Crystallography Open Database

Information card for entry 7708306

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Coordinates	7708306.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Hepta-tert-butyl-nonaphosphine(7)
Chemical name	'1,3,3',4,4',5,5'-Hepta-tert-butyl-nonaphosphine(7)'
Formula	C28 H63 P9
Calculated formula	C28 H63 P9
SMILES	C(C)(C)(C)P1P(C(C)(C)C)P(C(C)(C)C)P1P(C(C)(C)C)P1P(C(C)(C)C)P(C(C)(C)C)P1C(C)(C)C
Title of publication	Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes
Authors of publication	Eilrich, Volker Jens; Grell, Toni; Lönnecke, Peter; Hey-Hawkins, Evamarie
Journal of publication	Dalton Transactions
Year of publication	2021
a	9.8283 ± 0.0002 Å
b	13.4869 ± 0.0003 Å
c	15.1621 ± 0.0003 Å
α	84.231 ± 0.002°
β	82.229 ± 0.002°
γ	77.488 ± 0.002°
Cell volume	1938.76 ± 0.07 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0316
Residual factor for significantly intense reflections	0.0245
Weighted residual factors for significantly intense reflections	0.059
Weighted residual factors for all reflections included in the refinement	0.0623
Goodness-of-fit parameter for all reflections included in the refinement	1.062
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
269192 (current)	2021-09-18	cif/ Adding structures of 7708306, 7708307, 7708308, 7708309, 7708310, 7708311, 7708312 via cif-deposit CGI script.	7708306.cif