11.00000 0.16425 0.04209 = 0.05926 -0.00105 0.06729 -0.00387 AFIX 43 H36 2 0.844585 0.351796 0.436168 11.00000 -1.20000 AFIX 0 C37 1 0.898098 0.336742 0.528322 11.00000 0.11856 0.05569 = 0.07297 -0.01057 0.06621 -0.01713 AFIX 43 H37 2 0.984795 0.342459 0.532271 11.00000 -1.20000 AFIX 0 C38 1 0.851717 0.322629 0.579901 11.00000 0.07801 0.04368 = 0.04857 -0.01231 0.03610 -0.01056 AFIX 43 H38 2 0.907847 0.318673 0.619448 11.00000 -1.20000 AFIX 0 C39 1 0.645583 0.209757 0.634423 11.00000 0.02732 0.02396 = 0.02308 -0.00247 0.00305 0.00235 C40 1 0.735484 0.172651 0.617924 11.00000 0.02883 0.02922 = 0.04516 -0.01007 0.01129 0.00019 AFIX 43 H40 2 0.806228 0.190692 0.607804 11.00000 -1.20000 AFIX 0 C41 1 0.721692 0.110277 0.616330 11.00000 0.04168 0.03047 = 0.05860 -0.01236 0.01063 0.00701 AFIX 43 H41 2 0.783851 0.085078 0.606090 11.00000 -1.20000 AFIX 0 C42 1 0.616663 0.083862 0.629706 11.00000 0.04693 0.02430 = 0.05520 -0.00385 0.00627 -0.00236 AFIX 43 H42 2 0.607460 0.040617 0.628480 11.00000 -1.20000 AFIX 0 C43 1 0.526026 0.119822 0.644692 11.00000 0.04173 0.03159 = 0.04484 -0.00210 0.01182 -0.00774 AFIX 43 H43 2 0.454241 0.101563 0.653510 11.00000 -1.20000 AFIX 0 C44 1 0.540229 0.183036 0.646838 11.00000 0.03054 0.02739 = 0.03252 -0.00543 0.00790 0.00061 AFIX 43 H44 2 0.477600 0.208085 0.656841 11.00000 -1.20000 AFIX 0 C45 1 0.242104 0.252452 0.490576 11.00000 0.04999 0.08371 = 0.06294 0.03099 0.00608 -0.00696 C46 1 0.136812 0.159672 0.666937 11.00000 0.03619 0.05764 = 0.04552 -0.01447 0.00335 -0.00320 AU1 3 0.531504 0.434986 0.769473 11.00000 0.02209 0.02357 = 0.02063 0.00238 0.00338 -0.00294 AU2 3 0.488268 0.338231 0.646239 11.00000 0.02736 0.02186 = 0.03814 -0.00570 0.00200 0.00381 N1 5 0.506076 0.481494 0.684488 11.00000 0.02582 0.02066 = 0.01967 0.00124 0.00529 0.00037 N2 5 0.323560 0.375398 0.662289 11.00000 0.02281 0.02326 = 0.04015 -0.00132 0.00133 -0.00235 O7 6 0.256479 0.504982 0.481171 11.00000 0.02831 0.05343 = 0.02144 0.00114 0.00114 0.01075 O8 6 0.154670 0.494429 0.556787 11.00000 0.02890 0.09256 = 0.03046 0.01324 0.00320 0.00960 O9 6 0.066032 0.539337 0.687108 11.00000 0.03511 0.05608 = 0.05374 -0.01972 0.00720 0.01798 O10 6 0.264291 0.563397 0.688072 11.00000 0.05099 0.03179 = 0.05490 -0.00323 0.02182 0.00426 P1 7 0.542081 0.380030 0.855986 11.00000 0.02402 0.02337 = 0.02026 0.00155 0.00475 -0.00412 P2 7 0.665104 0.291898 0.639889 11.00000 0.02830 0.02239 = 0.02836 -0.00331 0.00535 0.00200 S1A 8 0.145637 0.079221 0.657103 10.80000 0.03595 S1B 8 0.146394 0.068905 0.688314 10.20000 0.04149 S2 8 0.237067 0.335138 0.477596 11.00000 0.03794 0.06241 = 0.04436 0.02156 0.01773 0.01354 PART 1 O5A 6 0.367276 0.362459 0.508487 10.50000 0.05837 O4A 6 0.204604 0.348508 0.416530 10.50000 0.06246 O6A 6 0.162743 0.362590 0.518970 10.50000 0.07906 F4A 4 0.144327 0.232542 0.468899 10.50000 0.12302 F5A 4 0.277547 0.245259 0.554588 10.50000 0.06955 F6A 4 0.351132 0.235578 0.478115 10.50000 0.09847 PART 2 O4B 6 0.107989 0.338869 0.434855 10.50000 0.06675 O5B 6 0.331762 0.340215 0.445856 10.50000 0.05978 O6B 6 0.249120 0.354823 0.534917 10.50000 0.06224 F6B 4 0.345080 0.230157 0.522881 10.50000 0.06983 F4B 4 0.211722 0.216482 0.438070 10.50000 0.05316 F5B 4 0.152734 0.232028 0.519694 10.50000 0.07373 PART 3 F3B 4 0.162608 0.165426 0.737115 10.20000 0.06437 F2B 4 0.244723 0.183765 0.691661 10.20000 0.05013 F1B 4 0.025371 0.169449 0.661159 10.20000 0.09363 O1A 6 0.278751 0.050630 0.687751 10.20000 0.02410 O2A 6 0.010200 0.063342 0.642898 10.20000 0.01696 O3A 6 0.164632 0.087379 0.752148 10.10000 0.05906 O7A 6 0.113030 0.046839 0.733633 10.10000 0.05142 PART 4 F1A 4 0.056269 0.187175 0.620787 10.80000 0.05656 F2A 4 0.245998 0.187139 0.667967 10.80000 0.05360 F3A 4 0.097355 0.178667 0.717168 10.80000 0.07382 O3B 6 0.234492 0.060405 0.710386 10.80000 0.07824 O1B 6 0.186946 0.076979 0.600171 10.80000 0.05245 O2B 6 0.032644 0.053006 0.655861 10.80000 0.08803 PART 0 HKLF 4 REM ns-327_150k_a.res in P2(1)/c REM R1 = 0.0334 for 11267 Fo > 4sig(Fo) and 0.0437 for all 13432 data REM 678 parameters refined using 36 restraints END WGHT 0.0300 9.1731 REM Highest difference peak 1.241, deepest hole -1.216, 1-sigma level 0.129 Q1 1 0.3289 0.2377 0.5500 11.00000 0.05 1.24 Q2 1 0.1846 0.0671 0.7222 11.00000 0.05 1.12 Q3 1 0.2822 0.2237 0.4568 11.00000 0.05 1.11 Q4 1 0.1073 0.2446 0.4910 11.00000 0.05 1.10 Q5 1 0.1407 0.1561 0.6111 11.00000 0.05 1.04 Q6 1 0.1799 0.2194 0.4614 11.00000 0.05 0.91 Q7 1 0.1365 0.0470 0.6735 11.00000 0.05 0.88 Q8 1 0.2754 0.0652 0.7057 11.00000 0.05 0.84 Q9 1 0.2285 0.2583 0.5573 11.00000 0.05 0.82 Q10 1 0.2050 0.1202 0.5891 11.00000 0.05 0.81 ; _shelx_res_checksum 66813 _shelx_hkl_file ; -1 0 0 6613.44 275.17 2 0 0 1097.29 57.59 -2 0 0 1130.99 58.59 -2 0 0 1105.09 53.69 -3 0 0 6819.52 290.67 -3 0 0 6815.42 298.77 3 0 0 6869.71 297.57 -4 0 0 2939.81 138.99 -4 0 0 3251.57 150.88 4 0 0 2789.82 145.69 -5 0 0 2690.33 138.19 5 0 0 2342.87 132.39 -5 0 0 2539.15 124.49 6 0 0 909.61 44.10 -6 0 0 906.91 38.00 6 0 0 858.31 37.70 -6 0 0 898.71 44.20 7 0 0 629.64 34.60 7 0 0 659.23 27.50 -7 0 0 633.54 27.80 -7 0 0 593.74 34.30 -8 0 0 670.63 29.80 8 0 0 732.53 29.60 8 0 0 665.63 37.70 -8 0 0 629.64 37.60 9 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1349.96 62.19 7 -4 -5 1166.98 53.69 7 -4 -5 1296.17 54.29 7 4 -5 1294.97 61.79 7 4 -5 1287.37 56.59 -7 4 5 1347.97 61.79 -6 -4 5 1971.50 85.79 -6 -4 5 2014.70 89.69 6 -4 -5 1990.00 89.29 6 -4 -5 2021.30 83.59 6 4 -5 2015.10 85.69 6 4 -5 1946.91 89.39 -6 4 5 2041.60 89.59 -5 -4 5 1613.54 69.99 5 -4 -5 1574.84 72.59 -5 -4 5 1659.73 72.89 5 -4 -5 1626.84 68.19 5 4 -5 1656.03 70.09 -5 4 5 1631.34 72.79 5 4 -5 1566.64 72.49 -4 -4 5 2938.71 157.98 4 -4 -5 2658.73 155.28 -4 -4 5 2969.60 145.49 4 4 -5 3151.98 147.09 -4 4 5 2929.51 145.79 -4 4 5 3274.77 161.68 -3 -4 5 3279.27 168.38 3 -4 -5 3358.86 169.98 -3 -4 5 3356.06 158.38 3 -4 -5 3420.26 159.68 -3 4 5 3420.16 169.98 3 4 -5 3424.76 168.48 3 4 -5 3537.65 160.08 -3 4 5 3354.56 158.68 2 -4 -5 3938.21 185.88 -2 -4 5 3717.23 175.58 2 -4 -5 3705.73 175.38 -2 -4 5 3895.71 184.28 -2 4 5 4249.77 177.18 -2 4 5 3826.82 184.18 2 4 -5 3891.01 176.48 2 4 -5 3990.20 184.28 -1 -4 5 2317.07 108.29 1 -4 -5 2118.29 112.49 1 -4 -5 2398.16 107.89 1 4 -5 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-5 28 15.40 7.80 1 -5 -28 6.00 5.80 -1 5 28 12.30 8.20 0 -5 28 78.29 13.70 0 -5 -28 65.89 12.20 0 5 -28 50.19 10.00 0 5 -28 62.19 11.50 0 5 28 63.69 20.80 -1 -5 -28 41.80 11.60 -1 -5 -28 44.70 10.80 1 5 28 78.99 15.00 -1 5 -28 50.09 11.10 -1 5 -28 53.09 10.70 -2 -5 -28 36.50 11.00 -2 -5 -28 40.40 11.00 -2 5 -28 49.00 10.60 -2 5 -28 48.60 10.50 -3 -5 -28 57.09 13.70 -3 5 -28 57.19 11.90 -3 5 -28 67.09 12.00 -4 5 -28 80.69 13.30 -4 5 -28 98.39 15.00 -10 -6 28 -4.50 4.90 9 -6 -28 4.10 5.40 -8 -6 28 -4.50 4.30 8 -6 -28 1.80 5.30 -8 6 28 0.50 7.10 7 -6 -28 34.50 8.80 -7 -6 28 30.10 10.10 -7 -6 28 34.10 9.80 -7 6 28 34.50 11.20 -6 -6 28 65.49 12.90 -6 -6 28 96.19 15.90 6 -6 -28 66.39 12.40 -6 6 28 55.59 13.70 -5 -6 28 67.69 13.40 5 -6 -28 53.99 11.40 -5 -6 28 58.59 11.30 -5 6 28 31.70 11.00 4 -6 -28 89.99 14.10 -4 -6 28 81.39 12.70 -4 -6 28 68.89 13.20 3 -6 -28 104.59 15.20 -3 -6 28 102.79 14.40 -3 -6 28 90.49 14.80 -3 6 28 101.09 20.80 -2 -6 28 109.79 14.70 -2 -6 28 120.99 16.80 2 -6 -28 110.59 16.30 -2 6 28 118.59 25.80 1 -6 -28 107.99 15.70 -1 -6 28 101.09 13.40 -1 -6 28 86.79 15.40 0 -6 28 157.18 19.60 0 -6 -28 172.78 19.80 0 6 -28 135.19 17.80 0 6 28 126.39 19.40 0 6 -28 117.69 15.10 -1 -6 -28 97.69 17.60 1 6 28 123.59 19.10 -1 6 -28 105.49 14.40 -1 6 -28 127.29 16.50 -2 -6 -28 97.89 18.10 -2 6 -28 114.29 15.70 -2 6 -28 98.49 14.40 -3 6 -28 75.59 12.60 -3 6 -28 45.60 10.20 -4 6 -28 50.79 10.80 -10 -7 28 10.90 7.60 9 -7 -28 37.40 11.10 8 -7 -28 42.20 10.00 -8 -7 28 36.40 10.10 -7 -7 28 22.90 13.00 7 -7 -28 19.70 8.10 -7 -7 28 6.00 6.30 -7 7 28 11.80 8.20 -6 -7 28 17.60 8.50 6 -7 -28 28.00 8.70 -6 -7 28 28.80 8.70 -6 7 28 50.19 13.80 5 -7 -28 23.40 8.60 -5 -7 28 16.10 8.20 -5 -7 28 34.10 8.80 -5 7 28 24.40 9.80 -4 -7 28 61.69 12.20 4 -7 -28 52.89 11.20 -4 -7 28 59.49 10.70 -4 7 28 37.70 11.30 -3 -7 28 45.50 9.60 3 -7 -28 31.30 9.70 -3 -7 28 48.20 11.10 -3 7 28 48.90 12.70 2 -7 -28 11.90 7.60 -2 -7 28 13.70 7.30 -2 7 28 17.70 8.80 1 -7 -28 8.50 6.80 -1 -7 28 27.30 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112.69 21.10 0 8 -28 59.09 10.10 0 8 28 58.99 13.60 1 -8 28 71.99 13.10 -1 -8 -28 74.09 15.70 -1 8 -28 73.39 11.60 1 8 28 72.89 15.00 -2 8 -28 54.79 11.20 -3 8 -28 45.80 9.70 -4 8 -28 12.20 7.00 -10 -9 28 -2.10 5.60 -9 -9 28 31.10 9.70 -8 -9 28 20.60 8.50 -7 -9 28 14.90 7.60 7 -9 -28 13.20 7.00 -6 -9 28 14.90 6.90 6 -9 -28 14.40 7.30 -6 9 28 10.60 8.00 -5 -9 28 32.80 10.40 -5 -9 28 16.50 6.70 5 -9 -28 20.00 8.70 -5 9 28 10.70 8.40 4 -9 -28 3.10 6.10 -4 -9 28 8.60 6.90 -4 9 28 9.70 7.50 -3 -9 28 27.00 7.20 -3 -9 28 19.40 8.60 3 -9 -28 13.10 7.50 -3 9 28 3.80 6.50 -2 -9 28 -5.00 2.60 2 -9 -28 5.60 6.40 -2 -9 28 3.50 5.40 -2 9 28 -7.10 4.60 -1 -9 28 15.30 7.30 1 -9 -28 -10.10 5.70 1 9 -28 0.90 3.30 -1 9 28 3.40 7.40 0 -9 28 3.80 6.20 0 9 -28 0.70 3.50 0 9 28 2.40 6.10 1 -9 28 3.90 6.20 -1 9 -28 6.70 5.00 2 -9 28 11.10 6.30 -2 9 -28 12.40 6.70 -3 9 -28 4.40 5.30 -10 -10 28 14.50 8.10 -9 -10 28 2.80 6.30 -8 -10 28 -0.60 5.00 -7 -10 28 3.80 5.10 6 -10 -28 0.70 6.30 -6 -10 28 2.20 5.00 5 -10 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5.90 -2 3 -29 16.10 9.70 -2 3 -29 5.20 5.10 -3 -3 -29 6.80 10.40 -3 3 -29 18.80 8.50 -4 3 -29 2.50 5.70 -9 -4 29 11.30 7.00 -8 -4 29 27.80 11.20 7 -4 -29 65.09 14.00 -7 -4 29 51.29 12.30 -7 4 29 62.59 14.00 6 -4 -29 86.49 14.40 -6 -4 29 76.49 16.20 -6 -4 29 104.79 16.10 -6 4 29 122.29 19.60 5 -4 -29 184.48 20.90 -5 -4 29 121.39 17.60 -5 -4 29 162.48 19.60 -5 4 29 176.18 23.20 -4 -4 29 132.79 17.70 -4 -4 29 160.98 19.90 4 -4 -29 164.88 19.50 -4 4 29 141.89 32.00 -3 -4 29 135.69 18.90 3 -4 -29 211.68 22.00 -3 -4 29 212.38 22.00 2 -4 -29 144.29 17.70 -2 -4 29 125.69 16.20 -2 -4 29 139.19 19.00 2 4 -29 144.59 18.80 -1 -4 29 121.29 15.70 1 -4 -29 119.99 16.20 1 4 -29 141.49 18.70 0 -4 -29 141.29 24.60 0 4 -29 183.98 21.00 0 4 29 184.38 22.60 0 4 -29 165.68 19.40 -1 -4 -29 163.68 21.90 -1 4 -29 140.69 18.20 -2 -4 -29 103.39 18.20 -2 4 -29 72.09 13.60 -3 4 -29 21.30 7.90 -4 4 -29 26.30 9.50 -9 -5 29 6.90 7.00 -7 -5 29 0.80 5.30 -7 5 29 -3.90 5.40 -6 -5 29 0.40 5.80 6 -5 -29 -6.90 3.60 -6 5 29 -4.70 5.00 -5 -5 29 -1.20 4.60 5 -5 -29 0.10 5.00 -5 -5 29 -4.00 4.70 -5 5 29 2.80 6.30 -4 -5 29 5.00 6.90 4 -5 -29 -4.00 4.90 -4 -5 29 8.60 5.90 -4 5 29 0.90 5.80 3 -5 -29 11.70 7.40 -3 -5 29 0.10 5.80 -3 -5 29 -4.90 4.20 -3 5 29 1.10 5.80 -2 -5 29 -1.80 5.60 2 -5 -29 8.10 6.40 -2 -5 29 1.10 4.70 -2 5 29 -0.40 6.10 1 -5 -29 -7.50 4.10 -1 -5 29 2.40 5.10 -1 -5 29 4.50 6.60 -1 5 29 5.80 7.00 1 5 -29 9.00 6.90 0 5 -29 0.70 5.80 0 5 -29 -2.30 3.40 0 5 29 -4.20 4.40 -1 -5 -29 1.80 4.90 -1 5 -29 -1.20 4.40 -1 5 -29 6.60 5.50 -2 5 -29 7.70 5.90 -3 5 -29 -0.10 3.80 -9 -6 29 7.40 6.50 -8 -6 29 27.10 9.30 -7 -6 29 16.40 7.60 -6 -6 29 41.00 10.70 6 -6 -29 31.60 12.80 -6 6 29 17.10 8.90 -5 -6 29 50.29 10.90 -5 -6 29 39.90 15.30 5 -6 -29 43.20 10.40 -5 6 29 34.40 11.90 4 -6 -29 64.59 12.10 -4 -6 29 64.19 11.90 -4 -6 29 47.90 11.70 -4 6 29 74.39 15.10 3 -6 -29 66.49 12.70 -3 -6 29 44.90 11.10 -3 -6 29 67.89 11.40 -3 6 29 46.80 11.90 -2 -6 29 79.49 14.00 2 -6 -29 110.89 17.60 -2 -6 29 90.89 13.10 -2 6 29 86.89 15.70 -1 -6 29 68.29 13.70 -1 -6 29 42.40 9.30 -1 6 29 89.29 16.50 0 -6 29 56.59 12.30 0 6 -29 56.29 11.70 0 6 -29 36.60 9.10 0 6 29 36.20 11.20 -1 -6 -29 54.99 13.20 -1 6 -29 27.60 8.00 -1 6 -29 26.00 9.10 -2 6 -29 27.40 8.40 -10 -7 29 96.49 22.70 -9 -7 29 47.80 12.10 -8 -7 29 43.30 10.30 -7 -7 29 49.00 11.30 -6 -7 29 21.70 8.20 -6 7 29 12.80 8.50 -5 -7 29 30.00 8.50 -5 7 29 20.60 10.10 -4 -7 29 14.10 6.80 -4 -7 29 24.30 11.30 -4 7 29 22.80 10.60 -3 -7 29 3.90 5.00 -3 -7 29 -0.40 5.20 -3 7 29 -5.50 4.80 -2 -7 29 7.60 6.40 -2 -7 29 1.50 4.40 -2 7 29 -5.40 4.50 -1 -7 29 10.10 7.30 -1 -7 29 -2.10 3.60 -1 7 29 7.10 7.50 1 7 -29 11.20 5.70 0 -7 29 35.60 10.20 0 7 29 32.80 11.10 0 7 -29 23.30 9.40 0 7 -29 23.80 7.20 -1 7 -29 5.10 4.60 -10 -8 29 -0.70 6.30 -9 -8 29 19.10 8.80 -8 -8 29 1.60 5.30 -7 -8 29 15.20 7.80 -6 -8 29 10.50 6.30 -5 -8 29 7.40 6.00 -5 8 29 11.90 9.30 -4 -8 29 26.80 7.60 -4 8 29 31.90 11.20 -3 -8 29 40.10 9.00 -3 8 29 62.09 14.40 -2 -8 29 43.70 13.60 -2 -8 29 56.19 11.20 -2 8 29 70.49 15.70 -1 -8 29 65.29 19.40 1 8 -29 24.90 7.00 -1 8 29 36.40 11.10 0 -8 29 46.60 17.20 0 8 -29 36.60 8.50 -10 -9 29 90.49 15.80 -9 -9 29 77.29 14.10 -8 -9 29 93.69 14.90 -7 -9 29 74.29 13.30 -6 -9 29 61.39 11.70 -5 -9 29 27.40 8.00 -4 -9 29 18.60 6.90 -3 9 29 -8.70 6.20 -2 -9 29 -0.30 3.70 1 9 -29 3.80 3.80 -10 -10 29 0.80 5.30 -9 -10 29 3.70 5.90 -8 -10 29 8.10 5.90 -7 -10 29 0.70 5.10 -6 -10 29 -2.00 4.20 -5 -10 29 37.20 9.00 -4 -10 29 25.80 8.60 -3 -10 29 7.30 4.70 -2 -10 29 45.40 8.50 -10 -11 29 5.00 6.30 -8 -11 29 -4.50 3.90 -7 -11 29 -5.70 4.10 -6 -11 29 1.50 4.20 -5 -11 29 4.10 4.50 -4 -11 29 4.90 4.80 -3 -11 29 -0.60 5.00 -10 -12 29 2.40 6.00 -8 -12 29 0.60 4.80 -7 -12 29 -6.80 3.00 -6 -12 29 6.80 5.10 -8 0 30 1.50 5.90 -7 0 30 4.30 6.90 -6 0 30 18.30 9.10 -4 0 30 12.40 7.30 -3 0 30 15.50 7.60 -2 0 30 35.80 10.50 -1 0 30 53.59 12.20 0 0 30 1.10 5.00 0 0 -30 -1.50 4.50 -1 0 -30 3.60 4.80 -2 0 -30 10.40 7.50 -3 0 -30 -1.60 4.30 -8 -1 30 5.30 6.50 -7 -1 30 4.10 6.70 -7 1 30 7.90 7.00 -6 1 30 0.50 6.00 -5 -1 30 -2.50 4.90 -5 1 30 7.50 7.10 -4 -1 30 -0.60 5.00 -4 1 30 2.80 8.30 -3 -1 30 -3.70 3.60 -3 1 30 -8.60 3.20 -2 -1 30 -2.00 4.10 -2 1 30 10.80 7.30 -1 -1 30 18.80 7.90 -1 1 30 1.00 5.60 0 -1 -30 24.40 8.80 0 1 -30 24.70 9.20 -1 -1 -30 14.30 7.20 -1 1 -30 14.60 8.60 -2 -1 -30 19.00 8.30 -2 1 -30 17.50 8.10 -3 1 -30 7.00 6.30 -8 -2 30 12.30 7.80 -7 -2 30 14.30 8.50 -7 2 30 3.20 6.60 -6 -2 30 17.40 9.50 -6 2 30 40.80 11.50 -5 -2 30 81.99 14.70 -5 2 30 74.79 14.80 -4 -2 30 51.09 11.10 -4 2 30 77.19 15.30 -3 -2 30 67.49 13.10 -2 -2 30 66.99 12.90 -1 -2 30 40.60 9.80 -1 2 30 36.80 12.50 0 2 30 21.90 8.50 0 2 -30 -0.20 4.20 -1 -2 -30 21.30 9.40 -1 2 -30 32.00 9.90 -2 -2 -30 38.20 11.50 -3 2 -30 22.10 8.60 -4 2 -30 -0.90 4.30 -8 -3 30 24.20 8.80 -7 -3 30 9.10 7.20 -7 3 30 19.20 9.50 -6 -3 30 14.80 8.30 -6 3 30 15.30 9.20 -5 -3 30 20.90 7.90 -5 3 30 0.00 5.80 -4 -3 30 3.70 5.40 -4 3 30 11.90 8.00 -3 -3 30 -3.70 4.20 -3 3 30 0.50 5.10 -2 -3 30 4.90 5.30 -2 3 30 1.10 5.20 -1 -3 30 12.30 11.40 -1 3 30 8.90 7.00 0 3 30 10.40 7.60 0 3 -30 3.80 5.00 -1 -3 -30 22.70 9.50 -1 3 -30 20.10 7.80 -2 3 -30 35.60 10.10 -3 3 -30 24.20 8.80 -9 -4 30 10.30 8.30 -8 -4 30 21.20 9.40 -6 -4 30 -0.90 5.40 -6 4 30 8.30 7.20 -5 -4 30 20.30 8.10 -5 4 30 13.60 8.30 -4 -4 30 6.50 6.60 -4 4 30 -1.40 5.70 -3 -4 30 4.30 5.70 -3 4 30 17.30 7.80 -2 -4 30 2.40 5.70 -2 4 30 -0.70 6.00 -1 -4 30 4.60 5.40 -1 4 30 3.60 6.20 0 4 -30 1.40 4.60 0 4 30 -1.60 5.00 -1 -4 -30 0.80 9.20 -1 4 -30 2.60 4.90 -2 4 -30 -2.40 4.00 -3 4 -30 1.00 6.20 -9 -5 30 53.59 13.10 -8 -5 30 39.30 11.50 -7 -5 30 32.40 11.30 -6 -5 30 45.80 11.00 -5 -5 30 31.60 8.90 -5 5 30 25.90 10.20 -4 -5 30 35.90 9.50 -4 5 30 35.60 11.10 -3 -5 30 5.10 5.50 -3 5 30 15.10 9.10 -2 -5 30 -5.40 3.50 -2 5 30 -3.00 5.10 -1 -5 30 -1.70 4.10 -1 5 30 1.30 6.10 0 5 -30 -2.30 3.60 0 5 30 3.60 6.50 -1 5 -30 15.60 6.70 -2 5 -30 22.80 7.90 -9 -6 30 34.60 11.10 -8 -6 30 41.60 11.00 -7 -6 30 43.40 11.40 -6 -6 30 60.89 12.00 -5 -6 30 101.69 14.90 -5 6 30 118.19 27.40 -4 -6 30 101.09 14.90 -4 6 30 116.49 19.30 -3 -6 30 72.49 12.20 -3 6 30 91.39 16.60 -2 -6 30 108.59 14.10 -2 6 30 78.99 15.10 -1 -6 30 135.79 16.40 -1 6 30 140.19 21.20 1 6 -30 115.19 15.30 0 6 -30 63.59 11.50 -1 6 -30 50.79 10.20 -9 -7 30 5.30 7.00 -8 -7 30 7.70 6.90 -7 -7 30 3.50 5.80 -6 -7 30 2.60 5.30 -5 -7 30 1.00 4.70 -4 -7 30 -1.90 3.90 -3 -7 30 4.80 5.40 -2 -7 30 -3.90 3.50 1 7 -30 6.90 5.30 0 7 -30 47.00 10.00 -9 -8 30 4.50 6.50 -7 -8 30 29.20 9.50 -6 -8 30 45.70 10.30 -5 -8 30 79.09 12.80 -4 -8 30 70.79 12.00 -3 -8 30 65.99 11.10 -2 -8 30 68.39 10.80 1 8 -30 82.89 12.50 -9 -9 30 25.90 9.30 -8 -9 30 13.90 12.40 -7 -9 30 2.80 5.50 -6 -9 30 6.10 5.90 -5 -9 30 6.50 5.80 -4 -9 30 -3.30 3.70 -3 -9 30 9.60 5.70 -2 -9 30 12.20 5.90 -9 -10 30 6.90 6.10 -8 -10 30 0.90 5.10 -7 -10 30 7.80 5.90 -6 -10 30 3.80 5.30 -5 -10 30 12.80 5.90 -4 -10 30 20.90 6.80 -9 -11 30 53.19 11.90 -8 -11 30 38.30 10.40 -7 -11 30 58.19 11.90 -6 -11 30 24.10 9.40 -7 0 31 0.20 5.50 -6 0 31 1.70 5.20 -5 0 31 -2.20 5.40 -4 0 31 -9.40 4.00 -3 0 31 0.50 5.30 -2 0 31 -3.40 4.80 -1 0 31 6.10 6.40 0 0 -31 1.70 5.20 -1 0 -31 1.30 5.60 -2 0 -31 2.10 6.40 -7 -1 31 13.00 7.80 -6 -1 31 5.70 6.50 -6 1 31 -3.60 4.30 -5 -1 31 0.80 5.40 -5 1 31 7.40 6.50 -4 1 31 5.30 7.10 -3 -1 31 4.70 7.70 -3 1 31 2.50 6.30 -2 -1 31 23.70 9.30 -2 1 31 28.20 10.10 -1 -1 31 74.29 20.00 -1 1 31 57.29 12.50 0 -1 -31 22.10 8.90 0 1 -31 45.30 11.00 -1 -1 -31 38.40 11.10 -1 1 -31 41.70 10.50 -2 1 -31 40.20 10.70 -7 -2 31 0.80 6.20 -6 -2 31 8.40 6.80 -6 2 31 -2.00 4.70 -5 -2 31 -1.30 5.50 -5 2 31 -1.00 5.10 -4 -2 31 17.00 8.20 -4 2 31 1.10 5.70 -3 -2 31 17.80 7.30 -3 2 31 -0.90 4.90 -2 -2 31 21.00 8.20 -2 2 31 26.90 10.10 -1 -2 31 6.70 6.50 -1 2 31 11.20 7.30 0 -2 -31 21.40 8.40 0 2 31 38.60 10.60 -1 2 -31 13.10 7.20 -2 2 -31 -2.20 4.30 -3 2 -31 16.70 9.00 -8 -3 31 53.69 19.50 -7 -3 31 -3.80 5.00 -6 -3 31 13.40 7.50 -5 -3 31 19.60 8.80 -5 3 31 16.10 8.30 -4 -3 31 11.70 7.20 -4 3 31 22.50 9.70 -3 -3 31 15.60 7.50 -3 3 31 16.00 8.60 -2 -3 31 12.40 6.90 -2 3 31 -1.10 5.30 -1 -3 31 8.30 5.80 -1 3 31 0.00 5.80 0 3 -31 -1.50 7.20 0 3 31 -5.40 4.30 -2 3 -31 4.60 5.80 -8 -4 31 28.50 10.50 -7 -4 31 29.40 9.90 -5 -4 31 97.39 15.70 -4 -4 31 50.39 11.40 -4 4 31 48.30 14.60 -3 -4 31 79.69 13.50 -3 4 31 104.49 17.80 -2 -4 31 133.99 17.00 -2 4 31 99.39 17.40 -1 -4 31 71.19 12.60 0 4 -31 60.89 11.70 -1 4 -31 43.10 10.10 -8 -5 31 8.40 7.30 -7 -5 31 3.90 6.40 -6 -5 31 -2.00 5.20 -5 -5 31 14.80 7.50 -4 -5 31 0.70 5.00 -3 -5 31 1.60 4.80 -2 -5 31 -1.20 3.90 1 5 -31 6.90 5.40 0 5 -31 9.00 6.10 -1 5 -31 7.80 7.00 -8 -6 31 34.20 10.50 -7 -6 31 36.30 10.50 -6 -6 31 38.40 10.10 -5 -6 31 62.59 12.50 -4 -6 31 12.30 6.50 -3 -6 31 23.50 7.30 -2 -6 31 18.40 6.90 1 6 -31 26.10 8.00 0 6 -31 11.40 6.60 -8 -7 31 93.09 15.80 -6 -7 31 18.30 7.50 -5 -7 31 35.50 9.90 -4 -7 31 13.30 6.50 -3 -7 31 -0.50 4.30 -2 -7 31 3.10 4.30 -8 -8 31 -0.90 5.80 -7 -8 31 1.50 5.50 -6 -8 31 7.30 6.20 -5 -8 31 8.20 6.10 -4 -8 31 5.40 5.50 -3 -8 31 14.40 6.60 -2 -8 31 8.30 8.80 -8 -9 31 0.60 6.00 -7 -9 31 0.50 5.00 -6 -9 31 -4.60 3.60 -5 -9 31 3.70 5.30 -4 -9 31 6.20 5.80 -8 -10 31 2.30 8.20 -7 -10 31 9.50 10.80 -5 0 32 58.79 12.90 -4 0 32 35.70 10.10 -3 0 32 24.20 9.20 -2 0 32 58.29 12.50 -1 0 32 105.79 16.90 0 0 -32 69.49 17.10 -6 -1 32 4.20 6.60 -5 -1 32 2.90 5.50 -4 -1 32 19.50 8.20 -4 1 32 8.60 6.80 -3 -1 32 18.30 8.30 -3 1 32 9.90 7.80 -2 -1 32 34.70 9.70 -2 1 32 27.80 9.70 -1 -1 32 12.50 7.80 -1 1 32 30.20 10.00 0 1 -32 9.80 7.10 -1 1 -32 48.80 18.90 -6 -2 32 2.90 6.00 -5 -2 32 24.50 8.40 -4 -2 32 20.00 8.50 -3 -2 32 11.10 6.80 -2 -2 32 42.30 11.10 -1 -2 32 18.50 7.50 0 2 -32 4.60 5.50 -1 2 -32 0.70 5.30 -6 -3 32 6.40 6.90 -5 -3 32 13.30 7.50 -4 -3 32 8.70 6.90 1 3 -32 20.40 8.00 0 3 -32 21.30 7.80 -1 3 -32 20.10 8.00 -7 -4 32 3.70 6.20 -6 -4 32 0.50 5.40 -5 -4 32 -2.40 4.90 -3 -4 32 5.10 5.20 -2 -4 32 5.50 5.10 -7 -5 32 30.30 9.90 -6 -5 32 29.90 9.60 -4 -5 32 2.20 5.30 -3 -5 32 -1.60 4.10 -2 -5 32 -3.70 4.20 1 5 -32 6.90 5.40 -7 -6 32 42.40 11.00 -6 -6 32 22.10 8.60 -5 -6 32 15.00 7.90 -4 -6 32 36.30 9.30 -3 -6 32 29.30 8.70 -2 -6 32 8.80 6.20 -7 -7 32 8.70 6.50 -5 -7 32 19.20 7.40 -4 -7 32 9.40 6.90 -3 -7 32 27.50 8.40 -8 -8 32 18.80 8.50 -7 -8 32 31.60 9.60 -6 -8 32 36.60 10.10 -5 -8 32 52.99 11.70 -3 -1 33 34.40 11.10 -2 -1 33 4.30 6.40 -4 -2 33 43.90 11.60 -3 -2 33 77.59 14.10 -2 -2 33 52.39 12.00 1 2 -33 18.00 8.50 -5 -3 33 12.10 7.20 -4 -3 33 -1.00 5.50 -3 -3 33 5.90 6.90 -2 -3 33 -2.00 4.70 1 3 -33 0.60 5.00 -5 -4 33 15.70 7.40 -4 -4 33 18.90 8.00 -3 -4 33 45.90 11.10 -2 -4 33 14.40 7.30 -6 -5 33 20.80 8.30 -5 -5 33 16.30 7.70 -4 -5 33 0.00 4.60 -3 -5 33 1.10 6.50 -6 -6 33 23.30 8.10 -5 -6 33 11.30 6.80 -7 -7 33 0.30 8.00 -6 -7 33 5.00 8.10 -3 -4 34 9.00 7.20 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 30192 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.4265(4) 0.40504(17) 0.89584(19) 0.0248(8) Uani 1 1 d . . . . . C00G C 0.8592(4) 0.2625(2) 0.7436(2) 0.0321(9) Uani 1 1 d . . . . . H00G H 0.851220 0.221320 0.729560 0.039 Uiso 1 1 calc R U . . . C00H C 0.8015(4) 0.36863(19) 0.7302(2) 0.0305(9) Uani 1 1 d . . . . . H00H H 0.753627 0.400272 0.706456 0.037 Uiso 1 1 calc R U . . . C00I C 0.7862(4) 0.30816(18) 0.70897(19) 0.0257(8) Uani 1 1 d . . . . . C2 C 0.3107(4) 0.4236(2) 0.8601(2) 0.0323(9) Uani 1 1 d . . . . . H2 H 0.294559 0.422355 0.816089 0.039 Uiso 1 1 calc R U . . . C01F C 0.9446(4) 0.2775(2) 0.7993(2) 0.0406(11) Uani 1 1 d . . . . . H01F H 0.994943 0.246413 0.822641 0.049 Uiso 1 1 calc R U . . . C01G C 0.9561(5) 0.3372(2) 0.8207(2) 0.0416(11) Uani 1 1 d . . . . . H01G H 1.011912 0.346836 0.859152 0.050 Uiso 1 1 calc R U . . . C3 C 0.2192(4) 0.4439(2) 0.8884(2) 0.0382(11) Uani 1 1 d . . . . . H3 H 0.140463 0.456358 0.863800 0.046 Uiso 1 1 calc R U . . . C4 C 0.2425(5) 0.4460(2) 0.9518(3) 0.0437(12) Uani 1 1 d . . . . . H4 H 0.179687 0.460176 0.971065 0.052 Uiso 1 1 calc R U . . . C5 C 0.3561(5) 0.4278(3) 0.9879(3) 0.0533(14) Uani 1 1 d . . . . . H5 H 0.371482 0.429301 1.031860 0.064 Uiso 1 1 calc R U . . . C6 C 0.4489(4) 0.4070(2) 0.9595(2) 0.0396(11) Uani 1 1 d . . . . . H6 H 0.527318 0.394289 0.984296 0.047 Uiso 1 1 calc R U . . . C7 C 0.6932(3) 0.38236(18) 0.90965(18) 0.0232(8) Uani 1 1 d . . . . . C8 C 0.7640(4) 0.43509(19) 0.9127(2) 0.0285(9) Uani 1 1 d . . . . . H8 H 0.731022 0.469768 0.888429 0.034 Uiso 1 1 calc R U . . . C9 C 0.8823(4) 0.4372(2) 0.9509(2) 0.0346(10) Uani 1 1 d . . . . . H9 H 0.930246 0.473619 0.953354 0.042 Uiso 1 1 calc R U . . . C10 C 0.9316(4) 0.3865(2) 0.9857(2) 0.0369(10) Uani 1 1 d . . . . . H10 H 1.013622 0.387948 1.011449 0.044 Uiso 1 1 calc R U . . . C11 C 0.8619(4) 0.3340(2) 0.9828(2) 0.0415(11) Uani 1 1 d . . . . . H11 H 0.895777 0.299371 1.006848 0.050 Uiso 1 1 calc R U . . . C12 C 0.7420(4) 0.3315(2) 0.9451(2) 0.0334(10) Uani 1 1 d . . . . . H12 H 0.693677 0.295319 0.943374 0.040 Uiso 1 1 calc R U . . . C13 C 0.5119(4) 0.30056(19) 0.83573(18) 0.0275(8) Uani 1 1 d . . . . . C14 C 0.6032(4) 0.2683(2) 0.8141(2) 0.0345(10) Uani 1 1 d . . . . . H14 H 0.678072 0.288160 0.811380 0.041 Uiso 1 1 calc R U . . . C014 C 0.8857(4) 0.3830(2) 0.7856(2) 0.0373(11) Uani 1 1 d . . . . . H014 H 0.895081 0.424220 0.799492 0.045 Uiso 1 1 calc R U . . . C15 C 0.5837(5) 0.2078(2) 0.7970(2) 0.0417(11) Uani 1 1 d . . . . . H15 H 0.645558 0.186124 0.782430 0.050 Uiso 1 1 calc R U . . . C16 C 0.4758(6) 0.1783(2) 0.8007(2) 0.0480(13) Uani 1 1 d . . . . . H16 H 0.463141 0.136703 0.788420 0.058 Uiso 1 1 calc R U . . . C17 C 0.3858(5) 0.2095(2) 0.8224(3) 0.0486(13) Uani 1 1 d . . . . . H17 H 0.311354 0.189074 0.825007 0.058 Uiso 1 1 calc R U . . . C18 C 0.4038(5) 0.2707(2) 0.8404(2) 0.0380(10) Uani 1 1 d . . . . . H18 H 0.342288 0.291787 0.855711 0.046 Uiso 1 1 calc R U . . . C19 C 0.2456(4) 0.3368(2) 0.6808(3) 0.0435(12) Uani 1 1 d . . . . . H19 H 0.262319 0.294081 0.681224 0.052 Uiso 1 1 calc R U . . . C20 C 0.1429(4) 0.3567(3) 0.6993(3) 0.0476(13) Uani 1 1 d . . . . . H20 H 0.088376 0.328181 0.711413 0.057 Uiso 1 1 calc R U . . . C21 C 0.1196(4) 0.4183(2) 0.6999(2) 0.0354(10) Uani 1 1 d . . . . . H21 H 0.048763 0.432893 0.712716 0.043 Uiso 1 1 calc R U . . . C22 C 0.2003(4) 0.45910(19) 0.68183(18) 0.0257(8) Uani 1 1 d . . . . . C23 C 0.3012(4) 0.43592(17) 0.66238(18) 0.0237(8) Uani 1 1 d . . . . . C24 C 0.1828(4) 0.5265(2) 0.68555(19) 0.0324(10) Uani 1 1 d . . . . . C25 C 0.0404(6) 0.6036(3) 0.6946(3) 0.075(2) Uani 1 1 d . . . . . H01R H 0.057910 0.627011 0.660023 0.113 Uiso 1 1 calc R U . . . H01S H 0.093389 0.618592 0.733770 0.113 Uiso 1 1 calc R U . . . H25 H -0.047301 0.608760 0.695236 0.113 Uiso 1 1 calc R U . . . C26 C 0.3954(3) 0.47554(17) 0.64268(18) 0.0222(8) Uani 1 1 d . . . . . C27 C 0.5968(4) 0.51507(18) 0.66998(19) 0.0271(8) Uani 1 1 d . . . . . H27 H 0.672981 0.520346 0.700222 0.033 Uiso 1 1 calc R U . . . C28 C 0.5830(4) 0.54208(19) 0.6128(2) 0.0284(9) Uani 1 1 d . . . . . H28 H 0.649031 0.565241 0.603579 0.034 Uiso 1 1 calc R U . . . C29 C 0.4718(4) 0.53506(19) 0.56881(19) 0.0287(9) Uani 1 1 d . . . . . H29 H 0.461265 0.552529 0.528707 0.034 Uiso 1 1 calc R U . . . C30 C 0.3754(4) 0.50215(19) 0.58395(18) 0.0264(8) Uani 1 1 d . . . . . C31 C 0.2491(4) 0.4990(2) 0.5401(2) 0.0327(10) Uani 1 1 d . . . . . C32 C 0.1381(4) 0.5027(3) 0.4356(2) 0.0424(12) Uani 1 1 d . . . . . H01C H 0.150858 0.512532 0.394556 0.064 Uiso 1 1 calc R U . . . H01H H 0.080669 0.532419 0.446663 0.064 Uiso 1 1 calc R U . . . H01N H 0.102714 0.461466 0.434929 0.064 Uiso 1 1 calc R U . . . C33 C 0.7260(5) 0.3143(2) 0.5745(2) 0.0368(10) Uani 1 1 d . U . . . C34 C 0.6425(7) 0.3206(2) 0.5168(2) 0.0547(14) Uani 1 1 d . U . . . H34 H 0.555436 0.315947 0.512582 0.066 Uiso 1 1 calc R U . . . C35 C 0.6898(9) 0.3338(3) 0.4655(3) 0.0739(19) Uani 1 1 d . U . . . H35 H 0.634533 0.337159 0.425614 0.089 Uiso 1 1 calc R U . . . C36 C 0.8148(10) 0.3421(3) 0.4717(3) 0.082(2) Uani 1 1 d . U . . . H36 H 0.844585 0.351796 0.436168 0.098 Uiso 1 1 calc R U . . . C37 C 0.8981(8) 0.3367(3) 0.5283(3) 0.0751(18) Uani 1 1 d . U . . . H37 H 0.984795 0.342459 0.532271 0.090 Uiso 1 1 calc R U . . . C38 C 0.8517(6) 0.3226(2) 0.5799(3) 0.0532(13) Uani 1 1 d . U . . . H38 H 0.907847 0.318673 0.619448 0.064 Uiso 1 1 calc R U . . . C39 C 0.6456(4) 0.20976(18) 0.63442(18) 0.0253(8) Uani 1 1 d . . . . . C40 C 0.7355(4) 0.1727(2) 0.6179(2) 0.0340(10) Uani 1 1 d . . . . . H40 H 0.806228 0.190692 0.607804 0.041 Uiso 1 1 calc R U . . . C41 C 0.7217(5) 0.1103(2) 0.6163(3) 0.0438(12) Uani 1 1 d . . . . . H41 H 0.783851 0.085078 0.606090 0.053 Uiso 1 1 calc R U . . . C42 C 0.6167(5) 0.0839(2) 0.6297(3) 0.0432(12) Uani 1 1 d . . . . . H42 H 0.607460 0.040617 0.628480 0.052 Uiso 1 1 calc R U . . . C43 C 0.5260(5) 0.1198(2) 0.6447(2) 0.0391(11) Uani 1 1 d . . . . . H43 H 0.454241 0.101563 0.653510 0.047 Uiso 1 1 calc R U . . . C44 C 0.5402(4) 0.18304(19) 0.6468(2) 0.0301(9) Uani 1 1 d . . . . . H44 H 0.477600 0.208085 0.656841 0.036 Uiso 1 1 calc R U . . . C45 C 0.2421(6) 0.2525(3) 0.4906(3) 0.0668(18) Uani 1 1 d . . . . . C46 C 0.1368(5) 0.1597(3) 0.6669(3) 0.0475(13) Uani 1 1 d . . . . . Au1 Au 0.53150(2) 0.43499(2) 0.76947(2) 0.02239(4) Uani 1 1 d . . . . . Au2 Au 0.48827(2) 0.33823(2) 0.64624(2) 0.03012(5) Uani 1 1 d . . . . . N1 N 0.5061(3) 0.48149(14) 0.68449(14) 0.0221(6) Uani 1 1 d . . . . . N2 N 0.3236(3) 0.37540(15) 0.66229(17) 0.0298(8) Uani 1 1 d . . . . . O7 O 0.2565(3) 0.50498(15) 0.48117(13) 0.0352(7) Uani 1 1 d . . . . . O8 O 0.1547(3) 0.4944(2) 0.55679(16) 0.0513(10) Uani 1 1 d . . . . . O9 O 0.0660(3) 0.53934(17) 0.68711(17) 0.0489(9) Uani 1 1 d . . . . . O10 O 0.2643(3) 0.56340(15) 0.68807(18) 0.0443(8) Uani 1 1 d . . . . . P1 P 0.54208(9) 0.38003(5) 0.85599(5) 0.0226(2) Uani 1 1 d . . . . . P2 P 0.66510(10) 0.29190(5) 0.63989(5) 0.0266(2) Uani 1 1 d . . . . . S1A S 0.14564(14) 0.07922(7) 0.65710(8) 0.0359(3) Uiso 0.8 1 d . . P C . S1B S 0.1464(6) 0.0689(3) 0.6883(4) 0.0415(14) Uiso 0.2 1 d . . P C . S2 S 0.23707(12) 0.33514(7) 0.47760(6) 0.0469(3) Uani 1 1 d . . . . . O5A O 0.3673(8) 0.3625(4) 0.5085(4) 0.058(2) Uiso 0.5 1 d . . P A 1 O4A O 0.2046(8) 0.3485(4) 0.4165(4) 0.062(2) Uiso 0.5 1 d . . P A 1 O6A O 0.1627(10) 0.3626(5) 0.5190(5) 0.079(3) Uiso 0.5 1 d . . P A 1 F4A F 0.1443(12) 0.2325(6) 0.4689(6) 0.123(4) Uiso 0.5 1 d . . P B 1 F5A F 0.2775(7) 0.2453(3) 0.5546(4) 0.0695(19) Uiso 0.5 1 d . . P B 1 F6A F 0.3511(9) 0.2356(5) 0.4781(5) 0.098(3) Uiso 0.5 1 d . . P B 1 O4B O 0.1080(9) 0.3389(4) 0.4349(4) 0.067(2) Uiso 0.5 1 d . . P A 2 O5B O 0.3318(8) 0.3402(4) 0.4459(4) 0.060(2) Uiso 0.5 1 d . . P A 2 O6B O 0.2491(9) 0.3548(4) 0.5349(4) 0.062(2) Uiso 0.5 1 d . . P A 2 F6B F 0.3451(7) 0.2302(4) 0.5229(4) 0.070(2) Uiso 0.5 1 d . . P B 2 F4B F 0.2117(6) 0.2165(3) 0.4381(3) 0.0532(15) Uiso 0.5 1 d . . P B 2 F5B F 0.1527(7) 0.2320(4) 0.5197(4) 0.074(2) Uiso 0.5 1 d . . P B 2 F3B F 0.1626(19) 0.1654(8) 0.7371(9) 0.064(5) Uiso 0.2 1 d . . P C 3 F2B F 0.2447(16) 0.1838(8) 0.6917(9) 0.050(5) Uiso 0.2 1 d . . P C 3 F1B F 0.025(2) 0.1694(11) 0.6612(12) 0.094(7) Uiso 0.2 1 d . . P C 3 O1A O 0.2788(13) 0.0506(6) 0.6878(7) 0.024(3) Uiso 0.2 1 d . . P C 3 O2A O 0.0102(14) 0.0633(7) 0.6429(7) 0.017(3) Uiso 0.2 1 d . . P C 3 O3A O 0.165(4) 0.087(2) 0.752(2) 0.059(10) Uiso 0.1 1 d . . P C 3 O7A O 0.113(4) 0.0468(18) 0.7336(18) 0.051(9) Uiso 0.1 1 d . . P C 3 F1A F 0.0563(4) 0.18718(19) 0.6208(2) 0.0566(10) Uiso 0.8 1 d . . P C 4 F2A F 0.2460(4) 0.1871(2) 0.6680(2) 0.0536(12) Uiso 0.8 1 d . . P C 4 F3A F 0.0974(5) 0.1787(2) 0.7172(3) 0.0738(13) Uiso 0.8 1 d . . P C 4 O3B O 0.2345(7) 0.0604(3) 0.7104(3) 0.0782(18) Uiso 0.8 1 d . . P C 4 O1B O 0.1869(5) 0.0770(2) 0.6002(2) 0.0525(12) Uiso 0.8 1 d . . P C 4 O2B O 0.0326(8) 0.0530(4) 0.6559(4) 0.088(3) Uiso 0.8 1 d . . P C 4 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.025(2) 0.0213(18) 0.029(2) 0.0003(16) 0.0095(16) -0.0027(15) C00G 0.032(2) 0.031(2) 0.033(2) -0.0030(18) 0.0066(18) -0.0022(17) C00H 0.029(2) 0.028(2) 0.039(2) -0.0041(18) 0.0165(18) -0.0021(16) C00I 0.026(2) 0.026(2) 0.027(2) -0.0036(16) 0.0112(16) -0.0031(15) C2 0.027(2) 0.034(2) 0.035(2) -0.0024(19) 0.0055(18) -0.0039(17) C01F 0.034(2) 0.044(3) 0.039(3) 0.000(2) 0.002(2) -0.004(2) C01G 0.039(3) 0.050(3) 0.034(3) -0.013(2) 0.006(2) -0.012(2) C3 0.024(2) 0.034(2) 0.055(3) -0.002(2) 0.007(2) -0.0021(18) C4 0.035(3) 0.046(3) 0.058(3) -0.010(2) 0.025(2) -0.001(2) C5 0.052(3) 0.078(4) 0.035(3) -0.006(3) 0.021(2) 0.010(3) C6 0.035(2) 0.057(3) 0.027(2) 0.000(2) 0.0087(19) 0.010(2) C7 0.0223(19) 0.0274(19) 0.0201(18) -0.0008(15) 0.0057(14) -0.0028(15) C8 0.029(2) 0.025(2) 0.030(2) -0.0047(17) 0.0048(17) -0.0021(16) C9 0.031(2) 0.037(2) 0.034(2) -0.0094(19) 0.0049(18) -0.0052(18) C10 0.025(2) 0.055(3) 0.026(2) -0.001(2) -0.0017(17) 0.003(2) C11 0.037(3) 0.047(3) 0.037(3) 0.015(2) 0.000(2) 0.005(2) C12 0.035(2) 0.032(2) 0.031(2) 0.0096(18) 0.0051(18) -0.0020(18) C13 0.037(2) 0.027(2) 0.0180(18) 0.0020(16) 0.0054(16) -0.0059(17) C14 0.043(3) 0.032(2) 0.032(2) -0.0012(19) 0.0146(19) -0.0028(19) C014 0.036(2) 0.037(2) 0.043(3) -0.016(2) 0.018(2) -0.013(2) C15 0.070(3) 0.030(2) 0.028(2) -0.0021(19) 0.018(2) 0.000(2) C16 0.083(4) 0.026(2) 0.036(3) -0.002(2) 0.016(3) -0.014(2) C17 0.058(3) 0.038(3) 0.052(3) -0.005(2) 0.020(3) -0.028(2) C18 0.046(3) 0.034(2) 0.037(3) -0.001(2) 0.016(2) -0.011(2) C19 0.029(2) 0.029(2) 0.066(4) 0.003(2) -0.001(2) -0.0075(18) C20 0.025(2) 0.052(3) 0.062(4) 0.008(3) 0.005(2) -0.016(2) C21 0.020(2) 0.048(3) 0.037(2) 0.007(2) 0.0038(17) -0.0030(18) C22 0.0236(19) 0.033(2) 0.0199(19) 0.0008(16) 0.0030(15) 0.0028(16) C23 0.0220(19) 0.0237(19) 0.0228(19) 0.0000(15) 0.0000(14) 0.0006(14) C24 0.033(2) 0.040(2) 0.023(2) -0.0044(18) 0.0043(17) 0.0139(19) C25 0.066(4) 0.073(4) 0.082(5) -0.032(4) 0.009(3) 0.038(3) C26 0.0238(19) 0.0197(18) 0.0234(19) -0.0054(15) 0.0060(14) 0.0048(14) C27 0.029(2) 0.026(2) 0.027(2) -0.0008(16) 0.0089(16) -0.0018(16) C28 0.030(2) 0.027(2) 0.031(2) -0.0003(17) 0.0132(17) -0.0019(16) C29 0.036(2) 0.030(2) 0.022(2) 0.0050(17) 0.0104(16) 0.0084(17) C30 0.029(2) 0.032(2) 0.0198(19) -0.0022(16) 0.0074(15) 0.0060(16) C31 0.033(2) 0.040(2) 0.024(2) 0.0036(18) 0.0034(17) 0.0105(19) C32 0.037(3) 0.061(3) 0.022(2) 0.002(2) -0.0065(18) 0.008(2) C33 0.060(3) 0.023(2) 0.030(2) -0.0031(17) 0.014(2) 0.0006(19) C34 0.097(4) 0.033(2) 0.030(2) -0.002(2) 0.008(3) 0.014(3) C35 0.157(6) 0.031(3) 0.032(3) 0.002(2) 0.021(4) 0.019(3) C36 0.164(6) 0.042(3) 0.059(4) -0.001(3) 0.067(4) -0.004(4) C37 0.119(5) 0.056(3) 0.073(4) -0.011(3) 0.066(4) -0.017(3) C38 0.078(4) 0.044(3) 0.049(3) -0.012(2) 0.036(3) -0.011(3) C39 0.027(2) 0.0240(19) 0.0231(19) -0.0025(16) 0.0031(15) 0.0024(15) C40 0.029(2) 0.029(2) 0.045(3) -0.010(2) 0.0113(19) 0.0002(17) C41 0.042(3) 0.030(2) 0.059(3) -0.012(2) 0.011(2) 0.007(2) C42 0.047(3) 0.024(2) 0.055(3) -0.004(2) 0.006(2) -0.002(2) C43 0.042(3) 0.032(2) 0.045(3) -0.002(2) 0.012(2) -0.008(2) C44 0.031(2) 0.027(2) 0.033(2) -0.0054(18) 0.0079(17) 0.0006(17) C45 0.050(4) 0.084(5) 0.063(4) 0.031(4) 0.006(3) -0.007(3) C46 0.036(3) 0.058(3) 0.046(3) -0.014(3) 0.003(2) -0.003(2) Au1 0.02209(8) 0.02357(8) 0.02063(7) 0.00238(6) 0.00338(5) -0.00294(5) Au2 0.02736(9) 0.02186(8) 0.03814(10) -0.00570(7) 0.00200(7) 0.00381(6) N1 0.0258(17) 0.0207(16) 0.0197(16) 0.0012(13) 0.0053(12) 0.0004(12) N2 0.0228(17) 0.0233(17) 0.040(2) -0.0013(15) 0.0013(15) -0.0024(13) O7 0.0283(16) 0.053(2) 0.0214(15) 0.0011(14) 0.0011(12) 0.0107(14) O8 0.0289(18) 0.093(3) 0.0305(18) 0.0132(18) 0.0032(14) 0.0096(18) O9 0.0351(18) 0.056(2) 0.054(2) -0.0197(18) 0.0072(16) 0.0180(16) O10 0.051(2) 0.0318(17) 0.055(2) -0.0032(16) 0.0218(18) 0.0043(15) P1 0.0240(5) 0.0234(5) 0.0203(5) 0.0015(4) 0.0047(4) -0.0041(4) P2 0.0283(5) 0.0224(5) 0.0284(5) -0.0033(4) 0.0054(4) 0.0020(4) S2 0.0379(7) 0.0624(8) 0.0444(7) 0.0216(6) 0.0177(5) 0.0135(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C6 C1 C2 119.4(4) . . ? C6 C1 P1 122.6(3) . . ? C2 C1 P1 118.0(3) . . ? C00I C00G C01F 119.9(4) . . ? C00I C00G H00G 120.1 . . ? C01F C00G H00G 120.1 . . ? C014 C00H C00I 120.8(4) . . ? C014 C00H H00H 119.6 . . ? C00I C00H H00H 119.6 . . ? C00G C00I C00H 118.8(4) . . ? C00G C00I P2 122.7(3) . . ? C00H C00I P2 118.4(3) . . ? C3 C2 C1 120.3(4) . . ? C3 C2 H2 119.8 . . ? C1 C2 H2 119.8 . . ? C01G C01F C00G 120.6(5) . . ? C01G C01F H01F 119.7 . . ? C00G C01F H01F 119.7 . . ? C01F C01G C014 119.7(4) . . ? C01F C01G H01G 120.2 . . ? C014 C01G H01G 120.2 . . ? C4 C3 C2 120.0(4) . . ? C4 C3 H3 120.0 . . ? C2 C3 H3 120.0 . . ? C3 C4 C5 120.5(4) . . ? C3 C4 H4 119.7 . . ? C5 C4 H4 119.7 . . ? C4 C5 C6 119.8(5) . . ? C4 C5 H5 120.1 . . ? C6 C5 H5 120.1 . . ? C1 C6 C5 120.0(4) . . ? C1 C6 H6 120.0 . . ? C5 C6 H6 120.0 . . ? C8 C7 C12 119.8(4) . . ? C8 C7 P1 118.6(3) . . ? C12 C7 P1 121.5(3) . . ? C9 C8 C7 120.0(4) . . ? C9 C8 H8 120.0 . . ? C7 C8 H8 120.0 . . ? C8 C9 C10 120.3(4) . . ? C8 C9 H9 119.9 . . ? C10 C9 H9 119.9 . . ? C11 C10 C9 120.0(4) . . ? C11 C10 H10 120.0 . . ? C9 C10 H10 120.0 . . ? C10 C11 C12 120.3(4) . . ? C10 C11 H11 119.9 . . ? C12 C11 H11 119.9 . . ? C11 C12 C7 119.6(4) . . ? C11 C12 H12 120.2 . . ? C7 C12 H12 120.2 . . ? C18 C13 C14 119.4(4) . . ? C18 C13 P1 123.0(4) . . ? C14 C13 P1 117.5(3) . . ? C15 C14 C13 119.8(4) . . ? C15 C14 H14 120.1 . . ? C13 C14 H14 120.1 . . ? C01G C014 C00H 120.1(4) . . ? C01G C014 H014 119.9 . . ? C00H C014 H014 119.9 . . ? C16 C15 C14 120.8(5) . . ? C16 C15 H15 119.6 . . ? C14 C15 H15 119.6 . . ? C15 C16 C17 119.9(5) . . ? C15 C16 H16 120.1 . . ? C17 C16 H16 120.1 . . ? C16 C17 C18 120.3(5) . . ? C16 C17 H17 119.8 . . ? C18 C17 H17 119.8 . . ? C13 C18 C17 119.7(5) . . ? C13 C18 H18 120.2 . . ? C17 C18 H18 120.2 . . ? N2 C19 C20 122.2(5) . . ? N2 C19 H19 118.9 . . ? C20 C19 H19 118.9 . . ? C19 C20 C21 119.2(4) . . ? C19 C20 H20 120.4 . . ? C21 C20 H20 120.4 . . ? C20 C21 C22 119.4(4) . . ? C20 C21 H21 120.3 . . ? C22 C21 H21 120.3 . . ? C23 C22 C21 118.5(4) . . ? C23 C22 C24 120.2(4) . . ? C21 C22 C24 121.2(4) . . ? N2 C23 C22 121.5(4) . . ? N2 C23 C26 115.2(3) . . ? C22 C23 C26 123.3(4) . . ? O10 C24 O9 125.5(4) . . ? O10 C24 C22 124.0(4) . . ? O9 C24 C22 110.5(4) . . ? O9 C25 H01R 109.5 . . ? O9 C25 H01S 109.5 . . ? H01R C25 H01S 109.5 . . ? O9 C25 H25 109.5 . . ? H01R C25 H25 109.5 . . ? H01S C25 H25 109.5 . . ? N1 C26 C30 121.0(4) . . ? N1 C26 C23 115.7(3) . . ? C30 C26 C23 123.2(3) . . ? N1 C27 C28 122.1(4) . . ? N1 C27 H27 118.9 . . ? C28 C27 H27 118.9 . . ? C27 C28 C29 119.1(4) . . ? C27 C28 H28 120.4 . . ? C29 C28 H28 120.4 . . ? C28 C29 C30 119.3(4) . . ? C28 C29 H29 120.3 . . ? C30 C29 H29 120.3 . . ? C29 C30 C26 118.8(4) . . ? C29 C30 C31 120.9(4) . . ? C26 C30 C31 120.1(4) . . ? O8 C31 O7 125.2(4) . . ? O8 C31 C30 123.3(4) . . ? O7 C31 C30 111.4(4) . . ? O7 C32 H01C 109.5 . . ? O7 C32 H01H 109.5 . . ? H01C C32 H01H 109.5 . . ? O7 C32 H01N 109.5 . . ? H01C C32 H01N 109.5 . . ? H01H C32 H01N 109.5 . . ? C38 C33 C34 120.0(5) . . ? C38 C33 P2 121.8(4) . . ? C34 C33 P2 118.1(4) . . ? C35 C34 C33 118.4(7) . . ? C35 C34 H34 120.8 . . ? C33 C34 H34 120.8 . . ? C36 C35 C34 120.9(7) . . ? C36 C35 H35 119.6 . . ? C34 C35 H35 119.6 . . ? C35 C36 C37 121.5(6) . . ? C35 C36 H36 119.3 . . ? C37 C36 H36 119.3 . . ? C36 C37 C38 118.1(8) . . ? C36 C37 H37 121.0 . . ? C38 C37 H37 121.0 . . ? C33 C38 C37 121.2(7) . . ? C33 C38 H38 119.4 . . ? C37 C38 H38 119.4 . . ? C44 C39 C40 119.4(4) . . ? C44 C39 P2 119.8(3) . . ? C40 C39 P2 120.8(3) . . ? C41 C40 C39 120.1(4) . . ? C41 C40 H40 120.0 . . ? C39 C40 H40 120.0 . . ? C40 C41 C42 120.0(4) . . ? C40 C41 H41 120.0 . . ? C42 C41 H41 120.0 . . ? C43 C42 C41 120.6(4) . . ? C43 C42 H42 119.7 . . ? C41 C42 H42 119.7 . . ? C42 C43 C44 119.5(4) . . ? C42 C43 H43 120.2 . . ? C44 C43 H43 120.2 . . ? C39 C44 C43 120.3(4) . . ? C39 C44 H44 119.9 . . ? C43 C44 H44 119.9 . . ? F4A C45 F6A 127.1(11) . . ? F6B C45 F5B 104.7(7) . . ? F6B C45 F4B 105.0(7) . . ? F5B C45 F4B 98.9(6) . . ? F4A C45 F5A 112.9(9) . . ? F6A C45 F5A 97.6(7) . . ? F4A C45 S2 108.4(8) . . ? F6B C45 S2 116.8(6) . . ? F6A C45 S2 103.4(6) . . ? F5B C45 S2 113.3(6) . . ? F4B C45 S2 116.0(5) . . ? F5A C45 S2 105.3(6) . . ? F1B C46 F2B 140.5(15) . . ? F1A C46 F2A 104.2(5) . . ? F1A C46 F3A 102.0(5) . . ? F2A C46 F3A 108.3(5) . . ? F1B C46 F3B 91.7(14) . . ? F2B C46 F3B 66.8(11) . . ? F1B C46 S1A 104.1(12) . . ? F2B C46 S1A 112.4(9) . . ? F1A C46 S1A 113.5(4) . . ? F2A C46 S1A 111.6(4) . . ? F3A C46 S1A 116.2(4) . . ? F3B C46 S1A 101.9(8) . . ? F1B C46 S1B 100.9(12) . . ? F2B C46 S1B 107.8(9) . . ? F1A C46 S1B 127.4(4) . . ? F2A C46 S1B 115.8(4) . . ? F3A C46 S1B 96.6(4) . . ? F3B C46 S1B 81.7(8) . . ? S1A C46 S1B 20.6(2) . . ? N1 Au1 P1 174.43(9) . . ? N2 Au2 P2 172.88(10) . . ? C27 N1 C26 119.5(3) . . ? C27 N1 Au1 122.2(3) . . ? C26 N1 Au1 118.3(3) . . ? C19 N2 C23 119.1(4) . . ? C19 N2 Au2 117.1(3) . . ? C23 N2 Au2 123.2(3) . . ? C31 O7 C32 115.0(4) . . ? C24 O9 C25 115.1(5) . . ? C13 P1 C7 106.15(19) . . ? C13 P1 C1 107.65(19) . . ? C7 P1 C1 108.68(19) . . ? C13 P1 Au1 109.44(13) . . ? C7 P1 Au1 113.56(13) . . ? C1 P1 Au1 111.10(14) . . ? C39 P2 C33 106.05(19) . . ? C39 P2 C00I 107.66(18) . . ? C33 P2 C00I 106.5(2) . . ? C39 P2 Au2 111.18(14) . . ? C33 P2 Au2 115.31(16) . . ? C00I P2 Au2 109.74(13) . . ? S1B S1A O2B 72.0(7) . . ? S1B S1A O3B 42.4(6) . . ? O2B S1A O3B 110.2(5) . . ? S1B S1A O1B 152.9(6) . . ? O2B S1A O1B 116.6(4) . . ? O3B S1A O1B 115.0(4) . . ? S1B S1A O2A 84.9(8) . . ? S1B S1A O1A 70.9(7) . . ? O2A S1A O1A 140.8(8) . . ? S1B S1A C46 100.3(6) . . ? O2B S1A C46 109.9(4) . . ? O3B S1A C46 103.5(3) . . ? O1B S1A C46 100.3(3) . . ? O2A S1A C46 100.0(6) . . ? O1A S1A C46 114.1(5) . . ? S1B S1A O7A 11.5(13) . . ? O2A S1A O7A 73.4(13) . . ? O1A S1A O7A 80.3(12) . . ? C46 S1A O7A 103.0(12) . . ? S1B S1A O3A 23.5(13) . . ? O2A S1A O3A 94.9(13) . . ? O1A S1A O3A 75.0(13) . . ? C46 S1A O3A 77.6(12) . . ? O7A S1A O3A 30.9(14) . . ? S1A S1B O3B 108.2(9) . . ? S1A S1B O7A 162(2) . . ? S1A S1B O2B 76.9(7) . . ? O3B S1B O2B 153.9(9) . . ? S1A S1B O3A 144.9(19) . . ? O7A S1B O3A 47(2) . . ? S1A S1B O1A 82.2(8) . . ? O7A S1B O1A 112.1(19) . . ? O3A S1B O1A 100.0(18) . . ? S1A S1B O2A 68.3(8) . . ? O7A S1B O2A 93.6(19) . . ? O3A S1B O2A 121.9(18) . . ? O1A S1B O2A 137.4(9) . . ? S1A S1B C46 59.2(5) . . ? O3B S1B C46 106.6(6) . . ? O7A S1B C46 123.7(19) . . ? O2B S1B C46 97.9(6) . . ? O3A S1B C46 86.8(18) . . ? O1A S1B C46 104.5(6) . . ? O2A S1B C46 86.5(7) . . ? S1A S1B O1B 18.1(4) . . ? O3B S1B O1B 94.1(7) . . ? O2B S1B O1B 84.5(5) . . ? C46 S1B O1B 73.4(3) . . ? O6B S2 O5B 123.0(6) . . ? O4A S2 O6A 118.5(6) . . ? O6B S2 O4B 116.7(5) . . ? O5B S2 O4B 112.8(5) . . ? O4A S2 O5A 110.8(5) . . ? O6A S2 O5A 99.3(5) . . ? O6B S2 C45 100.2(5) . . ? O4A S2 C45 111.3(4) . . ? O5B S2 C45 99.2(4) . . ? O6A S2 C45 107.4(5) . . ? O4B S2 C45 98.1(4) . . ? O5A S2 C45 108.6(4) . . ? C46 F3B F2B 49.8(9) . . ? C46 F3B O3A 96.1(17) . . ? F2B F3B O3A 113.1(19) . . ? C46 F2B F3B 63.4(11) . . ? S1B O1A S1A 26.9(4) . . ? S1A O2A S1B 26.8(4) . . ? O7A O3A S1B 57(3) . . ? O7A O3A F3B 139(4) . . ? S1B O3A F3B 95(2) . . ? O7A O3A S1A 68(3) . . ? S1B O3A S1A 11.6(7) . . ? F3B O3A S1A 84.0(18) . . ? O3A O7A S1B 76(3) . . ? O3A O7A S1A 81(3) . . ? S1B O7A S1A 6.7(7) . . ? S1B O3B S1A 29.4(5) . . ? S1A O1B S1B 9.0(2) . . ? S1B O2B S1A 31.1(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C6 1.377(6) . ? C1 C2 1.395(6) . ? C1 P1 1.806(4) . ? C00G C00I 1.393(6) . ? C00G C01F 1.404(6) . ? C00G H00G 0.9500 . ? C00H C014 1.389(6) . ? C00H C00I 1.399(6) . ? C00H H00H 0.9500 . ? C00I P2 1.813(4) . ? C2 C3 1.386(6) . ? C2 H2 0.9500 . ? C01F C01G 1.383(7) . ? C01F H01F 0.9500 . ? C01G C014 1.385(7) . ? C01G H01G 0.9500 . ? C3 C4 1.371(7) . ? C3 H3 0.9500 . ? C4 C5 1.377(8) . ? C4 H4 0.9500 . ? C5 C6 1.403(7) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 C8 1.386(5) . ? C7 C12 1.393(6) . ? C7 P1 1.805(4) . ? C8 C9 1.379(6) . ? C8 H8 0.9500 . ? C9 C10 1.386(7) . ? C9 H9 0.9500 . ? C10 C11 1.374(7) . ? C10 H10 0.9500 . ? C11 C12 1.390(6) . ? C11 H11 0.9500 . ? C12 H12 0.9500 . ? C13 C18 1.388(6) . ? C13 C14 1.406(6) . ? C13 P1 1.805(4) . ? C14 C15 1.379(6) . ? C14 H14 0.9500 . ? C014 H014 0.9500 . ? C15 C16 1.375(7) . ? C15 H15 0.9500 . ? C16 C17 1.384(8) . ? C16 H16 0.9500 . ? C17 C18 1.397(7) . ? C17 H17 0.9500 . ? C18 H18 0.9500 . ? C19 N2 1.340(6) . ? C19 C20 1.368(7) . ? C19 H19 0.9500 . ? C20 C21 1.371(7) . ? C20 H20 0.9500 . ? C21 C22 1.388(6) . ? C21 H21 0.9500 . ? C22 C23 1.385(6) . ? C22 C24 1.491(6) . ? C23 N2 1.345(5) . ? C23 C26 1.498(6) . ? C24 O10 1.200(6) . ? C24 O9 1.330(5) . ? C25 O9 1.451(7) . ? C25 H01R 0.9800 . ? C25 H01S 0.9800 . ? C25 H25 0.9800 . ? C26 N1 1.354(5) . ? C26 C30 1.396(5) . ? C27 N1 1.343(5) . ? C27 C28 1.375(6) . ? C27 H27 0.9500 . ? C28 C29 1.384(6) . ? C28 H28 0.9500 . ? C29 C30 1.392(6) . ? C29 H29 0.9500 . ? C30 C31 1.501(6) . ? C31 O8 1.194(5) . ? C31 O7 1.336(5) . ? C32 O7 1.451(5) . ? C32 H01C 0.9800 . ? C32 H01H 0.9800 . ? C32 H01N 0.9800 . ? C33 C38 1.379(8) . ? C33 C34 1.395(7) . ? C33 P2 1.809(5) . ? C34 C35 1.394(9) . ? C34 H34 0.9500 . ? C35 C36 1.368(11) . ? C35 H35 0.9500 . ? C36 C37 1.373(11) . ? C36 H36 0.9500 . ? C37 C38 1.397(8) . ? C37 H37 0.9500 . ? C38 H38 0.9500 . ? C39 C44 1.389(6) . ? C39 C40 1.398(6) . ? C39 P2 1.808(4) . ? C40 C41 1.371(6) . ? C40 H40 0.9500 . ? C41 C42 1.392(7) . ? C41 H41 0.9500 . ? C42 C43 1.376(7) . ? C42 H42 0.9500 . ? C43 C44 1.390(6) . ? C43 H43 0.9500 . ? C44 H44 0.9500 . ? C45 F4A 1.158(13) . ? C45 F6B 1.287(10) . ? C45 F6A 1.352(12) . ? C45 F5B 1.379(10) . ? C45 F4B 1.379(10) . ? C45 F5A 1.390(10) . ? C45 S2 1.828(7) . ? C46 F1B 1.23(2) . ? C46 F2B 1.300(18) . ? C46 F1A 1.329(7) . ? C46 F2A 1.344(7) . ? C46 F3A 1.357(7) . ? C46 F3B 1.52(2) . ? C46 S1A 1.777(6) . ? C46 S1B 2.036(9) . ? Au1 N1 2.102(3) . ? Au1 P1 2.2445(10) . ? Au2 N2 2.102(4) . ? Au2 P2 2.2367(11) . ? S1A S1B 0.727(7) . ? S1A O2B 1.369(9) . ? S1A O3B 1.406(7) . ? S1A O1B 1.444(5) . ? S1A O2A 1.496(15) . ? S1A O1A 1.594(14) . ? S1A O7A 1.95(4) . ? S1A O3A 2.08(4) . ? S1B O3B 0.998(8) . ? S1B O7A 1.25(4) . ? S1B O2B 1.337(10) . ? S1B O3A 1.44(4) . ? S1B O1A 1.520(16) . ? S1B O2A 1.604(17) . ? S1B O1B 2.118(9) . ? S2 O6B 1.320(9) . ? S2 O4A 1.349(9) . ? S2 O5B 1.400(9) . ? S2 O6A 1.497(11) . ? S2 O4B 1.515(9) . ? S2 O5A 1.558(8) . ? F3B F2B 1.56(3) . ? F3B O3A 1.74(5) . ? O3A O7A 1.08(5) . ?