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Information card for entry 7708309
Preview
| Coordinates | 7708309.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H51 Li N2 O P4 |
|---|---|
| Calculated formula | C22 H51 Li N2 O P4 |
| SMILES | P1(P(P(P1C(C)(C)C)C(C)(C)C)C(C)(C)C)[Li]1([O]2CCCC2)[N](CC[N]1(C)C)(C)C |
| Title of publication | Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes |
| Authors of publication | Eilrich, Volker Jens; Grell, Toni; Lönnecke, Peter; Hey-Hawkins, Evamarie |
| Journal of publication | Dalton Transactions |
| Year of publication | 2021 |
| a | 8.8751 ± 0.0002 Å |
| b | 15.4665 ± 0.0003 Å |
| c | 11.1923 ± 0.0003 Å |
| α | 90° |
| β | 105.434 ± 0.003° |
| γ | 90° |
| Cell volume | 1480.93 ± 0.06 Å3 |
| Cell temperature | 130 ± 2 K |
| Ambient diffraction temperature | 130 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.0491 |
| Residual factor for significantly intense reflections | 0.0384 |
| Weighted residual factors for significantly intense reflections | 0.0798 |
| Weighted residual factors for all reflections included in the refinement | 0.0861 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.028 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 269192 (current) | 2021-09-18 | cif/ Adding structures of 7708306, 7708307, 7708308, 7708309, 7708310, 7708311, 7708312 via cif-deposit CGI script. |
7708309.cif |
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Users of the data should acknowledge the original authors of the
structural data.