#------------------------------------------------------------------------------ #$Date: 2021-09-15 01:55:27 +0300 (Wed, 15 Sep 2021) $ #$Revision: 269138 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/82/7708290.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708290 loop_ _publ_author_name 'Saraiva Vilas Boas de Almeida, Patr\'icia Saraiva Vilas Boas' 'de Arruda, Henrique Jefferson' 'Sousa, Gleyton Silva' 'Vit\'orio, Felipe' 'Fran\,ca, Jos\'e' 'Ferreira, Larissa' 'Guedes, Guilherme P.' 'Silva, Heveline' 'K\"ummerle, Arthur Eugen' 'Neves, Amanda Porto' _publ_section_title ; Cytotoxic evaluation and DNA interaction of RuII-bipy complexes containing coumarin-based ligands ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT01567B _journal_year 2021 _chemical_formula_moiety 'C38 H36 N5 O5 Ru, F6 P' _chemical_formula_sum 'C38 H36 F6 N5 O5 P Ru' _chemical_formula_weight 888.76 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary difmap _audit_creation_date 2020-03-26 _audit_creation_method ; Olex2 1.3 (compiled 2020.02.04 svn.rd84adfe8 for OlexSys, GUI svn.r6032) ; _audit_update_record ; 2021-04-12 deposited with the CCDC. 2021-09-14 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 110.5490(10) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 28.3360(12) _cell_length_b 10.5670(3) _cell_length_c 26.8770(9) _cell_measurement_reflns_used 9913 _cell_measurement_temperature 298.15 _cell_measurement_theta_max 26.21 _cell_measurement_theta_min 2.32 _cell_volume 7535.6(5) _computing_cell_refinement 'APEX3 v2017.3-0 (Bruker AXS)' _computing_data_collection 'Bruker Instrument Service vV6.2.6' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_molecular_graphics 'Mercury 4.3.1 (Macrae et al., 2020)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2014/7 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 298.15 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8-Venture' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0521 _diffrn_reflns_av_unetI/netI 0.0325 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 33 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 31 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 41132 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.027 _diffrn_reflns_theta_max 25.027 _diffrn_reflns_theta_min 2.323 _diffrn_source_current 1.0 _diffrn_source_power 0.05 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.539 _exptl_absorpt_correction_T_max 0.7454 _exptl_absorpt_correction_T_min 0.6802 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0779 before and 0.0546 after correction. The Ratio of minimum to maximum transmission is 0.9125. The \l/2 correction factor is Not present. ; _exptl_crystal_colour purple _exptl_crystal_density_diffrn 1.567 _exptl_crystal_description block _exptl_crystal_F_000 3616 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: Ethanol' _exptl_crystal_size_max 0.244 _exptl_crystal_size_mid 0.228 _exptl_crystal_size_min 0.072 _refine_diff_density_max 0.462 _refine_diff_density_min -0.459 _refine_diff_density_rms 0.054 _refine_ls_extinction_coef 0.00021(6) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2014/7 (Sheldrick 2014' _refine_ls_goodness_of_fit_ref 1.047 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 509 _refine_ls_number_reflns 6651 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.047 _refine_ls_R_factor_all 0.0520 _refine_ls_R_factor_gt 0.0360 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0312P)^2^+14.2536P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0765 _refine_ls_wR_factor_ref 0.0839 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5341 _reflns_number_total 6651 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt01567b2.cif _cod_data_source_block mo_p2bce2_patricia_0m_a _cod_database_code 7708290 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.962 _shelx_estimated_absorpt_t_min 0.880 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Secondary CH2 refined with riding coordinates: C13(H13A,H13B), C17(H17A,H17B), C15(H15A,H15B) 2.b Aromatic/amide H refined with riding coordinates: C32(H32), C31(H31), C30(H30), C29(H29), C35(H35), C36(H36), C37(H37), C38(H38), C25(H25), C26(H26), C27(H27), C28(H28), C22(H22), C21(H21), C20(H20), C19(H19), C11(H11), C4(H4), C5(H5), C6(H6), C8(H8) 2.c Idealised Me refined as rotating group: C14(H14A,H14B,H14C), C18(H18A,H18B,H18C), C16(H16A,H16B,H16C) ; _shelx_res_file ; mo_p2bce2_patricia_0m_a.res created by SHELXL-2014/7 TITL mo_P2BCE2_Patricia_0m_a.res in C2/c CELL 0.71073 28.336 10.567 26.877 90 110.549 90 ZERR 8 0.0012 0.0003 0.0009 0 0.001 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H F N O P Ru UNIT 304 288 48 40 40 8 8 L.S. 50 PLAN 5 SIZE 0.072 0.228 0.244 TEMP 25 HTAB C28 F4 HTAB C20 O3 CONF BOND $H MORE -1 fmap 2 acta MERG 2 REM REM REM WGHT 0.031200 14.253600 EXTI 0.000207 FVAR 0.19526 RU1 7 0.607660 0.595438 0.409486 11.00000 0.03278 0.03586 = 0.03029 -0.00043 0.00568 0.00377 P1 6 0.468913 1.087957 0.363953 11.00000 0.06477 0.04551 = 0.05333 -0.00260 0.02408 -0.00469 O4 5 0.676348 0.648266 0.403504 11.00000 0.03515 0.04942 = 0.03650 0.00674 0.00943 0.00244 O3 5 0.643457 0.495235 0.479858 11.00000 0.03277 0.04818 = 0.03614 0.00712 0.00660 0.00548 F2 3 0.476783 1.211776 0.334753 11.00000 0.12048 0.06081 = 0.06598 0.00502 0.03028 -0.02252 F4 3 0.511841 1.019206 0.351164 11.00000 0.10716 0.08745 = 0.20573 -0.03559 0.09585 0.00135 F6 3 0.507549 1.141732 0.417712 11.00000 0.08170 0.09819 = 0.06658 -0.00048 0.00207 -0.01683 F3 3 0.428391 1.036491 0.310106 11.00000 0.10988 0.08299 = 0.06311 -0.02107 0.02685 -0.03091 F5 3 0.424520 1.155424 0.376649 11.00000 0.07855 0.09514 = 0.10527 -0.02736 0.04251 -0.00016 F1 3 0.459957 0.965069 0.393348 11.00000 0.11095 0.08035 = 0.11005 0.03516 0.02971 -0.01643 N4 4 0.603186 0.755683 0.450883 11.00000 0.03817 0.03881 = 0.03222 -0.00249 0.00686 0.00179 N5 4 0.540415 0.566847 0.418716 11.00000 0.03538 0.03788 = 0.03905 0.00087 0.00740 0.00529 N3 4 0.579116 0.672342 0.335804 11.00000 0.03395 0.03973 = 0.03580 0.00190 0.00585 0.00400 N2 4 0.602880 0.437932 0.363557 11.00000 0.02929 0.03868 = 0.03842 -0.00059 0.00799 0.00501 O5 5 0.760102 0.658690 0.432349 11.00000 0.04191 0.07889 = 0.06227 0.02961 0.01424 -0.00313 O2 5 0.797414 0.392264 0.559848 11.00000 0.04008 0.26065 = 0.19974 0.18911 0.02173 0.01246 C10 1 0.691204 0.472942 0.496506 11.00000 0.03994 0.04269 = 0.03675 0.00096 0.00712 0.00154 O1 5 0.773498 0.256253 0.606095 11.00000 0.03740 0.08900 = 0.07303 0.04589 0.01489 0.00975 C34 1 0.562168 0.762457 0.465796 11.00000 0.04294 0.04589 = 0.03457 0.00053 0.01042 0.00591 C33 1 0.526609 0.656663 0.447559 11.00000 0.04139 0.04307 = 0.04824 0.00030 0.01542 0.00661 C32 1 0.482058 0.646442 0.457375 11.00000 0.05862 0.05816 = 0.10227 -0.01309 0.04542 0.00291 AFIX 43 H32 2 0.473243 0.708282 0.477144 11.00000 -1.20000 AFIX 0 C31 1 0.450950 0.545258 0.437976 11.00000 0.05288 0.06437 = 0.14409 -0.01501 0.05348 -0.00409 AFIX 43 H31 2 0.421019 0.537510 0.444646 11.00000 -1.20000 AFIX 0 C30 1 0.464264 0.455630 0.408694 11.00000 0.04292 0.05082 = 0.10932 -0.01245 0.02923 -0.00577 AFIX 43 H30 2 0.443345 0.386803 0.394740 11.00000 -1.20000 AFIX 0 C29 1 0.508784 0.468838 0.400274 11.00000 0.04194 0.04129 = 0.06292 -0.00737 0.01272 -0.00073 AFIX 43 H29 2 0.517740 0.406717 0.380728 11.00000 -1.20000 AFIX 0 C35 1 0.554783 0.864053 0.494657 11.00000 0.05784 0.05737 = 0.05320 -0.01425 0.02197 0.00319 AFIX 43 H35 2 0.526883 0.866370 0.505258 11.00000 -1.20000 AFIX 0 C36 1 0.588937 0.961244 0.507486 11.00000 0.07158 0.05622 = 0.05654 -0.02310 0.01703 0.00161 AFIX 43 H36 2 0.584614 1.029677 0.527222 11.00000 -1.20000 AFIX 0 C37 1 0.629193 0.956931 0.491159 11.00000 0.05873 0.04915 = 0.06033 -0.01798 0.01356 -0.00957 AFIX 43 H37 2 0.652030 1.023643 0.498537 11.00000 -1.20000 AFIX 0 C38 1 0.635761 0.852909 0.463637 11.00000 0.04374 0.05185 = 0.05065 -0.00666 0.01316 -0.00437 AFIX 43 H38 2 0.663885 0.849692 0.453431 11.00000 -1.20000 AFIX 0 C24 1 0.574051 0.591349 0.294958 11.00000 0.03678 0.04596 = 0.03695 0.00128 0.00974 0.00438 C25 1 0.562091 0.635376 0.243196 11.00000 0.06386 0.06795 = 0.03594 0.00073 0.01551 0.00921 AFIX 43 H25 2 0.557889 0.578603 0.215528 11.00000 -1.20000 AFIX 0 C26 1 0.556537 0.762396 0.233145 11.00000 0.08360 0.07022 = 0.04631 0.01767 0.01913 0.01251 AFIX 43 H26 2 0.549252 0.793040 0.198820 11.00000 -1.20000 AFIX 0 C27 1 0.561865 0.843697 0.274376 11.00000 0.08848 0.04864 = 0.05728 0.01497 0.01783 0.00702 AFIX 43 H27 2 0.558301 0.930429 0.268353 11.00000 -1.20000 AFIX 0 C28 1 0.572477 0.796494 0.324557 11.00000 0.06407 0.04037 = 0.04762 0.00278 0.00924 0.00611 AFIX 43 H28 2 0.575213 0.852710 0.352056 11.00000 -1.20000 AFIX 0 C23 1 0.583745 0.457966 0.310139 11.00000 0.03651 0.04732 = 0.03566 -0.00677 0.01065 0.00379 C22 1 0.574026 0.358959 0.274862 11.00000 0.07169 0.05563 = 0.04511 -0.01077 0.01219 0.00705 AFIX 43 H22 2 0.560865 0.374421 0.238503 11.00000 -1.20000 AFIX 0 C21 1 0.583745 0.237448 0.293317 11.00000 0.07992 0.05102 = 0.06449 -0.01952 0.01603 0.00355 AFIX 43 H21 2 0.577106 0.169789 0.269724 11.00000 -1.20000 AFIX 0 C20 1 0.603446 0.216893 0.347187 11.00000 0.05368 0.04017 = 0.07294 -0.00425 0.01904 0.00895 AFIX 43 H20 2 0.610382 0.135166 0.360616 11.00000 -1.20000 AFIX 0 C19 1 0.612677 0.318403 0.380689 11.00000 0.04043 0.04225 = 0.04899 0.00441 0.01066 0.00990 AFIX 43 H19 2 0.626404 0.303890 0.417092 11.00000 -1.20000 AFIX 0 C12 1 0.717402 0.612374 0.436050 11.00000 0.03876 0.04788 = 0.04295 0.00498 0.01044 0.00072 C13 1 0.757162 0.754980 0.394050 11.00000 0.06336 0.06959 = 0.05055 0.01797 0.01833 -0.00413 AFIX 23 H13A 2 0.740790 0.829839 0.401222 11.00000 -1.20000 H13B 2 0.738022 0.725163 0.358541 11.00000 -1.20000 AFIX 0 C14 1 0.810176 0.784670 0.398704 11.00000 0.07401 0.09230 = 0.08338 0.02619 0.03558 -0.01295 AFIX 137 H14A 2 0.828189 0.817897 0.433458 11.00000 -1.50000 H14B 2 0.809930 0.846273 0.372361 11.00000 -1.50000 H14C 2 0.826424 0.708888 0.393279 11.00000 -1.50000 AFIX 0 C11 1 0.725934 0.526228 0.477878 11.00000 0.03339 0.06496 = 0.05534 0.02467 0.00891 0.00453 AFIX 43 H11 2 0.759270 0.502146 0.495175 11.00000 -1.20000 AFIX 0 C3 1 0.708689 0.379197 0.541230 11.00000 0.03508 0.04584 = 0.04143 0.00699 0.00821 0.00191 C4 1 0.674792 0.319972 0.558257 11.00000 0.03365 0.04631 = 0.04038 0.00325 0.00588 0.00240 AFIX 43 H4 2 0.640850 0.339610 0.541831 11.00000 -1.20000 AFIX 0 C9 1 0.688400 0.229571 0.599840 11.00000 0.04146 0.04243 = 0.03919 0.00190 0.01083 -0.00462 C5 1 0.655628 0.167918 0.620411 11.00000 0.04083 0.06293 = 0.05249 0.00840 0.00832 -0.00575 AFIX 43 H5 2 0.621396 0.186528 0.606443 11.00000 -1.20000 AFIX 0 C6 1 0.672347 0.081481 0.660269 11.00000 0.05443 0.06180 = 0.05882 0.01601 0.01553 -0.01868 AFIX 43 H6 2 0.649400 0.043838 0.673344 11.00000 -1.20000 AFIX 0 C7 1 0.723998 0.047404 0.682369 11.00000 0.06637 0.04447 = 0.04561 0.00625 0.00967 -0.00987 C8 1 0.757235 0.109834 0.662525 11.00000 0.04845 0.05125 = 0.05118 0.01375 0.01010 0.00500 AFIX 43 H8 2 0.791549 0.092057 0.676203 11.00000 -1.20000 AFIX 0 C1 1 0.738755 0.197566 0.622686 11.00000 0.04223 0.04498 = 0.04535 0.00505 0.01367 -0.00097 C2 1 0.761705 0.348045 0.567291 11.00000 0.04121 0.10551 = 0.08385 0.05482 0.01713 0.00692 N1 4 0.740171 -0.043076 0.721093 11.00000 0.07573 0.06601 = 0.06417 0.02776 0.01180 -0.00643 C17 1 0.794442 -0.085419 0.742188 11.00000 0.10659 0.07893 = 0.06427 0.02261 0.01901 0.00764 AFIX 23 H17A 2 0.796055 -0.173431 0.752915 11.00000 -1.20000 H17B 2 0.808581 -0.078913 0.714237 11.00000 -1.20000 AFIX 0 C18 1 0.824288 -0.008477 0.787598 11.00000 0.11860 0.17272 = 0.09624 -0.02066 0.03071 0.02630 AFIX 137 H18A 2 0.824677 0.077706 0.776449 11.00000 -1.50000 H18B 2 0.858151 -0.040325 0.801352 11.00000 -1.50000 H18C 2 0.809618 -0.012334 0.814785 11.00000 -1.50000 AFIX 0 C15 1 0.705732 -0.098345 0.745190 11.00000 0.09869 0.08250 = 0.07566 0.03652 0.00909 -0.02581 AFIX 23 H15A 2 0.719903 -0.177504 0.762190 11.00000 -1.20000 H15B 2 0.673957 -0.117488 0.717248 11.00000 -1.20000 AFIX 0 C16 1 0.695763 -0.015365 0.785031 11.00000 0.12073 0.17740 = 0.08442 0.01357 0.04615 -0.04185 AFIX 137 H16A 2 0.726611 -0.001095 0.814248 11.00000 -1.50000 H16B 2 0.671777 -0.055495 0.797747 11.00000 -1.50000 H16C 2 0.682458 0.064110 0.768840 11.00000 -1.50000 AFIX 0 HKLF 4 REM mo_P2BCE2_Patricia_0m_a.res in C2/c REM R1 = 0.0360 for 5341 Fo > 4sig(Fo) and 0.0520 for all 6637 data REM 509 parameters refined using 0 restraints END WGHT 0.0312 14.2534 REM Highest difference peak 0.462, deepest hole -0.459, 1-sigma level 0.054 Q1 1 0.7829 -0.0115 0.7636 11.00000 0.05 0.46 Q2 1 0.7882 0.4447 0.5795 11.00000 0.05 0.43 Q3 1 0.4906 0.9359 0.3747 11.00000 0.05 0.34 Q4 1 0.7797 0.3407 0.5317 11.00000 0.05 0.34 Q5 1 0.4919 1.1172 0.3149 11.00000 0.05 0.31 ; _shelx_res_checksum 74756 _shelx_hkl_file ; -4 0 0 1004.90 25.30 6 0 0 7301.37 171.08 -6 0 0 7876.81 171.48 -8 0 0 195.08 9.70 8 0 0 202.38 10.10 10 0 0 1466.25 40.00 -10 0 0 1456.15 39.90 -12 0 0 39.30 7.20 12 0 0 37.80 6.80 -14 0 0 1807.52 51.29 14 0 0 1846.12 51.49 -16 0 0 32.70 7.80 16 0 0 27.70 7.40 -18 0 0 219.38 16.60 18 0 0 198.88 15.20 18 0 0 255.87 17.80 20 0 0 38.20 10.10 20 0 0 44.90 11.20 22 0 0 287.17 23.00 -22 0 0 303.87 22.40 22 0 0 310.37 20.80 24 0 0 525.25 29.30 -24 0 0 511.15 29.40 24 0 0 515.35 30.60 26 0 0 68.39 15.90 26 0 0 65.49 16.60 -28 0 0 493.75 34.60 28 0 0 490.35 34.00 -30 0 0 79.89 22.00 30 0 0 26.30 17.30 30 0 0 34.20 16.50 -3 -1 0 2400.26 55.49 3 -1 0 2400.46 54.69 3 -1 0 2363.26 54.99 3 1 0 2394.06 55.79 -5 -1 0 3214.68 75.49 -5 1 0 3188.58 74.49 5 1 0 3265.67 75.49 -7 -1 0 18.30 4.20 7 -1 0 19.10 3.90 7 1 0 16.70 4.10 -7 1 0 22.70 3.90 -9 -1 0 863.81 26.80 9 -1 0 856.91 26.00 -9 1 0 911.41 26.40 9 1 0 927.71 27.10 11 -1 0 608.84 21.60 -11 -1 0 662.33 22.90 11 1 0 650.63 22.70 -11 1 0 648.04 21.90 -13 -1 0 1435.66 42.60 13 -1 0 1448.66 41.90 -13 1 0 1459.25 41.90 13 1 0 1456.05 42.50 -15 -1 0 494.05 22.10 15 -1 0 496.95 22.60 15 -1 0 476.45 20.80 -15 1 0 524.95 21.30 15 1 0 472.75 21.60 17 -1 0 75.79 11.70 17 -1 0 114.99 12.50 -17 -1 0 98.49 11.80 -17 1 0 93.89 12.00 17 1 0 92.69 11.90 19 -1 0 849.61 34.80 19 -1 0 866.91 33.20 -19 -1 0 843.72 34.30 -19 1 0 835.32 32.60 19 1 0 920.61 34.40 19 1 0 834.72 34.50 21 -1 0 3.40 8.60 21 -1 0 -0.30 8.30 -21 -1 0 0.70 8.90 -21 1 0 10.40 9.50 21 1 0 0.30 9.50 21 1 0 1.20 8.40 23 -1 0 168.28 20.50 23 -1 0 134.39 18.50 -23 -1 0 162.88 20.00 23 1 0 201.68 20.30 -23 1 0 167.58 19.40 23 1 0 145.49 17.30 -25 -1 0 121.39 20.10 25 -1 0 170.08 20.30 25 -1 0 148.39 19.80 -25 1 0 132.09 19.50 25 1 0 173.48 19.70 25 1 0 169.88 21.70 27 -1 0 371.46 28.10 -27 -1 0 365.66 31.70 27 1 0 384.76 31.50 27 1 0 374.66 28.40 -29 -1 0 52.99 19.90 29 -1 0 62.79 17.40 29 -1 0 47.40 16.20 29 1 0 31.30 16.60 29 1 0 87.19 21.80 29 1 0 65.49 18.70 -29 1 0 58.09 21.20 31 -1 0 99.99 20.20 31 -1 0 73.49 20.00 31 1 0 61.19 23.40 31 1 0 99.99 21.00 31 1 0 61.69 20.80 -31 1 0 45.10 24.00 0 -2 0 2287.97 53.59 0 -2 0 2182.88 53.29 0 2 0 2290.17 52.89 0 2 0 2271.17 53.59 2 -2 0 348.87 12.80 2 -2 0 393.26 12.70 2 -2 0 389.56 10.50 -2 -2 0 396.76 11.90 -2 -2 0 379.56 12.90 2 2 0 397.96 12.10 -2 2 0 382.66 12.70 2 2 0 405.76 12.90 -2 2 0 384.56 11.50 -4 -2 0 5.00 2.80 -4 -2 0 2.70 3.30 4 -2 0 3.10 2.70 4 -2 0 3.60 2.40 4 -2 0 4.10 2.40 -4 2 0 4.10 3.10 4 2 0 1.80 2.80 4 2 0 4.60 2.90 6 -2 0 607.04 18.60 6 -2 0 608.74 18.50 6 -2 0 611.54 18.00 -6 -2 0 628.44 19.30 6 2 0 630.44 19.30 6 2 0 585.84 19.50 -8 -2 0 99.29 7.90 8 -2 0 93.19 7.50 8 -2 0 92.39 6.90 8 2 0 87.19 7.80 8 2 0 90.19 7.90 -8 2 0 87.29 6.40 10 -2 0 165.38 10.70 10 -2 0 168.08 10.10 -10 -2 0 149.29 10.50 10 2 0 164.18 11.20 10 2 0 179.18 11.00 -10 2 0 178.48 9.80 -12 -2 0 655.83 24.60 12 -2 0 663.23 23.40 12 -2 0 669.93 25.10 -12 2 0 689.53 23.40 12 2 0 678.33 25.10 12 2 0 655.33 24.50 -14 -2 0 20.80 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8.60 10 2 -4 73.29 7.60 10 2 -4 66.59 7.50 -8 -2 4 469.55 16.40 -8 -2 4 469.65 17.20 8 -2 -4 480.15 17.00 8 2 -4 465.55 16.90 8 2 -4 452.25 16.50 -6 -2 4 46.00 4.90 6 -2 -4 46.00 5.40 -6 -2 4 47.00 6.00 6 2 -4 59.19 5.80 6 2 -4 41.50 5.20 4 -2 -4 279.07 7.40 4 -2 -4 284.27 11.30 -4 -2 4 288.37 9.80 -4 -2 4 279.37 11.70 -4 2 4 285.17 11.40 4 2 -4 267.27 11.00 4 2 -4 278.47 9.90 0 -2 4 1197.78 29.40 0 -2 4 1219.88 30.90 0 -2 -4 1163.88 28.10 0 -2 -4 1188.48 30.70 0 2 4 1215.68 28.30 0 2 -4 1198.18 29.40 0 2 4 1151.48 29.00 0 2 4 1168.38 30.70 0 2 -4 1173.68 30.40 0 2 -4 984.10 29.60 2 -2 4 3591.74 84.89 -2 -2 -4 3649.63 83.39 2 -2 4 3549.34 82.49 2 -2 4 3579.14 84.09 -2 -2 -4 3819.02 85.79 2 2 4 3567.74 84.99 -2 2 -4 3517.35 84.09 2 2 4 3543.55 82.99 -2 2 -4 4036.80 82.99 -2 2 -4 3529.75 80.79 4 -2 4 574.34 17.10 4 -2 4 678.63 21.40 -4 -2 -4 640.14 18.80 4 -2 4 624.74 18.90 -4 -2 -4 625.84 19.80 4 2 4 619.04 18.20 -4 2 -4 592.14 18.80 -4 2 -4 592.34 16.30 4 2 4 636.64 19.90 -6 -2 -4 244.28 11.10 6 -2 4 245.88 9.20 6 -2 4 238.98 11.10 -6 -2 -4 243.98 11.60 6 -2 4 244.78 9.40 -6 2 -4 245.68 9.40 -6 2 -4 247.18 11.50 6 2 4 240.68 10.70 6 2 4 249.18 11.80 8 -2 4 294.47 13.80 -8 -2 -4 301.07 14.20 8 -2 4 294.07 11.90 8 2 4 322.47 14.00 -8 2 -4 282.37 11.80 8 2 4 292.17 13.90 -8 2 -4 307.67 14.30 10 -2 4 138.69 9.30 -10 -2 -4 118.59 10.20 10 -2 4 119.39 10.70 10 2 4 122.69 10.70 10 2 4 142.69 10.70 -10 2 -4 128.39 8.90 12 -2 4 148.99 11.90 12 -2 4 141.99 10.30 -12 -2 -4 141.59 11.70 12 2 4 142.79 11.70 12 2 4 138.29 11.60 -12 2 -4 135.79 10.20 -14 -2 -4 299.07 17.50 14 -2 4 294.77 15.60 14 -2 4 272.17 17.20 -14 2 -4 302.37 15.90 14 2 4 292.67 17.60 14 2 4 283.57 17.30 16 -2 4 7.00 7.00 -16 -2 -4 4.50 7.80 16 -2 4 7.80 7.50 -16 2 -4 6.90 6.70 16 2 4 2.40 7.30 16 2 4 3.50 6.90 18 -2 4 93.39 13.30 18 -2 4 84.89 11.90 -18 -2 -4 98.29 14.20 18 2 4 75.49 12.40 18 2 4 87.79 13.30 -18 2 -4 88.09 12.50 20 -2 4 22.90 10.30 -20 -2 -4 28.30 11.50 20 -2 4 29.00 10.30 20 2 4 29.30 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4 871.81 28.20 9 -3 4 11.50 4.00 -9 -3 -4 19.00 5.80 9 -3 4 10.80 4.90 9 -3 4 13.00 3.90 -9 3 -4 5.20 4.20 -9 3 -4 22.00 4.20 9 3 4 14.50 5.90 9 3 4 18.10 6.30 9 3 4 9.20 4.50 11 -3 4 -2.10 3.70 -11 -3 -4 0.10 5.10 11 -3 4 -0.60 4.90 11 -3 4 2.50 4.20 -11 3 -4 -2.40 3.50 11 3 4 3.10 5.40 11 3 4 -3.90 4.60 13 -3 4 286.47 14.40 13 -3 4 267.77 13.70 13 -3 4 271.47 16.30 -13 -3 -4 269.37 17.20 13 3 4 265.17 16.50 13 3 4 295.17 16.80 -13 3 -4 280.27 14.20 -15 -3 -4 188.78 16.20 15 -3 4 165.28 14.70 15 -3 4 176.38 12.00 15 -3 4 186.38 13.20 -15 3 -4 189.18 13.50 15 3 4 199.78 15.30 15 3 4 162.48 15.60 -17 -3 -4 227.48 19.00 17 -3 4 229.58 18.20 17 -3 4 228.68 15.70 17 3 4 253.57 18.20 -17 3 -4 212.98 16.10 17 3 4 236.98 18.60 -19 -3 -4 4.90 10.00 19 -3 4 6.20 7.80 19 -3 4 -1.50 8.90 19 3 4 17.60 10.80 -19 3 -4 10.50 8.80 19 3 4 -1.00 8.90 19 3 4 33.30 10.50 21 -3 4 -5.30 8.60 -21 -3 -4 -16.30 11.00 21 -3 4 -9.70 7.80 -21 3 -4 2.30 10.60 21 3 4 -1.80 9.30 21 3 4 3.80 9.70 23 -3 4 6.20 11.60 23 -3 4 12.00 10.90 -23 3 -4 -3.10 11.40 23 3 4 -18.00 10.90 23 3 4 -4.40 11.10 25 -3 4 30.20 12.90 25 -3 4 12.00 13.00 -25 -3 -4 -1.60 16.00 25 3 4 3.70 13.00 -25 3 -4 -10.20 12.70 25 3 4 -2.00 16.30 25 3 4 -1.90 12.40 -27 -3 -4 53.39 20.40 27 -3 4 50.39 16.00 27 -3 4 30.70 15.00 27 3 4 70.59 20.90 27 3 4 29.40 15.80 27 3 4 48.80 16.30 30 -4 -4 66.29 19.30 30 -4 -4 26.30 17.30 30 -4 -4 21.40 18.80 30 4 -4 96.89 23.20 30 4 -4 78.99 20.10 30 4 -4 63.09 19.10 28 -4 -4 123.79 20.70 -28 -4 4 121.59 22.40 28 -4 -4 93.29 18.20 28 -4 -4 135.39 21.20 28 4 -4 155.78 25.80 28 4 -4 159.28 22.20 -26 -4 4 -11.50 14.00 26 -4 -4 -9.20 12.50 26 -4 -4 8.10 12.90 26 -4 -4 14.60 11.70 26 4 -4 -1.20 15.30 26 4 -4 23.10 16.10 -24 -4 4 91.19 18.20 24 -4 -4 70.19 14.50 24 -4 -4 87.99 15.70 24 -4 -4 100.09 15.50 24 4 -4 84.69 16.20 24 4 -4 122.39 20.70 22 -4 -4 8.10 9.80 22 -4 -4 -12.40 9.50 -22 -4 4 2.20 10.30 22 -4 -4 0.30 9.60 22 4 -4 -1.70 9.60 22 4 -4 3.50 10.90 20 -4 -4 100.89 14.50 -20 -4 4 90.39 14.40 20 -4 -4 121.19 15.60 20 4 -4 115.49 15.80 20 4 -4 109.09 16.50 18 -4 -4 15.30 7.60 18 -4 -4 22.50 8.10 18 4 -4 8.60 9.90 18 4 -4 16.80 8.60 16 -4 -4 474.45 22.30 -16 -4 4 449.36 23.10 16 -4 -4 513.85 22.90 16 4 -4 479.95 22.70 16 4 -4 503.15 24.00 -14 -4 4 690.13 28.90 14 -4 -4 751.62 28.00 14 -4 -4 751.72 27.20 -14 -4 4 726.93 28.80 14 4 -4 733.93 28.90 14 4 -4 704.73 27.10 -12 -4 4 1968.50 59.49 12 -4 -4 1999.40 55.09 12 -4 -4 1982.50 53.69 -12 -4 4 1898.21 55.79 12 4 -4 1968.20 55.99 12 4 -4 1943.31 53.79 10 -4 -4 351.46 12.70 10 -4 -4 343.47 16.60 -10 -4 4 352.06 17.70 -10 -4 4 355.46 16.20 10 4 -4 358.36 16.10 10 4 -4 369.56 18.00 -8 -4 4 81.29 7.70 8 -4 -4 83.69 6.10 -8 -4 4 84.59 10.00 8 -4 -4 82.49 8.70 -8 4 4 91.49 10.00 8 4 -4 77.09 7.70 8 4 -4 78.79 9.60 -6 -4 4 661.83 21.00 6 -4 -4 667.33 19.20 6 -4 -4 682.93 23.60 -6 -4 4 665.63 24.20 6 4 -4 687.13 21.10 -6 4 4 677.13 23.90 6 4 -4 667.33 23.60 4 -4 -4 1965.90 48.50 4 -4 -4 2043.30 53.09 -4 -4 4 1993.60 49.00 -4 -4 4 1983.40 52.99 4 4 -4 2007.10 52.59 -4 4 4 2022.10 52.99 -4 4 4 1957.70 48.00 4 4 -4 1990.50 48.70 2 -4 -4 503.15 12.70 -2 -4 4 496.45 14.60 2 -4 -4 511.05 19.20 -2 -4 4 510.05 19.00 2 -4 -4 490.55 16.20 -2 4 4 484.75 15.70 2 4 -4 539.85 18.40 2 4 -4 493.65 18.20 2 4 -4 504.65 14.90 -2 4 4 491.65 18.90 0 -4 4 494.55 13.40 0 -4 -4 521.55 17.10 0 -4 4 504.15 18.60 0 -4 -4 515.55 12.90 0 -4 4 515.15 15.40 0 -4 -4 472.45 18.50 0 4 -4 506.65 15.00 0 4 -4 500.95 17.60 0 4 4 492.25 18.90 0 4 -4 505.05 17.90 0 4 4 482.45 16.50 2 -4 4 473.65 15.10 2 -4 4 496.85 18.10 -2 -4 -4 475.65 17.30 2 -4 4 444.96 16.10 -2 -4 -4 449.06 17.20 -2 4 -4 475.05 15.10 2 4 4 470.05 18.60 2 4 4 474.35 17.00 -2 4 -4 473.85 16.90 -2 4 -4 463.95 17.10 4 -4 4 1657.63 43.80 4 -4 4 1718.73 39.90 -4 -4 -4 1736.73 46.00 4 -4 4 1692.83 45.50 4 -4 4 1672.73 42.90 -4 4 -4 1699.93 44.10 -4 4 -4 1743.63 43.90 4 4 4 1677.33 46.90 4 4 4 1689.83 45.90 4 4 4 1656.53 41.30 6 -4 4 31.40 5.10 6 -4 4 35.10 6.30 6 -4 4 33.70 5.50 6 -4 4 29.70 4.00 -6 -4 -4 36.80 6.80 6 4 4 33.00 6.80 -6 4 -4 32.60 5.70 6 4 4 42.40 5.60 -6 4 -4 26.00 5.10 6 4 4 30.90 6.90 -8 -4 -4 397.06 17.90 8 -4 4 384.16 15.90 8 -4 4 380.06 15.40 8 -4 4 404.26 13.80 8 -4 4 383.66 16.90 -8 4 -4 377.56 17.00 8 4 4 366.06 17.80 8 4 4 377.46 17.80 8 4 4 389.86 15.50 -10 -4 -4 4.90 5.10 10 -4 4 -4.00 3.60 10 -4 4 -3.20 3.40 10 -4 4 4.80 4.90 10 4 4 1.40 4.40 10 4 4 -2.70 5.40 10 4 4 -7.00 5.50 12 -4 4 837.32 26.40 -12 -4 -4 799.22 30.60 12 -4 4 819.52 29.20 12 -4 4 827.82 27.40 12 4 4 822.52 28.80 12 4 4 838.02 31.80 12 4 4 818.42 30.80 14 -4 4 255.67 14.40 -14 -4 -4 229.08 17.30 14 -4 4 240.98 13.70 14 -4 4 221.98 15.50 14 4 4 258.17 18.90 14 4 4 219.28 16.60 14 4 4 219.78 15.20 16 -4 4 62.29 9.90 16 -4 4 73.99 9.90 -16 -4 -4 91.59 13.90 16 -4 4 72.89 11.30 16 4 4 69.39 11.60 16 4 4 93.99 13.50 16 4 4 65.89 13.30 18 -4 4 196.28 15.20 18 -4 4 193.68 15.60 18 -4 4 191.58 17.00 -18 -4 -4 212.18 19.10 18 4 4 176.08 17.20 18 4 4 159.68 16.70 18 4 4 167.08 19.00 20 -4 4 9.50 9.30 20 -4 4 20.90 8.70 20 -4 4 2.50 8.30 20 4 4 5.00 9.60 20 4 4 6.90 10.10 22 -4 4 90.29 14.90 22 -4 4 80.59 14.70 22 4 4 67.39 14.20 22 4 4 72.89 15.40 24 -4 4 5.60 11.40 24 -4 4 17.80 10.90 24 -4 4 8.60 13.40 24 4 4 5.90 12.80 24 4 4 2.00 12.20 26 -4 4 125.39 18.70 26 -4 4 88.09 15.10 26 -4 4 68.69 17.50 -26 -4 -4 145.69 23.90 26 4 4 86.89 19.30 26 4 4 63.39 22.20 26 4 4 73.49 18.90 28 -4 4 19.80 16.00 28 -4 4 69.19 16.70 28 -4 4 13.10 16.70 28 4 4 14.10 17.00 28 4 4 8.20 16.50 29 -5 -4 102.29 19.70 29 -5 -4 138.79 23.60 -29 -5 4 165.38 41.70 29 -5 -4 131.29 26.90 29 5 -4 137.59 24.30 29 5 -4 109.99 21.00 29 5 -4 129.19 25.80 27 -5 -4 18.60 18.10 -27 -5 4 26.80 17.80 27 -5 -4 -18.50 14.50 27 -5 -4 21.30 14.50 27 5 -4 -7.60 14.70 25 -5 -4 307.97 25.10 -25 -5 4 247.68 41.30 25 -5 -4 328.47 25.40 25 -5 -4 321.97 27.20 25 5 -4 319.17 28.00 25 5 -4 319.27 30.30 23 -5 -4 100.39 16.10 23 -5 -4 71.69 15.20 23 -5 -4 91.89 15.30 -23 -5 4 92.19 20.40 23 5 -4 120.99 18.70 23 5 -4 120.29 18.80 21 -5 -4 421.56 25.20 -21 -5 4 399.86 26.40 21 -5 -4 356.76 23.60 21 -5 -4 390.66 23.90 21 5 -4 404.76 27.30 21 5 -4 411.06 24.80 -19 -5 4 619.34 30.10 19 -5 -4 599.84 28.00 19 -5 -4 629.74 28.40 19 -5 -4 623.04 29.40 19 5 -4 620.74 30.30 19 5 -4 615.94 28.50 17 -5 -4 106.49 15.30 17 -5 -4 109.49 13.70 17 5 -4 114.39 13.70 17 5 -4 125.49 16.50 15 -5 -4 869.81 33.00 15 -5 -4 864.71 31.40 15 -5 -4 863.11 27.20 -15 -5 4 882.51 34.20 -15 -5 4 892.71 33.00 15 5 -4 871.41 32.10 15 5 -4 897.51 35.10 13 -5 -4 14.60 4.40 -13 -5 4 19.10 7.90 -13 -5 4 24.80 8.40 13 -5 -4 18.10 7.80 13 -5 -4 11.90 6.10 13 5 -4 19.60 7.70 13 5 -4 5.30 6.90 -11 -5 4 681.83 25.40 -11 -5 4 741.13 28.60 11 -5 -4 665.03 26.40 11 -5 -4 655.13 21.40 11 5 -4 697.83 25.40 11 5 -4 674.93 27.30 9 -5 -4 532.55 18.00 9 -5 -4 546.55 22.40 -9 -5 4 520.45 23.20 -9 -5 4 554.84 20.90 9 5 -4 532.15 22.50 9 5 -4 538.55 20.30 -9 5 4 525.85 22.60 7 -5 -4 372.16 17.70 -7 -5 4 374.46 18.40 -7 -5 4 373.26 15.50 7 -5 -4 385.96 14.20 -7 5 4 357.66 17.80 7 5 -4 395.16 15.60 7 5 -4 363.46 17.80 5 -5 -4 629.74 23.40 -5 -5 4 571.54 19.20 5 -5 -4 606.54 19.20 -5 -5 4 576.54 23.00 5 5 -4 588.54 22.70 -5 5 4 610.14 18.40 -5 5 4 556.04 22.50 5 5 -4 589.24 19.20 3 -5 -4 64.99 6.80 3 -5 -4 79.29 9.50 -3 -5 4 58.29 9.30 3 -5 -4 60.09 2.60 -3 -5 4 52.99 5.30 3 5 -4 65.79 8.30 -3 5 4 64.69 8.90 3 5 -4 58.49 4.80 -3 5 4 59.89 6.10 3 5 -4 62.19 8.50 -1 -5 4 510.85 15.10 1 -5 -4 514.75 18.20 -1 -5 4 508.65 20.40 1 -5 -4 496.75 20.40 1 5 -4 525.05 15.20 1 5 -4 514.85 19.90 1 5 -4 489.85 19.20 -1 5 4 494.05 20.60 -1 5 4 489.65 17.50 -1 -5 -4 172.68 11.00 1 -5 4 193.08 12.20 1 -5 4 182.18 8.50 -1 -5 -4 191.88 12.90 1 -5 4 179.18 6.90 -1 5 -4 184.58 11.20 1 5 4 195.08 13.40 -1 5 -4 180.18 8.10 1 5 4 182.68 10.70 -1 5 -4 172.58 11.50 3 -5 4 2568.64 65.59 -3 -5 -4 2590.14 66.79 3 -5 4 2667.83 67.59 -3 -5 -4 2600.24 66.89 3 -5 4 2610.94 62.79 -3 5 -4 2656.43 66.29 3 5 4 2643.44 66.79 -3 5 -4 2594.54 65.99 -3 5 -4 2507.15 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24 6 4 43.00 20.50 26 -6 4 79.59 15.90 26 -6 4 41.20 16.80 26 -6 4 84.19 17.60 26 6 4 53.49 18.90 26 6 4 80.09 21.10 27 -7 -4 14.40 18.70 27 -7 -4 28.90 16.10 27 -7 -4 20.70 12.10 27 -7 -4 29.20 15.50 27 7 -4 17.30 16.10 25 -7 -4 23.90 14.20 25 -7 -4 6.80 14.60 25 -7 -4 38.30 17.60 -25 -7 4 20.20 19.60 25 -7 -4 11.10 10.60 25 7 -4 43.70 16.10 25 7 -4 16.90 15.00 25 7 -4 -5.50 20.20 23 -7 -4 11.90 12.00 23 -7 -4 47.90 16.10 23 -7 -4 20.20 12.30 -23 -7 4 67.79 18.50 23 -7 -4 16.80 9.30 21 -7 -4 115.89 16.60 21 -7 -4 113.59 14.00 21 -7 -4 135.99 17.70 21 -7 -4 104.19 17.60 -21 -7 4 110.99 19.60 21 7 -4 89.29 16.60 19 -7 -4 81.19 15.00 19 -7 -4 90.39 13.10 -19 -7 4 105.79 16.60 19 -7 -4 93.89 14.80 19 -7 -4 74.29 10.80 19 7 -4 90.19 15.20 17 -7 -4 13.80 7.80 17 -7 -4 20.80 9.20 -17 -7 4 14.40 10.90 17 -7 -4 18.20 7.80 17 -7 -4 13.40 10.50 17 7 -4 19.20 10.50 -15 -7 4 15.20 10.10 15 -7 -4 2.20 7.60 -15 -7 4 14.80 10.40 15 -7 -4 9.40 6.40 15 -7 -4 -2.30 5.90 15 -7 -4 10.50 10.20 15 7 -4 3.10 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23 -7 4 60.89 24.60 23 -7 4 45.40 15.00 -23 -7 -4 -3.60 20.20 23 -7 4 67.99 14.20 23 7 4 59.19 18.10 23 7 4 25.80 14.20 23 7 4 38.00 23.20 -24 -8 4 -27.70 17.30 24 -8 -4 10.30 10.90 24 -8 -4 30.90 18.80 24 -8 -4 37.90 15.30 24 -8 -4 -5.00 12.20 24 8 -4 13.40 15.90 24 8 -4 -9.30 13.80 -22 -8 4 -13.30 15.20 22 -8 -4 -19.80 15.30 22 -8 -4 15.00 11.20 22 -8 -4 10.30 12.30 22 -8 -4 5.50 9.40 22 8 -4 6.10 18.20 22 8 -4 -15.00 22.00 20 -8 -4 9.10 10.00 20 -8 -4 -18.50 10.30 -20 -8 4 16.30 14.40 20 -8 -4 19.40 14.50 20 -8 -4 2.00 8.20 20 8 -4 -14.80 11.70 18 -8 -4 -2.30 7.60 18 -8 -4 -1.60 8.00 18 -8 -4 35.10 13.70 18 -8 -4 12.50 10.10 18 8 -4 7.60 10.80 16 -8 -4 -0.60 8.70 -16 -8 4 23.60 12.50 16 -8 -4 6.50 7.70 16 -8 -4 -6.40 6.90 16 -8 -4 2.60 10.50 -16 -8 4 4.90 10.90 16 8 -4 5.30 10.50 -14 -8 4 5.10 10.10 14 -8 -4 4.80 10.20 14 -8 -4 2.90 6.00 14 -8 -4 6.20 7.30 -14 -8 4 1.40 10.60 14 8 -4 8.90 9.30 14 8 -4 -22.10 10.30 12 -8 -4 10.10 6.80 12 -8 -4 6.50 4.80 12 -8 -4 11.30 9.90 -12 -8 4 7.20 8.70 -12 -8 4 9.40 10.00 12 8 -4 12.30 10.80 -12 8 4 -0.80 9.60 12 8 -4 5.60 7.70 -10 -8 4 1.60 10.30 10 -8 -4 -3.00 6.60 -10 -8 4 8.00 7.00 10 -8 -4 0.80 3.80 10 -8 -4 -4.20 8.70 10 8 -4 8.10 7.60 -10 8 4 6.10 8.90 10 8 -4 12.50 9.50 8 -8 -4 5.30 7.00 8 -8 -4 27.90 18.20 -8 -8 4 19.70 7.30 -8 -8 4 16.10 11.00 8 8 -4 25.60 10.10 -8 8 4 10.50 8.70 8 8 -4 16.10 9.60 -6 -8 4 3.00 5.40 -6 -8 4 -1.10 8.70 6 -8 -4 0.50 8.80 6 -8 -4 2.70 6.50 6 8 -4 -6.50 7.80 -6 8 4 6.30 5.70 -6 8 4 2.50 8.70 6 8 -4 20.10 9.40 6 8 -4 -1.00 2.80 4 -8 -4 67.79 11.70 -4 -8 4 41.30 11.60 4 -8 -4 38.90 8.90 -4 -8 4 58.79 8.00 4 8 -4 53.39 4.70 -4 8 4 47.60 12.10 4 8 -4 54.09 11.50 -4 8 4 43.70 7.90 -2 -8 4 3.80 4.10 -2 -8 4 -1.20 8.20 2 -8 -4 -6.10 5.90 2 -8 -4 -7.20 6.50 2 8 -4 3.80 8.30 -2 8 4 0.60 8.10 -2 8 4 -3.70 5.90 2 8 -4 -7.80 7.70 2 8 -4 0.10 2.40 0 -8 4 214.18 10.80 0 -8 -4 207.88 15.90 0 -8 4 207.88 17.90 0 -8 -4 205.68 14.40 0 8 -4 205.38 8.90 0 8 4 210.88 18.20 0 8 -4 216.68 16.20 0 8 -4 211.08 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319.17 21.90 -9 7 -9 319.67 20.50 9 7 9 290.17 21.70 9 7 9 325.67 16.00 9 7 9 314.37 22.90 11 -7 9 125.89 16.60 11 -7 9 150.58 15.30 11 -7 9 111.79 11.80 -11 -7 -9 125.39 18.00 11 7 9 137.19 18.20 11 7 9 118.49 12.40 11 7 9 125.79 18.10 13 -7 9 27.50 5.00 13 -7 9 42.80 10.90 13 -7 9 25.40 12.30 -13 -7 -9 45.50 14.00 13 -7 9 24.60 7.40 13 7 9 47.10 13.30 13 7 9 26.20 8.50 13 7 9 43.80 14.30 -15 -7 -9 236.88 25.60 15 -7 9 248.08 19.90 15 -7 9 233.88 22.00 15 -7 9 208.68 16.00 15 -7 9 219.28 12.40 15 7 9 223.98 18.40 15 7 9 216.58 22.30 17 -7 9 30.00 9.20 17 -7 9 13.90 7.00 -17 -7 -9 24.10 17.00 17 -7 9 19.10 11.20 17 -7 9 8.80 20.90 17 7 9 5.30 13.60 17 7 9 -10.80 9.40 17 7 9 -6.80 15.80 19 -7 9 32.90 9.30 19 -7 9 26.70 10.50 -19 -7 -9 33.10 20.50 19 -7 9 22.00 13.30 19 -7 9 29.50 14.10 19 7 9 -0.90 11.50 19 7 9 17.20 19.80 19 7 9 18.30 13.80 21 -7 9 33.60 14.90 21 -7 9 49.00 12.90 21 -7 9 56.59 16.70 21 -7 9 24.60 10.80 21 7 9 20.60 13.80 26 -8 -9 44.20 11.00 -26 -8 9 61.29 27.40 26 -8 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251.17 11.00 -10 -8 9 276.47 22.80 10 -8 -9 267.17 21.10 10 -8 -9 289.87 14.20 10 8 -9 257.67 20.80 -10 8 9 232.78 20.10 10 8 -9 254.37 14.70 10 8 -9 258.47 15.90 -8 -8 9 695.83 33.60 8 -8 -9 652.83 18.50 8 -8 -9 673.33 32.70 -8 -8 9 685.23 24.40 8 -8 -9 697.03 23.90 8 8 -9 706.13 31.30 8 8 -9 703.43 23.90 -8 8 9 721.73 33.20 -8 8 9 643.04 21.70 8 8 -9 747.13 31.70 6 -8 -9 404.76 17.80 6 -8 -9 403.06 25.00 -6 -8 9 383.36 15.60 -6 -8 9 413.66 25.90 -6 8 9 355.86 15.80 -6 8 9 375.66 23.70 6 8 -9 421.06 23.40 6 8 -9 382.26 16.60 6 8 -9 381.06 22.90 4 -8 -9 917.21 29.90 4 -8 -9 876.11 36.60 -4 -8 9 910.21 37.30 -4 -8 9 890.71 24.90 4 8 -9 847.32 27.10 -4 8 9 858.31 35.80 4 8 -9 898.51 34.60 4 8 -9 875.61 34.60 -4 8 9 847.32 28.20 -2 -8 9 57.19 4.40 2 -8 -9 55.69 11.70 -2 -8 9 58.09 13.10 -2 8 9 61.29 9.50 2 8 -9 66.49 8.80 2 8 -9 51.79 11.20 -2 8 9 67.79 13.60 2 8 -9 68.99 12.10 0 -8 9 209.28 19.40 0 -8 -9 208.18 17.20 0 8 9 193.58 18.70 0 8 -9 214.88 17.60 0 8 9 208.18 15.40 0 8 -9 216.08 13.00 0 8 -9 221.78 17.10 2 -8 9 477.85 26.00 2 -8 9 462.75 19.80 -2 -8 -9 465.65 24.90 -2 8 -9 440.06 22.50 -2 8 -9 445.76 19.40 2 8 9 451.35 25.90 2 8 9 459.35 22.40 -2 8 -9 428.26 23.10 4 -8 9 89.09 13.90 4 -8 9 67.89 9.40 -4 -8 -9 54.59 11.60 -4 8 -9 61.29 10.90 -4 8 -9 59.89 9.00 4 8 9 70.89 14.10 4 8 9 71.99 12.00 -6 -8 -9 382.16 24.50 6 -8 9 409.46 24.80 6 -8 9 383.16 19.30 6 8 9 422.86 25.50 -6 8 -9 362.26 20.50 6 8 9 406.16 15.50 -6 8 -9 408.76 20.90 8 -8 9 4.40 6.80 -8 -8 -9 13.30 11.00 8 -8 9 1.10 9.60 8 8 9 29.80 12.50 -8 8 -9 2.60 8.00 8 8 9 3.30 5.00 8 8 9 4.80 10.80 -8 8 -9 17.60 8.50 10 -8 9 312.87 22.40 10 -8 9 328.97 20.10 -10 -8 -9 347.57 25.20 10 8 9 368.76 26.80 10 8 9 376.86 26.90 10 8 9 319.17 17.00 -12 -8 -9 45.20 15.70 12 -8 9 23.90 8.50 12 -8 9 29.60 9.30 12 -8 9 33.50 12.10 12 8 9 37.10 8.70 12 8 9 46.20 15.30 12 8 9 43.50 14.40 14 -8 9 130.19 19.30 -14 -8 -9 104.59 18.70 14 -8 9 103.39 14.80 14 -8 9 108.29 7.50 14 -8 9 108.29 15.20 14 8 9 116.99 20.00 14 8 9 89.69 12.50 16 -8 9 15.50 14.30 16 -8 9 11.40 11.50 16 -8 9 12.50 10.30 16 -8 9 14.10 5.80 16 8 9 19.10 15.20 16 8 9 34.00 19.40 16 8 9 5.50 9.80 18 -8 9 345.47 27.90 18 -8 9 269.47 24.10 18 -8 9 318.77 22.20 18 -8 9 254.37 14.80 18 8 9 288.17 23.20 18 8 9 297.57 29.10 18 8 9 233.78 31.20 23 -9 -9 156.08 21.80 23 -9 -9 84.09 30.40 23 -9 -9 85.29 31.20 -23 -9 9 85.09 20.90 23 -9 -9 134.59 15.90 23 9 -9 106.79 20.50 21 -9 -9 36.30 19.30 -21 -9 9 46.30 18.70 21 -9 -9 28.40 15.10 21 -9 -9 33.10 9.30 -21 -9 9 33.40 16.80 21 9 -9 18.40 14.70 21 9 -9 3.00 17.90 19 -9 -9 51.19 11.30 19 -9 -9 60.09 10.10 -19 -9 9 79.29 18.70 -19 -9 9 66.69 16.00 19 -9 -9 67.39 15.50 19 -9 -9 51.89 18.00 19 9 -9 28.70 14.00 19 9 -9 72.79 18.70 -17 -9 9 33.50 16.50 -17 -9 9 81.29 13.80 17 -9 -9 44.50 8.80 17 -9 -9 21.60 15.90 17 -9 -9 41.90 9.70 17 9 -9 71.89 14.70 15 -9 -9 60.89 9.40 15 -9 -9 85.09 21.50 -15 -9 9 71.39 13.30 15 -9 -9 54.69 8.90 15 9 -9 66.29 13.20 -13 -9 9 133.89 21.50 13 -9 -9 165.98 23.50 13 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18.30 1 9 -9 434.36 24.60 1 9 -9 406.56 24.70 -1 -9 -9 803.22 35.00 1 -9 9 835.52 36.70 -1 9 -9 834.12 28.40 -1 9 -9 778.92 33.60 -1 9 -9 838.22 34.10 1 9 9 785.12 36.50 1 9 9 880.01 32.60 -3 -9 -9 78.29 14.80 3 -9 9 108.89 17.00 -3 9 -9 63.19 13.00 -3 9 -9 74.69 10.30 3 9 9 66.29 15.10 3 9 9 74.29 13.90 5 -9 9 321.77 23.40 -5 -9 -9 335.67 23.70 5 -9 9 345.87 18.70 5 9 9 320.07 26.30 -5 9 -9 311.37 19.40 5 9 9 346.27 23.40 -5 9 -9 336.97 22.00 7 -9 9 23.10 7.80 7 -9 9 12.90 11.20 -7 -9 -9 8.00 11.90 7 9 9 10.80 5.10 -7 9 -9 22.30 10.20 7 9 9 9.10 12.40 7 9 9 26.40 12.70 9 -9 9 66.49 10.60 9 -9 9 67.49 16.20 -9 -9 -9 103.89 18.70 -9 9 -9 124.79 15.90 9 9 9 68.99 16.40 9 9 9 82.09 10.10 9 9 9 98.79 19.50 11 -9 9 73.79 12.10 11 -9 9 61.29 16.30 -11 -9 -9 47.10 15.70 11 9 9 55.09 8.80 11 9 9 19.70 20.10 11 9 9 68.09 17.10 13 -9 9 24.50 14.30 -13 -9 -9 18.80 17.00 13 -9 9 27.00 10.70 13 9 9 41.50 15.20 13 9 9 25.70 8.80 13 9 9 6.10 18.70 15 -9 9 117.69 16.80 -15 -9 -9 102.69 21.60 15 -9 9 111.49 15.40 15 -9 9 140.79 21.80 15 9 9 107.59 21.90 15 9 9 170.98 27.90 15 9 9 102.79 13.30 20 -10 -9 11.00 9.70 -20 -10 9 -7.20 17.50 -20 -10 9 -2.40 18.10 20 -10 -9 16.90 9.70 20 -10 -9 16.80 15.00 20 10 -9 24.90 16.70 18 -10 -9 35.50 9.50 18 -10 -9 57.79 20.70 18 -10 -9 24.40 9.80 -18 -10 9 45.00 18.00 -18 -10 9 29.50 15.10 18 10 -9 51.29 22.60 18 10 -9 33.00 14.90 16 -10 -9 20.90 18.10 16 -10 -9 3.80 6.80 -16 -10 9 11.40 16.50 16 -10 -9 3.70 8.80 -16 -10 9 -3.30 12.80 16 10 -9 11.30 9.10 16 10 -9 0.20 17.80 16 10 -9 6.70 13.00 14 -10 -9 19.20 15.50 14 -10 -9 44.80 6.60 -14 -10 9 47.30 16.40 -14 -10 9 74.09 13.70 14 -10 -9 35.20 9.30 14 10 -9 38.60 9.10 14 10 -9 -4.60 15.90 14 10 -9 30.90 15.60 -14 10 9 35.80 15.20 12 -10 -9 -0.10 8.00 12 -10 -9 -2.10 2.10 -12 -10 9 -12.60 14.60 12 -10 -9 -7.00 13.60 -12 -10 9 15.00 9.60 12 10 -9 1.20 6.40 12 10 -9 10.80 15.50 12 10 -9 5.30 13.90 -12 10 9 11.00 13.60 -10 -10 9 44.60 9.60 10 -10 -9 32.70 15.50 10 -10 -9 50.09 10.40 10 10 -9 41.40 7.80 10 10 -9 62.09 16.80 -10 10 9 18.90 16.40 10 10 -9 1.00 13.50 8 -10 -9 33.00 15.80 8 -10 -9 25.90 9.60 -8 -10 9 55.79 9.20 -8 -10 9 41.80 15.30 8 10 -9 27.20 6.70 8 10 -9 54.49 16.60 8 10 -9 62.99 16.20 -8 10 9 34.80 8.20 -6 -10 9 4.70 6.20 6 -10 -9 -6.80 8.30 -6 -10 9 -13.00 12.90 -6 10 9 -17.90 14.20 6 10 -9 12.90 5.50 6 10 -9 -9.20 11.60 -6 10 9 -13.70 6.90 -4 -10 9 2.90 4.80 4 -10 -9 -11.00 10.30 -4 -10 9 22.70 14.10 4 -10 -9 -0.60 8.80 4 10 -9 -10.90 11.10 -4 10 9 2.10 12.50 4 10 -9 0.80 5.30 -4 10 9 2.90 7.50 -2 -10 9 7.40 12.90 -2 -10 9 -0.20 3.30 2 -10 -9 -1.90 10.90 2 10 -9 -4.50 5.40 -2 10 9 -4.30 9.20 2 10 -9 3.00 11.30 -2 10 9 -5.00 11.70 0 -10 9 41.20 14.20 0 -10 -9 39.60 13.40 0 10 9 29.20 16.30 0 10 -9 28.10 7.50 0 10 9 35.20 11.20 0 10 -9 58.29 13.90 -2 -10 -9 12.00 11.90 2 -10 9 12.30 13.10 -2 10 -9 -2.00 6.60 -2 10 -9 -7.80 10.60 2 10 9 3.20 10.50 4 -10 9 17.80 13.80 -4 -10 -9 49.50 13.80 -4 10 -9 32.80 8.60 -4 10 -9 39.90 13.00 4 10 9 40.70 13.40 4 10 9 45.90 16.80 -6 -10 -9 25.80 15.50 6 -10 9 51.39 9.20 6 -10 9 53.79 16.10 -6 10 -9 46.70 13.40 6 10 9 30.00 15.50 6 10 9 52.59 15.70 -8 -10 -9 26.10 15.00 8 -10 9 32.10 24.30 8 -10 9 13.20 8.00 8 10 9 23.50 15.50 -8 10 -9 17.30 12.50 8 10 9 -2.80 14.80 -10 -10 -9 22.30 16.00 10 -10 9 34.80 10.00 10 -10 9 25.80 15.20 10 10 9 9.80 16.90 10 10 9 25.80 6.70 12 -10 9 -7.30 8.90 12 -10 9 -16.30 14.10 -12 -10 -9 0.70 18.10 12 10 9 33.90 16.90 12 10 9 0.00 7.20 12 10 9 23.70 19.60 -15 -11 9 -1.30 18.30 15 -11 -9 -8.20 9.90 15 -11 -9 2.40 3.30 -15 -11 9 19.20 14.30 15 11 -9 9.30 8.80 15 11 -9 -9.90 16.80 13 -11 -9 5.50 22.10 -13 -11 9 5.50 12.40 13 -11 -9 -1.60 9.90 -13 -11 9 18.80 18.40 13 11 -9 22.20 19.20 -13 11 9 13.70 15.40 13 11 -9 25.50 16.90 13 11 -9 9.50 7.70 11 -11 -9 -25.70 19.20 11 -11 -9 0.60 9.70 -11 -11 9 -15.90 14.70 -11 -11 9 13.50 10.50 -11 11 9 4.10 13.40 11 11 -9 20.80 19.30 11 11 -9 21.90 15.30 -9 -11 9 36.30 9.50 9 -11 -9 17.90 18.30 -9 -11 9 40.30 17.90 9 -11 -9 28.00 10.70 9 11 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-5 11 -9 45.60 15.60 5 11 9 2.20 15.90 7 -11 9 30.60 16.20 -7 -11 -9 28.50 17.80 -7 11 -9 20.70 14.90 7 11 9 30.30 15.90 9 -11 9 24.60 9.90 9 -11 9 7.10 15.50 -9 -11 -9 2.30 18.70 -9 11 -9 27.80 15.70 9 11 9 10.40 17.80 9 11 9 6.40 20.00 -6 -12 9 6.30 18.40 -6 -12 9 7.80 8.30 6 -12 -9 2.60 12.60 6 -12 -9 41.70 16.20 -6 12 9 41.70 17.20 -6 12 9 2.80 11.70 6 12 -9 -3.20 17.20 -4 -12 9 154.98 25.00 4 -12 -9 116.89 20.50 -4 -12 9 134.99 10.70 4 12 -9 149.39 23.10 4 12 -9 126.89 25.50 -4 12 9 151.98 19.90 -4 12 9 175.48 25.70 -2 -12 9 64.49 20.00 2 -12 -9 47.00 19.10 -2 12 9 26.80 17.80 2 12 -9 -22.20 19.20 -2 12 9 13.30 13.50 2 12 -9 4.30 16.10 32 0 -10 55.59 18.70 32 0 -10 58.39 19.10 30 0 -10 31.40 16.10 30 0 -10 61.69 16.60 28 0 -10 140.09 19.70 28 0 -10 106.59 20.10 26 0 -10 327.47 25.50 26 0 -10 295.17 21.80 24 0 -10 826.62 33.30 24 0 -10 837.52 36.40 22 0 -10 29.70 9.00 22 0 -10 57.79 12.70 20 0 -10 166.78 13.10 20 0 -10 133.99 14.70 18 0 -10 73.59 11.50 18 0 -10 65.69 8.90 16 0 -10 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-10 709.23 28.40 -14 0 -10 652.93 29.70 16 0 10 321.67 20.20 16 0 10 334.47 21.70 -18 0 -10 516.55 28.50 18 0 10 574.34 29.40 18 0 10 541.35 27.00 -20 0 -10 -9.20 12.10 20 0 10 12.80 10.90 20 0 10 -22.00 8.60 22 0 10 -8.50 10.80 22 0 10 31.20 12.30 -22 0 -10 -7.10 15.50 -24 0 -10 -35.90 17.40 24 0 10 -14.50 14.80 24 0 10 -16.80 11.10 -26 0 -10 152.08 27.80 26 0 10 135.89 21.30 26 0 10 187.48 26.60 33 -1 -10 74.59 20.40 33 -1 -10 108.59 20.50 33 1 -10 76.19 21.60 33 1 -10 114.49 22.40 31 -1 -10 1.00 15.50 31 -1 -10 22.10 15.30 31 1 -10 -0.20 15.00 31 1 -10 -7.50 15.80 29 -1 -10 253.97 23.40 29 1 -10 205.78 28.50 29 1 -10 201.18 24.50 27 -1 -10 120.89 19.80 27 -1 -10 87.39 14.80 27 1 -10 113.49 18.50 27 1 -10 104.69 16.60 25 -1 -10 13.90 11.10 25 -1 -10 17.60 9.00 25 1 -10 24.00 11.00 25 1 -10 5.00 11.00 23 -1 -10 180.88 15.30 -23 -1 10 167.28 18.30 23 -1 -10 181.68 17.90 23 1 -10 155.38 16.60 23 1 -10 166.28 17.60 -21 -1 10 104.99 14.10 21 -1 -10 103.59 15.00 21 -1 -10 99.59 11.40 21 1 -10 89.69 12.90 21 1 -10 95.89 14.10 19 -1 -10 461.55 24.50 19 -1 -10 489.65 19.90 -19 -1 10 471.85 23.20 19 1 -10 509.45 24.30 19 1 -10 479.75 21.70 17 -1 -10 -2.50 6.00 17 -1 -10 -3.60 3.90 17 1 -10 -7.10 4.70 17 1 -10 10.60 7.00 -15 -1 10 1284.27 38.40 15 -1 -10 1276.07 40.90 15 -1 -10 1267.27 35.50 15 1 -10 1334.17 38.40 15 1 -10 1308.57 40.90 13 -1 -10 525.05 17.00 13 -1 -10 530.55 21.80 -13 -1 10 522.25 20.10 13 1 -10 535.35 19.70 13 1 -10 518.35 21.40 -11 -1 10 1596.74 44.30 11 -1 -10 1670.33 40.80 11 1 -10 1684.63 44.10 11 1 -10 1690.23 46.10 -9 -1 10 114.79 8.40 9 -1 -10 108.39 5.20 -9 1 10 101.49 7.10 9 1 -10 117.79 9.00 9 1 -10 108.79 7.60 -7 -1 10 79.39 7.00 7 -1 -10 80.89 4.10 7 -1 -10 71.09 6.80 -5 -1 10 339.67 13.30 5 -1 -10 334.77 12.90 5 -1 -10 336.17 13.50 5 1 -10 337.37 12.50 5 1 -10 327.07 13.90 -5 1 10 330.37 10.70 3 -1 -10 19.90 4.20 -3 -1 10 15.80 4.60 -3 -1 10 23.30 4.70 3 -1 -10 20.00 3.90 3 1 -10 21.00 4.60 3 1 -10 19.90 3.80 -3 1 10 15.80 4.40 -1 -1 10 1175.28 32.50 -1 -1 10 1199.88 33.80 1 -1 -10 1194.48 33.20 1 -1 -10 1170.78 30.90 -1 1 10 1186.08 33.10 -1 1 10 1177.48 30.90 1 1 -10 1155.68 28.00 1 1 -10 1220.28 33.90 1 -1 10 272.67 13.10 -1 -1 -10 286.47 12.70 -1 1 -10 268.47 12.60 -1 1 -10 273.07 10.70 3 -1 10 881.41 28.10 -3 -1 -10 918.91 28.10 -3 -1 -10 912.41 27.70 3 1 10 870.21 27.50 -3 1 -10 916.61 28.40 3 1 10 855.61 24.20 -3 1 -10 919.61 25.60 -5 -1 -10 64.49 8.10 -5 -1 -10 44.70 6.50 5 -1 10 52.09 2.40 5 -1 10 45.30 7.20 5 1 10 46.30 6.90 -5 1 -10 44.20 6.20 -5 1 -10 58.29 8.10 5 1 10 49.30 5.70 7 -1 10 913.51 27.60 -7 -1 -10 948.61 30.10 7 -1 10 895.11 30.10 -7 -1 -10 936.61 31.10 -7 1 -10 886.91 27.80 -7 1 -10 928.31 31.10 7 1 10 893.01 29.70 -9 -1 -10 1048.50 34.10 -9 -1 -10 1033.40 35.30 9 -1 10 1013.90 34.20 9 -1 10 1101.89 32.20 9 1 10 1061.19 34.40 -9 1 -10 1057.79 36.00 -9 1 -10 1045.00 32.50 9 1 10 1056.69 34.00 11 -1 10 74.99 9.60 11 -1 10 57.19 9.50 -11 -1 -10 57.79 10.10 -11 -1 -10 72.59 10.70 -11 1 -10 57.19 10.30 11 1 10 62.19 10.00 -11 1 -10 66.69 9.30 11 1 10 63.39 10.30 -13 -1 -10 560.84 25.40 13 -1 10 562.04 25.70 -13 -1 -10 482.05 28.80 13 -1 10 533.25 22.50 13 1 10 539.15 24.90 -13 1 -10 537.25 23.40 -13 1 -10 517.55 26.80 13 1 10 508.45 23.50 15 -1 10 15.30 8.80 15 -1 10 11.90 7.60 -15 -1 -10 20.20 10.80 -15 1 -10 22.50 8.30 15 1 10 4.90 8.60 15 1 10 18.10 8.80 -17 -1 -10 238.38 19.90 17 -1 10 261.77 18.60 17 -1 10 244.58 19.70 17 1 10 269.77 20.20 17 1 10 265.97 21.10 -17 1 -10 204.38 23.90 19 -1 10 -4.70 8.70 -19 -1 -10 9.70 12.30 19 -1 10 4.60 8.80 -19 1 -10 -2.00 10.50 19 1 10 -6.20 9.10 19 1 10 10.60 9.60 21 -1 10 33.40 15.00 21 -1 10 17.30 10.90 -21 -1 -10 12.60 16.00 -21 1 -10 5.40 12.70 21 1 10 23.80 11.80 21 1 10 21.00 12.60 -23 -1 -10 116.29 21.40 23 -1 10 111.59 17.70 23 -1 10 109.49 17.80 23 1 10 104.69 18.30 23 1 10 113.69 21.50 -23 1 -10 57.49 20.00 25 -1 10 -15.70 12.80 -25 -1 -10 1.50 20.60 -25 1 -10 -22.50 17.70 25 1 10 -22.30 13.60 32 -2 -10 46.40 18.20 32 -2 -10 16.10 15.90 -32 -2 10 60.89 33.70 32 2 -10 48.30 21.60 32 2 -10 17.60 15.80 30 -2 -10 28.20 15.20 -30 -2 10 16.10 17.00 30 -2 -10 26.70 14.00 30 2 -10 37.10 18.20 30 2 -10 31.20 15.90 28 -2 -10 -13.50 10.70 -28 -2 10 14.90 14.50 28 -2 -10 29.50 15.00 28 2 -10 15.00 13.60 28 2 -10 24.30 14.10 26 -2 -10 16.50 9.00 -26 -2 10 34.60 12.80 26 -2 -10 12.70 11.40 26 2 -10 5.80 12.10 26 2 -10 5.90 11.00 24 -2 -10 45.70 10.00 -24 -2 10 44.00 13.50 24 -2 -10 47.60 13.50 24 2 -10 44.40 13.40 24 2 -10 45.40 11.30 22 -2 -10 67.19 13.50 -22 -2 10 71.09 13.20 22 -2 -10 69.29 9.90 22 2 -10 63.99 12.60 22 2 -10 73.89 12.10 20 -2 -10 77.49 9.90 20 -2 -10 111.39 15.10 20 2 -10 107.79 14.80 20 2 -10 82.49 12.70 -18 -2 10 7.60 7.20 18 -2 -10 4.00 4.50 18 -2 -10 4.40 7.50 18 2 -10 14.50 8.30 18 2 -10 -0.30 6.70 16 -2 -10 325.87 13.70 -16 -2 10 351.96 18.80 -16 -2 10 340.47 18.50 16 -2 -10 357.16 19.40 16 2 -10 363.96 18.30 16 2 -10 342.97 19.20 14 -2 -10 50.69 5.40 -14 -2 10 58.89 9.20 -14 -2 10 70.99 11.00 14 -2 -10 57.09 9.80 14 2 -10 77.89 10.50 14 2 -10 65.49 9.00 12 -2 -10 447.36 13.40 -12 -2 10 460.35 19.50 12 2 -10 452.95 18.60 12 2 -10 459.35 19.20 10 -2 -10 273.57 7.80 10 -2 -10 286.87 14.40 -10 -2 10 271.67 14.20 10 2 -10 283.47 15.70 10 2 -10 283.17 14.00 -8 -2 10 -1.00 4.40 8 -2 -10 3.30 4.30 8 2 -10 4.30 4.00 8 2 -10 5.60 3.70 6 -2 -10 300.97 13.20 6 -2 -10 326.77 14.20 -6 -2 10 330.07 14.60 6 2 -10 329.87 14.10 -6 2 10 312.17 8.60 6 2 -10 325.77 13.30 6 2 -10 323.77 12.50 4 -2 -10 202.68 10.60 4 -2 -10 195.88 9.90 -4 -2 10 191.08 11.00 4 2 -10 193.78 10.30 4 2 -10 204.88 10.60 -4 2 10 202.58 10.70 -2 -2 10 634.74 21.60 -2 -2 10 661.43 22.00 2 -2 -10 607.24 20.20 2 -2 -10 639.34 20.30 2 2 -10 623.34 20.40 -2 2 10 621.84 20.60 2 2 -10 652.33 21.40 -2 2 10 618.84 20.40 0 -2 -10 2015.70 51.39 0 -2 10 1986.20 52.79 0 -2 -10 2047.10 51.89 0 -2 10 2070.09 53.09 0 2 -10 2080.89 53.09 0 2 10 2011.10 51.19 0 2 10 2029.20 51.79 -2 -2 -10 941.11 28.60 -2 -2 -10 916.41 29.00 2 -2 10 896.51 28.40 2 -2 10 907.01 28.90 2 2 10 919.21 26.90 2 2 10 931.21 27.90 -2 2 -10 920.51 28.80 -2 2 -10 939.81 24.60 -4 -2 -10 1164.78 43.70 -4 -2 -10 1192.38 35.20 4 -2 10 1148.99 34.70 4 2 10 1131.99 32.20 -4 2 -10 1148.39 34.80 4 2 10 1114.19 33.40 -4 2 -10 1149.39 30.50 -6 -2 -10 300.97 23.60 6 -2 10 299.07 8.20 6 -2 10 326.57 15.90 -6 -2 -10 325.17 16.20 -6 2 -10 317.97 16.10 6 2 10 293.37 13.70 6 2 10 295.57 15.00 -6 2 -10 322.07 12.70 -8 -2 -10 10.60 5.80 8 -2 10 22.10 3.00 8 -2 10 17.00 4.80 -8 -2 -10 15.80 6.30 8 -2 10 8.20 5.80 8 2 10 11.20 5.80 -8 2 -10 11.50 6.00 -8 2 -10 14.20 4.60 10 -2 10 -2.30 4.10 -10 -2 -10 -5.00 5.50 -10 -2 -10 -5.00 5.10 10 -2 10 3.20 5.90 10 -2 10 2.50 2.60 10 2 10 6.60 6.80 -10 2 -10 -2.50 5.90 -10 2 -10 -4.70 4.20 10 2 10 -6.50 5.00 12 -2 10 302.97 15.60 -12 -2 -10 298.07 19.50 12 -2 10 290.27 17.90 -12 -2 -10 301.77 19.00 12 2 10 268.37 17.20 -12 2 -10 238.38 21.40 12 2 10 275.67 17.90 -12 2 -10 311.37 16.30 -14 -2 -10 38.30 10.20 14 -2 10 43.30 9.10 14 -2 10 36.60 9.50 14 2 10 46.10 9.40 -14 2 -10 34.80 8.40 14 2 10 33.40 10.00 -14 2 -10 19.40 10.00 16 -2 10 43.50 9.50 16 -2 10 37.90 10.60 -16 -2 -10 38.70 12.60 -16 2 -10 55.69 10.50 16 2 10 46.00 11.90 16 2 10 42.50 10.90 18 -2 10 49.00 10.60 -18 -2 -10 36.40 12.80 18 -2 10 57.29 12.50 -18 2 -10 60.59 14.50 18 2 10 52.69 12.60 18 2 10 51.49 11.80 20 -2 10 14.60 9.70 -20 -2 -10 9.40 17.10 20 -2 10 9.10 10.50 20 2 10 3.40 10.70 -20 2 -10 1.00 11.20 20 2 10 -9.60 9.60 22 -2 10 -0.60 11.80 22 -2 10 -10.90 10.10 -22 -2 -10 -6.60 15.90 22 2 10 1.00 13.80 -22 2 -10 -2.90 13.80 22 2 10 -3.60 13.90 24 -2 10 14.30 12.90 -24 -2 -10 -37.90 17.70 24 -2 10 2.00 13.70 24 2 10 20.50 14.40 24 2 10 -0.70 13.00 31 -3 -10 42.00 14.30 -31 -3 10 -19.40 18.60 31 -3 -10 -3.60 16.10 31 3 -10 28.40 18.90 31 3 -10 29.10 16.90 -29 -3 10 45.70 17.80 29 -3 -10 17.70 11.70 29 -3 -10 27.00 16.90 29 3 -10 20.00 16.00 29 3 -10 51.79 18.00 -27 -3 10 0.80 15.50 27 -3 -10 21.90 9.50 27 -3 -10 13.50 14.60 27 3 -10 -2.50 12.70 27 3 -10 6.20 14.20 25 -3 -10 20.50 12.00 -25 -3 10 -9.20 12.70 25 -3 -10 0.50 7.60 25 3 -10 7.20 11.30 25 3 -10 0.60 11.10 23 -3 -10 4.80 9.90 23 -3 -10 12.80 7.10 23 3 -10 36.20 11.80 23 3 -10 6.70 10.30 21 -3 -10 20.40 9.90 -21 -3 10 38.10 11.40 21 -3 -10 25.10 6.70 21 3 -10 30.50 13.20 21 3 -10 35.50 11.00 -19 -3 10 8.50 8.10 19 -3 -10 1.50 8.00 19 -3 -10 4.10 4.40 19 3 -10 -13.60 6.80 19 3 -10 0.40 7.90 -17 -3 10 -3.60 7.40 17 -3 -10 4.10 3.60 -17 -3 10 1.10 6.80 17 -3 -10 0.70 6.90 17 -3 -10 10.30 7.00 17 3 -10 -1.70 6.40 17 3 -10 3.80 7.10 -15 -3 10 161.28 13.00 15 -3 -10 172.88 8.20 -15 -3 10 182.48 14.80 15 -3 -10 168.68 13.60 15 3 -10 172.68 13.30 15 3 -10 179.18 14.20 13 -3 -10 383.46 11.70 13 -3 -10 440.86 20.20 -13 -3 10 390.96 19.80 -13 -3 10 423.76 18.90 13 3 -10 390.16 19.90 13 3 -10 400.06 18.80 11 -3 -10 -1.50 5.10 -11 -3 10 5.60 5.70 -11 -3 10 -4.00 3.90 11 3 -10 4.70 5.00 11 3 -10 1.70 4.60 -9 -3 10 602.64 23.50 9 -3 -10 636.24 23.40 9 3 -10 606.74 21.00 9 3 -10 586.34 22.30 7 -3 -10 290.97 15.20 -7 -3 10 293.37 15.60 7 3 -10 299.37 14.30 7 3 -10 297.17 14.70 -7 3 10 321.27 15.50 7 3 -10 307.47 12.70 5 -3 -10 453.25 16.10 -5 -3 10 450.75 18.70 5 -3 -10 441.26 18.10 -5 3 10 419.96 11.80 5 3 -10 446.46 17.10 5 3 -10 448.76 17.80 -5 3 10 445.26 18.20 5 3 -10 447.46 14.70 3 -3 -10 594.74 21.50 -3 -3 10 594.94 22.20 3 -3 -10 630.44 19.80 3 3 -10 603.64 17.80 3 3 -10 605.54 21.20 3 3 -10 597.94 20.90 -3 3 10 626.44 22.10 1 -3 -10 39.10 5.60 1 -3 -10 46.40 7.20 -1 -3 10 39.70 7.40 -1 -3 10 39.20 6.70 1 3 -10 39.40 6.70 -1 3 10 40.50 7.10 -1 3 10 39.40 5.80 1 3 -10 45.30 6.70 1 -3 10 174.98 11.10 1 -3 10 152.88 11.50 -1 -3 -10 149.49 9.00 -1 3 -10 138.69 5.50 1 3 10 137.49 10.50 -1 3 -10 173.18 10.50 1 3 10 131.29 9.10 -1 3 -10 112.09 7.70 3 -3 10 155.58 11.20 -3 -3 -10 152.18 11.30 3 -3 10 153.38 11.30 -3 -3 -10 144.69 9.50 3 3 10 158.78 9.90 -3 3 -10 146.69 6.40 3 3 10 129.99 10.30 -3 3 -10 169.18 11.20 5 -3 10 553.14 21.90 -5 -3 -10 530.45 22.30 -5 -3 -10 563.34 21.20 5 -3 10 566.84 21.70 -5 3 -10 584.24 22.20 -5 3 -10 558.84 16.80 5 3 10 549.05 20.90 5 3 10 554.14 20.50 7 -3 10 10.90 5.50 7 -3 10 3.00 2.00 -7 -3 -10 -1.60 4.30 7 -3 10 3.30 3.20 -7 -3 -10 1.10 5.30 7 3 10 0.10 4.80 -7 3 -10 7.10 5.40 7 3 10 3.50 4.70 -7 3 -10 1.00 3.00 9 -3 10 7.20 5.80 9 -3 10 11.40 3.00 -9 -3 -10 7.70 6.60 -9 -3 -10 -3.40 5.10 9 -3 10 4.60 3.90 9 3 10 0.70 5.10 -9 3 -10 13.00 4.50 -9 3 -10 15.30 6.80 -11 -3 -10 98.69 11.90 11 -3 10 70.89 10.10 11 -3 10 81.99 8.90 -11 -3 -10 74.59 12.20 11 -3 10 70.49 6.50 -11 3 -10 90.69 9.40 11 3 10 66.99 11.40 -11 3 -10 76.49 11.60 11 3 10 56.49 9.40 13 -3 10 34.20 7.20 13 -3 10 25.40 8.40 13 -3 10 49.80 6.80 -13 -3 -10 37.60 10.80 13 3 10 29.10 9.50 13 3 10 36.90 9.20 -13 3 -10 31.90 7.70 -13 3 -10 41.50 10.20 -15 -3 -10 50.09 12.20 15 -3 10 37.90 8.30 15 -3 10 31.80 9.60 15 -3 10 34.30 6.50 -15 3 -10 38.30 9.30 15 3 10 27.00 10.90 15 3 10 41.10 10.30 17 -3 10 71.19 11.30 -17 -3 -10 56.49 14.00 17 -3 10 52.69 12.10 17 -3 10 62.69 8.60 17 3 10 64.49 13.70 17 3 10 62.09 12.40 -17 3 -10 54.39 11.60 19 -3 10 55.69 11.50 19 -3 10 45.70 8.50 19 -3 10 49.50 12.70 19 3 10 32.60 12.50 19 3 10 34.00 11.90 21 -3 10 -3.00 12.50 -21 -3 -10 12.90 16.10 21 -3 10 1.20 7.80 21 -3 10 6.60 10.60 21 3 10 25.80 12.90 -21 3 -10 -0.40 12.40 -23 -3 -10 39.50 18.50 23 -3 10 62.79 11.50 23 -3 10 54.59 14.00 23 -3 10 64.29 16.40 23 3 10 47.50 16.30 23 3 10 64.59 16.40 -23 3 -10 38.80 16.50 25 -3 10 7.60 12.00 25 -3 10 3.50 13.30 25 -3 10 0.80 14.70 25 3 10 15.70 15.00 25 3 10 -16.90 14.20 30 -4 -10 36.00 13.20 30 -4 -10 39.80 19.60 -30 -4 10 19.60 21.60 30 -4 -10 38.50 18.20 30 4 -10 -5.40 19.40 30 4 -10 27.60 16.40 28 -4 -10 175.08 23.60 28 -4 -10 130.29 18.50 -28 -4 10 161.78 23.80 28 4 -10 227.18 24.10 28 4 -10 206.68 28.70 26 -4 -10 107.19 15.00 26 -4 -10 117.49 18.30 26 -4 -10 87.79 16.60 -26 -4 10 130.89 21.20 26 4 -10 118.69 19.30 26 4 -10 89.69 18.70 24 -4 -10 291.57 24.90 -24 -4 10 302.97 25.70 24 -4 -10 313.57 24.50 24 4 -10 283.67 24.30 24 4 -10 300.17 23.70 22 -4 -10 29.00 11.00 22 -4 -10 15.10 10.80 -22 -4 10 17.40 12.10 22 4 -10 22.00 11.30 22 4 -10 5.20 10.30 20 -4 -10 417.56 24.80 20 -4 -10 449.16 24.40 -20 -4 10 434.86 24.10 20 4 -10 427.16 24.30 20 4 -10 419.06 24.30 18 -4 -10 650.73 29.20 -18 -4 10 666.63 29.00 18 -4 -10 617.54 28.40 -18 -4 10 634.64 29.70 18 4 -10 623.54 28.30 18 4 -10 687.83 40.90 -16 -4 10 -0.70 6.20 -16 -4 10 -6.90 7.80 16 -4 -10 -14.10 6.20 16 4 -10 -13.90 7.40 16 4 -10 7.60 7.10 -14 -4 10 268.07 15.30 -14 -4 10 273.57 18.40 14 -4 -10 274.27 17.50 14 4 -10 273.17 16.10 14 4 -10 262.87 16.60 12 -4 -10 317.47 18.10 -12 -4 10 282.97 15.20 -12 -4 10 278.87 17.40 12 4 -10 311.27 16.00 12 4 -10 295.87 16.80 -10 -4 10 1569.84 44.20 -10 -4 10 1597.84 48.40 10 -4 -10 1714.73 48.40 10 4 -10 1600.54 44.30 10 4 -10 1601.84 47.20 -8 -4 10 234.38 15.60 8 -4 -10 252.17 15.20 -8 -4 10 245.98 11.40 -8 4 10 251.57 15.30 8 4 -10 218.78 13.60 8 4 -10 225.88 11.60 8 4 -10 239.08 13.10 6 -4 -10 67.09 7.10 -6 -4 10 77.39 10.20 6 -4 -10 84.19 10.50 -6 4 10 72.39 3.50 6 4 -10 73.39 9.00 6 4 -10 81.09 6.70 -6 4 10 89.49 10.40 6 4 -10 80.89 8.80 4 -4 -10 1167.78 35.90 4 -4 -10 1135.79 31.20 -4 -4 10 1111.19 36.10 -4 4 10 1125.19 29.10 4 4 -10 1153.18 29.10 4 4 -10 1195.38 33.70 4 4 -10 1163.28 35.10 -4 4 10 1125.69 35.80 2 -4 -10 3063.29 77.09 -2 -4 10 3019.80 75.19 2 -4 -10 2887.51 71.79 -2 -4 10 2961.50 77.39 2 4 -10 3050.69 75.99 2 4 -10 3142.89 74.99 2 4 -10 2978.60 67.29 -2 4 10 2975.90 71.59 -2 4 10 2909.81 76.29 0 -4 -10 148.49 11.80 0 -4 -10 146.89 8.80 0 -4 10 169.88 11.40 0 -4 10 153.08 12.00 0 4 10 168.78 9.70 0 4 10 142.69 11.70 0 4 -10 171.58 8.80 0 4 -10 182.28 10.90 0 4 -10 141.69 10.80 0 4 10 150.78 9.40 -2 -4 -10 -1.50 3.10 2 -4 10 3.50 4.40 2 -4 10 7.40 5.60 -2 -4 -10 11.20 5.40 -2 4 -10 6.20 3.20 -2 4 -10 8.00 4.20 2 4 10 3.90 3.70 2 4 10 9.50 5.70 2 4 10 4.90 4.30 -4 -4 -10 1468.35 44.00 4 -4 10 1402.86 42.80 4 -4 10 1388.26 41.30 -4 -4 -10 1439.86 40.40 -4 4 -10 1441.56 42.00 4 4 10 1458.35 42.50 4 4 10 1438.06 39.70 -4 4 -10 1401.16 36.10 6 -4 10 115.69 10.90 -6 -4 -10 126.89 11.80 -6 -4 -10 122.99 10.70 6 -4 10 114.29 12.20 -6 4 -10 116.29 6.10 6 4 10 115.69 11.40 6 4 10 119.59 10.10 -6 4 -10 133.49 11.40 -8 -4 -10 449.16 20.60 8 -4 10 463.55 21.40 8 -4 10 447.16 15.00 8 -4 10 461.85 15.00 -8 -4 -10 472.85 22.40 8 -4 10 448.36 20.90 8 4 10 489.15 21.20 -8 4 -10 491.85 22.40 -8 4 -10 463.75 15.50 8 4 10 451.15 19.40 10 -4 10 1.10 7.30 10 -4 10 6.20 3.50 10 -4 10 -2.50 6.20 -10 -4 -10 -1.00 7.50 10 -4 10 4.20 4.00 10 4 10 10.50 6.70 10 4 10 1.20 5.50 -10 4 -10 2.20 4.00 -10 4 -10 -3.40 6.60 12 -4 10 82.89 7.70 12 -4 10 99.39 12.90 12 -4 10 91.39 8.90 -12 -4 -10 72.59 12.80 -12 4 -10 68.49 12.90 12 4 10 77.69 10.90 -12 4 -10 82.89 9.50 -14 -4 -10 525.15 27.80 14 -4 10 466.05 20.00 14 -4 10 482.75 24.70 14 -4 10 512.55 18.60 14 4 10 469.05 24.20 14 4 10 477.85 26.30 -14 4 -10 493.15 21.00 -14 4 -10 498.15 27.20 16 -4 10 26.40 7.90 16 -4 10 22.30 6.10 -16 -4 -10 29.60 12.00 16 -4 10 42.20 11.20 -16 4 -10 23.40 8.60 16 4 10 24.90 10.20 16 4 10 20.80 12.00 18 -4 10 650.53 26.60 18 -4 10 646.24 32.00 18 -4 10 620.24 24.10 18 4 10 622.04 31.00 18 4 10 617.44 32.20 -18 4 -10 614.64 28.00 20 -4 10 -5.30 7.50 -20 -4 -10 -11.70 14.30 20 -4 10 7.20 14.40 20 -4 10 2.80 9.40 20 4 10 -0.10 10.90 22 -4 10 149.59 21.30 22 -4 10 123.69 16.30 -22 -4 -10 135.49 22.60 22 -4 10 136.59 16.20 22 4 10 132.99 23.30 -22 4 -10 171.08 23.70 22 4 10 158.98 24.90 22 4 10 147.29 22.10 24 -4 10 31.90 15.30 24 -4 10 49.50 14.00 24 -4 10 45.90 12.30 -24 4 -10 36.20 16.70 24 4 10 55.99 16.90 24 4 10 44.70 17.50 29 -5 -10 274.37 31.30 29 -5 -10 328.67 30.40 -29 -5 10 328.37 32.60 29 5 -10 306.07 28.30 29 5 -10 275.37 35.10 27 -5 -10 62.19 17.60 -27 -5 10 59.79 19.30 27 -5 -10 69.89 17.80 27 5 -10 64.39 18.20 27 5 -10 56.19 20.30 -25 -5 10 79.39 17.40 25 -5 -10 41.60 16.00 25 -5 -10 82.99 16.20 25 5 -10 52.89 16.80 25 5 -10 47.80 15.50 23 -5 -10 34.50 23.00 -23 -5 10 -6.00 12.30 23 -5 -10 22.90 11.80 23 5 -10 35.60 13.50 23 5 -10 5.40 10.60 -21 -5 10 75.89 14.70 21 -5 -10 54.99 13.30 21 -5 -10 58.79 12.50 21 5 -10 52.89 12.80 21 5 -10 77.79 15.20 19 -5 -10 202.88 10.60 -19 -5 10 199.88 18.40 -19 -5 10 211.68 20.20 19 -5 -10 223.38 18.80 19 -5 -10 195.28 17.40 19 5 -10 211.28 18.80 19 5 -10 238.78 24.10 17 -5 -10 152.88 16.50 17 -5 -10 136.59 7.90 -17 -5 10 139.19 16.40 -17 -5 10 132.79 15.40 17 5 -10 134.39 16.80 17 5 -10 142.69 15.10 15 -5 -10 1195.48 47.40 -15 -5 10 1252.37 40.60 -15 -5 10 1247.28 43.40 15 -5 -10 1230.38 31.10 15 5 -10 1246.98 40.10 13 -5 -10 432.46 12.30 -13 -5 10 455.65 20.40 -13 -5 10 453.85 24.00 13 -5 -10 441.96 22.50 13 5 -10 452.25 22.50 13 5 -10 480.85 20.60 -11 -5 10 93.89 13.30 11 -5 -10 89.29 12.10 -11 -5 10 79.89 9.20 11 5 -10 74.09 9.30 11 5 -10 76.19 11.40 -9 -5 10 58.99 11.00 9 -5 -10 63.99 10.30 -9 -5 10 63.99 7.60 9 5 -10 55.89 9.40 9 5 -10 57.49 7.40 -9 5 10 75.69 11.40 9 5 -10 66.19 8.70 7 -5 -10 1181.68 32.40 -7 -5 10 1205.58 39.80 -7 -5 10 1174.48 32.40 7 -5 -10 1226.98 39.10 7 5 -10 1248.68 38.60 7 5 -10 1210.38 35.10 -7 5 10 1092.19 28.10 7 5 -10 1177.28 32.30 -7 5 10 1127.29 38.10 5 -5 -10 1854.21 46.40 -5 -5 10 1839.62 54.09 5 -5 -10 1935.91 53.99 5 5 -10 1846.62 45.10 5 5 -10 1834.92 49.10 -5 5 10 1794.62 44.60 5 5 -10 1871.01 52.49 -5 5 10 1834.42 53.29 3 -5 -10 12.80 6.60 -3 -5 10 15.20 6.90 3 -5 -10 7.00 3.30 3 5 -10 12.40 4.60 3 5 -10 9.80 1.90 3 5 -10 15.60 6.40 -3 5 10 8.20 6.90 -3 5 10 13.10 3.80 -1 -5 10 1780.82 52.49 -1 -5 10 1822.42 49.20 1 -5 -10 1800.22 45.50 1 -5 -10 1862.21 52.49 -1 5 10 1798.22 47.20 1 5 -10 1774.12 48.30 1 5 -10 1783.82 50.69 1 5 -10 1792.62 47.70 -1 5 10 1808.42 51.99 1 -5 10 6.50 5.00 -1 -5 -10 2.70 3.20 1 -5 10 5.60 6.30 -1 -5 -10 16.40 6.40 1 5 10 2.60 3.60 1 5 10 5.10 6.10 -1 5 -10 9.90 4.20 -1 5 -10 2.90 5.70 -1 5 -10 7.40 4.50 1 5 10 13.20 5.40 -3 -5 -10 403.06 16.10 3 -5 10 406.76 20.40 3 -5 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175.88 26.70 22 4 -21 194.38 20.60 22 4 -21 175.38 20.80 -20 -4 21 57.39 14.50 20 4 -21 62.49 13.20 20 4 -21 59.39 13.80 18 -4 -21 54.99 14.30 -18 -4 21 69.79 14.80 18 4 -21 45.10 10.90 18 4 -21 64.29 14.00 18 4 -21 62.69 13.20 16 -4 -21 103.69 14.30 16 -4 -21 157.98 19.80 -16 -4 21 129.39 18.60 16 4 -21 152.98 16.40 16 4 -21 130.69 17.30 16 4 -21 141.49 16.00 14 -4 -21 292.17 19.90 -14 -4 21 281.17 21.90 14 4 -21 278.07 19.10 14 4 -21 309.57 22.40 14 4 -21 275.97 19.00 -12 -4 21 20.70 11.50 12 -4 -21 19.70 8.30 12 -4 -21 7.00 9.90 12 4 -21 3.40 7.60 12 4 -21 11.00 9.00 12 4 -21 29.70 9.50 10 -4 -21 64.09 12.50 -10 -4 21 70.99 13.70 10 -4 -21 68.49 11.10 10 4 -21 51.89 10.70 10 4 -21 74.99 12.00 10 4 -21 71.49 10.40 8 -4 -21 287.77 19.80 8 -4 -21 259.97 20.50 -8 -4 21 265.37 21.00 -8 4 21 244.28 10.80 8 4 -21 255.07 18.90 8 4 -21 296.77 18.70 8 4 -21 278.87 15.60 6 -4 -21 111.89 14.90 -6 -4 21 128.19 16.70 6 -4 -21 113.99 16.20 6 4 -21 114.29 11.00 6 4 -21 133.29 16.50 -6 4 21 107.59 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592.84 19.90 16 2 -23 603.24 29.10 14 -2 -23 492.85 26.90 -14 -2 23 501.55 25.90 14 -2 -23 558.14 27.70 14 2 -23 511.35 22.90 14 2 -23 493.55 25.60 -14 2 23 510.15 18.60 12 -2 -23 107.79 14.90 -12 -2 23 104.29 14.00 12 -2 -23 118.79 15.90 -12 2 23 98.49 9.90 10 -2 -23 43.50 10.20 -10 -2 23 42.70 11.30 10 -2 -23 31.50 10.00 -10 2 23 40.70 7.30 8 -2 -23 5.30 7.20 8 -2 -23 -7.70 7.20 -8 -2 23 -7.70 7.80 -8 2 23 -1.40 5.30 8 2 -23 1.60 5.20 -6 -2 23 234.48 18.40 6 -2 -23 206.18 15.10 6 -2 -23 170.98 17.50 6 2 -23 194.28 10.30 -6 2 23 205.88 13.80 -4 -2 23 5.90 9.00 4 -2 -23 1.00 6.50 4 -2 -23 15.00 8.60 4 2 -23 5.70 2.80 -4 2 23 12.30 6.60 -2 -2 23 118.09 15.20 2 -2 -23 88.19 12.70 -2 -2 23 78.39 13.60 -2 2 23 97.49 12.50 2 2 -23 91.89 12.10 -2 2 23 91.09 14.70 0 -2 23 46.00 12.30 0 -2 -23 49.30 13.20 0 -2 -23 58.59 12.70 0 -2 23 55.39 12.50 0 2 -23 47.90 9.10 0 2 23 38.00 11.50 -2 -2 -23 190.38 20.70 2 -2 23 212.88 19.80 -2 -2 -23 195.18 20.50 2 -2 23 177.18 19.50 2 2 23 220.08 19.70 -2 2 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-1 -30 55.89 18.20 -21 1 30 66.89 13.00 21 1 -30 82.99 21.20 19 -1 -30 4.20 19.10 19 -1 -30 15.90 18.10 -19 -1 30 28.80 14.80 -19 1 30 3.80 10.90 19 1 -30 9.40 15.20 -17 -1 30 12.00 13.50 17 -1 -30 -6.60 14.60 17 -1 -30 29.70 15.70 17 1 -30 20.60 15.30 17 1 -30 13.30 13.60 -17 1 30 24.40 10.80 17 1 -30 18.20 17.90 15 -1 -30 4.60 15.40 -15 -1 30 -0.30 12.70 15 -1 -30 7.70 13.80 -15 1 30 23.10 10.40 15 1 -30 -2.60 12.80 15 1 -30 -5.20 13.50 -13 -1 30 97.49 17.20 13 -1 -30 77.49 16.20 13 -1 -30 81.29 17.60 13 1 -30 94.29 14.30 -13 1 30 88.19 14.00 13 1 -30 97.39 18.00 11 -1 -30 69.19 17.40 11 -1 -30 95.69 15.00 -11 -1 30 93.69 16.50 -11 1 30 116.39 15.40 11 1 -30 87.79 18.00 11 1 -30 104.19 12.90 9 -1 -30 4.50 14.30 9 -1 -30 3.00 9.70 -9 -1 30 3.80 12.50 -9 1 30 5.40 11.70 9 1 -30 -2.40 7.60 9 1 -30 0.20 14.80 7 -1 -30 270.77 17.50 -7 -1 30 266.97 24.00 7 -1 -30 245.18 26.60 -7 1 30 280.37 22.50 7 1 -30 256.07 12.40 7 1 -30 173.18 25.20 -5 -1 30 8.90 13.30 5 -1 -30 -30.40 13.90 5 1 -30 22.60 18.50 -5 1 30 11.30 11.70 5 1 -30 11.00 13.80 3 -1 -30 55.09 19.20 -3 -1 30 60.09 16.40 3 -1 -30 44.50 17.50 3 1 -30 66.19 16.70 -3 1 30 66.19 15.80 1 -1 -30 42.70 17.70 -1 -1 30 36.30 16.30 -1 1 30 78.79 16.70 1 1 -30 49.99 17.00 -20 -2 30 5.50 15.60 20 -2 -30 55.29 19.80 18 -2 -30 -13.30 15.00 -18 -2 30 -3.20 14.20 18 2 -30 -1.00 14.20 -18 2 30 17.10 8.70 18 2 -30 1.20 14.50 16 -2 -30 50.99 17.00 -16 -2 30 57.79 17.10 16 -2 -30 36.60 16.10 16 2 -30 57.19 16.30 16 2 -30 35.30 14.50 -16 2 30 64.29 10.40 -14 -2 30 -16.10 13.30 14 -2 -30 -10.80 14.20 14 -2 -30 15.30 14.60 14 2 -30 -7.10 11.30 -14 2 30 -9.80 8.90 14 2 -30 23.30 14.10 14 2 -30 -2.00 16.00 -12 -2 30 -5.90 12.90 12 -2 -30 22.80 15.70 12 -2 -30 2.00 13.40 -12 2 30 9.40 9.80 12 2 -30 -15.50 15.50 12 2 -30 4.20 9.70 -10 -2 30 45.20 16.20 10 -2 -30 23.90 14.20 10 -2 -30 31.10 17.30 10 2 -30 48.10 16.30 -10 2 30 24.20 11.10 10 2 -30 32.20 8.90 8 -2 -30 4.60 11.20 -8 -2 30 -14.40 13.80 8 -2 -30 -4.00 14.20 8 2 -30 9.00 15.90 -8 2 30 11.10 10.70 8 2 -30 -4.20 5.40 -6 -2 30 -0.50 13.40 6 -2 -30 2.80 14.90 -6 2 30 10.40 11.40 4 -2 -30 0.90 17.90 4 -2 -30 24.30 15.20 -4 2 30 -10.00 11.30 4 2 -30 -18.70 13.10 2 -2 -30 63.09 20.80 -2 -2 30 49.10 16.60 2 -2 -30 18.50 20.20 -2 2 30 49.90 14.30 2 2 -30 35.50 14.80 19 -3 -30 -6.00 16.60 19 -3 -30 2.20 17.70 -19 -3 30 -22.10 15.80 19 3 -30 18.10 16.00 -17 -3 30 21.90 16.80 17 -3 -30 8.20 15.90 17 3 -30 -3.20 14.80 -15 -3 30 23.10 16.40 15 -3 -30 13.90 15.50 15 -3 -30 -6.00 15.70 -15 3 30 11.40 6.80 15 3 -30 -2.00 13.80 15 3 -30 -1.10 12.70 13 -3 -30 43.40 15.90 13 -3 -30 25.40 15.90 -13 -3 30 9.50 15.10 13 3 -30 15.00 10.20 13 3 -30 52.59 15.20 -13 3 30 28.50 8.90 11 -3 -30 14.00 14.30 11 -3 -30 -9.40 13.80 -11 -3 30 16.20 15.00 11 3 -30 31.50 13.60 -11 3 30 16.00 9.60 9 -3 -30 1.80 14.40 9 -3 -30 14.70 13.70 -9 -3 30 8.20 15.40 -9 3 30 13.80 9.60 9 3 -30 11.60 6.10 7 -3 -30 -14.70 12.90 -7 -3 30 -22.60 25.10 7 -3 -30 -24.50 13.90 -7 3 30 20.80 10.20 5 -3 -30 28.70 15.30 5 -3 -30 2.20 17.10 -5 -3 30 -17.30 14.40 5 3 -30 -3.00 13.80 -5 3 30 4.60 11.20 14 -4 -30 -30.10 15.00 -14 -4 30 10.00 18.00 14 4 -30 2.30 13.50 12 -4 -30 56.89 18.20 12 -4 -30 103.99 18.50 -12 -4 30 117.69 22.80 12 4 -30 67.69 16.30 12 4 -30 83.59 11.90 -12 4 30 79.39 10.30 10 -4 -30 4.80 15.20 -10 -4 30 35.50 15.80 10 -4 -30 -2.80 15.70 10 4 -30 8.50 12.10 10 4 -30 11.10 7.20 -10 4 30 18.20 8.70 -8 -4 30 76.09 18.10 8 -4 -30 48.40 15.80 8 -4 -30 36.90 15.80 8 4 -30 54.59 14.20 -8 4 30 46.30 10.50 18 0 -31 5.70 16.40 -18 0 31 -10.80 12.50 -16 0 31 13.40 12.60 16 0 -31 -17.30 14.60 14 0 -31 11.50 13.30 -14 0 31 18.30 13.50 12 0 -31 -22.20 19.30 12 0 -31 -4.50 11.80 -12 0 31 16.30 13.00 -10 0 31 -17.40 11.90 10 0 -31 -5.90 9.70 -8 0 31 10.40 12.50 8 0 -31 8.60 8.30 -6 0 31 26.50 14.50 -4 0 31 0.70 13.10 17 -1 -31 39.20 16.90 -17 -1 31 11.70 15.10 -17 1 31 16.70 11.20 17 1 -31 14.30 15.30 -15 -1 31 128.09 19.70 15 -1 -31 102.69 18.50 -15 1 31 123.49 15.80 15 1 -31 147.69 21.50 13 -1 -31 7.20 16.00 -13 -1 31 35.00 14.30 13 -1 -31 28.60 14.30 13 1 -31 31.20 12.40 -13 1 31 29.80 12.50 11 -1 -31 -14.10 11.90 -11 -1 31 6.30 13.50 11 -1 -31 -13.60 15.70 11 1 -31 -14.70 9.30 -11 1 31 6.00 12.20 -9 -1 31 88.59 17.70 9 -1 -31 50.99 12.20 9 -1 -31 63.49 17.80 -9 1 31 104.69 15.70 9 1 -31 65.09 9.70 7 -1 -31 14.70 9.20 -7 -1 31 6.20 14.10 -7 1 31 17.00 12.50 -5 -1 31 29.60 15.30 5 -1 -31 13.70 17.90 -5 1 31 5.20 13.10 5 1 -31 16.30 16.20 16 -2 -31 9.60 18.70 -16 -2 31 59.29 17.70 16 -2 -31 30.80 17.60 16 2 -31 57.19 17.20 -16 2 31 54.69 11.10 16 2 -31 47.50 15.00 14 -2 -31 94.99 18.20 14 -2 -31 62.49 18.80 -14 -2 31 69.99 18.30 -14 2 31 98.19 13.50 14 2 -31 89.89 18.20 14 2 -31 94.49 14.70 -12 -2 31 63.39 17.90 12 -2 -31 51.39 16.40 12 -2 -31 32.80 15.50 12 2 -31 25.00 11.00 -12 2 31 54.29 12.30 10 -2 -31 106.89 17.10 10 -2 -31 90.39 18.50 -10 -2 31 117.29 19.40 -10 2 31 107.59 15.30 10 2 -31 104.49 13.30 8 -2 -31 88.39 18.80 8 -2 -31 158.98 19.40 -8 -2 31 114.09 19.10 -8 2 31 98.49 15.70 8 2 -31 97.29 7.20 6 2 -31 4.10 14.50 -6 2 31 15.70 12.00 -13 -3 31 220.48 27.70 13 -3 -31 133.49 21.60 13 -3 -31 167.88 22.80 13 3 -31 177.78 24.40 13 3 -31 195.08 18.50 -13 3 31 198.88 15.90 11 -3 -31 7.50 15.50 11 -3 -31 -0.30 14.70 -11 3 31 -4.10 9.80 11 3 -31 -10.60 13.20 11 3 -31 -9.00 8.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 18782 _olex2_submission_special_instructions 'No special instructions were received' _publcif_funding_html ; ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.60766(2) 0.59544(2) 0.40949(2) 0.03441(9) Uani 1 1 d . . . . . P1 P 0.46891(4) 1.08796(9) 0.36395(4) 0.0536(2) Uani 1 1 d . . . . . O4 O 0.67635(8) 0.64827(19) 0.40350(8) 0.0412(5) Uani 1 1 d . . . . . O3 O 0.64346(7) 0.49523(19) 0.47986(7) 0.0405(5) Uani 1 1 d . . . . . F2 F 0.47678(10) 1.2118(2) 0.33475(8) 0.0831(7) Uani 1 1 d . . . . . F4 F 0.51184(12) 1.0192(3) 0.35116(15) 0.1225(11) Uani 1 1 d . . . . . F6 F 0.50755(9) 1.1417(2) 0.41771(9) 0.0886(8) Uani 1 1 d . . . . . F3 F 0.42839(10) 1.0365(2) 0.31011(9) 0.0863(7) Uani 1 1 d . . . . . F5 F 0.42452(10) 1.1554(2) 0.37665(10) 0.0902(8) Uani 1 1 d . . . . . F1 F 0.45996(11) 0.9651(2) 0.39335(11) 0.1029(9) Uani 1 1 d . . . . . N4 N 0.60319(9) 0.7557(2) 0.45088(9) 0.0379(6) Uani 1 1 d . . . . . N5 N 0.54042(9) 0.5668(2) 0.41872(9) 0.0389(6) Uani 1 1 d . . . . . N3 N 0.57912(9) 0.6723(2) 0.33580(9) 0.0382(6) Uani 1 1 d . . . . . N2 N 0.60288(9) 0.4379(2) 0.36356(9) 0.0365(6) Uani 1 1 d . . . . . O5 O 0.76010(9) 0.6587(2) 0.43235(9) 0.0621(7) Uani 1 1 d . . . . . O2 O 0.79741(12) 0.3923(5) 0.55985(18) 0.172(2) Uani 1 1 d . . . . . C10 C 0.69120(12) 0.4729(3) 0.49651(11) 0.0415(7) Uani 1 1 d . . . . . O1 O 0.77350(9) 0.2563(3) 0.60610(10) 0.0677(8) Uani 1 1 d . . . . . C34 C 0.56217(12) 0.7625(3) 0.46580(11) 0.0420(7) Uani 1 1 d . . . . . C33 C 0.52661(12) 0.6567(3) 0.44756(12) 0.0443(8) Uani 1 1 d . . . . . C32 C 0.48206(15) 0.6464(4) 0.45737(17) 0.0684(11) Uani 1 1 d . . . . . H32 H 0.4732 0.7083 0.4771 0.082 Uiso 1 1 calc R U . . . C31 C 0.45095(16) 0.5453(4) 0.4380(2) 0.0821(14) Uani 1 1 d . . . . . H31 H 0.4210 0.5375 0.4446 0.098 Uiso 1 1 calc R U . . . C30 C 0.46426(14) 0.4556(4) 0.40869(17) 0.0670(11) Uani 1 1 d . . . . . H30 H 0.4433 0.3868 0.3947 0.080 Uiso 1 1 calc R U . . . C29 C 0.50878(12) 0.4688(3) 0.40027(14) 0.0502(8) Uani 1 1 d . . . . . H29 H 0.5177 0.4067 0.3807 0.060 Uiso 1 1 calc R U . . . C35 C 0.55478(14) 0.8641(3) 0.49466(13) 0.0555(9) Uani 1 1 d . . . . . H35 H 0.5269 0.8664 0.5053 0.067 Uiso 1 1 calc R U . . . C36 C 0.58894(15) 0.9612(4) 0.50749(14) 0.0629(10) Uani 1 1 d . . . . . H36 H 0.5846 1.0297 0.5272 0.075 Uiso 1 1 calc R U . . . C37 C 0.62919(14) 0.9569(3) 0.49116(14) 0.0580(9) Uani 1 1 d . . . . . H37 H 0.6520 1.0236 0.4985 0.070 Uiso 1 1 calc R U . . . C38 C 0.63576(13) 0.8529(3) 0.46364(13) 0.0497(8) Uani 1 1 d . . . . . H38 H 0.6639 0.8497 0.4534 0.060 Uiso 1 1 calc R U . . . C24 C 0.57405(11) 0.5913(3) 0.29496(11) 0.0408(7) Uani 1 1 d . . . . . C25 C 0.56209(14) 0.6354(4) 0.24320(13) 0.0564(9) Uani 1 1 d . . . . . H25 H 0.5579 0.5786 0.2155 0.068 Uiso 1 1 calc R U . . . C26 C 0.55654(16) 0.7624(4) 0.23314(15) 0.0677(11) Uani 1 1 d . . . . . H26 H 0.5493 0.7930 0.1988 0.081 Uiso 1 1 calc R U . . . C27 C 0.56186(16) 0.8437(4) 0.27438(15) 0.0669(11) Uani 1 1 d . . . . . H27 H 0.5583 0.9304 0.2684 0.080 Uiso 1 1 calc R U . . . C28 C 0.57248(13) 0.7965(3) 0.32456(13) 0.0535(9) Uani 1 1 d . . . . . H28 H 0.5752 0.8527 0.3521 0.064 Uiso 1 1 calc R U . . . C23 C 0.58375(11) 0.4580(3) 0.31014(11) 0.0404(7) Uani 1 1 d . . . . . C22 C 0.57403(15) 0.3590(3) 0.27486(14) 0.0597(10) Uani 1 1 d . . . . . H22 H 0.5609 0.3744 0.2385 0.072 Uiso 1 1 calc R U . . . C21 C 0.58375(15) 0.2374(4) 0.29332(15) 0.0676(11) Uani 1 1 d . . . . . H21 H 0.5771 0.1698 0.2697 0.081 Uiso 1 1 calc R U . . . C20 C 0.60345(13) 0.2169(3) 0.34719(15) 0.0564(9) Uani 1 1 d . . . . . H20 H 0.6104 0.1352 0.3606 0.068 Uiso 1 1 calc R U . . . C19 C 0.61268(12) 0.3184(3) 0.38069(13) 0.0452(8) Uani 1 1 d . . . . . H19 H 0.6264 0.3039 0.4171 0.054 Uiso 1 1 calc R U . . . C12 C 0.71740(12) 0.6124(3) 0.43605(12) 0.0442(8) Uani 1 1 d . . . . . C13 C 0.75716(14) 0.7550(4) 0.39405(14) 0.0616(10) Uani 1 1 d . . . . . H13A H 0.7408 0.8298 0.4012 0.074 Uiso 1 1 calc R U . . . H13B H 0.7380 0.7252 0.3585 0.074 Uiso 1 1 calc R U . . . C14 C 0.81018(16) 0.7847(4) 0.39870(17) 0.0811(13) Uani 1 1 d . . . . . H14A H 0.8282 0.8179 0.4335 0.122 Uiso 1 1 calc R U . . . H14B H 0.8099 0.8463 0.3724 0.122 Uiso 1 1 calc R U . . . H14C H 0.8264 0.7089 0.3933 0.122 Uiso 1 1 calc R U . . . C11 C 0.72593(12) 0.5262(3) 0.47788(13) 0.0530(9) Uani 1 1 d . . . . . H11 H 0.7593 0.5021 0.4952 0.064 Uiso 1 1 calc R U . . . C3 C 0.70869(12) 0.3792(3) 0.54123(12) 0.0422(7) Uani 1 1 d . . . . . C4 C 0.67479(12) 0.3200(3) 0.55826(12) 0.0420(7) Uani 1 1 d . . . . . H4 H 0.6408 0.3396 0.5418 0.050 Uiso 1 1 calc R U . . . C9 C 0.68840(12) 0.2296(3) 0.59984(12) 0.0419(7) Uani 1 1 d . . . . . C5 C 0.65563(13) 0.1679(3) 0.62041(13) 0.0542(9) Uani 1 1 d . . . . . H5 H 0.6214 0.1865 0.6064 0.065 Uiso 1 1 calc R U . . . C6 C 0.67235(14) 0.0815(3) 0.66027(14) 0.0595(10) Uani 1 1 d . . . . . H6 H 0.6494 0.0438 0.6733 0.071 Uiso 1 1 calc R U . . . C7 C 0.72400(14) 0.0474(3) 0.68237(13) 0.0548(9) Uani 1 1 d . . . . . C8 C 0.75723(13) 0.1098(3) 0.66253(13) 0.0523(9) Uani 1 1 d . . . . . H8 H 0.7915 0.0921 0.6762 0.063 Uiso 1 1 calc R U . . . C1 C 0.73876(12) 0.1976(3) 0.62269(12) 0.0446(8) Uani 1 1 d . . . . . C2 C 0.76170(15) 0.3480(4) 0.56729(17) 0.0781(13) Uani 1 1 d . . . . . N1 N 0.74017(13) -0.0431(3) 0.72109(13) 0.0720(10) Uani 1 1 d . . . . . C17 C 0.79444(19) -0.0854(4) 0.74219(17) 0.0862(14) Uani 1 1 d . . . . . H17A H 0.7961 -0.1734 0.7529 0.103 Uiso 1 1 calc R U . . . H17B H 0.8086 -0.0789 0.7142 0.103 Uiso 1 1 calc R U . . . C18 C 0.8243(2) -0.0085(7) 0.7876(2) 0.131(2) Uani 1 1 d . . . . . H18A H 0.8247 0.0777 0.7764 0.197 Uiso 1 1 calc R U . . . H18B H 0.8582 -0.0403 0.8014 0.197 Uiso 1 1 calc R U . . . H18C H 0.8096 -0.0123 0.8148 0.197 Uiso 1 1 calc R U . . . C15 C 0.70573(19) -0.0983(4) 0.74519(18) 0.0914(16) Uani 1 1 d . . . . . H15A H 0.7199 -0.1775 0.7622 0.110 Uiso 1 1 calc R U . . . H15B H 0.6740 -0.1175 0.7172 0.110 Uiso 1 1 calc R U . . . C16 C 0.6958(2) -0.0154(7) 0.7850(2) 0.125(2) Uani 1 1 d . . . . . H16A H 0.7266 -0.0011 0.8142 0.187 Uiso 1 1 calc R U . . . H16B H 0.6718 -0.0555 0.7977 0.187 Uiso 1 1 calc R U . . . H16C H 0.6825 0.0641 0.7688 0.187 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.03278(14) 0.03586(14) 0.03029(13) -0.00043(10) 0.00568(9) 0.00377(11) P1 0.0648(6) 0.0455(5) 0.0533(5) -0.0026(4) 0.0241(5) -0.0047(5) O4 0.0351(12) 0.0494(12) 0.0365(11) 0.0067(9) 0.0094(10) 0.0024(10) O3 0.0328(12) 0.0482(12) 0.0361(11) 0.0071(9) 0.0066(9) 0.0055(9) F2 0.120(2) 0.0608(14) 0.0660(14) 0.0050(11) 0.0303(14) -0.0225(13) F4 0.107(2) 0.0874(19) 0.206(3) -0.036(2) 0.096(2) 0.0013(17) F6 0.0817(18) 0.0982(18) 0.0666(15) -0.0005(13) 0.0021(13) -0.0168(14) F3 0.110(2) 0.0830(16) 0.0631(14) -0.0211(12) 0.0269(14) -0.0309(15) F5 0.0785(17) 0.0951(18) 0.1053(19) -0.0274(15) 0.0425(15) -0.0002(14) F1 0.111(2) 0.0804(17) 0.110(2) 0.0352(15) 0.0297(17) -0.0164(15) N4 0.0382(15) 0.0388(14) 0.0322(13) -0.0025(10) 0.0069(11) 0.0018(11) N5 0.0354(14) 0.0379(14) 0.0390(13) 0.0009(11) 0.0074(11) 0.0053(11) N3 0.0340(14) 0.0397(14) 0.0358(13) 0.0019(11) 0.0059(11) 0.0040(11) N2 0.0293(13) 0.0387(14) 0.0384(13) -0.0006(10) 0.0080(11) 0.0050(10) O5 0.0419(14) 0.0789(17) 0.0623(15) 0.0296(13) 0.0142(12) -0.0031(12) O2 0.0401(18) 0.261(5) 0.200(4) 0.189(4) 0.022(2) 0.012(2) C10 0.0399(19) 0.0427(17) 0.0368(16) 0.0010(13) 0.0071(14) 0.0015(14) O1 0.0374(14) 0.0890(19) 0.0730(17) 0.0459(15) 0.0149(12) 0.0097(13) C34 0.0429(19) 0.0459(18) 0.0346(16) 0.0005(13) 0.0104(14) 0.0059(14) C33 0.0414(19) 0.0431(17) 0.0482(18) 0.0003(14) 0.0154(15) 0.0066(15) C32 0.059(3) 0.058(2) 0.102(3) -0.013(2) 0.045(2) 0.003(2) C31 0.053(3) 0.064(3) 0.144(4) -0.015(3) 0.053(3) -0.004(2) C30 0.043(2) 0.051(2) 0.109(3) -0.012(2) 0.029(2) -0.0058(17) C29 0.042(2) 0.0413(18) 0.063(2) -0.0074(16) 0.0127(17) -0.0007(15) C35 0.058(2) 0.057(2) 0.053(2) -0.0142(17) 0.0220(18) 0.0032(18) C36 0.072(3) 0.056(2) 0.057(2) -0.0231(18) 0.017(2) 0.002(2) C37 0.059(2) 0.049(2) 0.060(2) -0.0180(17) 0.0136(19) -0.0096(18) C38 0.044(2) 0.0519(19) 0.0506(19) -0.0067(16) 0.0132(16) -0.0044(16) C24 0.0368(17) 0.0460(17) 0.0370(16) 0.0013(14) 0.0097(13) 0.0044(14) C25 0.064(2) 0.068(2) 0.0359(18) 0.0007(16) 0.0155(16) 0.0092(19) C26 0.084(3) 0.070(3) 0.046(2) 0.0177(19) 0.019(2) 0.013(2) C27 0.088(3) 0.049(2) 0.057(2) 0.0150(18) 0.018(2) 0.007(2) C28 0.064(2) 0.0404(18) 0.0476(19) 0.0028(15) 0.0092(17) 0.0061(16) C23 0.0365(17) 0.0473(17) 0.0357(16) -0.0068(14) 0.0107(13) 0.0038(14) C22 0.072(3) 0.056(2) 0.045(2) -0.0108(17) 0.0122(18) 0.0071(19) C21 0.080(3) 0.051(2) 0.064(2) -0.0195(19) 0.016(2) 0.004(2) C20 0.054(2) 0.0402(18) 0.073(2) -0.0043(17) 0.0190(19) 0.0089(16) C19 0.0404(19) 0.0422(18) 0.0490(19) 0.0044(14) 0.0107(15) 0.0099(14) C12 0.0388(18) 0.0479(19) 0.0430(17) 0.0050(14) 0.0104(15) 0.0007(15) C13 0.063(2) 0.070(2) 0.051(2) 0.0180(18) 0.0183(18) -0.0041(19) C14 0.074(3) 0.092(3) 0.083(3) 0.026(3) 0.036(2) -0.013(2) C11 0.0334(18) 0.065(2) 0.055(2) 0.0247(18) 0.0089(15) 0.0045(16) C3 0.0351(17) 0.0458(18) 0.0414(17) 0.0070(14) 0.0082(14) 0.0019(14) C4 0.0337(17) 0.0463(18) 0.0404(17) 0.0033(14) 0.0059(14) 0.0024(14) C9 0.0415(19) 0.0424(17) 0.0392(16) 0.0019(13) 0.0108(14) -0.0046(14) C5 0.041(2) 0.063(2) 0.052(2) 0.0084(17) 0.0083(16) -0.0058(17) C6 0.054(2) 0.062(2) 0.059(2) 0.0160(18) 0.0155(18) -0.0187(18) C7 0.066(2) 0.0445(18) 0.0456(19) 0.0062(15) 0.0097(17) -0.0099(17) C8 0.048(2) 0.051(2) 0.0512(19) 0.0137(16) 0.0101(16) 0.0050(16) C1 0.0422(19) 0.0450(18) 0.0454(18) 0.0051(14) 0.0137(15) -0.0010(15) C2 0.041(2) 0.106(3) 0.084(3) 0.055(3) 0.017(2) 0.007(2) N1 0.076(2) 0.066(2) 0.064(2) 0.0278(17) 0.0118(18) -0.0064(18) C17 0.107(4) 0.079(3) 0.064(3) 0.023(2) 0.019(3) 0.008(3) C18 0.119(5) 0.173(6) 0.096(4) -0.021(4) 0.031(4) 0.026(5) C15 0.099(4) 0.083(3) 0.076(3) 0.037(3) 0.009(3) -0.026(3) C16 0.121(5) 0.177(6) 0.084(4) 0.014(4) 0.046(3) -0.042(4) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0.00 1.00 0.00 0.0680 0.00 -1.00 0.00 0.1220 4.00 0.00 -1.00 0.1100 -4.00 0.00 1.00 0.0630 0.00 0.00 1.00 0.0310 0.00 0.00 -1.00 0.0360 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O4 Ru1 O3 92.05(8) . . ? N4 Ru1 O4 93.32(9) . . ? N4 Ru1 O3 91.72(8) . . ? N5 Ru1 O4 172.66(9) . . ? N5 Ru1 O3 89.55(9) . . ? N5 Ru1 N4 79.48(10) . . ? N5 Ru1 N2 94.96(10) . . ? N3 Ru1 O4 83.14(9) . . ? N3 Ru1 O3 170.38(9) . . ? N3 Ru1 N4 96.85(9) . . ? N3 Ru1 N5 96.28(10) . . ? N3 Ru1 N2 79.50(9) . . ? N2 Ru1 O4 92.13(9) . . ? N2 Ru1 O3 92.41(8) . . ? N2 Ru1 N4 173.04(9) . . ? F2 P1 F3 90.79(13) . . ? F2 P1 F5 89.74(15) . . ? F2 P1 F1 178.77(17) . . ? F4 P1 F2 91.11(16) . . ? F4 P1 F6 91.46(17) . . ? F4 P1 F3 90.57(17) . . ? F4 P1 F5 178.83(17) . . ? F4 P1 F1 90.11(17) . . ? F6 P1 F2 89.03(13) . . ? F6 P1 F3 177.96(16) . . ? F6 P1 F5 89.36(14) . . ? F6 P1 F1 91.12(14) . . ? F5 P1 F3 88.61(14) . . ? F5 P1 F1 89.03(16) . . ? F1 P1 F3 89.01(14) . . ? C12 O4 Ru1 122.1(2) . . ? C10 O3 Ru1 121.53(19) . . ? C34 N4 Ru1 115.17(19) . . ? C38 N4 Ru1 127.0(2) . . ? C38 N4 C34 117.9(3) . . ? C33 N5 Ru1 115.7(2) . . ? C29 N5 Ru1 127.1(2) . . ? C29 N5 C33 117.2(3) . . ? C24 N3 Ru1 115.42(19) . . ? C28 N3 Ru1 125.9(2) . . ? C28 N3 C24 117.8(3) . . ? C23 N2 Ru1 115.27(19) . . ? C19 N2 Ru1 126.7(2) . . ? C19 N2 C23 117.8(3) . . ? C12 O5 C13 119.2(3) . . ? O3 C10 C11 126.8(3) . . ? O3 C10 C3 114.2(3) . . ? C11 C10 C3 119.1(3) . . ? C1 O1 C2 123.8(3) . . ? N4 C34 C33 114.8(3) . . ? N4 C34 C35 121.4(3) . . ? C35 C34 C33 123.8(3) . . ? N5 C33 C34 114.7(3) . . ? N5 C33 C32 121.1(3) . . ? C32 C33 C34 124.2(3) . . ? C33 C32 H32 120.1 . . ? C31 C32 C33 119.9(4) . . ? C31 C32 H32 120.1 . . ? C32 C31 H31 120.3 . . ? C30 C31 C32 119.4(4) . . ? C30 C31 H31 120.3 . . ? C31 C30 H30 120.6 . . ? C29 C30 C31 118.9(4) . . ? C29 C30 H30 120.6 . . ? N5 C29 C30 123.6(3) . . ? N5 C29 H29 118.2 . . ? C30 C29 H29 118.2 . . ? C34 C35 H35 120.3 . . ? C36 C35 C34 119.4(3) . . ? C36 C35 H35 120.3 . . ? C35 C36 H36 120.2 . . ? C37 C36 C35 119.5(3) . . ? C37 C36 H36 120.2 . . ? C36 C37 H37 120.4 . . ? C36 C37 C38 119.2(3) . . ? C38 C37 H37 120.4 . . ? N4 C38 C37 122.6(3) . . ? N4 C38 H38 118.7 . . ? C37 C38 H38 118.7 . . ? N3 C24 C25 121.1(3) . . ? N3 C24 C23 115.1(2) . . ? C25 C24 C23 123.8(3) . . ? C24 C25 H25 120.1 . . ? C26 C25 C24 119.8(3) . . ? C26 C25 H25 120.1 . . ? C25 C26 H26 120.5 . . ? C25 C26 C27 119.0(3) . . ? C27 C26 H26 120.5 . . ? C26 C27 H27 120.2 . . ? C26 C27 C28 119.5(3) . . ? C28 C27 H27 120.2 . . ? N3 C28 C27 122.8(3) . . ? N3 C28 H28 118.6 . . ? C27 C28 H28 118.6 . . ? N2 C23 C24 114.2(2) . . ? N2 C23 C22 121.2(3) . . ? C22 C23 C24 124.6(3) . . ? C23 C22 H22 120.1 . . ? C21 C22 C23 119.9(3) . . ? C21 C22 H22 120.1 . . ? C22 C21 H21 120.5 . . ? C22 C21 C20 119.1(3) . . ? C20 C21 H21 120.5 . . ? C21 C20 H20 120.5 . . ? C19 C20 C21 118.9(3) . . ? C19 C20 H20 120.5 . . ? N2 C19 C20 123.1(3) . . ? N2 C19 H19 118.5 . . ? C20 C19 H19 118.5 . . ? O4 C12 O5 118.8(3) . . ? O4 C12 C11 128.2(3) . . ? O5 C12 C11 113.0(3) . . ? O5 C13 H13A 110.4 . . ? O5 C13 H13B 110.4 . . ? O5 C13 C14 106.6(3) . . ? H13A C13 H13B 108.6 . . ? C14 C13 H13A 110.4 . . ? C14 C13 H13B 110.4 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C10 C11 C12 128.0(3) . . ? C10 C11 H11 116.0 . . ? C12 C11 H11 116.0 . . ? C4 C3 C10 120.1(3) . . ? C4 C3 C2 117.9(3) . . ? C2 C3 C10 122.0(3) . . ? C3 C4 H4 118.3 . . ? C3 C4 C9 123.3(3) . . ? C9 C4 H4 118.3 . . ? C5 C9 C4 126.3(3) . . ? C1 C9 C4 117.9(3) . . ? C1 C9 C5 115.8(3) . . ? C9 C5 H5 119.0 . . ? C6 C5 C9 121.9(3) . . ? C6 C5 H5 119.0 . . ? C5 C6 H6 119.2 . . ? C5 C6 C7 121.5(3) . . ? C7 C6 H6 119.2 . . ? C8 C7 C6 117.0(3) . . ? N1 C7 C6 121.1(3) . . ? N1 C7 C8 121.9(4) . . ? C7 C8 H8 120.3 . . ? C1 C8 C7 119.5(3) . . ? C1 C8 H8 120.3 . . ? O1 C1 C9 119.6(3) . . ? O1 C1 C8 116.1(3) . . ? C8 C1 C9 124.3(3) . . ? O2 C2 O1 114.1(3) . . ? O2 C2 C3 128.6(3) . . ? O1 C2 C3 117.3(3) . . ? C7 N1 C17 121.2(3) . . ? C7 N1 C15 121.1(4) . . ? C15 N1 C17 117.6(3) . . ? N1 C17 H17A 109.4 . . ? N1 C17 H17B 109.4 . . ? H17A C17 H17B 108.0 . . ? C18 C17 N1 111.3(4) . . ? C18 C17 H17A 109.4 . . ? C18 C17 H17B 109.4 . . ? C17 C18 H18A 109.5 . . ? C17 C18 H18B 109.5 . . ? C17 C18 H18C 109.5 . . ? H18A C18 H18B 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? N1 C15 H15A 108.7 . . ? N1 C15 H15B 108.7 . . ? N1 C15 C16 114.0(4) . . ? H15A C15 H15B 107.6 . . ? C16 C15 H15A 108.7 . . ? C16 C15 H15B 108.7 . . ? C15 C16 H16A 109.5 . . ? C15 C16 H16B 109.5 . . ? C15 C16 H16C 109.5 . . ? H16A C16 H16B 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 O4 2.085(2) . ? Ru1 O3 2.0930(19) . ? Ru1 N4 2.054(2) . ? Ru1 N5 2.029(3) . ? Ru1 N3 2.028(2) . ? Ru1 N2 2.048(2) . ? P1 F2 1.581(2) . ? P1 F4 1.555(3) . ? P1 F6 1.581(2) . ? P1 F3 1.594(2) . ? P1 F5 1.584(3) . ? P1 F1 1.586(2) . ? O4 C12 1.244(4) . ? O3 C10 1.289(4) . ? N4 C34 1.358(4) . ? N4 C38 1.343(4) . ? N5 C33 1.367(4) . ? N5 C29 1.345(4) . ? N3 C24 1.359(4) . ? N3 C28 1.345(4) . ? N2 C23 1.361(4) . ? N2 C19 1.340(4) . ? O5 C12 1.341(4) . ? O5 C13 1.429(4) . ? O2 C2 1.193(5) . ? C10 C11 1.372(4) . ? C10 C3 1.501(4) . ? O1 C1 1.364(4) . ? O1 C2 1.377(4) . ? C34 C33 1.469(4) . ? C34 C35 1.383(4) . ? C33 C32 1.382(5) . ? C32 H32 0.9300 . ? C32 C31 1.367(5) . ? C31 H31 0.9300 . ? C31 C30 1.366(5) . ? C30 H30 0.9300 . ? C30 C29 1.365(5) . ? C29 H29 0.9300 . ? C35 H35 0.9300 . ? C35 C36 1.370(5) . ? C36 H36 0.9300 . ? C36 C37 1.359(5) . ? C37 H37 0.9300 . ? C37 C38 1.374(5) . ? C38 H38 0.9300 . ? C24 C25 1.391(4) . ? C24 C23 1.466(4) . ? C25 H25 0.9300 . ? C25 C26 1.367(5) . ? C26 H26 0.9300 . ? C26 C27 1.368(5) . ? C27 H27 0.9300 . ? C27 C28 1.369(5) . ? C28 H28 0.9300 . ? C23 C22 1.373(4) . ? C22 H22 0.9300 . ? C22 C21 1.369(5) . ? C21 H21 0.9300 . ? C21 C20 1.374(5) . ? C20 H20 0.9300 . ? C20 C19 1.365(4) . ? C19 H19 0.9300 . ? C12 C11 1.400(4) . ? C13 H13A 0.9700 . ? C13 H13B 0.9700 . ? C13 C14 1.496(5) . ? C14 H14A 0.9600 . ? C14 H14B 0.9600 . ? C14 H14C 0.9600 . ? C11 H11 0.9300 . ? C3 C4 1.354(4) . ? C3 C2 1.455(5) . ? C4 H4 0.9300 . ? C4 C9 1.417(4) . ? C9 C5 1.397(4) . ? C9 C1 1.383(4) . ? C5 H5 0.9300 . ? C5 C6 1.360(5) . ? C6 H6 0.9300 . ? C6 C7 1.419(5) . ? C7 C8 1.400(5) . ? C7 N1 1.368(4) . ? C8 H8 0.9300 . ? C8 C1 1.374(4) . ? N1 C17 1.508(6) . ? N1 C15 1.469(5) . ? C17 H17A 0.9700 . ? C17 H17B 0.9700 . ? C17 C18 1.463(7) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C15 H15A 0.9700 . ? C15 H15B 0.9700 . ? C15 C16 1.486(7) . ? C16 H16A 0.9600 . ? C16 H16B 0.9600 . ? C16 H16C 0.9600 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A C28 H28 F4 0.93 2.51 3.141(4) 125.5 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Ru1 O4 C12 O5 -174.4(2) . . . . ? Ru1 O4 C12 C11 5.9(5) . . . . ? Ru1 O3 C10 C11 12.0(4) . . . . ? Ru1 O3 C10 C3 -168.60(19) . . . . ? Ru1 N4 C34 C33 -2.8(3) . . . . ? Ru1 N4 C34 C35 178.9(2) . . . . ? Ru1 N4 C38 C37 179.4(2) . . . . ? Ru1 N5 C33 C34 2.0(3) . . . . ? Ru1 N5 C33 C32 -178.8(3) . . . . ? Ru1 N5 C29 C30 179.2(3) . . . . ? Ru1 N3 C24 C25 -170.4(3) . . . . ? Ru1 N3 C24 C23 7.7(3) . . . . ? Ru1 N3 C28 C27 167.6(3) . . . . ? Ru1 N2 C23 C24 5.1(3) . . . . ? Ru1 N2 C23 C22 -173.8(3) . . . . ? Ru1 N2 C19 C20 172.8(3) . . . . ? O4 C12 C11 C10 -8.4(6) . . . . ? O3 C10 C11 C12 -2.3(6) . . . . ? O3 C10 C3 C4 4.3(4) . . . . ? O3 C10 C3 C2 -176.2(3) . . . . ? N4 C34 C33 N5 0.5(4) . . . . ? N4 C34 C33 C32 -178.6(3) . . . . ? N4 C34 C35 C36 1.5(5) . . . . ? N5 C33 C32 C31 -0.1(6) . . . . ? N3 C24 C25 C26 1.7(5) . . . . ? N3 C24 C23 N2 -8.4(4) . . . . ? N3 C24 C23 C22 170.4(3) . . . . ? N2 C23 C22 C21 -0.2(6) . . . . ? O5 C12 C11 C10 171.8(3) . . . . ? C10 C3 C4 C9 179.4(3) . . . . ? C10 C3 C2 O2 3.6(8) . . . . ? C10 C3 C2 O1 -176.9(3) . . . . ? C34 N4 C38 C37 0.4(5) . . . . ? C34 C33 C32 C31 178.9(4) . . . . ? C34 C35 C36 C37 0.7(6) . . . . ? C33 N5 C29 C30 0.3(5) . . . . ? C33 C34 C35 C36 -176.7(3) . . . . ? C33 C32 C31 C30 -0.4(7) . . . . ? C32 C31 C30 C29 0.9(7) . . . . ? C31 C30 C29 N5 -0.9(6) . . . . ? C29 N5 C33 C34 -178.9(3) . . . . ? C29 N5 C33 C32 0.2(5) . . . . ? C35 C34 C33 N5 178.8(3) . . . . ? C35 C34 C33 C32 -0.3(5) . . . . ? C35 C36 C37 C38 -2.2(6) . . . . ? C36 C37 C38 N4 1.7(5) . . . . ? C38 N4 C34 C33 176.3(3) . . . . ? C38 N4 C34 C35 -2.0(4) . . . . ? C24 N3 C28 C27 -1.2(5) . . . . ? C24 C25 C26 C27 -1.4(6) . . . . ? C24 C23 C22 C21 -178.9(4) . . . . ? C25 C24 C23 N2 169.6(3) . . . . ? C25 C24 C23 C22 -11.6(5) . . . . ? C25 C26 C27 C28 -0.1(6) . . . . ? C26 C27 C28 N3 1.5(6) . . . . ? C28 N3 C24 C25 -0.4(5) . . . . ? C28 N3 C24 C23 177.6(3) . . . . ? C23 N2 C19 C20 -1.3(5) . . . . ? C23 C24 C25 C26 -176.2(4) . . . . ? C23 C22 C21 C20 -0.4(6) . . . . ? C22 C21 C20 C19 0.1(6) . . . . ? C21 C20 C19 N2 0.8(5) . . . . ? C19 N2 C23 C24 179.9(3) . . . . ? C19 N2 C23 C22 1.0(5) . . . . ? C12 O5 C13 C14 -178.8(3) . . . . ? C13 O5 C12 O4 5.0(5) . . . . ? C13 O5 C12 C11 -175.2(3) . . . . ? C11 C10 C3 C4 -176.2(3) . . . . ? C11 C10 C3 C2 3.3(5) . . . . ? C3 C10 C11 C12 178.3(3) . . . . ? C3 C4 C9 C5 177.9(3) . . . . ? C3 C4 C9 C1 -2.3(5) . . . . ? C4 C3 C2 O2 -176.9(6) . . . . ? C4 C3 C2 O1 2.7(6) . . . . ? C4 C9 C5 C6 179.5(3) . . . . ? C4 C9 C1 O1 2.3(5) . . . . ? C4 C9 C1 C8 -178.7(3) . . . . ? C9 C5 C6 C7 -1.3(6) . . . . ? C5 C9 C1 O1 -178.0(3) . . . . ? C5 C9 C1 C8 1.1(5) . . . . ? C5 C6 C7 C8 2.1(5) . . . . ? C5 C6 C7 N1 -177.5(4) . . . . ? C6 C7 C8 C1 -1.3(5) . . . . ? C6 C7 N1 C17 176.1(4) . . . . ? C6 C7 N1 C15 -6.6(6) . . . . ? C7 C8 C1 O1 178.8(3) . . . . ? C7 C8 C1 C9 -0.3(5) . . . . ? C7 N1 C17 C18 89.9(5) . . . . ? C7 N1 C15 C16 -77.3(5) . . . . ? C8 C7 N1 C17 -3.5(6) . . . . ? C8 C7 N1 C15 173.8(4) . . . . ? C1 O1 C2 O2 176.8(5) . . . . ? C1 O1 C2 C3 -2.8(6) . . . . ? C1 C9 C5 C6 -0.3(5) . . . . ? C2 O1 C1 C9 0.3(5) . . . . ? C2 O1 C1 C8 -178.8(4) . . . . ? C2 C3 C4 C9 -0.2(5) . . . . ? N1 C7 C8 C1 178.3(3) . . . . ? C17 N1 C15 C16 100.1(5) . . . . ? C15 N1 C17 C18 -87.5(5) . . . . ?