#------------------------------------------------------------------------------ #$Date: 2021-09-09 01:53:06 +0300 (Thu, 09 Sep 2021) $ #$Revision: 269052 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/82/7708241.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708241 loop_ _publ_author_name 'Lei, Caijin' 'Yang, Hongwei' 'Zhang, Qinghua' 'Cheng, Guangbin' _publ_section_title ; Synthesis of nitrogen-rich and thermostable energetic materials based on hetarenecarboxylic acids ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT02854E _journal_year 2021 _chemical_formula_moiety 'C5 H6 N10 O' _chemical_formula_sum 'C5 H6 N10 O' _chemical_formula_weight 222.20 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _audit_creation_date 2021-03-18 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-04-19 deposited with the CCDC. 2021-09-08 downloaded from the CCDC. ; _cell_angle_alpha 108.619(5) _cell_angle_beta 109.314(5) _cell_angle_gamma 92.750(5) _cell_formula_units_Z 2 _cell_length_a 6.8113(9) _cell_length_b 8.2072(10) _cell_length_c 8.5119(12) _cell_measurement_reflns_used 1467 _cell_measurement_temperature 170(2) _cell_measurement_theta_max 26.381 _cell_measurement_theta_min 2.659 _cell_volume 419.23(10) _computing_cell_refinement 'SAINT V8.40A (?, 2016)' _computing_data_reduction 'SAINT V8.40A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 170.0 _diffrn_measured_fraction_theta_full 0.995 _diffrn_measured_fraction_theta_max 0.988 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0468 _diffrn_reflns_av_unetI/netI 0.0580 _diffrn_reflns_Laue_measured_fraction_full 0.995 _diffrn_reflns_Laue_measured_fraction_max 0.988 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 4856 _diffrn_reflns_point_group_measured_fraction_full 0.995 _diffrn_reflns_point_group_measured_fraction_max 0.988 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.421 _diffrn_reflns_theta_min 2.658 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.138 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6784 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0670 before and 0.0544 after correction. The Ratio of minimum to maximum transmission is 0.9101. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.760 _exptl_crystal_description block _exptl_crystal_F_000 228 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.249 _refine_diff_density_min -0.246 _refine_diff_density_rms 0.056 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.031 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 155 _refine_ls_number_reflns 1710 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.031 _refine_ls_R_factor_all 0.0782 _refine_ls_R_factor_gt 0.0461 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0474P)^2^+0.2140P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1013 _refine_ls_wR_factor_ref 0.1219 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1207 _reflns_number_total 1710 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL mo_2021278_0m_a.res in P-1 mo_2021278_0m.res created by SHELXL-2018/3 at 09:25:16 on 18-Mar-2021 REM Old TITL mo_2021278_0m_a.res in P-1 REM SHELXT solution in P-1 REM R1 0.171, Rweak 0.008, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C15 O CELL 0.71073 6.8113 8.2072 8.5119 108.619 109.314 92.75 ZERR 2 0.0009 0.001 0.0012 0.005 0.005 0.005 LATT 1 SFAC C H N O UNIT 10 12 20 2 L.S. 20 PLAN 10 SIZE 0.15 0.08 0.05 TEMP -103.15 BOND $H list 4 fmap 2 ACTA REM REM REM WGHT 0.047400 0.214000 FVAR 1.44066 O1 4 0.400286 0.056089 0.822834 11.00000 0.03908 0.03506 = 0.02585 0.01727 0.01280 0.00417 N6 3 0.238985 0.249553 0.392702 11.00000 0.01751 0.02818 = 0.02102 0.01225 0.00708 0.00131 N4 3 0.593190 0.285813 0.465863 11.00000 0.02300 0.02358 = 0.01618 0.00956 0.00402 0.00339 N5 3 0.492210 0.335426 0.322131 11.00000 0.02024 0.02321 = 0.01630 0.00957 0.00494 0.00390 N8 3 0.354675 0.425699 0.101602 11.00000 0.02428 0.02933 = 0.02136 0.01142 0.00761 0.00342 N9 3 0.735998 0.458129 0.219840 11.00000 0.02521 0.03182 = 0.02331 0.01421 0.01093 0.00753 AFIX 7 H9A 2 0.811005 0.374996 0.230827 11.00000 -1.20000 H9B 2 0.730001 0.477491 0.122337 11.00000 -1.20000 AFIX 0 N7 3 0.184820 0.368027 0.145352 11.00000 0.02126 0.03183 = 0.02388 0.01346 0.00496 0.00275 N2 3 0.859327 0.204268 0.778622 11.00000 0.02270 0.04395 = 0.02571 0.01929 0.00128 0.00061 N3 3 0.308425 0.105326 0.680389 11.00000 0.03266 0.02978 = 0.02435 0.01492 0.01121 0.00636 N10 3 0.036009 0.219864 0.394327 11.00000 0.02135 0.04457 = 0.03808 0.02256 0.01056 0.00287 AFIX 7 H10A 2 -0.001770 0.107560 0.369641 11.00000 -1.20000 H10B 2 0.036004 0.279144 0.500915 11.00000 -1.20000 AFIX 0 N1 3 0.621436 0.089341 0.879171 11.00000 0.03377 0.03055 = 0.02350 0.01270 0.00644 0.00286 C4 1 0.280461 0.315659 0.275951 11.00000 0.01854 0.02136 = 0.02131 0.00874 0.00496 0.00236 C3 1 0.433456 0.234474 0.503193 11.00000 0.01986 0.01953 = 0.01773 0.00675 0.00575 0.00321 C1 1 0.661074 0.159189 0.772226 11.00000 0.02851 0.02064 = 0.01850 0.00622 0.00616 0.00314 C2 1 0.463978 0.168589 0.647585 11.00000 0.02410 0.01799 = 0.01979 0.00721 0.00807 0.00326 C5 1 0.535513 0.405424 0.207910 11.00000 0.02489 0.02092 = 0.01824 0.00814 0.00683 0.00296 H2A 2 0.960815 0.230744 0.886300 11.00000 0.04493 H2B 2 0.868643 0.275883 0.721301 11.00000 0.04057 HKLF 4 REM mo_2021278_0m_a.res in P-1 REM wR2 = 0.1219, GooF = S = 1.031, Restrained GooF = 1.031 for all data REM R1 = 0.0461 for 1207 Fo > 4sig(Fo) and 0.0782 for all 1710 data REM 155 parameters refined using 0 restraints END WGHT 0.0417 0.1893 REM Highest difference peak 0.249, deepest hole -0.246, 1-sigma level 0.056 Q1 1 0.4585 0.2201 0.5979 11.00000 0.05 0.25 Q2 1 0.8023 -0.0172 0.9088 11.00000 0.05 0.21 Q3 1 0.6245 0.5722 0.1273 11.00000 0.05 0.20 Q4 1 0.4026 0.2165 0.7024 11.00000 0.05 0.20 Q5 1 0.9565 0.1380 0.7428 11.00000 0.05 0.20 Q6 1 0.4047 0.3471 0.3124 11.00000 0.05 0.20 Q7 1 0.5103 0.4358 -0.0370 11.00000 0.05 0.19 Q8 1 0.5806 0.0908 0.6696 11.00000 0.05 0.19 Q9 1 0.6983 0.2635 0.5133 11.00000 0.05 0.18 Q10 1 0.5104 0.5402 0.3959 11.00000 0.05 0.18 REM The information below was added by Olex2. REM REM R1 = 0.0461 for 1207 Fo > 4sig(Fo) and 0.0782 for all 4856 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.25, deepest hole -0.25 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0782 REM R1_gt = 0.0461 REM wR_ref = 0.1219 REM GOOF = 1.031 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 4856 REM Reflections_gt = 1207 REM Parameters = n/a REM Hole = -0.25 REM Peak = 0.25 REM Flack = n/a ; _cod_data_source_file d1dt02854e2.cif _cod_data_source_block mo_2021278_0m _cod_database_code 7708241 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.993 _shelx_estimated_absorpt_t_min 0.980 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All N(H,H) groups 2.a Rotating group: N9(H9A,H9B), N10(H10A,H10B) ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.4003(3) 0.0561(2) 0.8228(2) 0.0315(4) Uani 1 1 d . . . . . N6 N 0.2390(3) 0.2496(2) 0.3927(2) 0.0214(4) Uani 1 1 d . . . . . N4 N 0.5932(3) 0.2858(2) 0.4659(2) 0.0211(4) Uani 1 1 d . . . . . N5 N 0.4922(3) 0.3354(2) 0.3221(2) 0.0197(4) Uani 1 1 d . . . . . N8 N 0.3547(3) 0.4257(2) 0.1016(2) 0.0246(5) Uani 1 1 d . . . . . N9 N 0.7360(3) 0.4581(2) 0.2198(2) 0.0250(5) Uani 1 1 d . . . . . H9A H 0.811005 0.374996 0.230827 0.030 Uiso 1 1 d GR . . . . H9B H 0.730001 0.477491 0.122337 0.030 Uiso 1 1 d GR . . . . N7 N 0.1848(3) 0.3680(2) 0.1454(2) 0.0257(5) Uani 1 1 d . . . . . N2 N 0.8593(3) 0.2043(3) 0.7786(3) 0.0312(5) Uani 1 1 d . . . . . N3 N 0.3084(3) 0.1053(2) 0.6804(3) 0.0273(5) Uani 1 1 d . . . . . N10 N 0.0360(3) 0.2199(3) 0.3943(3) 0.0328(5) Uani 1 1 d . . . . . H10A H -0.001770 0.107560 0.369641 0.039 Uiso 1 1 d GR . . . . H10B H 0.036004 0.279144 0.500915 0.039 Uiso 1 1 d GR . . . . N1 N 0.6214(3) 0.0893(3) 0.8792(3) 0.0297(5) Uani 1 1 d . . . . . C4 C 0.2805(3) 0.3157(3) 0.2760(3) 0.0208(5) Uani 1 1 d . . . . . C3 C 0.4335(3) 0.2345(3) 0.5032(3) 0.0193(5) Uani 1 1 d . . . . . C1 C 0.6611(3) 0.1592(3) 0.7722(3) 0.0234(5) Uani 1 1 d . . . . . C2 C 0.4640(3) 0.1686(3) 0.6476(3) 0.0205(5) Uani 1 1 d . . . . . C5 C 0.5355(3) 0.4054(3) 0.2079(3) 0.0214(5) Uani 1 1 d . . . . . H2A H 0.961(4) 0.231(3) 0.886(4) 0.045(8) Uiso 1 1 d . . . . . H2B H 0.869(4) 0.276(3) 0.721(4) 0.041(8) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0391(10) 0.0351(10) 0.0259(9) 0.0173(8) 0.0128(8) 0.0042(7) N6 0.0175(9) 0.0282(10) 0.0210(10) 0.0122(8) 0.0071(8) 0.0013(7) N4 0.0230(10) 0.0236(10) 0.0162(10) 0.0096(8) 0.0040(8) 0.0034(7) N5 0.0202(10) 0.0232(10) 0.0163(9) 0.0096(8) 0.0049(7) 0.0039(7) N8 0.0243(10) 0.0293(11) 0.0214(10) 0.0114(9) 0.0076(8) 0.0034(8) N9 0.0252(10) 0.0318(11) 0.0233(11) 0.0142(9) 0.0109(8) 0.0075(8) N7 0.0213(10) 0.0318(11) 0.0239(11) 0.0135(9) 0.0050(8) 0.0028(8) N2 0.0227(11) 0.0440(13) 0.0257(12) 0.0193(11) 0.0013(9) 0.0006(9) N3 0.0327(11) 0.0298(11) 0.0244(11) 0.0149(9) 0.0112(9) 0.0064(8) N10 0.0214(11) 0.0446(13) 0.0381(13) 0.0226(11) 0.0106(9) 0.0029(9) N1 0.0338(12) 0.0305(11) 0.0235(11) 0.0127(9) 0.0064(9) 0.0029(9) C4 0.0185(11) 0.0214(11) 0.0213(12) 0.0087(10) 0.0050(9) 0.0024(8) C3 0.0199(11) 0.0195(11) 0.0177(11) 0.0067(9) 0.0057(9) 0.0032(8) C1 0.0285(12) 0.0206(12) 0.0185(12) 0.0062(9) 0.0062(9) 0.0031(9) C2 0.0241(11) 0.0180(11) 0.0198(12) 0.0072(9) 0.0081(9) 0.0033(9) C5 0.0249(12) 0.0209(11) 0.0182(12) 0.0081(10) 0.0068(9) 0.0030(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N3 O1 N1 111.03(16) . . ? C4 N6 N10 122.63(17) . . ? C4 N6 C3 105.74(17) . . ? C3 N6 N10 131.49(18) . . ? C3 N4 N5 101.96(16) . . ? C4 N5 N4 113.42(17) . . ? C4 N5 C5 105.56(17) . . ? C5 N5 N4 140.99(18) . . ? C5 N8 N7 109.80(17) . . ? H9A N9 H9B 109.2 . . ? C5 N9 H9A 109.1 . . ? C5 N9 H9B 109.5 . . ? C4 N7 N8 102.99(17) . . ? C1 N2 H2A 114.4(18) . . ? C1 N2 H2B 114.5(17) . . ? H2A N2 H2B 115(2) . . ? C2 N3 O1 105.79(17) . . ? N6 N10 H10A 109.2 . . ? N6 N10 H10B 109.4 . . ? H10A N10 H10B 109.2 . . ? C1 N1 O1 105.27(17) . . ? N5 C4 N6 105.23(17) . . ? N7 C4 N6 140.8(2) . . ? N7 C4 N5 113.91(19) . . ? N6 C3 C2 124.53(19) . . ? N4 C3 N6 113.65(18) . . ? N4 C3 C2 121.83(18) . . ? N2 C1 C2 128.0(2) . . ? N1 C1 N2 123.6(2) . . ? N1 C1 C2 108.4(2) . . ? N3 C2 C3 123.40(19) . . ? N3 C2 C1 109.54(19) . . ? C1 C2 C3 127.1(2) . . ? N5 C5 N9 123.90(19) . . ? N8 C5 N5 107.75(19) . . ? N8 C5 N9 128.1(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 N3 1.364(2) . ? O1 N1 1.404(2) . ? N6 N10 1.398(2) . ? N6 C4 1.370(3) . ? N6 C3 1.386(3) . ? N4 N5 1.387(2) . ? N4 C3 1.316(3) . ? N5 C4 1.350(3) . ? N5 C5 1.376(3) . ? N8 N7 1.430(3) . ? N8 C5 1.320(3) . ? N9 H9A 0.8820 . ? N9 H9B 0.8821 . ? N9 C5 1.373(3) . ? N7 C4 1.303(3) . ? N2 C1 1.362(3) . ? N2 H2A 0.90(3) . ? N2 H2B 0.89(3) . ? N3 C2 1.306(3) . ? N10 H10A 0.8819 . ? N10 H10B 0.8820 . ? N1 C1 1.308(3) . ? C3 C2 1.453(3) . ? C1 C2 1.433(3) . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -2 0 0 5.3 2.3 -2 0 0 4.8 1.9 2 0 0 10.4 3 2 0 0 10.9 2.5 -3 0 0 67.89 7 -3 0 0 82.39 8.6 3 0 0 76.19 7 3 0 0 74.79 8.5 -4 0 0 18.3 4.5 -4 0 0 6.5 3.6 -4 0 0 14.1 5.3 4 0 0 14.1 4 4 0 0 19.6 5.8 -5 0 0 33.1 8.4 -5 0 0 18.2 5.5 -5 0 0 13.9 6.6 5 0 0 27.7 6.3 5 0 0 16.5 7.1 -6 0 0 1 4.2 -6 0 0 4.9 3.6 -6 0 0 -2.8 3.9 6 0 0 0.7 3.3 -7 0 0 -5 5.9 -7 0 0 5.2 6.8 -7 0 0 17.8 6.5 7 0 0 6.4 4.9 8 -1 0 9.9 6.9 -8 1 0 14.4 10.5 -8 1 0 7.7 9 7 -1 0 111.29 14.4 -7 1 0 103.99 19.3 -7 1 0 109.79 20.3 6 -1 0 -5.5 3.1 -6 1 0 -2.4 4.4 -6 1 0 3.1 3.8 -6 1 0 -3.4 3 5 -1 0 845.92 36.3 5 -1 0 744.53 47.9 -5 1 0 817.02 39.6 -5 1 0 836.02 36.9 4 -1 0 392.86 21 4 -1 0 385.56 23.2 -4 1 0 375.86 22.5 -4 1 0 378.36 21.4 3 -1 0 25.4 5.3 3 -1 0 29.1 6 -3 1 0 19.3 4.9 -3 1 0 27.1 5.4 2 -1 0 183.38 10.9 2 -1 0 196.78 11.5 -2 1 0 178.78 10.9 -2 1 0 203.48 11.1 1 -1 0 511.75 16.4 1 -1 0 530.95 18.9 -1 1 0 531.85 16.4 -1 1 0 530.75 17.4 0 -1 0 38.1 1.8 0 -1 0 40.6 3.3 0 1 0 36.4 1.8 0 1 0 41.4 3.3 -1 -1 0 886.41 29.8 -1 -1 0 905.71 27.5 -1 -1 0 917.21 26.8 1 1 0 929.01 27.1 1 1 0 903.91 27.7 1 1 0 887.81 29.8 -2 -1 0 311.07 17.7 -2 -1 0 299.07 15.6 -2 -1 0 301.77 13.5 2 1 0 303.67 15.8 2 1 0 312.57 13.8 -3 -1 0 1170.38 37.5 -3 -1 0 1223.18 43.1 -3 -1 0 1053.09 47.4 3 1 0 1133.29 37.1 3 1 0 1120.49 42.4 -4 -1 0 454.75 21.9 -4 -1 0 429.86 25.6 -4 -1 0 440.96 28.6 4 1 0 448.06 21.4 4 1 0 496.35 28 -5 -1 0 175.48 14.2 -5 -1 0 196.18 18.3 -5 -1 0 213.38 21.3 5 1 0 222.88 20.3 5 1 0 194.58 14.5 -6 -1 0 6.6 4.5 -6 -1 0 7.4 4.8 -6 -1 0 -0.6 3.5 6 1 0 3.2 3.9 -7 -1 0 30.5 7.8 -7 -1 0 32 11.5 -7 -1 0 52.79 12.6 7 1 0 14.7 6.8 8 -2 0 11 8.3 -8 2 0 8.4 7.9 -8 2 0 13.3 10.1 7 -2 0 6.4 6.6 -7 2 0 23.9 9.4 -7 2 0 14.5 8 6 -2 0 49.4 10.5 -6 2 0 76.39 14.4 5 -2 0 448.26 26.6 5 -2 0 451.75 28 -5 2 0 472.75 28 4 -2 0 218.08 21.9 4 -2 0 266.37 18.7 -4 2 0 309.07 19.4 3 -2 0 694.23 30.3 3 -2 0 685.13 28.3 -3 2 0 693.93 28 2 -2 0 1075.69 33.6 2 -2 0 1079.09 38.6 -2 2 0 1060.89 33.1 -2 2 0 1081.39 35.3 1 -2 0 988.8 30.7 1 -2 0 999.3 25.8 -1 2 0 920.71 29.9 -1 2 0 969.1 25.6 0 -2 0 2358.36 57.09 0 -2 0 2378.36 65.09 0 2 0 2405.96 57.29 0 2 0 2400.26 64.79 -1 -2 0 8.1 2.2 -1 -2 0 9.4 2.3 -1 -2 0 4.7 2.1 1 2 0 6.7 2 1 2 0 9.6 3.2 -2 -2 0 38.2 6.5 -2 -2 0 36.1 7.3 -2 -2 0 41.3 5.1 2 2 0 41.2 5.4 2 2 0 36.5 6.5 2 2 0 31 6.8 -3 -2 0 72.69 8.7 -3 -2 0 58.39 10.9 -3 -2 0 62.39 7.1 3 2 0 70.79 8.7 3 2 0 70.79 7.6 -4 -2 0 27.6 7.5 -4 -2 0 33.7 6.3 -4 -2 0 18.5 7.3 4 2 0 30.4 6.1 4 2 0 24.6 7.1 -5 -2 0 407.06 27.9 -5 -2 0 390.06 22.2 -5 -2 0 427.26 31.7 5 2 0 381.26 28.3 5 2 0 293.57 26.3 -6 -2 0 91.09 16.9 -6 -2 0 106.19 12.4 -6 -2 0 111.49 20.9 6 2 0 103.19 11.6 -7 -2 0 16.8 8.2 -7 -2 0 15.8 11.1 -7 -2 0 33.4 8.2 7 2 0 33.8 9 7 -3 0 -3.3 6.6 -7 3 0 -14.5 5.4 6 -3 0 4.6 4.5 -6 3 0 -0.6 5.6 -6 3 0 10.1 6.3 5 -3 0 399.06 27 5 -3 0 423.46 26.4 -5 3 0 406.36 25.7 -5 3 0 413.56 25.5 4 -3 0 17.5 5.7 -4 3 0 17.4 5.4 -4 3 0 11.8 3.8 3 -3 0 25.9 6.7 3 -3 0 33.6 6.4 -3 3 0 24.2 4.8 -3 3 0 22.1 5.2 2 -3 0 1.9 1.2 2 -3 0 0 1.4 -2 3 0 0.3 1.1 -2 3 0 1.2 1.9 1 -3 0 103.39 8.8 -1 3 0 107.09 8.7 0 -3 0 43.7 6.1 0 -3 0 51.89 3.1 0 3 0 53.89 6.5 0 3 0 48.7 3.2 -1 -3 0 208.98 11.2 -1 -3 0 226.18 15.7 -1 -3 0 214.58 14.5 1 3 0 234.98 11.9 -2 -3 0 74.69 7.8 -2 -3 0 67.29 7.6 -2 -3 0 62.79 9 2 3 0 56.99 7.1 2 3 0 63.89 9.1 -3 -3 0 450.95 27.1 -3 -3 0 483.05 25.5 -3 -3 0 484.15 30.2 3 3 0 456.95 25.6 -4 -3 0 0.9 2.6 -4 -3 0 4.3 4.7 -4 -3 0 15 5.6 4 3 0 5.1 5.8 -5 -3 0 605.04 39.3 -5 -3 0 648.04 31 -5 -3 0 647.94 42.7 -6 -3 0 16.2 6.2 -6 -3 0 16.1 6.7 -6 -3 0 13.2 9.1 -7 -3 0 17.2 11.7 -7 -3 0 14.2 8.5 -7 -3 0 0.6 8.3 7 -4 0 72.29 14.7 -7 4 0 31.4 10 6 -4 0 905.71 48.4 6 -4 0 928.21 46.1 -6 4 0 874.21 43.7 -6 4 0 864.71 44.2 5 -4 0 95.19 12.2 5 -4 0 116.89 15.7 -5 4 0 100.19 12.6 -5 4 0 85.19 10 4 -4 0 58.79 12.2 4 -4 0 77.99 8.8 -4 4 0 50.89 10.3 -4 4 0 80.19 8.6 3 -4 0 278.77 21.9 3 -4 0 241.98 14 -3 4 0 243.88 17 -3 4 0 250.87 13.6 2 -4 0 69.09 8.2 2 -4 0 59.19 4.6 -2 4 0 60.69 7.7 -2 4 0 58.59 4.4 1 -4 0 1278.07 45.5 -1 4 0 1309.67 45.2 0 -4 0 26 6.4 0 -4 0 30.7 2.6 0 4 0 29.9 7.1 0 4 0 39 2.9 -1 -4 0 2.8 3 -1 -4 0 3.7 3 -1 -4 0 1.3 1.6 1 4 0 2.7 2 1 4 0 -1.5 2.4 -2 -4 0 37.2 7.8 -2 -4 0 37.6 9.1 -2 -4 0 23.5 5.7 2 4 0 31.5 7.2 2 4 0 30.6 8.4 -3 -4 0 284.87 19.4 -3 -4 0 268.97 23.4 -3 -4 0 263.07 18.5 3 4 0 238.28 27.6 3 4 0 270.37 19.2 -4 -4 0 8 4.6 -4 -4 0 -6 2.6 -4 -4 0 0.8 3.3 4 4 0 3.1 5 -5 -4 0 41.6 13.5 -5 -4 0 42.6 9.4 -5 -4 0 62.09 13.2 -6 -4 0 14.4 10.2 -6 -4 0 15 7.7 -6 -4 0 16 8 7 -5 0 24.6 11.3 -7 5 0 7.5 10.6 -7 5 0 4.2 9.2 6 -5 0 276.67 22.1 6 -5 0 283.77 27.3 -6 5 0 295.27 22.7 -6 5 0 275.57 23.6 5 -5 0 6.5 3.4 -5 5 0 -3.5 3.9 -5 5 0 2.4 3.4 4 -5 0 19.6 5.2 4 -5 0 13 6.4 -4 5 0 20.8 6 -4 5 0 20.2 5.1 3 -5 0 24.6 4.3 3 -5 0 41.6 10.2 3 -5 0 44.2 9 -3 5 0 30.3 7.1 -3 5 0 41 4.6 2 -5 0 -0.5 2.4 -2 5 0 1.6 3.2 -1 5 0 172.48 14.7 0 -5 0 -0.1 2.6 0 5 0 -1.5 2.8 -1 -5 0 85.89 7.1 -1 -5 0 73.69 12.7 -1 -5 0 78.89 14 1 5 0 77.59 7.3 1 5 0 72.79 12.7 -2 -5 0 331.37 23.7 -2 -5 0 399.66 28.2 -2 -5 0 410.06 25.2 2 5 0 381.16 29.4 2 5 0 373.56 20.8 -3 -5 0 360.06 29.4 -3 -5 0 386.06 24.7 -3 -5 0 384.16 23.3 3 5 0 363.96 32.1 3 5 0 377.66 23.9 -4 -5 0 14.9 6.7 -4 -5 0 19.1 6.1 -4 -5 0 13.9 6.3 4 5 0 22.6 7.9 -5 -5 0 14.5 8.2 -5 -5 0 23.2 8.4 -5 -5 0 24.6 8.4 -6 -5 0 14.1 8.5 -6 -5 0 -1.5 8.9 -6 -5 0 -4.9 6.9 7 -6 0 -7 8.1 -7 6 0 8.2 7.6 6 -6 0 272.37 22.3 6 -6 0 267.57 29.4 -6 6 0 394.06 33.7 -6 6 0 286.37 21.8 5 -6 0 34.2 10.5 5 -6 0 28.3 7.3 -5 6 0 15.9 7.8 -5 6 0 20.1 5.3 4 -6 0 -4.4 2.5 4 -6 0 -2.8 5.4 -4 6 0 -2.3 2.8 -4 6 0 5 4.8 3 -6 0 3 4.1 3 -6 0 2.9 5.3 -3 6 0 4.6 3.7 2 -6 0 31.5 8 -2 6 0 30.1 8 1 -6 0 136.39 14.2 -1 6 0 168.28 15.4 0 -6 0 156.28 17.2 0 6 0 173.88 17.2 -1 -6 0 4.7 4.5 -1 -6 0 3.4 5 -1 -6 0 14.4 3.1 1 6 0 8.3 3.2 -2 -6 0 64.79 14.7 -2 -6 0 72.89 8.7 2 6 0 54.09 9.3 2 6 0 71.79 14.7 -3 -6 0 181.08 16.4 -3 -6 0 177.48 18 -3 -6 0 192.18 22.1 3 6 0 212.18 18.4 -4 -6 0 164.28 18.4 -4 -6 0 166.88 23.1 -4 -6 0 173.48 17.8 -5 -6 0 177.98 21.5 -5 -6 0 234.58 24.4 6 -7 0 35.2 11.6 6 -7 0 17.8 7.6 -6 7 0 10.7 7.1 -6 7 0 27 10.7 5 -7 0 -3.5 3.7 5 -7 0 21.8 9.2 -5 7 0 4.3 6.9 4 -7 0 33.9 12.2 -4 7 0 37.3 9.6 3 -7 0 335.37 31.6 3 -7 0 392.46 26.3 -3 7 0 312.27 23.4 2 -7 0 73.29 13.3 -2 7 0 54.89 11.6 1 -7 0 308.67 24.9 -1 7 0 294.77 23.7 0 -7 0 16.2 7.9 0 7 0 16 7.4 -1 -7 0 0.7 2.3 -1 -7 0 -3.4 4.2 -2 -7 0 4.5 6.1 -2 -7 0 4.9 3.3 2 7 0 -7 3.6 -3 -7 0 9 5.5 -3 -7 0 -2.3 6.4 3 7 0 8.8 6.6 -4 -7 0 16.3 12.6 5 -8 0 3.6 9.5 -5 8 0 -11.9 8.3 4 -8 0 13.8 12.2 -4 8 0 6.8 11.4 3 -8 0 56.09 12.3 3 -8 0 57.09 15.4 -3 8 0 80.59 22.8 2 -8 0 2.3 5 -2 8 0 -13.5 5.1 1 -8 0 21.3 9.4 -1 8 0 8 7.9 -1 -8 0 96.59 19.5 -2 -8 0 51.69 13.6 -3 -8 0 -8.5 6.2 -3 -8 0 8.9 7.8 3 8 0 6.7 9.2 4 -9 0 25.3 14 -4 9 0 -1.5 10.3 3 -9 0 30.6 11.5 3 -9 0 64.39 17.7 -3 9 0 59.39 20 2 -9 0 -13 11.5 1 -9 0 17 9.5 0 -9 0 7.5 8.5 -1 -9 0 -2.4 8.8 1 -10 1 98.29 22.6 1 -10 1 111.19 19.7 -2 -9 1 66.69 7.2 -2 -9 1 78.19 17.7 -1 -9 1 16.3 7.8 0 -9 1 8.7 7.2 -1 9 -1 -8.1 7.7 1 -9 1 1.6 7 1 -9 1 -11.6 6.2 -2 9 -1 3.3 7.3 2 -9 1 6.8 5.4 2 -9 1 4.1 6.5 -3 9 -1 118.19 16.3 3 -9 1 130.29 15.8 3 -9 1 145.49 26.2 -4 9 -1 -9.5 8.1 4 -9 1 -6.5 9.1 3 8 -1 84.89 13.1 -3 -8 1 70.29 11.3 -3 -8 1 47.3 14.1 -2 -8 1 76.69 8.5 -2 -8 1 79.09 16.6 -1 -8 1 6 1.8 -1 -8 1 12.5 7.2 0 8 -1 103.29 14.5 0 -8 1 61.29 14.1 -1 8 -1 116.09 14.6 1 -8 1 113.79 15.4 -2 8 -1 43.2 10.4 2 -8 1 62.39 12 2 -8 1 39.7 13.8 -3 8 -1 18.4 6.2 3 -8 1 -5.3 4.9 3 -8 1 6.5 7 -4 8 -1 20.8 6.4 4 -8 1 10.8 8.9 -5 8 -1 40.1 9.8 5 -8 1 3.2 7.9 5 -8 1 13.6 5.3 -5 -7 1 232.68 23.6 -5 -7 1 178.58 22.4 -5 -7 1 202.28 26.4 4 7 -1 188.08 21.5 -4 -7 1 245.78 27.1 -4 -7 1 204.48 19.8 -4 -7 1 183.18 18.2 3 7 -1 28.5 8 -3 -7 1 28.8 7.6 -3 -7 1 37.9 9.9 -3 -7 1 24.4 10.1 -2 -7 1 69.19 13.3 -2 -7 1 87.79 16.7 1 7 -1 9.4 6.7 -1 -7 1 15.1 3.4 -1 -7 1 11.3 5.9 0 7 -1 3.3 4.8 0 -7 1 -3.6 4 -1 7 -1 75.69 12.8 1 -7 1 80.99 13.5 -2 7 -1 -0.4 4.1 2 -7 1 1 3.3 2 -7 1 -3.5 4.6 -3 7 -1 188.18 15.5 3 -7 1 194.28 22.9 3 -7 1 213.08 17 -4 7 -1 -8.4 4.2 4 -7 1 0.4 3.2 4 -7 1 -10.1 5.4 -5 7 -1 44.4 9.5 -5 7 -1 24.9 6.8 5 -7 1 22.2 6.8 5 -7 1 23 10.1 -6 7 -1 -3.9 7.7 -6 7 -1 0.6 7.2 6 -7 1 24 8.2 6 -7 1 23.7 11.1 -5 -6 1 57.89 12.2 -5 -6 1 52.29 10.7 4 6 -1 45.1 11.1 -4 -6 1 55.49 14 -4 -6 1 36.9 8.9 -4 -6 1 40 9.5 3 6 -1 28.5 7.9 -3 -6 1 43.7 8.7 -3 -6 1 36.8 8.6 -3 -6 1 46.7 12.6 2 6 -1 85.79 16 2 6 -1 93.59 10.2 -2 -6 1 75.89 8.9 -2 -6 1 104.09 13.5 -2 -6 1 83.39 11.8 1 6 -1 276.77 21.9 -1 -6 1 288.17 14 -1 -6 1 275.77 22 0 6 -1 49.2 10 0 -6 1 56.59 10.8 -1 6 -1 84.59 10.2 1 -6 1 77.09 11 -2 6 -1 39.2 13 2 -6 1 27 8.6 2 -6 1 38.3 7.6 3 -6 1 113.79 8.6 3 -6 1 110.39 15.8 -4 6 -1 34.3 7.5 4 -6 1 13.4 8.1 4 -6 1 26.5 6.1 -5 6 -1 -7.3 3.7 -5 6 -1 4.8 5 5 -6 1 7.1 5 5 -6 1 1.3 7.2 -6 6 -1 55.99 11.8 -6 6 -1 53.69 12.4 6 -6 1 51.39 12.3 6 -6 1 74.19 15.6 -6 -5 1 16.9 6.9 -6 -5 1 10 8.1 -6 -5 1 31.5 10.8 -5 -5 1 28.7 7.8 -5 -5 1 38.4 12.7 -5 -5 1 26 8.2 4 5 -1 20.6 8.2 -4 -5 1 27 6.1 -4 -5 1 30.2 10.1 -4 -5 1 35.9 8.5 3 5 -1 14.1 4.7 -3 -5 1 5.3 3.1 -3 -5 1 7.8 4.8 2 5 -1 8 4.7 2 5 -1 -2.1 2.9 -2 -5 1 0 2.6 -2 -5 1 8.8 3.1 -2 -5 1 7.6 3.3 1 5 -1 164.88 15.3 -1 -5 1 164.78 10.1 -1 -5 1 155.88 14.7 0 5 -1 117.69 11.8 0 -5 1 138.49 6.3 0 -5 1 149.29 13.1 -1 5 -1 356.46 19.2 1 -5 1 367.86 20 -2 5 -1 1259.37 42.7 2 -5 1 1275.67 36.5 2 -5 1 1217.48 54.09 2 -5 1 1297.57 43.6 -3 5 -1 383.96 19.9 -3 5 -1 392.06 18.8 3 -5 1 404.66 28.6 3 -5 1 395.36 19 -4 5 -1 4.1 2.9 4 -5 1 1.9 4.1 4 -5 1 6.6 3.8 -5 5 -1 6.1 4.6 -5 5 -1 11.4 4.9 5 -5 1 2.2 5.8 5 -5 1 -2.4 5.6 -6 5 -1 53.69 10.8 -6 5 -1 28.4 9.9 6 -5 1 29.1 10.7 -7 5 -1 19.5 7.9 -7 5 -1 2.5 8.5 -7 5 -1 -12.8 9.8 7 -5 1 5.4 8.5 -7 -4 1 4.3 10.4 -7 -4 1 2.9 14.1 -6 -4 1 38.7 7.4 -6 -4 1 60.99 16.2 -6 -4 1 62.09 13.1 -5 -4 1 479.75 37.1 -5 -4 1 487.45 24.6 -5 -4 1 487.95 32.1 4 4 -1 299.37 23 -4 -4 1 314.67 22.3 -4 -4 1 339.37 27.7 -4 -4 1 279.47 17.4 3 4 -1 642.74 31.6 -3 -4 1 631.44 36.2 -3 -4 1 667.53 31.2 2 4 -1 56.49 9.1 2 4 -1 41.5 8.9 -2 -4 1 56.49 7.1 -2 -4 1 56.99 7.8 -2 -4 1 62.89 9 1 4 -1 18.4 3.8 1 4 -1 27.8 6.7 -1 -4 1 17.8 3.7 -1 -4 1 20.3 5.3 0 4 -1 1149.58 39.8 0 -4 1 1114.69 30.9 0 -4 1 1143.09 40.1 -1 4 -1 213.68 12.3 1 -4 1 240.18 13.5 1 -4 1 230.88 8.9 1 -4 1 193.98 16.6 -2 4 -1 9.2 3.1 -2 4 -1 9.3 2.9 2 -4 1 8.7 3.1 2 -4 1 11.6 3.1 2 -4 1 14 5 -3 4 -1 52.69 6.7 -3 4 -1 59.29 7.2 3 -4 1 69.79 12.2 3 -4 1 59.89 7.5 -4 4 -1 21 6.1 -4 4 -1 32.8 7.9 4 -4 1 32.1 7.4 4 -4 1 25.7 7.3 -5 4 -1 413.06 24.7 -5 4 -1 399.96 26.4 5 -4 1 430.46 30 5 -4 1 381.96 25.9 -6 4 -1 266.47 22.5 6 -4 1 277.07 25.8 -7 4 -1 6.9 9.4 -7 4 -1 -6.4 5.3 -7 4 -1 0.8 6 7 -4 1 -6.8 5.5 -7 -3 1 17.5 7.7 -7 -3 1 4.4 10 -6 -3 1 9.9 7.7 -6 -3 1 3.6 4.2 -6 -3 1 24.7 10.2 5 3 -1 2.8 4.9 -5 -3 1 -1 4 -5 -3 1 17.2 7.7 -5 -3 1 8 3.8 4 3 -1 16.3 6.2 -4 -3 1 26.2 7.8 -4 -3 1 26.3 8.7 -4 -3 1 21.9 4.9 3 3 -1 2025.8 66.09 -3 -3 1 1998.2 71.69 -3 -3 1 2038.5 58.89 -3 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867.61 27.7 2 2 -1 9.4 2.8 -2 -2 1 2.1 1.8 -2 -2 1 4 1.3 -2 -2 1 6.2 2.6 1 2 -1 32.4 3.8 -1 -2 1 27.4 4.8 -1 -2 1 31.4 3.7 0 2 -1 2038.1 51.69 0 -2 1 2007.7 56.39 0 -2 1 1938.41 51.39 -1 2 -1 1852.61 50.59 -1 2 -1 1995.2 47.7 -1 2 -1 1910.81 56.99 1 -2 1 1846.62 50.29 1 -2 1 1883.61 56.59 -2 2 -1 1991.5 62.39 -2 2 -1 1987.9 57.69 2 -2 1 2072.09 62.79 2 -2 1 1941.01 57.19 -3 2 -1 74.69 9.1 -3 2 -1 88.29 9.2 3 -2 1 72.09 8.9 3 -2 1 73.49 8.5 -4 2 -1 57.79 10.5 -4 2 -1 52.19 10.4 -4 2 -1 64.39 9.2 4 -2 1 80.39 12.5 4 -2 1 75.59 9.9 -5 2 -1 882.91 42.5 -5 2 -1 910.11 43.1 -5 2 -1 858.91 41.7 5 -2 1 909.31 42.4 5 -2 1 867.01 42.8 -6 2 -1 723.83 61.79 -6 2 -1 641.54 38.2 -6 2 -1 626.64 37.5 6 -2 1 581.14 34.9 -7 2 -1 16.1 9.4 -7 2 -1 8 6.3 7 -2 1 26.8 8.5 8 1 -1 2.7 5.3 -8 -1 1 17.5 8.9 -8 -1 1 19.1 15.2 7 1 -1 0 4 -7 -1 1 -2.3 5.7 -7 -1 1 2 6.1 6 1 -1 204.68 13.5 -6 -1 1 211.18 14.3 -6 -1 1 211.78 21.1 5 1 -1 653.63 25.2 5 1 -1 612.14 34.8 -5 -1 1 672.13 25.9 -5 -1 1 648.44 38.4 -5 -1 1 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43.8 4 -8 3 280.87 30.7 4 -8 3 285.07 19 5 -8 3 18.9 9.6 5 -8 3 22.9 13.2 -5 -7 3 8.7 5.3 -5 -7 3 4.4 8.3 -5 -7 3 0.3 7 -5 -7 3 -3 5.1 -4 -7 3 143.29 15.6 -4 -7 3 148.09 19.5 -4 -7 3 153.28 15.5 -4 -7 3 112.49 12.9 -3 -7 3 67.49 14.5 -3 -7 3 69.89 12.1 -2 -7 3 32.2 8.6 -2 -7 3 38.1 8.6 -2 -7 3 25.2 6.2 -1 -7 3 11.2 3.4 -1 -7 3 18.4 6.3 -1 -7 3 11.8 5.7 0 -7 3 15 3.9 0 -7 3 2.6 5.5 0 -7 3 16.7 5.3 0 -7 3 18.1 4 1 -7 3 2.3 2.5 1 -7 3 0.2 2.3 1 -7 3 -3.8 3.6 2 -7 3 38.5 6.2 3 -7 3 14 8.2 3 -7 3 2 4.5 4 -7 3 378.06 33.9 4 -7 3 315.87 22.4 -5 7 -3 149.49 17.8 5 -7 3 131.69 18.7 5 -7 3 170.28 27.7 -6 -6 3 2.1 2.4 -6 -6 3 4.6 7.6 -6 -6 3 -3.1 1.9 -6 -6 3 -8.3 6.9 -5 -6 3 3.2 3.3 -5 -6 3 8.3 3.9 -5 -6 3 8.1 5.6 -5 -6 3 6.3 7.7 4 6 -3 22.8 7.3 -4 -6 3 4.9 4.1 -4 -6 3 5.6 4.3 -4 -6 3 4.5 4.5 -3 -6 3 89.29 11.4 -3 -6 3 90.79 15.7 -3 -6 3 107.09 11.7 -2 -6 3 145.49 12.5 -2 -6 3 182.08 16.3 -2 -6 3 166.88 16.3 -1 -6 3 321.17 23.6 -1 -6 3 296.27 16.6 -1 -6 3 281.77 20.9 0 -6 3 809.72 30.3 0 -6 3 790.72 40.9 0 -6 3 821.92 32.2 1 -6 3 61.69 7.1 1 -6 3 76.89 6.4 1 -6 3 83.99 15.1 2 -6 3 195.98 13.5 2 -6 3 215.38 21.9 3 -6 3 88.69 16.6 3 -6 3 96.19 10.6 -4 6 -3 202.88 18.1 4 -6 3 219.88 17 4 -6 3 194.08 23.7 -5 6 -3 3 2.9 -5 6 -3 8.7 3.6 -5 6 -3 7.2 6.8 5 -6 3 6.5 7.1 -6 6 -3 8 8.4 -6 6 -3 7.3 6.3 -6 6 -3 0.6 4.4 6 -6 3 10.7 8.9 -7 -5 3 3.9 8.8 -7 -5 3 11.7 10.5 -6 -5 3 160.48 22.8 -6 -5 3 179.58 20.4 -5 -5 3 394.16 31.6 -5 -5 3 454.55 35.1 -5 -5 3 398.26 16.2 -5 -5 3 406.86 17 4 5 -3 4.3 6.2 -4 -5 3 12.8 3.4 -4 -5 3 11.7 6 -4 -5 3 0.1 2.7 -4 -5 3 3.1 3.3 -3 -5 3 444.26 25.7 -3 -5 3 448.56 23.2 -3 -5 3 433.66 28.4 -2 -5 3 91.09 10.4 -2 -5 3 96.19 11.1 -1 -5 3 2.2 1.9 -1 -5 3 -1.7 1.6 -1 -5 3 1.4 2.1 0 -5 3 8.2 2.8 0 -5 3 -2.1 2.6 1 -5 3 10.1 4.5 1 -5 3 -1.9 2 2 -5 3 1059.89 38.3 2 -5 3 951.6 47.4 -3 5 -3 97.89 16.8 -3 5 -3 93.69 10.8 3 -5 3 113.59 11.1 3 -5 3 98.89 17.3 -4 5 -3 2.8 2.1 -4 5 -3 -4.4 3.9 -4 5 -3 -1.5 1.9 4 -5 3 -4.1 4.4 4 -5 3 16.5 5.6 -5 5 -3 6.1 4.2 -5 5 -3 3.3 4.1 -5 5 -3 14.1 5 5 -5 3 -0.5 5.3 -6 5 -3 36.9 8.7 -6 5 -3 28.4 7.9 -6 5 -3 39.6 10.3 6 -5 3 17.9 12.6 -7 -4 3 15.1 8.8 -7 -4 3 12.4 8.3 -6 -4 3 -1.4 4.4 -6 -4 3 5.2 6.6 5 4 -3 458.95 31.7 -5 -4 3 431.66 29.7 -5 -4 3 469.55 36.3 4 4 -3 114.79 12.8 -4 -4 3 100.89 14.2 -4 -4 3 109.69 7.2 -4 -4 3 109.59 6.6 -4 -4 3 122.79 13.3 3 4 -3 528.15 28.6 -3 -4 3 498.95 21.3 -3 -4 3 533.65 30.6 -3 -4 3 527.25 27.7 -2 -4 3 48.7 8.3 -2 -4 3 36.6 7.7 -2 -4 3 38.2 6.6 -1 -4 3 261.77 16 -1 -4 3 287.77 16 -1 -4 3 272.57 17.5 0 4 -3 800.62 36.1 0 -4 3 768.22 24.8 -1 4 -3 46.9 9.2 1 -4 3 61.89 7.3 1 -4 3 53.09 10.1 -2 4 -3 250.97 17.3 -2 4 -3 265.67 21.6 2 -4 3 297.87 17.9 2 -4 3 277.37 21.5 -3 4 -3 33.5 7.8 -3 4 -3 35.6 3.8 -3 4 -3 48 10.6 -3 4 -3 30.5 3.7 3 -4 3 25.2 7.6 3 -4 3 30.8 7.2 -4 4 -3 11.9 7.7 -4 4 -3 21.8 7.5 -4 4 -3 17.4 4.5 4 -4 3 17.4 7.3 4 -4 3 24.7 7.5 -5 4 -3 5.4 4.2 -5 4 -3 20.6 10.6 5 -4 3 6.4 7.3 -6 4 -3 30.5 8.6 -6 4 -3 39.7 10.8 6 -4 3 16.6 11.1 -7 -3 3 9 6.8 -7 -3 3 10.8 8.1 -6 -3 3 385.26 32.6 -6 -3 3 368.96 29.6 5 3 -3 904.51 45.2 -5 -3 3 940.11 45.3 -5 -3 3 910.81 49.4 4 3 -3 366.56 24.6 -4 -3 3 328.07 23.1 3 3 -3 410.76 24.1 -3 -3 3 382.46 22.5 -3 -3 3 365.76 13.8 -2 -3 3 88.09 7.3 -2 -3 3 94.09 9.6 1 3 -3 2 1.7 -1 -3 3 3 2 0 3 -3 1210.98 44.4 0 -3 3 1226.38 44.3 -1 3 -3 62.29 8.4 1 -3 3 44.4 9 1 -3 3 32.2 7.6 -2 3 -3 406.96 14.4 -2 3 -3 405.16 22.6 -2 3 -3 361.06 24.2 2 -3 3 418.16 25.7 2 -3 3 419.36 22.4 -3 3 -3 5.7 2.7 -3 3 -3 9.2 4.1 -3 3 -3 9 5 3 -3 3 11.2 5 3 -3 3 5.1 4.2 -4 3 -3 103.49 14.2 -4 3 -3 98.49 15.4 -4 3 -3 99.49 10.4 4 -3 3 120.69 15 4 -3 3 111.99 12.9 -5 3 -3 3.2 4.6 -5 3 -3 10.2 4.4 5 -3 3 -0.2 4.6 -6 3 -3 3.8 5.7 -6 3 -3 0.7 5.2 6 -3 3 -5.3 5.1 -8 -2 3 9.8 12.3 -8 -2 3 3.6 5.1 -7 -2 3 -3.4 7.3 -7 -2 3 -6.9 6.1 -6 -2 3 96.79 16.7 5 2 -3 57.29 11.6 -5 -2 3 50.09 11 4 2 -3 117.59 13.4 -4 -2 3 99.59 11.9 3 2 -3 186.48 15.2 -3 -2 3 172.58 14.2 2 2 -3 1164.58 34.5 -2 -2 3 1149.78 33.7 -2 -2 3 1149.58 41.6 1 2 -3 575.74 23.2 -1 -2 3 546.35 22.5 -1 -2 3 606.34 23.2 0 2 -3 16.7 4.5 0 -2 3 20 4.8 0 -2 3 17.6 3.3 -1 2 -3 77.29 5.7 -1 2 -3 66.09 8.6 1 -2 3 55.29 8.5 1 -2 3 64.09 5.2 1 -2 3 64.79 8.6 -2 2 -3 506.15 28.4 -2 2 -3 547.05 27.1 -2 2 -3 551.84 21.9 2 -2 3 545.85 28.8 2 -2 3 511.65 26 -3 2 -3 231.98 19.4 -3 2 -3 232.48 18.2 -3 2 -3 219.78 15.1 3 -2 3 209.88 18.3 3 -2 3 209.38 16.9 -4 2 -3 32.7 8.8 -4 2 -3 51.19 14.3 -4 2 -3 46.7 9 4 -2 3 39.8 10.1 4 -2 3 30.3 8 -5 2 -3 57.79 12.1 -5 2 -3 62.09 14.5 -5 2 -3 52.79 12.1 5 -2 3 65.39 14.1 -6 2 -3 100.19 18.2 -6 2 -3 109.29 19.1 6 -2 3 97.29 17.7 -8 -1 3 0.9 7 -8 -1 3 9.6 10 -7 -1 3 0.7 6.7 -6 -1 3 264.07 25.7 -5 -1 3 -2 2.1 4 1 -3 8.6 3.7 -4 -1 3 20.4 6.3 3 1 -3 114.79 5.5 3 1 -3 91.29 10.2 -3 -1 3 108.09 11.9 2 1 -3 144.69 8.4 -2 -1 3 144.79 8.6 -2 -1 3 158.58 12.4 -2 -1 3 143.29 11.6 1 1 -3 82.49 7.3 1 1 -3 72.19 7.4 -1 -1 3 76.29 7 -1 -1 3 69.69 7.2 0 1 -3 1971.7 57.29 0 1 -3 1985.4 61.09 0 -1 3 2082.59 61.19 0 -1 3 2016.4 60.49 0 -1 3 1983.5 57.49 -1 1 -3 3720.03 101.79 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0 -3 7.6 3.2 -1 0 -3 4.7 3 1 0 3 14.8 4.7 1 0 3 8.9 3.6 1 0 3 9 3.6 -2 0 -3 82.29 14.3 -2 0 -3 72.49 9.4 -2 0 -3 72.89 9.6 2 0 3 95.99 10.3 2 0 3 77.39 9.9 2 0 3 71.49 9.2 -3 0 -3 20.5 5.9 -3 0 -3 10.8 5.5 -3 0 -3 19 5.8 3 0 3 13.4 4.7 3 0 3 8.2 4.5 3 0 3 17 6.4 -4 0 -3 308.57 32 -4 0 -3 395.06 28 -4 0 -3 354.76 26.5 4 0 3 344.27 32.1 4 0 3 404.26 27.4 -5 0 -3 590.34 38.5 -5 0 -3 604.84 38.1 -5 0 -3 663.43 40.5 5 0 3 615.74 37.8 -6 0 -3 15.5 8.2 -6 0 -3 2.7 6.1 6 0 3 11.1 8.4 8 -1 -3 -1.7 3.9 -8 1 3 7.4 8.4 7 -1 -3 7.9 4.2 -7 1 3 0.4 4.7 6 -1 -3 6.6 3.8 6 -1 -3 -3.8 4.5 -6 1 3 0.7 4.7 -6 1 3 2.1 5 5 -1 -3 72.99 8.7 5 -1 -3 90.79 11.6 -5 1 3 86.89 14 -5 1 3 83.29 14.6 4 -1 -3 1025.6 42.9 -4 1 3 1118.69 43.8 -4 1 3 1021.9 46.4 3 -1 -3 17.1 4.6 -3 1 3 11.7 4.3 -3 1 3 13.2 5 2 -1 -3 404.56 23.3 2 -1 -3 378.46 19.9 -2 1 3 412.96 23.4 1 -1 -3 0 1.8 1 -1 -3 2.3 1.7 -1 1 3 2.1 2.1 0 -1 -3 377.76 22 0 -1 -3 385.46 21.5 0 1 3 379.06 22 0 1 3 373.06 21.8 0 1 3 380.76 19.4 -1 -1 -3 139.39 13.1 -1 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586.94 31.2 -1 -2 -3 601.04 28.5 -1 -2 -3 590.54 32.9 1 2 3 607.04 32.7 1 2 3 590.04 27.5 1 2 3 604.54 33.1 -2 -2 -3 127.69 14.3 -2 -2 -3 187.78 18.1 -2 -2 -3 155.18 14.7 2 2 3 132.99 13.3 2 2 3 163.38 16.8 2 2 3 156.18 17 -3 -2 -3 20.5 9.6 -3 -2 -3 13.5 7 -3 -2 -3 16.4 7 3 2 3 8.8 7.3 3 2 3 20.7 7.6 3 2 3 17.5 5.7 -4 -2 -3 287.47 24.6 -4 -2 -3 281.97 27 -4 -2 -3 274.97 24 4 2 3 330.77 26.1 -5 -2 -3 579.54 42.8 -5 -2 -3 590.54 39.8 5 2 3 586.24 37.7 -6 -2 -3 6.6 8.5 -6 -2 -3 2.3 7.6 6 2 3 21.4 10.2 8 -3 -3 5 6.8 -8 3 3 -4.9 7.1 7 -3 -3 108.09 15 -7 3 3 129.99 19.4 6 -3 -3 250.57 21.8 6 -3 -3 288.37 22.8 -6 3 3 283.37 23 -5 3 3 171.58 19 -5 3 3 166.58 15.9 -4 3 3 177.88 18.5 -4 3 3 164.68 13.7 3 -3 -3 21.5 7 -3 3 3 25.8 7.7 -3 3 3 17.9 4.9 2 -3 -3 13.8 5.3 2 -3 -3 13.2 4.8 -2 3 3 14.6 5.6 1 -3 -3 4.2 4.2 1 -3 -3 2.8 3.2 -1 3 3 4 4 -1 3 3 1.2 2 0 -3 -3 180.28 17 0 -3 -3 177.88 17.6 0 3 3 181.18 16.3 0 3 3 175.48 16.2 -1 -3 -3 32.4 7.5 -1 -3 -3 27.2 8.2 -1 -3 -3 29.8 8.5 1 3 3 24.7 6.5 1 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