#------------------------------------------------------------------------------ #$Date: 2021-11-03 02:03:18 +0200 (Wed, 03 Nov 2021) $ #$Revision: 270220 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/86/7708680.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708680 loop_ _publ_author_name 'Meyer, Marco' 'Mardegan, Lorenzo' 'Tordera, Daniel' 'Prescimone, Alessandro' 'Sessolo, Michele' 'Bolink, Henk J.' 'Constable, Edwin C.' 'Housecroft, Catherine E.' _publ_section_title ; A counterion study of a series of [Cu(P^P)(N^N)][A] compounds with bis(phosphane) and 6-methyl and 6,6'-dimethyl-substituted 2,2'-bipyridine ligands for light-emitting electrochemical cells ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03239A _journal_year 2021 _chemical_absolute_configuration ad _chemical_formula_moiety 'C51 H44 Cu N2 O P2, 0.7(C3 H6 O), C24 H20 B' _chemical_formula_sum 'C77.1 H68.2 B Cu N2 O1.7 P2' _chemical_formula_weight 1186.22 _space_group_crystal_system orthorhombic _space_group_IT_number 33 _space_group_name_Hall 'P 2c -2n' _space_group_name_H-M_alt 'P n a 21' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2021-03-12 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6272) ; _audit_update_record ; 2021-05-01 deposited with the CCDC. 2021-11-02 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 28.7566(8) _cell_length_b 14.3706(4) _cell_length_c 30.3845(10) _cell_measurement_reflns_used 9895 _cell_measurement_temperature 150 _cell_measurement_theta_max 69.245 _cell_measurement_theta_min 3.074 _cell_volume 12556.4(6) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection 'Apex2 (Bruker AXS, 2006)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 150 _diffrn_measured_fraction_theta_full 0.980 _diffrn_measured_fraction_theta_max 0.943 _diffrn_measurement_device Area _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0895 _diffrn_reflns_av_unetI/netI 0.0931 _diffrn_reflns_Laue_measured_fraction_full 0.980 _diffrn_reflns_Laue_measured_fraction_max 0.943 _diffrn_reflns_limit_h_max 34 _diffrn_reflns_limit_h_min -32 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 36 _diffrn_reflns_limit_l_min -31 _diffrn_reflns_number 48359 _diffrn_reflns_point_group_measured_fraction_full 0.826 _diffrn_reflns_point_group_measured_fraction_max 0.793 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 70.005 _diffrn_reflns_theta_min 3.733 _diffrn_source_current 0.6 _diffrn_source_power 0.03 _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.345 _exptl_absorpt_correction_T_max 0.7533 _exptl_absorpt_correction_T_min 0.5416 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.1127 before and 0.0805 after correction. The Ratio of minimum to maximum transmission is 0.7190. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.255 _exptl_crystal_description plate _exptl_crystal_F_000 4979 _exptl_crystal_size_max 0.23 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.776 _refine_diff_density_min -0.436 _refine_diff_density_rms 0.078 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.10(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.009 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 1507 _refine_ls_number_reflns 18870 _refine_ls_number_restraints 7 _refine_ls_restrained_S_all 1.009 _refine_ls_R_factor_all 0.0764 _refine_ls_R_factor_gt 0.0592 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0820P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1389 _refine_ls_wR_factor_ref 0.1509 _reflns_Friedel_coverage 0.648 _reflns_Friedel_fraction_full 0.667 _reflns_Friedel_fraction_max 0.636 _reflns_number_gt 15392 _reflns_number_total 18870 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03239a2.cif _cod_data_source_block mem054_150k _cod_original_formula_sum 'C77.10 H68.20 B Cu N2 O1.70 P2' _cod_database_code 7708680 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.889 _shelx_estimated_absorpt_t_min 0.747 _olex2_refinement_description ; 1. Twinned data refinement Scales: 0.90(3) 0.10(3) 2. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 3. Restrained distances O4-C154 1.2 with sigma of 0.02 C155-C154 = C156-C154 1.48 with sigma of 0.005 C155-C156 2.58 with sigma of 0.02 O4-C155 \\sim O4-C156 with sigma of 0.02 C155-C154 \\sim C156-C154 with sigma of 0.02 4. Uiso/Uaniso restraints and constraints Uanis(C24) = Uanis(C23) = Uanis(C22) = Uanis(C21) = Uanis(C20) = Uanis(C19) Uiso(O4) = Uiso(C154) = Uiso(C155) = Uiso(C156) 5. Others Fixed Sof: C154(0.4) C155(0.4) H15G(0.4) H15H(0.4) H15I(0.4) O4(0.4) C156(0.4) H15J(0.4) H15K(0.4) H15L(0.4) 6.a Riding coordinates: C155(H15G,H15H,H15I), C156(H15J,H15K,H15L) 6.b Aromatic/amide H refined with riding coordinates: C88(H88), C68(H68), C86(H86), C55(H55), C69(H69), C66(H66), C34(H34), C54(H54), C116(H116), C67(H67), C42(H42), C43(H43), C47(H47), C100(H100), C79(H79), C41(H41), C26(H26), C9(H9), C45(H45), C48(H48), C71(H71), C146(H146), C87(H87), C2(H2), C114(H114), C81(H81), C75(H75), C28(H28), C119(H119), C148(H148), C120(H120), C149(H149), C80(H80), C101(H101), C53(H53), C74(H74), C117(H117), C4(H4), C118(H118), C113(H113), C129(H129), C60(H60), C98(H98), C110(H110), C32(H32), C58(H58), C59(H59), C122(H122), C92(H92), C33(H33), C27(H27), C112(H112), C111(H111), C130(H130), C8(H8), C44(H44), C3(H3), C102(H102), C99(H99), C147(H147), C140(H140), C126(H126), C128(H128), C137(H137), C14(H14), C7(H7), C49(H49), C93(H93), C65(H65), C51(H51), C104(H104), C73(H73), C106(H106), C18(H18), C134(H134), C150(H150), C136(H136), C138(H138), C144(H144), C72(H72), C105(H105), C50(H50), C132(H132), C96(H96), C108(H108), C141(H141), C107(H107), C135(H135), C131(H131), C20(H20), C94(H94), C123(H123), C95(H95), C125(H125), C142(H142), C124(H124), C143(H143), C17(H17), C24(H24), C15(H15), C16(H16), C21(H21), C22(H22), C23(H23) 6.c Idealised Me refined as rotating group: C11(H11A,H11B,H11C), C38(H38A,H38B,H38C), C62(H62A,H62B,H62C), C89(H89A,H89B, H89C), C63(H63A,H63B,H63C), C90(H90A,H90B,H90C), C37(H37A,H37B,H37C), C12(H12A, H12B,H12C), C152(H15A,H15B,H15C), C153(H15D,H15E,H15F) ; _shelx_res_file ; TITL mem054_150k_a.res in Pna2(1) mem054_150k.res created by SHELXL-2018/3 at 18:00:05 on 12-Mar-2021 REM Old TITL MEM054_150K in Pna2(1) REM SHELXT solution in Pna2(1): R1 0.104, Rweak 0.014, Alpha 0.006 REM 0.281 for 745 systematic absences, Orientation as input REM Flack x = 0.101 ( 0.017 ) from 5249 Parsons quotients REM Formula found by SHELXT: C148 B2 N8 O8 P4 Cu2 CELL 1.54178 28.7566 14.3706 30.3845 90 90 90 ZERR 8 0.0008 0.0004 0.001 0 0 0 LATT -1 SYMM -X,-Y,0.5+Z SYMM 0.5+X,0.5-Y,+Z SYMM 0.5-X,0.5+Y,0.5+Z SFAC C H B Cu N O P UNIT 616.8 545.6 8 8 16 13.6 16 EADP C24 C23 C22 C21 C20 C19 SADI O4 C155 O4 C156 DFIX 1.2 O4 C154 SADI C155 C154 C156 C154 EADP O4 C154 C155 C156 DFIX 1.48 0.005 C155 C154 C156 C154 DFIX 2.58 C155 C156 L.S. 10 PLAN 5 SIZE 0.09 0.2 0.23 TEMP -123.15 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 acta TWIN -1 0 0 0 -1 0 0 0 -1 2 OMIT 0 0 -2 OMIT 2 0 0 OMIT 0 1 -1 OMIT 1 1 0 OMIT 1 2 -5 OMIT 3 1 2 OMIT 1 2 3 OMIT 1 2 -3 REM REM REM WGHT 0.082000 BASF 0.09562 FVAR 0.12824 CU1 4 0.600353 0.758416 0.422587 11.00000 0.02155 0.02269 = 0.02409 -0.00083 0.00219 -0.00222 CU2 4 0.658977 1.241095 0.598738 11.00000 0.02044 0.02304 = 0.02040 -0.00063 0.00074 -0.00161 P2 7 0.673586 0.796394 0.442140 11.00000 0.02229 0.01997 = 0.02261 0.00089 0.00146 -0.00193 P3 7 0.585180 1.204643 0.576624 11.00000 0.01987 0.02269 = 0.02015 -0.00045 0.00018 -0.00147 P4 7 0.668656 1.237390 0.674071 11.00000 0.02521 0.02545 = 0.01771 -0.00089 -0.00172 -0.00485 P1 7 0.583417 0.748073 0.348450 11.00000 0.02777 0.02504 = 0.02300 -0.00252 0.00068 -0.00160 O2 6 0.596752 1.104262 0.657809 11.00000 0.02576 0.02221 = 0.01996 0.00021 -0.00594 -0.00269 O1 6 0.655235 0.886362 0.361126 11.00000 0.02812 0.02271 = 0.02386 -0.00055 -0.00283 0.00069 N4 5 0.692364 1.356118 0.568376 11.00000 0.01915 0.02001 = 0.02433 -0.00050 0.00078 -0.00134 N1 5 0.562507 0.648989 0.450634 11.00000 0.02702 0.01860 = 0.02493 0.00098 0.00121 -0.00324 O3 6 0.841037 1.109509 0.163183 11.00000 0.05484 0.05427 = 0.05456 0.01427 0.01275 0.01143 N2 5 0.540692 0.831057 0.445815 11.00000 0.02462 0.02390 = 0.02100 -0.00396 0.00129 -0.00091 N3 5 0.716445 1.175627 0.569232 11.00000 0.02298 0.02504 = 0.02188 -0.00028 -0.00178 -0.00368 C78 1 0.572173 0.950135 0.637035 11.00000 0.02115 0.02463 = 0.02638 -0.00143 0.00102 -0.00414 C88 1 0.651181 0.945644 0.735728 11.00000 0.03080 0.03051 = 0.02760 0.00667 0.00047 0.00265 AFIX 43 H88 2 0.647594 0.884985 0.747684 11.00000 -1.20000 AFIX 0 C76 1 0.570457 1.081290 0.585541 11.00000 0.01638 0.02604 = 0.02406 0.00191 -0.00140 -0.00124 C56 1 0.749331 1.236049 0.555469 11.00000 0.02564 0.02597 = 0.01326 -0.00092 -0.00185 0.00056 C68 1 0.522834 1.232795 0.455700 11.00000 0.03486 0.03478 = 0.03194 -0.00574 -0.00791 0.00584 AFIX 43 H68 2 0.492252 1.230766 0.443914 11.00000 -1.20000 AFIX 0 C77 1 0.579328 1.043433 0.625973 11.00000 0.02048 0.02166 = 0.02871 -0.00652 0.00429 -0.00328 C39 1 0.625488 0.915822 0.328499 11.00000 0.02455 0.02370 = 0.02270 -0.00089 0.00560 0.00701 C5 1 0.518869 0.672349 0.461643 11.00000 0.02425 0.02665 = 0.02676 -0.00577 -0.00246 -0.00396 C97 1 0.624473 1.307202 0.702499 11.00000 0.03489 0.03340 = 0.01923 0.00178 -0.00317 0.00675 C86 1 0.693266 1.090151 0.734056 11.00000 0.02903 0.03312 = 0.02606 0.00053 -0.00280 -0.00229 AFIX 43 H86 2 0.718002 1.127857 0.744615 11.00000 -1.20000 AFIX 0 C55 1 0.792718 1.205446 0.541501 11.00000 0.02432 0.02705 = 0.03392 0.00309 0.00329 0.00000 AFIX 43 H55 2 0.815571 1.248476 0.531724 11.00000 -1.20000 AFIX 0 C61 1 0.677606 1.444176 0.565214 11.00000 0.02877 0.02749 = 0.02259 -0.00098 -0.00307 -0.00285 C57 1 0.736356 1.335459 0.555277 11.00000 0.02312 0.02248 = 0.01911 -0.00326 0.00022 0.00136 C30 1 0.666460 1.074269 0.329278 11.00000 0.03529 0.02957 = 0.02932 0.00658 0.01174 -0.00104 C69 1 0.530210 1.218604 0.499917 11.00000 0.02294 0.03155 = 0.03177 -0.00538 -0.00105 0.00374 AFIX 43 H69 2 0.504401 1.206647 0.518596 11.00000 -1.20000 AFIX 0 C40 1 0.686191 0.782116 0.500604 11.00000 0.02407 0.01919 = 0.03225 0.00717 -0.00337 -0.00076 C10 1 0.531324 0.923454 0.441967 11.00000 0.02937 0.02573 = 0.02993 -0.00413 0.00066 0.00349 C66 1 0.605578 1.252738 0.445478 11.00000 0.03929 0.03325 = 0.02331 -0.00081 0.00765 0.00170 AFIX 43 H66 2 0.631408 1.264598 0.426810 11.00000 -1.20000 AFIX 0 C1 1 0.575180 0.558099 0.452690 11.00000 0.02798 0.02551 = 0.03777 -0.00041 0.00173 -0.00129 C34 1 0.705716 0.981662 0.460221 11.00000 0.03185 0.02488 = 0.02754 -0.00251 -0.00067 -0.00128 AFIX 43 H34 2 0.714193 0.961879 0.488955 11.00000 -1.20000 AFIX 0 C29 1 0.632215 1.003501 0.308906 11.00000 0.02636 0.03049 = 0.02804 0.00205 0.00814 0.00320 C54 1 0.802034 1.109889 0.542140 11.00000 0.02641 0.03490 = 0.04328 0.00417 0.00652 0.00807 AFIX 43 H54 2 0.831633 1.087068 0.533404 11.00000 -1.20000 AFIX 0 C25 1 0.590601 0.854913 0.315581 11.00000 0.02594 0.02777 = 0.02268 -0.00129 0.00378 0.00813 C83 1 0.620368 0.975777 0.703011 11.00000 0.02891 0.02385 = 0.02713 0.00056 0.00294 -0.00084 C116 1 0.272524 1.168429 0.427094 11.00000 0.03087 0.02745 = 0.02468 -0.00113 -0.00117 0.00617 AFIX 43 H116 2 0.283973 1.178294 0.456049 11.00000 -1.20000 AFIX 0 C67 1 0.561046 1.250304 0.428233 11.00000 0.05483 0.02910 = 0.01885 -0.00060 0.00004 0.00396 AFIX 43 H67 2 0.556342 1.260535 0.397666 11.00000 -1.20000 AFIX 0 C91 1 0.723961 1.277057 0.696710 11.00000 0.03780 0.02328 = 0.02361 0.00393 -0.00743 -0.01011 C35 1 0.686866 0.918908 0.430096 11.00000 0.02099 0.02451 = 0.03191 -0.00248 0.00107 -0.00021 C46 1 0.722592 0.736512 0.415504 11.00000 0.02497 0.02626 = 0.02925 0.00096 -0.00050 -0.00230 C42 1 0.739491 0.770586 0.561637 11.00000 0.02991 0.02572 = 0.04044 0.00121 -0.00628 0.00065 AFIX 43 H42 2 0.770358 0.769866 0.572776 11.00000 -1.20000 AFIX 0 C43 1 0.702425 0.759207 0.590076 11.00000 0.04156 0.02886 = 0.02544 0.00029 -0.00644 0.00323 AFIX 43 H43 2 0.707985 0.751715 0.620692 11.00000 -1.20000 AFIX 0 C139 1 0.371781 0.717224 0.554678 11.00000 0.01746 0.04521 = 0.04062 0.00270 0.00072 -0.00426 C47 1 0.733379 0.643458 0.427606 11.00000 0.02738 0.02742 = 0.03960 0.00366 -0.00343 -0.00411 AFIX 43 H47 2 0.716868 0.614817 0.451055 11.00000 -1.20000 AFIX 0 C100 1 0.554570 1.418757 0.738390 11.00000 0.04685 0.04506 = 0.03553 -0.00540 0.00464 0.01275 AFIX 43 H100 2 0.530455 1.456771 0.749942 11.00000 -1.20000 AFIX 0 C79 1 0.556106 0.893614 0.603139 11.00000 0.03008 0.02240 = 0.03491 -0.00559 0.00026 -0.00271 AFIX 43 H79 2 0.551259 0.829319 0.608780 11.00000 -1.20000 AFIX 0 C11 1 0.569310 0.986115 0.427390 11.00000 0.03765 0.02544 = 0.03856 -0.00356 0.01224 0.00042 AFIX 137 H11A 2 0.575265 0.976422 0.395965 11.00000 -1.50000 H11B 2 0.597589 0.972368 0.444173 11.00000 -1.50000 H11C 2 0.560172 1.050953 0.432400 11.00000 -1.50000 AFIX 0 C41 1 0.731984 0.782968 0.517243 11.00000 0.02083 0.03093 = 0.03284 0.00384 0.00022 -0.00058 AFIX 43 H41 2 0.757547 0.792044 0.497910 11.00000 -1.20000 AFIX 0 C26 1 0.564059 0.877531 0.279164 11.00000 0.02721 0.03746 = 0.03269 -0.00408 -0.00028 0.00164 AFIX 43 H26 2 0.540042 0.836961 0.269533 11.00000 -1.20000 AFIX 0 C36 1 0.674346 0.951957 0.388838 11.00000 0.02389 0.02305 = 0.02526 -0.00598 0.00502 0.00118 C9 1 0.487583 0.958140 0.452240 11.00000 0.03551 0.02715 = 0.03248 -0.00413 0.00102 0.00221 AFIX 43 H9 2 0.481335 1.022736 0.449206 11.00000 -1.20000 AFIX 0 C145 1 0.438447 0.689684 0.614683 11.00000 0.03073 0.02762 = 0.03779 -0.00757 -0.00043 -0.00609 C45 1 0.648996 0.769299 0.529790 11.00000 0.02174 0.03277 = 0.02970 0.00253 0.00416 0.00126 AFIX 43 H45 2 0.618026 0.767941 0.518926 11.00000 -1.20000 AFIX 0 C64 1 0.574905 1.221418 0.517921 11.00000 0.02303 0.02055 = 0.02381 -0.00395 -0.00102 0.00425 C48 1 0.767282 0.594384 0.405927 11.00000 0.03071 0.02169 = 0.06574 -0.00521 -0.00475 0.00317 AFIX 43 H48 2 0.773830 0.532110 0.414393 11.00000 -1.20000 AFIX 0 C38 1 0.643155 1.170159 0.329804 11.00000 0.05621 0.02738 = 0.03909 0.00400 -0.00497 0.00115 AFIX 137 H38A 2 0.637926 1.191093 0.299510 11.00000 -1.50000 H38B 2 0.663339 1.214709 0.345016 11.00000 -1.50000 H38C 2 0.613295 1.165999 0.345223 11.00000 -1.50000 AFIX 0 C71 1 0.520929 1.351159 0.583688 11.00000 0.03010 0.02891 = 0.04282 -0.00422 -0.00357 0.00214 AFIX 43 H71 2 0.537657 1.377191 0.559702 11.00000 -1.20000 AFIX 0 C146 1 0.449908 0.642772 0.652881 11.00000 0.03942 0.04618 = 0.03786 -0.00632 0.00132 0.00836 AFIX 43 H146 2 0.426924 0.636154 0.675121 11.00000 -1.20000 AFIX 0 C121 1 0.351901 1.331177 0.376404 11.00000 0.03238 0.03625 = 0.04076 0.00333 -0.00955 -0.01011 C87 1 0.686507 1.001517 0.751022 11.00000 0.03182 0.03014 = 0.03677 0.00558 -0.00360 0.00205 AFIX 43 H87 2 0.706550 0.979118 0.773506 11.00000 -1.20000 AFIX 0 C2 1 0.544373 0.489304 0.465718 11.00000 0.04058 0.02323 = 0.04441 0.00347 0.00124 -0.00157 AFIX 43 H2 2 0.554099 0.426216 0.467313 11.00000 -1.20000 AFIX 0 C82 1 0.579083 0.921722 0.684585 11.00000 0.03313 0.02573 = 0.02601 0.00082 0.00454 -0.00140 C114 1 0.376687 1.139615 0.470519 11.00000 0.03143 0.03999 = 0.02888 -0.00466 0.00197 0.00686 AFIX 43 H114 2 0.365055 1.084835 0.456912 11.00000 -1.20000 AFIX 0 C81 1 0.553787 1.021849 0.552529 11.00000 0.02685 0.02901 = 0.02487 -0.00409 -0.00371 -0.00373 AFIX 43 H81 2 0.547124 1.045434 0.524010 11.00000 -1.20000 AFIX 0 C75 1 0.509999 1.228353 0.636012 11.00000 0.03052 0.03563 = 0.02972 -0.00690 0.00006 0.00295 AFIX 43 H75 2 0.518933 1.170376 0.648429 11.00000 -1.20000 AFIX 0 C70 1 0.534763 1.265131 0.601026 11.00000 0.02086 0.02968 = 0.02239 -0.00889 -0.00260 -0.00074 C28 1 0.605415 1.021949 0.271266 11.00000 0.03544 0.03159 = 0.03669 0.00808 0.00623 0.00870 AFIX 43 H28 2 0.610082 1.078449 0.255646 11.00000 -1.20000 AFIX 0 C119 1 0.236684 1.139854 0.344089 11.00000 0.04147 0.02948 = 0.03683 -0.00512 -0.01166 0.00054 AFIX 43 H119 2 0.224576 1.129650 0.315402 11.00000 -1.20000 AFIX 0 C127 1 0.348967 0.699518 0.641663 11.00000 0.02869 0.03121 = 0.03985 0.00678 -0.00586 0.00351 C148 1 0.528461 0.613161 0.627837 11.00000 0.03169 0.04106 = 0.05488 -0.01424 -0.00404 0.00847 AFIX 43 H148 2 0.558707 0.588606 0.632654 11.00000 -1.20000 AFIX 0 C120 1 0.282226 1.169961 0.349492 11.00000 0.03844 0.03157 = 0.02716 -0.00079 -0.00184 0.00267 AFIX 43 H120 2 0.300577 1.181350 0.324058 11.00000 -1.20000 AFIX 0 C13 1 0.521302 0.720536 0.346269 11.00000 0.03749 0.05128 = 0.01764 -0.00082 -0.00111 -0.01715 C149 1 0.518098 0.657375 0.589158 11.00000 0.02812 0.02996 = 0.06286 -0.00831 -0.00376 0.00415 AFIX 43 H149 2 0.540956 0.662350 0.566708 11.00000 -1.20000 AFIX 0 C85 1 0.663172 1.123954 0.701018 11.00000 0.02725 0.02465 = 0.02483 -0.00026 0.00447 0.00103 C80 1 0.547046 0.927490 0.561940 11.00000 0.03743 0.02815 = 0.02440 -0.00796 0.00004 -0.00500 AFIX 43 H80 2 0.536120 0.886731 0.539602 11.00000 -1.20000 AFIX 0 C101 1 0.588160 1.456023 0.710859 11.00000 0.04808 0.03532 = 0.03975 0.00345 0.00002 0.00634 AFIX 43 H101 2 0.587690 1.520751 0.704523 11.00000 -1.20000 AFIX 0 C53 1 0.768253 1.050253 0.555397 11.00000 0.03063 0.02310 = 0.03240 -0.00051 -0.00065 0.00585 AFIX 43 H53 2 0.774112 0.985194 0.555344 11.00000 -1.20000 AFIX 0 C31 1 0.680126 1.043763 0.375072 11.00000 0.02568 0.02431 = 0.03093 0.00135 0.00365 0.00304 C74 1 0.471692 1.276814 0.653103 11.00000 0.03892 0.05159 = 0.03170 -0.00516 0.00909 0.00211 AFIX 43 H74 2 0.454732 1.251296 0.677067 11.00000 -1.20000 AFIX 0 C115 1 0.302197 1.184222 0.391220 11.00000 0.03226 0.02399 = 0.03462 0.00057 0.00048 0.00245 C117 1 0.226476 1.138526 0.421527 11.00000 0.02727 0.03018 = 0.04024 0.00017 0.00464 -0.00202 AFIX 43 H117 2 0.207533 1.127923 0.446646 11.00000 -1.20000 AFIX 0 C4 1 0.486145 0.605986 0.474294 11.00000 0.03429 0.03430 = 0.05134 -0.00354 0.01078 -0.00713 AFIX 43 H4 2 0.455252 0.623976 0.481387 11.00000 -1.20000 AFIX 0 C52 1 0.725217 1.083201 0.569040 11.00000 0.02537 0.02441 = 0.01982 -0.00311 -0.00226 0.00104 C118 1 0.208765 1.124644 0.381006 11.00000 0.03071 0.02923 = 0.04930 -0.00533 -0.00278 -0.00033 AFIX 43 H118 2 0.177488 1.104640 0.377567 11.00000 -1.20000 AFIX 0 C113 1 0.394772 1.132080 0.512726 11.00000 0.02953 0.04954 = 0.02996 0.00531 0.00212 0.01031 AFIX 43 H113 2 0.395453 1.073457 0.527162 11.00000 -1.20000 AFIX 0 C151 1 0.808098 1.110483 0.187265 11.00000 0.04585 0.04175 = 0.04510 0.01889 0.00053 0.01387 C129 1 0.285570 0.594612 0.662978 11.00000 0.04668 0.05115 = 0.04439 0.01401 -0.00968 -0.02697 AFIX 43 H129 2 0.265487 0.544758 0.655212 11.00000 -1.20000 AFIX 0 C60 1 0.706873 1.515681 0.551037 11.00000 0.03882 0.02126 = 0.03709 -0.00276 -0.00222 -0.00436 AFIX 43 H60 2 0.695626 1.577686 0.548975 11.00000 -1.20000 AFIX 0 C98 1 0.591662 1.269110 0.731154 11.00000 0.04123 0.03381 = 0.02758 -0.00281 0.00780 -0.00175 AFIX 43 H98 2 0.593226 1.204968 0.738576 11.00000 -1.20000 AFIX 0 C110 1 0.393212 1.300746 0.468656 11.00000 0.02388 0.04454 = 0.03142 -0.00551 0.00413 -0.00387 AFIX 43 H110 2 0.393584 1.359059 0.453932 11.00000 -1.20000 AFIX 0 C62 1 0.628085 1.464591 0.576950 11.00000 0.03106 0.02929 = 0.03976 0.00405 0.00196 0.00398 AFIX 137 H62A 2 0.626777 1.520455 0.595406 11.00000 -1.50000 H62B 2 0.614979 1.411733 0.593119 11.00000 -1.50000 H62C 2 0.610081 1.474948 0.550007 11.00000 -1.50000 AFIX 0 C32 1 0.699815 1.104624 0.405749 11.00000 0.03520 0.02592 = 0.03430 0.00184 -0.00093 0.00439 AFIX 43 H32 2 0.704973 1.167793 0.397929 11.00000 -1.20000 AFIX 0 C58 1 0.767594 1.405152 0.541753 11.00000 0.02445 0.02734 = 0.02985 0.00118 0.00370 -0.00336 AFIX 43 H58 2 0.798655 1.389792 0.533969 11.00000 -1.20000 AFIX 0 C84 1 0.627612 1.066061 0.687877 11.00000 0.02531 0.03051 = 0.01699 -0.00007 -0.00168 0.00208 C59 1 0.752590 1.495181 0.539986 11.00000 0.03505 0.02482 = 0.04349 0.00142 0.00691 -0.00988 AFIX 43 H59 2 0.773239 1.543382 0.531273 11.00000 -1.20000 AFIX 0 C122 1 0.323324 1.395439 0.397064 11.00000 0.03959 0.03200 = 0.05508 0.00213 -0.01223 -0.00323 AFIX 43 H122 2 0.308854 1.376863 0.423763 11.00000 -1.20000 AFIX 0 C92 1 0.728226 1.317389 0.738089 11.00000 0.04701 0.04607 = 0.03665 -0.00505 -0.01399 -0.00353 AFIX 43 H92 2 0.701078 1.331694 0.754570 11.00000 -1.20000 AFIX 0 C33 1 0.711880 1.073895 0.447387 11.00000 0.03770 0.02423 = 0.03981 -0.00772 -0.00264 -0.00522 AFIX 43 H33 2 0.724723 1.116910 0.467781 11.00000 -1.20000 AFIX 0 C89 1 0.586275 0.815513 0.689844 11.00000 0.05094 0.02776 = 0.02779 0.00548 -0.00582 -0.00438 AFIX 137 H89A 2 0.587459 0.799712 0.721199 11.00000 -1.50000 H89B 2 0.615534 0.797263 0.675738 11.00000 -1.50000 H89C 2 0.560385 0.782349 0.675922 11.00000 -1.50000 AFIX 0 C27 1 0.572782 0.960202 0.256704 11.00000 0.03136 0.04481 = 0.03250 0.00639 -0.00408 0.01401 AFIX 43 H27 2 0.555687 0.973889 0.230744 11.00000 -1.20000 AFIX 0 C112 1 0.411758 1.210354 0.533574 11.00000 0.02332 0.06424 = 0.03170 0.00016 -0.00070 0.00506 AFIX 43 H112 2 0.423683 1.206905 0.562687 11.00000 -1.20000 AFIX 0 C63 1 0.687904 1.019675 0.584277 11.00000 0.03400 0.01982 = 0.04545 -0.00101 0.00646 0.00016 AFIX 137 H63A 2 0.677219 1.039193 0.613480 11.00000 -1.50000 H63B 2 0.700005 0.956015 0.585886 11.00000 -1.50000 H63C 2 0.661829 1.021835 0.563534 11.00000 -1.50000 AFIX 0 C103 1 0.393678 1.160504 0.368847 11.00000 0.03805 0.04608 = 0.01736 0.00315 -0.00357 0.00988 C19 1 0.611738 0.664458 0.311968 11.00000 0.11091 0.05320 = 0.04185 -0.00363 0.01275 0.03585 C111 1 0.410967 1.295485 0.510599 11.00000 0.02440 0.05252 = 0.03192 -0.00960 0.00161 -0.00727 AFIX 43 H111 2 0.422857 1.349976 0.524264 11.00000 -1.20000 AFIX 0 C109 1 0.374532 1.223153 0.446727 11.00000 0.02373 0.03766 = 0.02806 -0.00498 0.00300 0.00039 C130 1 0.281054 0.637236 0.702774 11.00000 0.03520 0.05355 = 0.04787 0.02203 0.00432 0.00435 AFIX 43 H130 2 0.258100 0.616887 0.723095 11.00000 -1.20000 AFIX 0 C8 1 0.453324 0.898947 0.466804 11.00000 0.02732 0.04227 = 0.03990 -0.00268 0.00191 0.00264 AFIX 43 H8 2 0.423508 0.922508 0.474361 11.00000 -1.20000 AFIX 0 C90 1 0.535100 0.950330 0.710401 11.00000 0.03063 0.04891 = 0.03249 0.00131 0.00595 -0.00953 AFIX 137 H90A 2 0.508102 0.916973 0.698632 11.00000 -1.50000 H90B 2 0.530174 1.017509 0.707393 11.00000 -1.50000 H90C 2 0.539107 0.934667 0.741562 11.00000 -1.50000 AFIX 0 C44 1 0.657213 0.758633 0.574307 11.00000 0.03444 0.02574 = 0.03569 0.00022 0.00878 0.00186 AFIX 43 H44 2 0.631908 0.750919 0.594072 11.00000 -1.20000 AFIX 0 C3 1 0.499308 0.513784 0.476355 11.00000 0.03703 0.03206 = 0.05520 -0.00082 0.01039 -0.01274 AFIX 43 H3 2 0.477561 0.467515 0.485017 11.00000 -1.20000 AFIX 0 C102 1 0.621767 1.401665 0.692755 11.00000 0.04754 0.03645 = 0.03094 0.00067 -0.00319 -0.00061 AFIX 43 H102 2 0.643732 1.428543 0.673163 11.00000 -1.20000 AFIX 0 C99 1 0.556851 1.324166 0.748836 11.00000 0.04432 0.04953 = 0.03319 0.00037 0.00971 -0.00315 AFIX 43 H99 2 0.534477 1.297595 0.768104 11.00000 -1.20000 AFIX 0 C147 1 0.494246 0.604450 0.660126 11.00000 0.05398 0.06368 = 0.03329 -0.00534 -0.00622 0.02754 AFIX 43 H147 2 0.500864 0.572810 0.686854 11.00000 -1.20000 AFIX 0 C140 1 0.356273 0.786064 0.524898 11.00000 0.02562 0.05615 = 0.03638 0.00363 0.00176 0.00021 AFIX 43 H140 2 0.353851 0.848459 0.534971 11.00000 -1.20000 AFIX 0 C126 1 0.371787 1.361234 0.336926 11.00000 0.05746 0.06581 = 0.03846 0.01402 -0.01063 -0.02247 AFIX 43 H126 2 0.391170 1.320457 0.320522 11.00000 -1.20000 AFIX 0 C128 1 0.319963 0.624562 0.633511 11.00000 0.04015 0.04405 = 0.03232 0.00771 -0.00661 -0.01361 AFIX 43 H128 2 0.323554 0.591764 0.606578 11.00000 -1.20000 AFIX 0 C137 1 0.435905 0.996557 0.624533 11.00000 0.04086 0.03319 = 0.05968 0.00312 -0.00245 -0.01007 AFIX 43 H137 2 0.465383 1.025989 0.626874 11.00000 -1.20000 AFIX 0 C14 1 0.507941 0.628021 0.349806 11.00000 0.06693 0.07166 = 0.03879 0.01541 -0.02294 -0.04090 AFIX 43 H14 2 0.530314 0.579866 0.346567 11.00000 -1.20000 AFIX 0 C7 1 0.462562 0.805369 0.470346 11.00000 0.02505 0.03088 = 0.03291 -0.00126 0.00101 0.00009 AFIX 43 H7 2 0.439266 0.763284 0.480105 11.00000 -1.20000 AFIX 0 C49 1 0.792332 0.635190 0.371438 11.00000 0.04048 0.04136 = 0.05304 -0.00821 0.01228 0.00370 AFIX 43 H49 2 0.815683 0.601011 0.356344 11.00000 -1.20000 AFIX 0 C93 1 0.771746 1.337007 0.755603 11.00000 0.07189 0.04567 = 0.05040 -0.01189 -0.01961 -0.01728 AFIX 43 H93 2 0.774357 1.361266 0.784583 11.00000 -1.20000 AFIX 0 C6 1 0.506685 0.773705 0.459348 11.00000 0.02531 0.02835 = 0.02274 -0.00191 -0.00112 -0.00267 C65 1 0.612355 1.237790 0.490136 11.00000 0.03026 0.02671 = 0.02832 -0.00029 0.00078 -0.00173 AFIX 43 H65 2 0.642985 1.238769 0.501841 11.00000 -1.20000 AFIX 0 C51 1 0.748057 0.775271 0.381182 11.00000 0.03405 0.03007 = 0.03310 0.00374 0.00623 0.00492 AFIX 43 H51 2 0.741558 0.837289 0.372274 11.00000 -1.20000 AFIX 0 C104 1 0.384484 1.072030 0.351667 11.00000 0.05263 0.05533 = 0.03657 -0.00719 -0.00048 0.01105 AFIX 43 H104 2 0.353613 1.048657 0.352980 11.00000 -1.20000 AFIX 0 C73 1 0.458425 1.361118 0.635456 11.00000 0.03359 0.04624 = 0.04856 -0.01760 0.00374 0.01281 AFIX 43 H73 2 0.432223 1.392998 0.647087 11.00000 -1.20000 AFIX 0 C106 1 0.464610 1.048050 0.331681 11.00000 0.05644 0.10444 = 0.03335 -0.00720 0.00192 0.04364 AFIX 43 H106 2 0.488342 1.010017 0.319454 11.00000 -1.20000 AFIX 0 C18 1 0.488330 0.789550 0.351598 11.00000 0.03384 0.07565 = 0.02627 -0.00650 0.00209 -0.00959 AFIX 43 H18 2 0.496923 0.853233 0.349537 11.00000 -1.20000 AFIX 0 C134 1 0.351874 0.909070 0.616477 11.00000 0.03113 0.03954 = 0.05151 -0.00051 -0.00488 0.00183 AFIX 43 H134 2 0.322331 0.880385 0.613056 11.00000 -1.20000 AFIX 0 C150 1 0.473633 0.695362 0.582720 11.00000 0.02755 0.03865 = 0.04430 -0.00001 0.00206 -0.00256 AFIX 43 H150 2 0.467093 0.726062 0.555731 11.00000 -1.20000 AFIX 0 C133 1 0.391384 0.853101 0.613498 11.00000 0.03299 0.04051 = 0.02915 -0.00075 0.00175 -0.00107 C136 1 0.395897 1.048501 0.628148 11.00000 0.04909 0.03550 = 0.03540 0.00396 0.00237 0.00051 AFIX 43 H136 2 0.397368 1.113639 0.633300 11.00000 -1.20000 AFIX 0 C138 1 0.433306 0.900848 0.617445 11.00000 0.03026 0.03474 = 0.04334 0.00118 -0.00145 -0.00289 AFIX 43 H138 2 0.461463 0.866599 0.615202 11.00000 -1.20000 AFIX 0 C144 1 0.374676 0.627857 0.536736 11.00000 0.03034 0.05180 = 0.04367 -0.01448 0.00281 -0.00552 AFIX 43 H144 2 0.385910 0.579009 0.554923 11.00000 -1.20000 AFIX 0 C37 1 0.711278 1.079896 0.300595 11.00000 0.03850 0.04644 = 0.03592 0.00614 0.00777 -0.01149 AFIX 137 H37A 2 0.726677 1.019065 0.300259 11.00000 -1.50000 H37B 2 0.732418 1.126502 0.313008 11.00000 -1.50000 H37C 2 0.702931 1.097661 0.270474 11.00000 -1.50000 AFIX 0 C72 1 0.482995 1.399167 0.601086 11.00000 0.03631 0.03114 = 0.04711 -0.01014 -0.01202 0.00828 AFIX 43 H72 2 0.474201 1.457776 0.589257 11.00000 -1.20000 AFIX 0 C105 1 0.418633 1.017555 0.332898 11.00000 0.07947 0.06402 = 0.04627 -0.01379 -0.00088 0.02551 AFIX 43 H105 2 0.410743 0.958767 0.320702 11.00000 -1.20000 AFIX 0 C50 1 0.782495 0.726210 0.359701 11.00000 0.04000 0.04404 = 0.04448 0.00156 0.01744 0.00588 AFIX 43 H50 2 0.799584 0.755079 0.336689 11.00000 -1.20000 AFIX 0 C132 1 0.343489 0.740267 0.682847 11.00000 0.04666 0.03242 = 0.04528 -0.00629 0.01013 -0.00561 AFIX 43 H132 2 0.363193 0.790646 0.690725 11.00000 -1.20000 AFIX 0 C96 1 0.763429 1.260601 0.672444 11.00000 0.03337 0.06659 = 0.02536 -0.00294 -0.00013 -0.01710 AFIX 43 H96 2 0.760822 1.233545 0.644023 11.00000 -1.20000 AFIX 0 C108 1 0.440670 1.188222 0.366995 11.00000 0.03757 0.07703 = 0.02582 -0.00260 -0.00255 0.00120 AFIX 43 H108 2 0.448968 1.246884 0.379083 11.00000 -1.20000 AFIX 0 C141 1 0.344491 0.766716 0.481846 11.00000 0.01919 0.09327 = 0.04406 0.00814 -0.00222 -0.00189 AFIX 43 H141 2 0.334587 0.815668 0.463040 11.00000 -1.20000 AFIX 0 C107 1 0.474901 1.134674 0.348621 11.00000 0.03856 0.10263 = 0.02970 -0.00301 0.00151 0.01598 AFIX 43 H107 2 0.505921 1.157293 0.347529 11.00000 -1.20000 AFIX 0 C135 1 0.353221 1.003607 0.624099 11.00000 0.04125 0.03608 = 0.05229 0.00206 -0.00159 0.00290 AFIX 43 H135 2 0.325125 1.037982 0.626578 11.00000 -1.20000 AFIX 0 C12 1 0.624270 0.535326 0.440346 11.00000 0.03695 0.02562 = 0.08836 0.00666 0.01840 0.00385 AFIX 137 H12A 2 0.645526 0.561821 0.462222 11.00000 -1.50000 H12B 2 0.631216 0.561631 0.411324 11.00000 -1.50000 H12C 2 0.628209 0.467617 0.439411 11.00000 -1.50000 AFIX 0 C131 1 0.310009 0.709927 0.713239 11.00000 0.05911 0.04182 = 0.04016 -0.00277 0.01557 0.00367 AFIX 43 H131 2 0.307379 0.739678 0.741049 11.00000 -1.20000 AFIX 0 C20 1 0.656029 0.634592 0.322121 11.00000 0.11091 0.05320 = 0.04185 -0.00363 0.01275 0.03585 AFIX 43 H20 2 0.669616 0.652990 0.349259 11.00000 -1.20000 AFIX 0 C94 1 0.811262 1.321171 0.730794 11.00000 0.04833 0.06603 = 0.04892 0.00591 -0.02078 -0.02709 AFIX 43 H94 2 0.840954 1.336399 0.742456 11.00000 -1.20000 AFIX 0 C123 1 0.314203 1.483937 0.382060 11.00000 0.05271 0.03793 = 0.08606 0.00254 -0.02702 -0.00795 AFIX 43 H123 2 0.294493 1.524566 0.398194 11.00000 -1.20000 AFIX 0 C152 1 0.808603 1.163609 0.229412 11.00000 0.05656 0.07996 = 0.05218 0.00287 0.00693 -0.01083 AFIX 137 H15A 2 0.840693 1.180247 0.236894 11.00000 -1.50000 H15B 2 0.795402 1.125119 0.252924 11.00000 -1.50000 H15C 2 0.790045 1.220381 0.226121 11.00000 -1.50000 AFIX 0 C95 1 0.807790 1.283336 0.689154 11.00000 0.03519 0.10386 = 0.04958 0.01404 -0.00800 -0.02353 AFIX 43 H95 2 0.834890 1.272751 0.671988 11.00000 -1.20000 AFIX 0 C125 1 0.362970 1.453376 0.321208 11.00000 0.08821 0.07642 = 0.05331 0.03188 -0.01681 -0.04723 AFIX 43 H125 2 0.377508 1.473789 0.294844 11.00000 -1.20000 AFIX 0 C142 1 0.346964 0.676119 0.465652 11.00000 0.02903 0.11254 = 0.03550 -0.01667 0.00456 -0.01352 AFIX 43 H142 2 0.338531 0.662578 0.436108 11.00000 -1.20000 AFIX 0 C124 1 0.334247 1.512318 0.343181 11.00000 0.07225 0.03859 = 0.08761 0.00739 -0.02821 -0.01758 AFIX 43 H124 2 0.328047 1.572630 0.331804 11.00000 -1.20000 AFIX 0 B2 3 0.387634 0.739711 0.605912 11.00000 0.02391 0.03322 = 0.03516 -0.00525 0.00030 -0.00598 C143 1 0.361984 0.606423 0.493608 11.00000 0.03606 0.06840 = 0.06021 -0.02238 0.00690 -0.01677 AFIX 43 H143 2 0.363658 0.543990 0.483453 11.00000 -1.20000 AFIX 0 B1 3 0.355369 1.223997 0.395715 11.00000 0.03180 0.02973 = 0.02970 -0.00153 -0.00099 -0.00413 C17 1 0.442088 0.764626 0.360074 11.00000 0.03354 0.14025 = 0.04209 -0.01610 -0.00240 -0.01576 AFIX 43 H17 2 0.419634 0.812518 0.363669 11.00000 -1.20000 AFIX 0 C24 1 0.590924 0.638000 0.272192 11.00000 0.11091 0.05320 = 0.04185 -0.00363 0.01275 0.03585 AFIX 43 H24 2 0.560815 0.660068 0.264669 11.00000 -1.20000 AFIX 0 C15 1 0.460984 0.605818 0.358232 11.00000 0.08940 0.11302 = 0.03550 0.02736 -0.02557 -0.07045 AFIX 43 H15 2 0.451697 0.542549 0.360443 11.00000 -1.20000 AFIX 0 C153 1 0.764272 1.058744 0.176437 11.00000 0.05677 0.08647 = 0.05470 0.00438 0.00580 -0.00174 AFIX 137 H15D 2 0.739221 1.103308 0.170614 11.00000 -1.50000 H15E 2 0.755607 1.018993 0.201328 11.00000 -1.50000 H15F 2 0.769352 1.020122 0.150293 11.00000 -1.50000 AFIX 0 C16 1 0.428359 0.675994 0.363295 11.00000 0.04854 0.15139 = 0.04955 0.01285 -0.01184 -0.05770 AFIX 43 H16 2 0.396708 0.661338 0.368969 11.00000 -1.20000 AFIX 0 C21 1 0.681144 0.578573 0.293811 11.00000 0.11091 0.05320 = 0.04185 -0.00363 0.01275 0.03585 AFIX 43 H21 2 0.711359 0.557586 0.301640 11.00000 -1.20000 AFIX 0 C22 1 0.662084 0.554030 0.254772 11.00000 0.11091 0.05320 = 0.04185 -0.00363 0.01275 0.03585 AFIX 43 H22 2 0.680120 0.519742 0.234200 11.00000 -1.20000 AFIX 0 C23 1 0.614929 0.578953 0.243831 11.00000 0.11091 0.05320 = 0.04185 -0.00363 0.01275 0.03585 AFIX 43 H23 2 0.600580 0.555671 0.217910 11.00000 -1.20000 AFIX 0 C154 1 0.541195 0.366903 0.300535 10.40000 0.11036 C155 1 0.531211 0.289923 0.269803 10.40000 0.11036 AFIX 3 H15G 2 0.525281 0.233083 0.285413 10.40000 -1.50000 H15H 2 0.503991 0.307413 0.253483 10.40000 -1.50000 H15I 2 0.556741 0.280973 0.249893 10.40000 -1.50000 AFIX 0 O4 6 0.509930 0.381595 0.325273 10.40000 0.11036 C156 1 0.585146 0.383475 0.324320 10.40000 0.11036 AFIX 3 H15J 2 0.598346 0.329005 0.337680 10.40000 -1.50000 H15K 2 0.603006 0.400165 0.298820 10.40000 -1.50000 H15L 2 0.585566 0.433915 0.345030 10.40000 -1.50000 AFIX 0 HKLF 4 REM mem054_150k_a.res in Pna2(1) REM wR2 = 0.1509, GooF = S = 1.009, Restrained GooF = 1.009 for all data REM R1 = 0.0592 for 15392 Fo > 4sig(Fo) and 0.0764 for all 18870 data REM 1507 parameters refined using 7 restraints END WGHT 0.0820 0.0000 REM Highest difference peak 0.776, deepest hole -0.436, 1-sigma level 0.078 Q1 1 0.5755 0.3585 0.2775 11.00000 0.05 0.78 Q2 1 0.5549 0.3813 0.3193 11.00000 0.05 0.73 Q3 1 0.6604 1.2461 0.6390 11.00000 0.05 0.68 Q4 1 0.6215 0.8074 0.4207 11.00000 0.05 0.63 Q5 1 0.6393 1.1845 0.6003 11.00000 0.05 0.63 ; _shelx_res_checksum 22391 _shelx_hkl_file ; 0 -1 0 -10.00 0.60 0 -2 0 7418.36 371.66 0 -3 0 -1.90 3.30 0 -4 0 1180.18 62.69 0 -5 0 -0.80 4.00 0 5 0 -1.70 3.20 0 6 0 2043.00 92.09 0 7 0 0.80 4.30 0 8 0 981.30 48.20 0 9 0 -3.20 4.10 0 10 0 106.19 12.30 0 11 0 2.50 5.70 0 12 0 82.59 6.60 0 12 0 78.89 12.60 0 -13 0 -3.60 2.10 0 13 0 -1.70 2.40 0 -14 0 24.50 3.90 0 14 0 18.60 3.50 0 -15 0 -1.90 2.70 0 16 0 -3.50 3.90 -1 0 0 0.50 0.60 1 0 0 -0.60 0.40 -1 1 0 144.09 9.00 -1 2 0 169.88 10.70 1 -2 0 180.18 11.90 1 -3 0 788.82 43.10 1 -4 0 1334.57 74.79 -1 -4 0 1480.85 72.89 -1 5 0 644.94 32.40 1 -5 0 681.83 39.60 1 5 0 679.93 32.50 1 6 0 100.69 9.10 -1 6 0 81.09 8.90 -1 7 0 756.62 39.10 1 7 0 823.32 39.30 -1 8 0 22.40 5.70 1 8 0 22.00 5.80 -1 9 0 77.49 10.30 1 9 0 76.89 9.80 1 10 0 2.30 5.10 -1 10 0 11.20 5.50 1 11 0 29.90 8.40 1 11 0 24.70 4.60 -1 11 0 23.20 7.60 1 -12 0 -1.70 2.10 1 12 0 -1.60 6.20 1 12 0 -2.40 2.50 -1 12 0 7.60 6.40 -1 12 0 -4.50 2.50 1 13 0 30.70 5.20 -1 13 0 34.40 5.20 1 -13 0 33.10 4.80 -1 13 0 40.50 4.50 1 14 0 3.70 4.20 -1 14 0 18.70 3.50 1 -14 0 13.20 3.50 1 14 0 13.70 3.30 -1 -14 0 12.20 3.10 1 -15 0 11.70 3.50 -1 -15 0 6.90 3.10 1 15 0 8.40 3.00 1 16 0 -5.60 3.70 -2 0 0 21.40 3.20 2 -1 0 2.30 2.40 -2 1 0 5.40 2.60 -2 2 0 4.40 3.60 2 -2 0 8.20 3.90 -2 3 0 273.87 17.60 2 -3 0 294.57 19.70 2 -4 0 3.40 5.10 -2 5 0 16.90 4.70 2 -5 0 14.10 6.70 2 5 0 34.30 5.90 -2 6 0 7.40 4.50 2 6 0 7.00 4.20 -2 7 0 175.38 13.50 2 7 0 194.78 13.90 2 8 0 14.00 5.20 -2 8 0 13.80 5.20 2 9 0 11.70 5.50 -2 9 0 16.50 6.20 -2 10 0 -3.00 4.90 2 10 0 2.30 5.30 -2 11 0 10.50 6.60 -2 11 0 9.20 3.20 2 11 0 9.70 3.00 2 11 0 8.90 6.00 2 -11 0 8.20 2.60 2 12 0 17.20 8.10 -2 12 0 17.80 7.50 2 12 0 6.70 2.90 -2 12 0 6.20 3.00 2 -12 0 4.90 2.70 -2 12 0 9.10 2.80 2 -13 0 2.70 2.80 -2 13 0 5.10 2.50 2 13 0 -1.40 2.90 -2 13 0 5.90 2.90 2 13 0 1.00 2.90 2 -14 0 1.30 3.10 2 14 0 -2.40 3.50 2 14 0 0.10 2.60 -2 14 0 2.70 2.20 -2 14 0 -4.50 3.50 2 -15 0 0.80 3.30 -2 -15 0 -3.50 2.50 2 15 0 2.20 2.60 2 15 0 -5.00 3.90 2 16 0 -0.30 4.00 3 0 0 1.50 1.90 -3 0 0 -0.80 2.10 -3 1 0 264.77 17.70 -3 -1 0 299.67 15.00 3 -1 0 257.07 17.20 3 -2 0 224.78 16.40 -3 3 0 283.47 19.10 3 -3 0 260.37 20.00 3 -4 0 1072.89 58.19 -3 4 0 988.90 55.09 -3 5 0 106.89 9.30 3 -5 0 127.69 14.70 3 5 0 119.79 9.40 -3 6 0 -1.50 3.60 3 6 0 1.60 3.80 3 7 0 96.09 10.10 -3 7 0 98.49 10.50 3 8 0 -0.30 4.00 -3 8 0 1.80 4.70 -3 8 0 -5.40 1.70 -3 9 0 137.09 13.00 3 9 0 131.09 12.80 3 -10 0 -0.50 1.80 3 10 0 1.80 4.90 -3 10 0 3.50 5.70 -3 11 0 -1.70 2.30 3 11 0 4.50 5.90 3 -11 0 -2.90 2.10 -3 11 0 5.00 6.30 3 11 0 0.80 2.40 -3 12 0 1.60 2.50 3 12 0 -3.10 6.70 -3 12 0 -5.10 5.80 3 -12 0 -4.10 2.30 -3 12 0 -7.10 2.30 3 12 0 -2.20 2.70 3 13 0 87.59 20.20 3 13 0 103.09 7.30 -3 13 0 93.39 6.60 -3 13 0 68.29 19.90 3 -13 0 94.29 7.70 3 14 0 3.80 2.90 -3 14 0 -2.90 3.40 3 14 0 -2.60 3.40 3 -14 0 0.30 3.20 -3 14 0 5.50 2.40 3 15 0 18.40 3.40 -3 15 0 20.50 3.90 3 -15 0 20.70 4.50 -3 16 0 -2.50 4.30 4 0 0 756.32 40.80 4 -1 0 33.40 7.20 -4 -1 0 45.20 5.10 4 -2 0 38.40 8.80 4 -3 0 60.09 11.40 4 -4 0 1056.89 61.59 4 4 0 1109.89 49.80 4 -5 0 20.70 7.50 4 5 0 21.00 4.70 -4 6 0 361.66 21.00 4 6 0 391.26 21.10 4 -6 0 381.26 28.80 4 7 0 137.29 11.60 -4 7 0 136.29 11.90 4 8 0 49.90 8.30 -4 8 0 58.09 9.10 -4 8 0 52.39 4.40 4 -9 0 341.57 18.10 4 9 0 318.57 21.40 -4 9 0 344.87 22.00 4 -10 0 80.49 6.20 4 10 0 76.89 10.90 -4 10 0 71.19 11.00 4 -11 0 382.96 20.00 4 11 0 347.07 17.70 -4 11 0 377.36 25.20 4 11 0 362.06 24.80 -4 11 0 349.07 17.90 -4 12 0 -3.50 5.70 4 -12 0 -1.80 2.80 4 12 0 13.60 7.50 -4 12 0 7.80 2.80 4 12 0 0.20 2.60 -4 13 0 2.80 3.80 4 13 0 8.00 4.00 4 13 0 14.30 3.50 -4 13 0 25.80 4.50 4 -13 0 20.50 4.00 -4 14 0 43.50 4.80 4 -14 0 42.80 6.50 4 14 0 34.20 5.20 -4 15 0 -0.60 5.10 4 -15 0 23.50 4.40 -4 15 0 25.00 3.80 4 15 0 7.80 4.60 -4 16 0 50.19 4.30 5 0 0 1.10 3.20 5 1 0 738.63 36.00 5 -1 0 610.94 39.00 5 -2 0 569.24 38.10 -5 -2 0 703.03 34.20 5 -3 0 22.20 7.00 5 4 0 12.50 3.80 5 -4 0 8.90 6.40 5 5 0 179.88 11.80 5 -5 0 140.59 16.90 -5 6 0 54.99 8.10 5 -6 0 89.09 14.70 5 6 0 59.89 8.40 -5 7 0 275.37 17.90 5 7 0 288.87 18.00 -5 8 0 94.99 10.70 -5 8 0 98.79 6.50 5 8 0 103.59 10.80 5 -9 0 69.69 5.50 5 9 0 66.99 9.70 -5 9 0 63.09 5.00 -5 9 0 63.49 10.00 5 -10 0 3.70 2.40 5 10 0 13.40 6.20 -5 10 0 4.00 5.40 -5 11 0 -1.70 5.50 5 11 0 5.40 6.80 5 11 0 4.70 3.00 -5 11 0 4.20 2.50 5 -11 0 1.50 2.60 5 -12 0 8.00 3.40 -5 12 0 11.90 7.80 5 12 0 21.60 8.30 5 12 0 7.60 3.50 5 12 0 7.00 3.00 -5 12 0 10.20 2.90 5 13 0 -1.00 2.70 -5 13 0 -4.10 2.70 5 13 0 3.40 2.80 -5 13 0 0.70 2.40 5 -13 0 -2.80 3.10 5 -14 0 56.69 7.20 5 14 0 43.80 5.50 -5 14 0 61.99 5.40 -5 15 0 -7.20 4.60 -5 15 0 10.50 2.40 5 15 0 2.30 3.80 5 -15 0 18.00 4.60 -5 16 0 29.50 3.70 6 0 0 0.60 3.90 6 1 0 59.79 6.60 6 -1 0 43.90 10.30 6 -2 0 3.10 5.80 6 -3 0 122.29 14.70 6 -4 0 5.10 6.30 6 4 0 2.90 3.50 6 -5 0 -4.20 5.50 6 5 0 3.70 3.60 -6 6 0 63.99 8.70 6 6 0 90.49 9.10 6 -6 0 64.49 14.90 6 7 0 77.69 8.70 -6 7 0 52.79 5.20 -6 7 0 55.79 9.00 -6 8 0 25.50 6.90 6 8 0 14.80 5.70 -6 8 0 21.30 3.90 -6 9 0 18.70 6.60 6 9 0 18.80 6.50 6 -9 0 16.70 3.10 -6 9 0 19.30 3.30 6 -10 0 39.50 5.20 -6 10 0 73.99 11.10 6 10 0 66.19 11.30 6 11 0 -1.20 5.00 -6 11 0 1.90 6.70 6 11 0 9.20 3.00 6 -11 0 -2.40 2.60 6 12 0 6.80 6.70 6 -12 0 12.20 3.90 -6 12 0 6.40 7.10 -6 12 0 16.50 3.20 6 12 0 13.10 3.20 6 12 0 19.20 3.70 6 -13 0 5.60 3.90 6 13 0 -0.30 2.60 -6 13 0 -0.80 3.10 6 13 0 6.60 3.10 -6 13 0 1.80 2.50 6 14 0 1.90 3.60 6 -14 0 9.70 4.50 6 14 0 -1.10 2.70 -6 14 0 -4.70 3.90 6 -15 0 6.30 4.60 -6 15 0 4.30 2.30 -6 16 0 0.20 1.90 7 0 0 -2.30 4.20 7 1 0 1051.79 53.69 7 -1 0 964.90 56.99 7 -2 0 30.20 8.40 7 -3 0 7.10 6.60 7 4 0 13.00 4.40 7 -4 0 6.40 7.10 7 5 0 6.10 4.60 7 -5 0 2.50 7.00 7 -6 0 34.60 11.00 7 6 0 24.90 6.00 -7 7 0 2.30 2.60 7 7 0 4.00 4.60 -7 7 0 3.80 4.60 7 8 0 49.90 8.80 -7 8 0 39.70 8.70 -7 8 0 53.69 5.20 7 -9 0 1.50 2.40 7 9 0 -3.80 4.30 -7 9 0 2.00 2.30 -7 9 0 9.80 5.90 -7 10 0 176.48 15.60 -7 10 0 142.29 8.80 7 10 0 175.38 15.30 7 -10 0 147.49 10.10 7 -11 0 201.08 12.90 7 11 0 207.08 11.50 -7 11 0 191.88 18.30 7 11 0 204.18 18.00 -7 11 0 192.48 11.00 7 12 0 29.40 4.80 7 12 0 6.00 7.30 -7 12 0 32.90 5.00 7 -12 0 32.80 6.30 -7 12 0 31.20 9.80 7 12 0 34.60 5.40 -7 13 0 48.40 5.40 7 -13 0 55.69 7.50 7 13 0 49.60 5.80 -7 14 0 96.59 25.70 -7 14 0 137.19 8.50 7 -14 0 166.68 11.20 7 -15 0 5.30 4.80 -7 15 0 6.20 2.40 -7 16 0 71.29 5.10 8 0 0 313.77 21.50 8 1 0 1011.40 53.39 8 -1 0 979.90 56.89 8 -2 0 154.18 16.50 8 -3 0 2815.82 150.28 8 -4 0 5.30 7.60 8 4 0 10.20 4.00 8 5 0 937.31 44.20 8 -5 0 896.51 58.39 8 -6 0 -1.10 7.40 8 6 0 0.10 4.40 -8 7 0 77.29 9.80 8 -7 0 85.49 18.10 8 7 0 86.29 10.40 -8 7 0 96.19 6.80 -8 8 0 26.90 7.10 8 -8 0 19.40 3.40 8 8 0 27.00 6.70 -8 8 0 23.30 4.50 -8 9 0 373.06 24.80 8 9 0 404.16 24.70 8 -9 0 391.56 21.40 -8 9 0 393.36 18.90 -8 10 0 61.89 5.70 8 -10 0 66.69 6.80 -8 10 0 69.79 11.00 8 10 0 62.49 11.40 -8 11 0 204.98 11.40 8 -11 0 220.28 13.60 8 11 0 197.48 11.60 -8 11 0 208.78 19.00 8 11 0 187.38 18.20 8 12 0 5.00 2.60 -8 12 0 9.50 7.40 8 -12 0 6.60 4.00 8 12 0 9.10 7.10 -8 12 0 0.20 3.20 8 12 0 6.50 3.00 -8 12 0 4.70 2.80 -8 13 0 115.29 24.50 8 13 0 134.39 9.00 -8 13 0 141.89 8.80 8 -13 0 172.08 11.90 8 13 0 149.99 8.90 8 -14 0 13.60 5.30 -8 14 0 -6.00 4.10 -8 14 0 0.50 2.40 8 -15 0 49.30 9.50 -8 15 0 34.80 4.70 -8 16 0 20.60 3.60 9 0 0 -2.10 3.70 9 -1 0 110.79 14.10 9 1 0 121.79 10.70 9 -2 0 88.49 13.80 9 -3 0 25.00 8.80 9 4 0 128.59 9.70 9 -4 0 105.09 17.10 9 5 0 40.30 7.10 9 -5 0 22.40 9.70 -9 6 0 31.80 4.80 9 -6 0 26.90 10.10 9 6 0 34.90 6.60 9 7 0 76.89 9.40 -9 7 0 58.59 9.40 9 -7 0 71.99 17.70 -9 7 0 62.49 5.90 -9 8 0 44.80 8.60 9 -8 0 40.80 5.20 -9 8 0 41.30 5.10 9 8 0 42.80 9.00 -9 9 0 67.69 11.10 9 9 0 70.69 11.20 -9 9 0 74.39 6.30 9 -9 0 72.19 6.90 9 10 0 3.30 2.80 9 -10 0 -1.40 3.20 -9 10 0 2.10 2.60 -9 10 0 1.80 6.00 9 10 0 5.80 6.30 -9 11 0 16.80 3.70 9 11 0 10.60 7.40 9 -11 0 15.50 4.50 9 11 0 17.40 3.30 9 11 0 23.20 4.00 -9 11 0 6.40 7.40 9 12 0 13.80 3.10 -9 12 0 26.50 5.00 -9 12 0 23.70 8.90 9 12 0 21.80 4.00 9 -12 0 30.50 7.20 9 12 0 23.70 8.40 -9 13 0 14.80 3.10 9 13 0 16.00 3.50 -9 13 0 6.00 4.40 9 -13 0 37.90 8.10 9 -14 0 6.00 5.60 -9 14 0 0.20 2.40 -9 14 0 -2.60 4.30 -9 15 0 -1.90 4.10 9 -15 0 6.20 5.40 -9 15 0 -1.60 2.20 -9 16 0 22.30 3.80 10 0 0 7.70 4.80 10 -1 0 -3.10 4.40 10 1 0 1.60 3.60 10 -2 0 4.50 6.50 10 -3 0 27.40 9.40 10 -4 0 4.60 7.80 10 5 0 84.19 9.20 10 -5 0 79.99 17.20 10 6 0 0.20 3.90 10 -6 0 0.10 7.90 -10 6 0 -1.90 2.90 10 -7 0 2.90 8.80 -10 7 0 5.60 4.60 -10 7 0 -1.70 2.60 10 7 0 6.90 4.80 10 8 0 -2.20 4.40 10 -8 0 1.00 2.80 -10 8 0 6.70 5.60 -10 8 0 0.60 2.60 10 -9 0 41.00 6.30 -10 9 0 42.40 8.90 -10 9 0 44.80 5.60 10 9 0 54.39 10.30 -10 10 0 2.60 3.00 10 -10 0 1.90 3.70 10 10 0 5.20 2.90 -10 10 0 3.80 6.00 10 10 0 9.60 6.90 -10 10 0 4.80 2.80 10 11 0 35.90 5.60 10 -11 0 41.60 7.30 10 11 0 35.60 4.70 -10 11 0 36.10 9.80 -10 11 0 35.10 5.20 10 11 0 66.29 12.70 10 -12 0 11.70 5.20 10 12 0 2.90 2.60 -10 12 0 4.10 2.70 -10 12 0 3.90 3.50 -10 13 0 4.20 3.90 -10 13 0 7.70 2.80 10 -13 0 16.40 5.80 10 13 0 3.60 2.90 -10 14 0 3.20 2.50 -10 14 0 2.30 4.30 10 -14 0 11.30 6.10 10 -15 0 2.30 4.80 -10 15 0 5.50 4.30 -10 15 0 2.90 2.50 -10 16 0 6.40 2.10 11 0 0 0.10 4.00 11 1 0 5.20 4.00 11 -1 0 9.50 5.70 11 -2 0 0.90 5.70 11 -3 0 92.59 16.20 11 -4 0 40.80 12.00 11 -5 0 340.37 31.00 -11 5 0 304.77 15.70 -11 6 0 11.80 3.60 11 -6 0 10.10 9.30 -11 7 0 20.70 4.10 -11 7 0 18.10 6.30 11 7 0 21.10 6.50 11 -8 0 11.10 3.60 11 8 0 15.50 6.60 -11 8 0 20.80 6.70 -11 8 0 15.30 3.80 11 9 0 23.10 7.60 11 -9 0 31.50 6.00 -11 9 0 14.90 7.10 -11 9 0 20.80 4.10 11 10 0 17.30 8.20 -11 10 0 27.40 8.30 -11 10 0 24.80 4.70 11 -10 0 32.00 7.10 -11 10 0 13.70 3.90 11 -11 0 123.69 11.60 11 11 0 123.79 7.80 -11 11 0 125.39 8.90 -11 11 0 137.79 22.10 -11 11 0 148.89 8.90 -11 11 0 88.59 14.90 11 -12 0 101.99 11.00 -11 12 0 95.19 7.50 -11 12 0 115.69 21.10 11 12 0 93.49 6.90 11 13 0 5.60 2.90 -11 13 0 4.40 2.80 11 -13 0 14.30 6.20 -11 13 0 49.10 15.70 11 -14 0 22.30 6.60 -11 14 0 46.80 15.50 -11 14 0 16.90 3.30 -11 15 0 4.20 2.70 -11 16 0 2.00 2.00 12 0 0 159.98 14.90 12 -1 0 800.82 48.90 12 -2 0 671.63 43.90 12 -3 0 145.69 19.40 12 -4 0 953.90 62.19 12 -5 0 0.90 7.80 -12 5 0 -0.20 2.90 -12 6 0 405.46 19.90 12 -7 0 26.80 4.40 -12 7 0 33.00 7.60 -12 7 0 35.70 5.50 12 -8 0 87.39 8.30 -12 8 0 85.29 11.50 -12 8 0 94.59 7.70 -12 9 0 25.50 8.00 12 -9 0 29.20 7.00 -12 9 0 16.00 4.00 -12 10 0 48.10 6.30 12 -10 0 60.09 8.80 -12 10 0 54.99 5.80 12 11 0 32.00 4.80 -12 11 0 28.70 5.40 12 -11 0 53.29 9.40 -12 11 0 37.40 5.60 -12 12 0 4.80 2.80 12 12 0 2.70 2.50 12 -12 0 11.60 6.30 -12 13 0 33.40 5.50 12 -13 0 51.29 11.40 12 13 0 37.70 4.90 12 -14 0 14.70 5.80 -12 15 0 -0.10 2.40 -12 16 0 18.80 3.50 13 0 0 -0.10 4.30 13 -1 0 5.40 5.30 13 -2 0 70.69 13.50 13 -3 0 31.80 9.90 13 -4 0 13.40 8.90 -13 4 0 9.20 3.30 -13 5 0 26.70 4.60 -13 6 0 3.30 2.90 13 -7 0 69.89 7.80 -13 7 0 103.99 7.70 -13 8 0 2.30 3.30 13 -8 0 4.10 4.00 13 -9 0 142.09 12.00 -13 9 0 169.48 10.50 13 10 0 14.80 3.10 -13 10 0 17.10 3.50 13 -10 0 18.40 5.70 -13 10 0 7.50 3.90 13 -11 0 6.30 6.00 13 11 0 5.90 2.70 -13 11 0 5.70 3.50 -13 12 0 13.10 3.30 13 -12 0 21.80 7.10 13 12 0 13.00 3.00 -13 12 0 8.20 3.70 -13 13 0 3.20 2.70 13 -13 0 7.40 6.50 13 13 0 4.50 2.60 -13 14 0 2.00 2.50 -13 15 0 13.10 2.70 14 0 0 -0.90 4.40 14 -1 0 0.60 4.70 14 -2 0 54.49 13.10 14 -3 0 35.80 10.30 14 -4 0 44.60 12.40 -14 4 0 44.60 5.40 -14 5 0 8.50 3.40 -14 6 0 39.90 5.40 -14 7 0 2.80 3.30 -14 8 0 15.50 4.10 -14 9 0 2.40 3.40 14 -9 0 1.80 5.10 14 10 0 33.20 4.50 14 -10 0 27.10 6.60 -14 10 0 27.80 5.90 -14 10 0 45.70 5.70 14 11 0 -0.40 2.30 14 -11 0 9.40 6.60 -14 11 0 7.80 3.00 -14 11 0 8.50 3.90 -14 12 0 -2.00 2.90 14 12 0 3.10 2.50 -14 12 0 2.90 2.80 -14 13 0 -0.60 2.50 14 13 0 -0.10 2.30 -14 14 0 -1.50 2.40 -14 15 0 2.00 2.20 15 0 0 5.80 5.10 15 -1 0 -1.70 4.50 15 -2 0 218.38 21.80 -15 3 0 111.49 8.00 15 -3 0 130.69 18.40 -15 4 0 101.99 7.70 -15 5 0 -1.70 2.80 -15 6 0 145.69 9.80 -15 7 0 43.80 6.30 -15 8 0 142.89 10.20 -15 9 0 10.20 4.00 -15 9 0 15.80 3.30 -15 10 0 -3.30 3.30 -15 10 0 1.90 2.80 15 10 0 -0.10 2.40 -15 11 0 24.60 4.90 -15 11 0 31.90 5.60 15 11 0 22.90 4.30 15 12 0 10.20 2.90 -15 12 0 11.40 3.60 -15 12 0 16.00 3.50 15 13 0 1.80 2.40 -15 13 0 -0.70 2.50 -15 14 0 3.70 2.90 -15 15 0 16.80 2.70 16 -1 0 12.60 6.80 16 -2 0 1004.60 62.09 -16 4 0 106.69 8.00 -16 5 0 15.40 3.90 -16 6 0 230.38 13.50 -16 7 0 32.90 5.70 -16 8 0 66.99 7.40 -16 9 0 133.99 10.50 -16 9 0 165.08 9.80 16 9 0 147.89 8.40 -16 10 0 115.39 8.40 16 10 0 114.09 7.50 -16 10 0 140.29 9.90 -16 11 0 18.90 3.80 -16 11 0 15.10 4.50 16 11 0 18.80 3.20 -16 12 0 27.80 5.20 16 12 0 34.70 4.60 -16 12 0 30.00 5.30 -16 13 0 68.39 6.10 16 13 0 59.89 5.20 -16 14 0 36.00 5.20 -16 15 0 8.50 2.50 17 -1 0 18.50 7.40 -17 -3 0 14.80 2.90 -17 -3 0 20.60 3.10 -17 4 0 3.70 3.00 -17 -4 0 6.10 1.60 -17 -4 0 4.70 2.00 -17 5 0 3.50 3.40 -17 6 0 -0.20 3.30 -17 7 0 9.20 3.90 -17 8 0 13.70 4.40 17 9 0 36.60 4.50 -17 9 0 44.30 6.80 -17 9 0 39.70 5.70 -17 10 0 1.50 3.50 17 10 0 3.50 2.50 -17 10 0 11.00 3.30 -17 11 0 1.60 3.50 17 11 0 4.60 2.60 -17 11 0 4.70 3.10 -17 12 0 0.80 3.00 -17 12 0 -1.60 2.50 17 12 0 1.60 2.40 -17 13 0 2.60 2.80 17 13 0 -4.10 2.10 -17 14 0 -0.10 2.30 -18 0 0 28.20 3.90 -18 -1 0 14.90 2.50 -18 -2 0 32.30 3.60 -18 -3 0 1.00 1.70 -18 -4 0 5.50 2.20 -18 -4 0 5.10 1.90 -18 4 0 3.90 3.20 -18 -5 0 2.70 2.00 -18 5 0 -1.30 3.20 -18 -5 0 4.60 1.70 -18 6 0 19.20 4.60 -18 7 0 1.30 3.50 -18 8 0 49.60 7.00 18 8 0 55.19 4.80 18 9 0 7.30 2.70 -18 9 0 7.30 4.20 -18 10 0 75.19 7.90 18 10 0 72.99 5.70 -18 10 0 62.89 7.00 -18 11 0 4.00 3.70 18 11 0 5.80 2.60 -18 12 0 50.89 5.70 18 12 0 39.80 4.50 18 13 0 0.00 2.30 -18 13 0 1.10 2.70 -18 14 0 31.70 4.40 -19 0 0 0.70 2.10 -19 1 0 5.20 2.50 -19 -1 0 8.00 2.30 -19 -2 0 8.30 2.20 -19 -3 0 41.10 4.10 -19 -4 0 13.60 2.40 -19 4 0 14.80 4.30 -19 -5 0 41.00 4.00 -19 5 0 23.90 5.00 -19 -5 0 40.70 4.80 -19 6 0 12.30 4.30 -19 -6 0 26.40 4.00 -19 -6 0 25.70 3.20 -19 7 0 9.50 4.40 19 8 0 -3.50 2.10 -19 8 0 -2.80 3.30 19 9 0 0.70 2.30 -19 9 0 2.60 4.10 19 10 0 4.00 2.50 -19 10 0 2.30 3.80 -19 11 0 64.79 7.20 19 11 0 65.19 5.40 -19 11 0 67.59 6.60 -19 12 0 121.79 8.80 19 12 0 133.29 7.50 -19 13 0 3.20 2.60 19 13 0 1.90 2.20 -19 14 0 58.29 5.10 -20 0 0 10.70 2.70 -20 -1 0 210.98 10.60 -20 1 0 191.28 10.70 -20 -2 0 72.19 5.60 -20 -3 0 104.49 6.50 -20 -4 0 20.40 3.70 -20 -5 0 251.67 12.10 -20 6 0 2.30 3.70 -20 -6 0 7.50 2.10 20 6 0 6.60 2.10 -20 -7 0 164.78 8.40 20 7 0 160.58 8.80 -20 7 0 153.58 11.40 20 8 0 227.98 11.30 -20 8 0 231.48 14.40 20 9 0 41.00 4.60 -20 9 0 46.90 7.20 20 10 0 2.30 2.50 -20 10 0 2.30 3.70 20 11 0 123.39 7.50 -20 11 0 138.09 9.60 20 12 0 60.79 4.90 -20 12 0 60.79 6.30 20 13 0 30.20 3.90 -20 13 0 36.40 4.70 -21 0 0 0.00 2.20 -21 -1 0 4.70 2.50 -21 -2 0 39.90 4.70 -21 -3 0 8.00 2.50 -21 -4 0 5.90 2.20 21 4 0 4.50 2.50 -21 5 0 3.80 3.70 -21 -5 0 6.60 2.20 21 5 0 3.50 2.10 -21 -6 0 -1.50 1.60 21 6 0 1.00 2.40 -21 6 0 -1.10 3.40 21 6 0 0.60 1.90 -21 7 0 5.30 4.00 -21 -7 0 5.30 2.10 21 7 0 6.20 2.50 21 7 0 6.20 2.10 21 8 0 -0.60 2.20 -21 -8 0 5.00 1.90 -21 8 0 8.00 4.40 21 9 0 17.50 3.00 -21 9 0 18.80 4.90 -21 10 0 1.20 3.70 21 10 0 2.80 2.30 21 11 0 21.80 3.80 21 12 0 -3.40 1.90 21 13 0 -0.70 2.10 -22 0 0 10.30 2.90 -22 -1 0 86.99 6.70 -22 -2 0 24.70 4.60 22 2 0 30.40 4.50 22 3 0 49.50 3.80 22 -3 0 57.69 5.30 -22 -3 0 66.09 5.60 22 3 0 67.69 5.30 -22 -4 0 8.60 2.70 22 4 0 12.80 2.70 22 -4 0 13.40 3.20 -22 -5 0 16.10 2.90 22 5 0 10.90 2.50 -22 5 0 11.50 4.40 22 5 0 7.80 2.60 22 6 0 40.20 4.50 22 6 0 43.20 4.30 -22 6 0 42.60 6.90 -22 -6 0 46.20 4.60 -22 7 0 47.30 7.30 22 7 0 47.10 4.30 22 7 0 47.50 4.70 -22 -7 0 54.29 4.60 -22 -8 0 62.79 5.00 22 8 0 59.89 5.20 -22 8 0 64.29 8.00 -22 -9 0 7.20 2.30 -22 9 0 8.60 4.40 22 9 0 5.40 2.50 -22 10 0 30.90 6.10 22 10 0 28.40 4.00 22 11 0 5.30 2.30 22 12 0 28.50 3.60 22 13 0 2.80 2.10 23 0 0 0.40 2.10 -23 0 0 2.00 2.50 23 0 0 2.20 2.40 23 1 0 7.90 2.60 -23 -1 0 1.50 2.60 23 1 0 1.50 2.00 23 -1 0 6.30 2.50 23 -1 0 3.20 2.50 23 -2 0 16.80 3.10 -23 -2 0 10.10 3.00 23 2 0 11.10 2.30 23 2 0 13.50 3.00 -23 -3 0 130.99 8.50 23 -3 0 141.19 8.20 23 3 0 124.49 6.60 23 3 0 154.28 8.40 23 -4 0 72.49 6.40 -23 -4 0 84.29 6.40 23 4 0 93.69 6.20 23 5 0 59.29 5.30 23 5 0 71.39 5.30 -23 -5 0 68.69 5.80 -23 6 0 1.30 3.60 23 6 0 -1.90 2.10 23 6 0 0.50 2.00 -23 -6 0 3.10 2.30 -23 -7 0 12.60 2.70 23 7 0 11.30 2.30 23 7 0 7.80 2.50 -23 7 0 11.40 4.60 23 8 0 73.29 5.40 -23 -8 0 74.09 5.60 23 9 0 68.29 5.60 -23 -9 0 90.89 5.90 -23 9 0 101.79 8.80 23 10 0 14.60 2.80 -23 -10 0 16.90 2.70 23 11 0 14.10 2.60 23 12 0 64.99 4.60 24 0 0 5.00 2.60 24 0 0 3.60 2.20 24 -1 0 16.40 3.20 24 -1 0 17.50 3.10 24 1 0 24.90 3.60 24 1 0 24.10 3.50 -24 -1 0 17.20 3.60 24 -2 0 4.00 2.60 24 2 0 1.10 1.80 24 2 0 0.60 2.30 -24 -2 0 -2.10 2.50 24 -3 0 317.27 14.80 24 3 0 287.87 13.30 -24 -3 0 278.17 15.20 24 3 0 372.36 15.90 24 -4 0 56.49 5.60 24 4 0 69.99 5.50 24 4 0 50.19 4.80 -24 -4 0 57.39 5.70 24 -5 0 0.30 2.70 24 5 0 2.50 2.10 -24 -5 0 2.90 2.60 24 5 0 3.30 2.30 24 6 0 17.70 3.00 -24 6 0 21.90 5.40 -24 -6 0 14.70 3.00 24 6 0 18.00 3.60 24 7 0 33.10 3.80 -24 7 0 17.20 5.00 -24 -7 0 38.40 4.70 24 7 0 31.20 3.80 -24 8 0 -0.80 3.70 -24 -8 0 1.70 2.30 24 8 0 3.00 2.10 -24 -9 0 -0.30 2.10 -24 9 0 0.00 3.50 24 9 0 -2.80 1.90 24 10 0 3.60 2.10 -24 -10 0 2.90 2.20 24 11 0 29.80 3.60 24 12 0 14.30 2.80 25 0 0 0.20 2.00 25 0 0 -5.70 2.00 25 -1 0 -1.10 2.20 -25 -1 0 0.70 2.80 25 -1 0 -0.20 2.20 25 1 0 2.30 2.00 25 1 0 0.70 2.30 25 2 0 0.30 1.60 25 -2 0 1.90 2.40 25 2 0 1.10 2.30 -25 -2 0 -1.30 2.70 -25 -3 0 11.20 3.30 25 3 0 17.20 3.00 25 4 0 10.00 2.70 25 -4 0 7.90 3.00 25 4 0 8.20 2.50 -25 -4 0 5.60 3.00 -25 -5 0 0.00 2.60 25 -5 0 1.30 2.60 25 5 0 1.20 2.00 25 5 0 4.00 2.20 -25 6 0 12.30 4.80 25 6 0 7.60 2.30 25 6 0 6.00 2.40 -25 -6 0 13.40 3.10 -25 -7 0 25.40 4.40 25 7 0 20.10 3.30 -25 7 0 24.10 5.30 25 7 0 22.90 3.60 25 8 0 0.00 2.00 -25 8 0 2.20 3.70 25 8 0 -0.20 1.50 -25 -8 0 -1.80 2.20 -25 -9 0 1.60 2.20 25 9 0 1.30 2.10 25 10 0 -2.70 1.80 25 11 0 2.40 1.80 26 0 0 22.80 4.50 26 0 0 27.40 3.80 26 -1 0 29.40 4.00 26 1 0 32.00 3.60 26 1 0 31.20 4.60 26 -1 0 30.10 4.70 -26 -2 0 -0.60 2.90 26 2 0 1.20 1.70 26 -2 0 -0.70 2.20 26 2 0 -0.20 2.20 -26 -3 0 3.40 3.10 26 -3 0 5.90 2.70 26 3 0 1.90 2.30 26 4 0 2.10 2.10 -26 -4 0 5.40 3.00 26 -4 0 1.90 2.40 26 4 0 4.20 2.20 26 5 0 23.90 3.80 -26 -5 0 13.70 3.40 26 5 0 20.90 3.60 26 -5 0 17.70 3.40 26 -6 0 0.50 2.30 26 6 0 1.20 2.00 26 6 0 2.30 1.80 -26 -6 0 -1.90 2.50 26 7 0 6.10 2.20 26 7 0 5.50 1.90 -26 -7 0 10.90 2.90 -26 7 0 8.40 4.30 26 8 0 3.90 2.10 -26 -8 0 -1.90 2.40 26 8 0 -1.30 1.40 26 9 0 8.00 2.30 -26 -9 0 6.10 2.50 26 10 0 8.70 2.10 26 11 0 0.20 1.60 27 0 0 1.10 2.30 27 0 0 -1.00 1.90 27 1 0 20.90 3.40 27 1 0 23.80 3.30 27 -1 0 21.90 3.40 27 -1 0 21.20 3.10 27 -2 0 -1.40 2.10 27 2 0 -2.40 1.40 27 2 0 0.50 2.10 27 3 0 5.30 2.30 -27 -3 0 7.00 3.30 27 3 0 5.60 2.40 27 -3 0 0.30 2.30 27 4 0 -1.10 1.90 -27 -4 0 3.70 3.00 27 -4 0 -0.90 2.20 27 4 0 2.30 2.10 27 -5 0 -1.20 2.30 27 5 0 -0.10 1.80 27 5 0 0.00 2.00 -27 -5 0 -7.70 2.30 27 -6 0 15.20 3.10 27 6 0 13.20 2.50 27 6 0 16.40 3.20 -27 -6 0 16.50 3.30 -27 -7 0 1.50 2.50 27 7 0 0.90 1.90 27 7 0 -1.00 1.50 -27 -8 0 4.30 2.50 27 8 0 3.30 2.10 27 8 0 4.40 1.50 27 9 0 44.60 3.80 27 10 0 13.50 2.70 28 0 0 57.69 5.20 28 0 0 62.49 4.60 28 1 0 18.90 3.10 28 -1 0 22.10 4.00 28 -1 0 26.80 3.80 28 1 0 25.30 4.10 28 2 0 53.29 5.00 28 -2 0 55.99 4.70 28 2 0 53.29 3.60 28 3 0 15.50 2.70 28 -3 0 17.10 2.90 28 3 0 16.00 2.80 28 4 0 1.80 1.90 28 -4 0 2.50 2.30 28 4 0 2.10 2.10 28 -5 0 5.10 2.40 28 5 0 5.90 2.10 28 5 0 6.70 2.20 -28 -5 0 4.70 3.10 28 6 0 6.00 2.00 28 -6 0 11.90 2.70 28 6 0 5.10 2.10 -28 -6 0 6.90 2.90 28 7 0 0.20 1.40 28 7 0 -0.60 1.80 28 -7 0 1.70 2.20 28 8 0 22.60 2.50 28 8 0 19.30 3.00 28 9 0 -1.20 1.70 29 0 0 1.50 2.00 29 0 0 0.50 1.70 29 1 0 8.40 1.90 29 -1 0 5.70 2.30 29 1 0 7.50 2.40 29 -1 0 8.50 2.20 29 -2 0 1.70 2.00 29 2 0 0.70 1.90 29 3 0 3.60 2.10 29 3 0 3.90 2.10 29 -3 0 3.00 2.20 29 4 0 29.40 3.70 29 -4 0 38.00 4.10 29 4 0 28.60 3.50 29 -5 0 0.90 2.10 29 5 0 -1.20 1.80 29 5 0 1.40 1.80 29 -6 0 4.20 2.20 29 6 0 3.60 1.90 29 6 0 5.20 1.80 29 7 0 -0.70 1.70 29 -7 0 -2.30 1.90 29 7 0 1.00 1.30 29 8 0 3.80 1.90 29 9 0 -1.00 1.60 30 0 0 0.90 1.70 30 0 0 0.90 1.90 30 -1 0 14.20 2.60 30 -1 0 16.70 3.10 30 1 0 14.10 2.60 30 1 0 20.00 2.60 30 2 0 0.30 1.80 30 -2 0 3.50 1.90 30 -3 0 34.20 3.70 30 3 0 30.30 3.60 30 -4 0 0.90 2.00 30 4 0 1.70 1.70 30 -5 0 38.00 4.00 30 5 0 30.40 3.40 30 6 0 10.80 1.90 30 -6 0 14.90 2.60 30 7 0 2.10 1.40 30 -7 0 0.50 1.80 31 0 0 0.70 1.70 31 0 0 -2.50 1.40 31 -1 0 -0.40 1.60 31 -1 0 0.70 1.70 31 1 0 -3.60 1.60 31 -2 0 9.20 2.10 31 2 0 7.10 2.10 31 3 0 -2.00 1.60 31 -3 0 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9.40 2.70 21 7 -2 15.20 2.60 -21 -8 2 5.60 2.10 -21 8 -2 3.70 4.00 21 8 2 9.00 2.40 21 8 -2 6.10 2.40 -21 8 2 3.30 4.20 -21 -8 -2 4.00 2.00 -21 9 -2 4.60 4.00 21 9 2 2.20 2.30 21 9 -2 4.70 2.40 -21 9 2 -0.30 3.90 21 10 2 25.20 3.90 -21 10 -2 21.90 4.90 21 10 -2 23.20 4.00 -21 10 2 21.30 4.80 21 11 2 31.50 4.20 21 11 -2 36.60 4.20 21 12 2 3.70 2.10 21 12 -2 4.10 2.30 21 13 2 5.40 2.40 21 13 -2 7.50 2.20 -22 0 2 76.59 6.30 -22 0 -2 89.69 6.60 -22 -1 2 30.90 4.70 -22 -1 -2 38.50 5.10 22 2 2 79.29 6.20 -22 -2 2 54.29 5.70 22 -2 -2 67.59 5.70 22 2 -2 71.49 5.80 -22 -2 -2 75.69 5.90 22 -2 2 64.69 5.70 22 3 2 7.90 1.90 22 3 2 10.00 2.90 -22 -3 2 8.70 2.80 22 -3 -2 16.50 3.30 22 3 -2 10.60 2.70 22 -3 2 9.00 3.00 -22 -3 -2 9.20 2.80 22 3 -2 7.70 2.00 22 4 2 118.99 7.70 -22 -4 2 120.59 7.70 22 -4 -2 108.49 7.70 -22 -4 -2 113.99 7.50 22 4 -2 131.89 7.50 22 -4 2 107.09 7.60 22 5 2 64.89 5.40 -22 -5 2 63.89 5.60 22 5 2 56.89 5.20 -22 5 -2 68.89 7.60 22 5 -2 70.89 5.50 22 5 -2 79.69 5.40 -22 5 2 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102.69 8.30 -15 8 -3 86.99 7.30 -15 8 3 97.09 8.70 -15 9 -3 41.60 5.50 -15 9 -3 27.40 5.10 -15 9 -3 39.00 6.10 -15 9 3 38.80 6.80 -15 9 3 49.20 6.00 -15 10 -3 18.60 3.60 -15 10 -3 17.20 4.30 15 10 3 21.10 3.30 -15 10 -3 17.80 3.90 15 10 -3 20.60 4.10 -15 10 3 29.10 5.60 -15 10 3 19.10 5.00 -15 11 -3 32.10 5.70 15 11 3 29.60 4.50 -15 11 -3 37.20 5.80 -15 11 -3 27.60 5.60 -15 11 3 39.00 6.10 -15 11 3 26.40 4.20 15 11 -3 29.00 4.50 -15 12 -3 6.20 3.30 15 12 3 1.50 2.40 -15 12 -3 2.30 2.80 -15 12 3 -2.10 2.70 15 12 -3 4.30 2.60 -15 12 3 2.90 3.10 -15 13 -3 5.40 2.80 15 13 3 1.50 2.60 -15 13 3 4.20 2.90 15 13 -3 2.20 2.40 -15 14 -3 -1.00 2.30 -15 14 3 1.20 2.50 15 14 -3 1.10 2.50 -15 15 -3 -2.10 2.00 -15 15 3 2.00 2.00 16 -1 -3 352.76 29.20 16 -1 3 426.56 30.80 16 -2 -3 107.49 18.30 16 -2 3 108.79 17.10 -16 4 -3 42.50 5.30 -16 4 3 48.90 5.80 -16 5 -3 170.38 10.50 -16 5 3 158.68 10.60 -16 6 -3 24.70 4.80 -16 6 3 32.20 5.40 -16 7 -3 177.98 11.30 -16 7 3 163.48 11.50 -16 8 -3 8.90 3.40 -16 8 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11.00 2.10 -23 -3 -3 9.90 2.90 23 -3 3 13.60 3.30 23 3 -3 9.10 2.60 23 3 -3 10.30 2.00 -23 -4 3 86.79 6.70 23 -4 -3 80.89 6.70 23 4 3 92.29 6.70 -23 -4 -3 83.99 6.60 23 -4 3 90.39 6.80 23 4 -3 108.89 6.50 23 5 3 11.00 2.70 -23 -5 3 9.40 2.80 23 5 -3 14.50 3.00 23 5 -3 10.50 2.50 -23 -5 -3 9.20 2.80 23 6 3 4.00 2.30 -23 -6 3 5.10 2.50 -23 6 -3 4.10 3.90 -23 -6 -3 6.80 2.50 -23 6 3 8.10 4.30 23 6 -3 8.40 2.70 23 6 -3 10.10 2.30 -23 7 -3 76.29 8.10 -23 7 -3 73.09 6.80 23 7 3 51.59 4.70 -23 -7 3 60.29 5.30 23 7 -3 64.69 5.30 23 7 -3 68.79 4.80 -23 7 3 62.49 8.10 -23 -7 -3 65.59 5.30 -23 8 -3 9.90 4.30 -23 -8 3 6.60 2.40 23 8 3 7.30 2.30 23 8 -3 12.90 2.70 -23 8 3 10.60 4.80 -23 -8 -3 7.20 2.40 -23 9 -3 9.00 4.30 -23 -9 3 10.60 2.70 23 9 3 10.60 2.60 -23 -9 -3 13.70 2.60 -23 9 3 11.10 4.70 23 9 -3 11.90 2.70 23 10 3 0.80 2.10 23 10 -3 -0.10 2.20 -23 -10 -3 1.20 2.00 23 11 3 24.60 3.50 23 11 -3 31.40 3.90 23 12 3 2.10 2.00 23 12 -3 3.20 2.00 23 13 -3 10.40 2.30 24 0 3 65.39 5.90 24 0 -3 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6.70 26 2 -3 97.29 5.50 26 -3 -3 53.29 5.10 26 3 3 36.80 4.70 -26 -3 -3 37.90 5.80 26 -3 3 44.30 4.90 26 3 -3 46.80 4.80 26 4 3 91.69 6.70 26 -4 -3 121.19 7.10 -26 -4 -3 107.59 8.00 26 4 -3 117.89 6.90 26 -4 3 102.99 7.00 26 4 -3 99.29 6.60 26 -5 -3 0.50 2.50 26 5 3 0.80 2.00 -26 -5 3 4.10 2.80 26 5 -3 1.20 2.20 26 5 -3 1.30 1.90 26 -5 3 -1.70 2.50 -26 -5 -3 0.40 2.80 -26 -6 3 97.69 7.10 26 6 3 88.49 6.10 26 -6 -3 97.89 6.70 -26 6 -3 123.89 7.80 26 -6 3 91.09 6.80 26 6 -3 98.29 6.00 26 6 -3 95.69 6.20 -26 -6 -3 100.79 7.40 26 7 3 12.90 2.30 -26 7 -3 16.90 5.00 26 7 -3 11.70 2.10 -26 7 3 12.80 4.60 -26 -7 -3 16.40 3.40 26 7 -3 12.50 2.50 26 8 3 28.10 3.30 -26 -8 -3 41.90 4.70 26 8 -3 34.40 3.10 26 8 -3 31.70 3.80 26 9 -3 1.10 2.10 -26 -9 -3 1.60 2.20 26 10 -3 13.60 2.40 26 11 -3 0.40 1.80 27 0 -3 0.30 1.90 27 0 3 -1.30 1.80 27 0 -3 -0.20 2.10 27 0 3 -1.30 2.20 27 1 3 31.90 4.80 27 -1 -3 38.80 4.30 27 -1 -3 31.80 4.70 27 1 3 40.80 3.70 27 1 -3 33.50 4.60 27 -1 3 33.40 4.70 27 -1 3 45.10 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101.99 7.90 7 -4 4 92.29 14.20 7 -5 -4 53.09 12.70 7 5 4 36.90 7.70 -7 5 4 37.50 6.80 7 -5 4 36.10 9.80 7 5 -4 38.90 6.50 7 6 4 96.89 10.70 7 -6 -4 78.59 17.40 7 6 -4 118.79 9.60 7 -6 4 99.59 16.00 -7 6 4 87.99 9.70 7 7 4 3.80 5.20 -7 7 4 17.30 3.40 -7 7 4 26.00 6.10 7 7 -4 15.80 5.10 7 -8 -4 6.50 2.80 7 8 4 9.70 5.70 -7 8 -4 13.20 5.90 -7 8 -4 9.60 2.80 7 8 -4 14.20 5.40 7 -8 4 3.50 2.40 -7 8 4 9.10 5.60 -7 8 4 13.10 3.10 -7 9 -4 14.50 6.30 7 9 4 22.30 7.50 -7 9 -4 19.70 3.90 7 -9 -4 10.00 3.20 -7 9 4 22.20 10.30 7 9 -4 23.00 5.90 7 -9 4 13.80 3.10 -7 9 4 11.20 6.40 -7 9 4 19.70 3.50 7 10 4 58.09 11.40 -7 10 -4 57.79 11.00 -7 10 -4 58.49 5.20 7 -10 -4 55.09 6.30 -7 10 4 56.89 15.10 7 10 -4 58.19 10.90 -7 10 4 44.70 10.20 7 -10 4 60.29 6.10 -7 10 4 53.49 5.10 -7 11 -4 101.59 8.00 7 11 4 90.29 7.70 -7 11 -4 111.89 7.10 7 11 4 96.39 15.40 -7 11 -4 113.09 14.50 7 -11 -4 103.99 9.10 -7 11 4 99.99 21.80 7 11 -4 118.39 8.00 7 11 -4 88.29 13.90 -7 11 4 144.49 15.70 -7 11 4 101.09 7.50 7 -11 4 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8 6 4 59.09 9.50 -8 6 4 69.59 9.00 8 -6 4 46.30 12.10 -8 6 4 67.29 6.00 8 6 -4 72.79 7.60 8 -7 -4 10.10 9.80 8 7 4 3.80 4.80 -8 7 4 13.60 5.50 -8 7 4 12.40 3.40 8 7 -4 16.80 4.60 8 -7 4 8.20 8.00 -8 8 -4 32.80 4.60 8 8 4 25.70 7.80 8 -8 -4 29.40 4.70 8 8 -4 26.70 6.50 -8 8 4 28.30 7.30 -8 8 4 31.30 4.80 8 -8 4 28.20 4.50 8 -9 -4 85.59 7.50 8 9 4 96.59 13.10 -8 9 -4 93.19 6.80 -8 9 -4 66.69 11.40 8 -9 4 87.19 7.30 -8 9 4 108.49 17.70 -8 9 4 92.39 7.00 8 9 -4 80.79 11.10 -8 9 4 86.19 11.80 8 -10 -4 7.60 3.70 -8 10 -4 6.30 2.80 -8 10 -4 12.40 7.20 8 10 4 2.40 6.90 -8 10 -4 4.10 3.10 8 10 -4 7.80 2.80 -8 10 4 4.70 2.70 -8 10 4 2.00 6.40 8 10 -4 0.90 6.00 8 -10 4 8.10 3.20 8 -11 -4 309.47 17.70 -8 11 -4 293.27 14.70 -8 11 -4 279.97 15.40 -8 11 -4 318.77 23.40 8 11 4 284.27 23.30 8 11 4 283.67 14.60 -8 11 4 332.47 23.50 8 11 -4 297.07 15.20 8 11 -4 283.17 21.80 -8 11 4 256.27 39.00 -8 11 4 304.87 15.20 8 11 -4 283.27 14.00 8 -11 4 298.17 17.50 -8 12 -4 5.50 7.00 8 12 4 -1.20 2.90 8 -12 -4 6.60 4.70 -8 12 -4 -1.30 2.20 -8 12 -4 2.60 3.20 -8 12 4 2.10 4.50 8 12 -4 1.20 6.20 8 12 -4 2.90 2.80 8 12 -4 1.50 2.60 8 -12 4 2.00 3.80 -8 12 4 6.70 3.00 -8 13 -4 61.69 5.80 -8 13 -4 62.69 6.60 8 -13 -4 83.69 10.40 -8 13 4 40.40 19.70 8 13 -4 64.59 6.00 -8 13 4 57.19 6.20 8 -13 4 63.49 8.50 8 13 -4 52.89 6.00 8 -14 -4 41.70 8.80 -8 14 -4 28.40 5.00 -8 14 -4 21.60 4.50 -8 14 4 39.70 5.30 8 -14 4 43.00 7.90 8 14 -4 24.30 5.00 -8 15 -4 26.40 4.30 8 -15 -4 38.20 8.70 -8 15 -4 26.50 4.50 8 -15 4 33.90 8.00 -8 15 4 33.00 4.70 -8 16 -4 8.80 2.30 9 0 -4 1.50 4.30 9 -1 -4 -5.30 4.80 9 1 -4 2.90 4.00 9 -1 4 0.10 4.90 9 -2 -4 160.48 18.00 9 -2 4 191.08 18.10 9 -3 -4 245.58 23.50 9 -3 4 242.48 21.60 9 -4 -4 16.50 8.50 9 -4 4 13.00 7.20 9 -5 -4 22.70 10.40 9 -5 4 36.50 10.50 9 -6 -4 260.67 28.20 9 6 -4 276.47 16.90 9 -6 4 298.07 27.80 -9 6 4 289.77 14.60 9 -7 -4 0.20 7.40 9 7 4 15.20 6.50 -9 7 4 7.30 3.30 9 -7 4 -4.10 7.20 9 7 -4 21.20 5.60 9 8 4 68.99 11.20 9 -8 -4 62.49 6.30 -9 8 -4 72.09 6.00 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100.39 18.70 -11 6 4 92.69 7.60 11 -7 -4 55.99 6.70 -11 7 4 60.89 6.20 11 -7 4 53.59 6.10 -11 8 -4 17.60 3.90 11 -8 -4 21.00 4.30 11 -8 4 20.10 4.10 -11 8 4 18.00 4.10 -11 9 -4 43.20 9.60 -11 9 -4 38.10 5.40 11 -9 -4 51.59 7.50 -11 9 4 45.50 6.10 11 -9 4 48.40 6.80 -11 10 -4 14.70 8.30 -11 10 -4 27.10 4.30 -11 10 -4 29.30 4.70 11 -10 -4 50.29 8.50 -11 10 -4 23.80 4.80 11 -10 4 26.50 5.40 11 10 -4 23.30 3.90 -11 10 4 21.60 4.50 -11 11 -4 79.19 6.90 11 11 4 73.49 5.90 -11 11 -4 83.79 13.90 11 -11 -4 98.49 10.70 -11 11 -4 70.19 6.60 -11 11 -4 72.49 6.40 -11 11 4 72.69 6.80 11 11 -4 71.39 6.80 11 11 -4 80.09 6.00 11 -11 4 74.59 9.40 -11 11 4 81.59 7.10 -11 12 -4 11.90 3.60 -11 12 -4 10.50 3.20 11 -12 -4 23.80 6.70 11 12 4 12.20 3.00 11 12 -4 13.40 3.10 -11 12 4 11.20 3.30 11 -12 4 10.00 5.50 -11 13 -4 44.20 5.50 -11 13 -4 54.59 14.80 11 -13 -4 45.10 9.90 -11 13 -4 41.80 5.80 -11 13 4 49.90 6.00 11 -13 4 58.09 10.20 11 13 -4 40.40 5.10 -11 14 -4 41.80 5.00 -11 14 -4 30.70 4.60 11 -14 -4 29.40 6.80 -11 14 -4 53.09 14.50 11 -14 4 35.30 7.10 -11 14 4 75.69 21.50 -11 14 4 38.80 5.10 -11 15 -4 4.40 2.40 -11 15 4 12.50 2.80 -11 16 -4 8.50 2.30 12 0 -4 427.66 29.40 12 -1 -4 96.19 13.90 12 -1 4 94.09 13.90 12 1 -4 81.19 10.20 12 -2 -4 29.80 9.80 12 -2 4 29.40 9.20 12 -3 -4 44.40 12.10 12 -3 4 65.79 13.80 12 -4 -4 67.79 16.20 12 -4 4 66.39 14.60 12 -5 -4 257.37 27.70 12 -5 4 242.28 25.60 -12 5 4 236.98 13.20 -12 6 4 113.09 8.30 -12 7 -4 45.30 5.60 12 -7 -4 43.00 6.60 -12 7 4 63.69 6.40 12 -7 4 37.60 6.00 -12 8 -4 51.09 5.80 12 -8 -4 39.70 7.10 12 -8 4 35.50 6.60 -12 8 4 44.40 6.20 12 -9 -4 21.80 5.30 -12 9 -4 16.20 3.90 -12 9 -4 24.70 7.80 -12 9 -4 29.60 5.10 12 9 -4 21.70 3.70 -12 9 4 17.00 4.50 12 -9 4 25.70 5.10 -12 10 -4 6.30 3.40 -12 10 -4 4.70 2.60 -12 10 -4 9.40 7.70 12 -10 -4 11.70 5.70 -12 10 -4 3.60 3.30 12 10 -4 6.40 3.10 -12 10 4 5.80 3.80 -12 10 4 1.70 2.80 12 -10 4 9.30 4.90 12 10 -4 7.00 2.70 12 -11 -4 22.00 6.40 -12 11 -4 11.90 3.20 -12 11 -4 22.90 8.40 -12 11 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14 -3 4 15.20 3.70 14 -3 4 13.60 8.20 -14 4 4 123.69 8.60 -14 5 4 63.69 6.50 -14 6 4 65.99 6.70 -14 7 -4 2.00 3.10 -14 7 4 2.30 3.50 -14 8 -4 6.80 3.60 -14 8 4 8.10 4.10 -14 9 -4 198.28 17.40 -14 9 -4 185.28 10.60 -14 9 -4 178.78 11.40 -14 9 -4 164.68 10.10 -14 9 4 187.08 12.10 -14 9 4 158.48 10.30 -14 10 -4 36.40 5.50 14 10 4 37.60 4.80 -14 10 -4 47.50 6.20 -14 10 -4 25.40 9.80 -14 10 -4 29.70 5.70 -14 10 4 47.10 6.00 -14 10 4 50.49 6.90 14 10 -4 46.10 4.80 -14 11 -4 26.20 5.10 -14 11 -4 21.20 4.20 -14 11 -4 12.80 4.00 14 11 4 14.10 3.00 -14 11 4 9.20 3.40 -14 11 4 19.00 4.50 14 11 -4 16.20 3.10 -14 12 -4 8.50 3.10 -14 12 -4 6.90 3.20 14 12 4 9.60 2.80 -14 12 -4 10.20 3.30 14 12 -4 12.30 3.10 -14 12 4 17.10 3.90 -14 12 4 9.40 3.30 -14 13 -4 -3.00 2.60 -14 13 -4 2.60 2.50 14 13 4 -1.10 2.80 14 13 -4 -2.70 2.20 -14 13 4 2.40 2.70 -14 14 -4 18.20 3.40 14 14 -4 22.70 4.20 -14 14 4 23.60 4.70 -14 15 -4 3.90 2.20 15 0 -4 -3.10 4.20 15 -1 -4 21.60 7.70 15 -2 -4 122.09 18.20 15 -2 4 156.28 19.00 -15 3 4 23.50 4.20 -15 4 4 1.90 2.90 -15 5 4 8.10 3.50 -15 6 -4 5.90 3.20 -15 6 4 10.10 3.90 -15 7 -4 17.30 4.20 -15 7 4 16.10 4.50 -15 8 -4 46.70 6.10 -15 8 -4 41.90 6.30 -15 8 4 55.89 7.00 -15 9 -4 4.80 3.60 -15 9 -4 9.30 3.40 -15 9 -4 6.20 3.00 15 9 -4 6.30 2.60 -15 9 4 9.70 3.20 -15 9 4 2.70 4.00 15 10 4 1.90 2.40 -15 10 -4 1.00 3.50 -15 10 -4 -0.20 3.00 -15 10 -4 -1.30 2.50 -15 10 4 4.10 2.90 -15 10 4 -7.00 3.30 15 10 -4 -4.40 2.20 15 11 4 12.70 3.00 -15 11 -4 23.70 4.30 -15 11 -4 17.40 4.20 -15 11 -4 22.60 3.90 15 11 -4 22.30 4.30 -15 11 4 15.50 3.70 -15 11 4 14.20 4.30 -15 12 -4 6.50 3.40 -15 12 -4 6.90 2.90 15 12 4 7.30 2.70 -15 12 -4 8.00 3.30 -15 12 4 3.50 3.20 -15 12 4 7.40 3.40 15 12 -4 9.50 2.90 -15 13 -4 1.80 2.50 15 13 4 2.90 2.90 -15 13 4 6.30 2.80 15 13 -4 4.20 2.40 -15 14 -4 7.40 2.60 15 14 -4 10.30 3.00 -15 14 4 6.90 2.80 -15 15 -4 10.30 2.70 16 -1 -4 27.20 8.50 -16 4 4 2.90 3.10 -16 5 4 25.60 4.90 -16 6 -4 65.89 6.70 -16 6 4 71.39 7.30 -16 7 -4 44.60 6.20 -16 7 4 63.49 7.20 -16 8 -4 137.99 9.10 -16 8 -4 137.79 9.90 -16 8 4 120.29 8.60 -16 8 4 133.99 10.50 -16 9 -4 58.09 6.10 16 9 4 35.80 4.80 -16 9 -4 53.29 6.70 -16 9 -4 54.79 6.00 -16 9 4 54.29 7.40 -16 9 4 49.00 6.20 16 9 -4 56.89 4.90 -16 10 -4 14.00 3.80 -16 10 -4 21.40 4.60 -16 10 -4 12.90 3.60 16 10 4 14.60 2.90 -16 10 4 7.70 4.40 16 10 -4 16.20 3.10 -16 10 4 28.10 5.50 -16 11 -4 16.80 4.30 16 11 4 16.70 3.10 -16 11 -4 9.20 3.20 -16 11 -4 11.20 3.60 -16 11 4 11.60 4.10 -16 11 4 12.60 3.60 16 11 -4 10.10 2.80 -16 12 -4 41.60 5.60 -16 12 -4 38.20 5.50 -16 12 -4 45.60 5.40 16 12 4 35.40 4.50 16 12 -4 40.60 4.80 -16 12 4 43.80 5.70 -16 12 4 38.60 6.10 16 13 4 4.60 2.90 -16 13 -4 3.10 2.70 16 13 -4 1.90 2.40 -16 13 4 3.80 2.80 -16 14 -4 10.90 2.80 16 14 -4 13.10 3.00 -16 14 4 13.10 2.90 -16 15 -4 6.00 2.30 -17 -1 4 10.60 2.40 17 -1 -4 7.60 6.50 -17 -1 -4 17.00 3.10 -17 -2 4 12.90 2.50 -17 -2 -4 12.20 2.30 -17 -2 -4 10.90 2.90 -17 -3 4 39.50 3.80 -17 -3 -4 42.60 4.70 -17 -3 -4 32.00 3.70 -17 -4 4 21.80 3.00 -17 -4 -4 23.70 3.90 -17 4 4 14.40 3.90 -17 -4 -4 20.30 2.90 -17 -5 4 113.49 6.10 -17 5 -4 104.29 8.40 -17 -5 -4 107.69 6.20 -17 -5 -4 112.19 7.50 -17 5 4 117.09 8.80 -17 6 -4 7.10 3.70 -17 6 4 10.80 4.10 -17 7 -4 66.79 7.40 -17 7 -4 59.99 6.50 -17 7 4 59.39 7.60 -17 8 -4 48.30 6.80 -17 8 -4 57.39 6.60 17 8 -4 65.49 5.40 -17 8 4 65.49 8.00 -17 9 -4 12.40 4.40 -17 9 -4 14.10 3.60 17 9 4 17.20 3.00 -17 9 -4 12.60 3.50 -17 9 4 12.00 4.70 17 9 -4 11.80 2.90 17 10 4 3.10 2.40 -17 10 -4 0.50 2.80 -17 10 -4 3.70 3.80 -17 10 -4 4.10 3.30 -17 10 4 4.00 3.20 17 10 -4 3.90 2.50 -17 10 4 1.50 4.00 -17 11 -4 21.80 4.90 17 11 4 22.40 4.20 -17 11 -4 21.70 3.90 -17 11 -4 29.10 5.40 -17 11 4 34.00 6.10 -17 11 4 33.70 6.50 17 11 -4 21.90 4.30 17 12 4 34.80 4.40 -17 12 -4 40.40 5.50 -17 12 -4 43.90 5.60 -17 12 4 51.09 6.00 -17 12 4 33.30 5.50 17 12 -4 38.50 4.70 17 13 4 5.00 2.80 -17 13 -4 4.60 2.60 17 13 -4 3.30 2.40 -17 13 4 4.80 2.70 -17 14 -4 7.10 2.60 17 14 -4 9.20 2.80 -17 14 4 3.50 2.40 -18 0 4 262.37 13.00 -18 0 -4 279.27 13.00 -18 1 -4 7.40 2.40 -18 -1 4 7.50 2.30 -18 -1 -4 16.30 3.20 -18 -2 4 299.67 14.50 -18 -2 -4 315.57 14.60 -18 -2 -4 319.07 17.70 -18 -3 4 70.19 5.10 -18 -3 -4 69.29 5.10 -18 -3 -4 74.19 6.40 -18 -4 4 82.99 5.50 -18 4 -4 74.19 7.10 -18 4 4 81.09 7.50 -18 -4 -4 89.09 6.80 -18 -4 -4 91.19 5.60 -18 5 -4 60.79 6.90 -18 -5 4 71.69 4.60 -18 -5 -4 58.19 5.60 -18 -5 -4 66.39 4.60 -18 5 4 55.79 6.90 -18 6 -4 18.80 4.50 -18 6 4 12.80 4.30 -18 7 -4 67.09 6.90 -18 7 -4 76.29 7.70 -18 7 4 72.49 8.20 -18 8 -4 98.79 9.10 18 8 4 101.69 6.80 -18 8 -4 111.29 8.30 -18 8 4 117.09 10.00 18 8 -4 127.89 7.10 18 9 4 4.60 2.40 -18 9 -4 9.60 3.50 -18 9 -4 1.80 3.60 -18 9 4 4.20 4.40 18 9 -4 11.30 2.80 18 10 4 3.90 2.50 -18 10 -4 6.20 3.10 -18 10 -4 10.10 4.10 -18 10 -4 3.00 3.20 18 10 -4 5.60 2.60 -18 10 4 4.30 3.40 -18 10 4 9.10 4.40 -18 11 -4 37.40 5.60 -18 11 -4 30.10 5.70 -18 11 -4 33.40 5.50 18 11 4 31.30 4.40 -18 11 4 39.20 6.10 18 11 -4 36.10 4.60 -18 11 4 40.80 6.30 -18 12 -4 10.20 3.20 18 12 4 11.70 2.70 18 12 -4 9.50 2.70 -18 12 4 6.80 3.10 -18 13 -4 28.40 4.70 18 13 -4 21.00 3.90 -18 13 4 34.60 5.00 -18 14 -4 -1.10 2.40 18 14 -4 2.80 2.40 -19 0 4 -0.30 2.10 -19 0 -4 -3.10 1.90 -19 -1 4 37.30 4.40 -19 1 -4 35.80 4.50 -19 -1 -4 37.20 4.10 -19 -2 4 12.50 2.70 -19 -2 -4 13.00 2.60 -19 -3 4 79.29 5.70 -19 -3 -4 86.89 5.90 -19 -3 -4 82.19 7.00 -19 -4 4 24.40 3.70 -19 -4 -4 23.00 3.80 -19 4 4 13.20 4.10 -19 -4 -4 24.60 4.60 -19 -5 4 49.70 4.30 -19 5 -4 38.00 6.40 -19 -5 -4 50.19 5.30 -19 5 4 43.50 6.70 -19 -5 -4 42.80 4.30 -19 6 -4 36.50 6.50 -19 -6 4 35.80 4.00 -19 6 4 30.90 6.40 19 6 -4 37.00 4.30 -19 -6 -4 43.80 4.00 -19 -6 -4 44.40 4.80 -19 7 -4 4.90 4.00 -19 7 4 9.00 4.30 19 7 -4 12.00 2.90 -19 8 -4 72.89 6.90 -19 8 -4 52.39 7.10 19 8 4 38.70 4.50 -19 8 4 53.09 7.70 19 8 -4 54.29 4.90 -19 9 -4 66.89 6.40 19 9 4 55.49 5.20 -19 9 -4 68.49 7.70 19 9 -4 62.79 5.30 -19 9 4 65.49 8.20 -19 10 -4 27.80 5.30 -19 10 -4 20.90 4.80 19 10 4 18.00 3.10 19 10 -4 24.60 4.20 -19 10 4 23.90 5.30 -19 11 -4 3.00 3.00 19 11 4 2.00 2.30 -19 11 -4 -2.00 3.10 -19 11 -4 0.00 3.00 19 11 -4 2.40 2.40 -19 11 4 3.30 3.70 -19 11 4 2.70 2.90 19 12 4 9.20 2.60 -19 12 -4 7.30 2.90 19 12 -4 8.00 2.60 -19 12 4 11.20 3.10 -19 13 -4 31.90 4.80 -19 13 4 26.60 4.50 19 13 -4 28.50 3.90 -20 0 -4 0.70 2.10 -20 -1 4 92.69 6.20 -20 -1 -4 74.59 5.90 -20 -2 4 80.49 5.80 -20 -2 -4 76.49 5.70 -20 -3 4 103.89 6.70 -20 -3 -4 104.99 6.80 -20 -4 4 0.40 2.10 -20 -4 -4 2.70 2.10 -20 -4 -4 4.10 2.80 -20 -5 4 79.79 5.60 -20 5 -4 69.09 7.90 -20 -5 -4 78.69 7.00 -20 5 4 57.19 7.50 -20 -5 -4 75.99 5.70 20 5 -4 85.39 5.60 -20 -6 4 16.90 2.80 -20 6 -4 17.00 4.60 -20 -6 -4 29.30 3.80 20 6 -4 16.70 2.60 20 6 -4 16.40 3.40 -20 6 4 9.50 4.40 -20 -6 -4 22.10 4.50 -20 7 -4 40.90 6.50 -20 7 -4 53.79 6.40 -20 -7 4 51.79 4.40 20 7 -4 37.60 4.80 -20 -7 -4 42.10 4.30 -20 -7 -4 48.50 5.30 20 7 -4 47.40 4.10 -20 7 4 40.60 7.30 -20 -8 4 10.80 2.40 -20 8 -4 11.10 4.30 -20 8 -4 7.20 3.50 20 8 -4 8.40 2.70 -20 8 4 7.20 4.60 -20 9 -4 44.40 6.80 20 9 4 28.90 4.30 -20 9 -4 37.30 5.70 20 9 -4 40.00 4.60 -20 9 4 43.40 7.40 -20 10 -4 7.50 3.20 -20 10 -4 3.10 3.80 20 10 4 3.40 2.40 -20 10 4 0.70 4.00 20 10 -4 3.20 2.40 -20 11 -4 14.90 4.10 20 11 4 14.50 2.80 20 11 -4 11.60 2.70 -20 11 4 20.00 4.50 20 12 4 12.80 2.60 20 12 -4 16.90 2.90 -20 13 -4 8.20 3.00 20 13 -4 10.80 2.50 -21 0 -4 -0.70 2.20 -21 -1 4 3.90 2.50 -21 -1 -4 1.50 2.30 -21 -2 4 18.30 3.20 -21 -2 -4 18.70 3.10 -21 -3 4 13.70 2.90 -21 -3 -4 11.70 2.70 -21 -4 4 30.00 4.30 21 -4 -4 25.10 4.90 21 -4 4 28.80 4.80 -21 -4 -4 28.40 4.30 21 4 -4 32.00 4.10 -21 -5 4 88.99 6.10 -21 5 -4 67.59 8.00 21 5 -4 92.79 6.00 -21 5 4 80.99 8.50 -21 -5 -4 86.99 7.80 -21 -5 -4 82.39 6.30 -21 -6 4 26.80 4.00 -21 6 -4 22.60 5.10 21 6 -4 22.40 3.60 -21 -6 -4 23.40 4.00 -21 6 4 32.40 6.30 21 6 -4 26.00 4.20 -21 -6 -4 27.30 4.90 -21 -7 4 5.10 2.30 -21 7 -4 0.30 3.70 -21 7 -4 7.30 3.50 21 7 -4 5.90 2.00 -21 -7 -4 4.50 2.70 -21 -7 -4 8.10 2.40 -21 7 4 3.50 4.20 21 7 -4 4.00 2.60 -21 8 -4 1.90 3.70 -21 -8 4 0.30 1.90 -21 8 -4 -2.00 3.20 -21 -8 -4 0.90 1.90 21 8 -4 -1.00 2.20 -21 -8 -4 2.60 2.40 -21 8 4 4.00 4.20 -21 -9 4 15.90 2.70 -21 9 -4 29.40 5.20 -21 9 -4 17.70 4.60 21 9 4 19.20 3.10 21 9 -4 15.70 3.00 -21 9 4 11.20 4.60 -21 -9 -4 27.90 3.80 -21 -9 -4 31.50 4.50 -21 10 -4 16.70 3.70 -21 10 -4 21.40 4.90 21 10 4 23.10 3.80 21 10 -4 14.50 3.00 -21 10 4 11.30 4.20 21 11 4 4.20 2.20 21 11 -4 6.90 2.40 21 12 4 13.70 2.50 21 12 -4 8.40 2.50 21 13 -4 4.10 2.20 -22 0 -4 121.29 8.00 -22 -1 4 1.10 2.50 22 -1 -4 3.20 2.20 22 1 4 3.90 2.30 22 -1 4 3.70 2.50 22 1 -4 1.80 2.50 -22 -1 -4 3.10 2.50 22 1 -4 4.10 2.00 -22 -2 4 90.99 6.80 22 -2 -4 88.99 6.20 22 2 4 89.89 5.60 22 -2 4 82.19 6.40 22 2 -4 109.79 6.80 22 2 -4 92.29 5.40 -22 -2 -4 86.79 6.70 -22 -3 4 61.49 5.40 22 -3 -4 45.80 5.20 22 3 4 46.70 3.90 -22 -3 -4 55.59 5.50 22 3 -4 50.79 3.70 22 -3 4 51.79 5.30 22 3 -4 73.59 5.30 22 -4 -4 6.40 2.90 -22 -4 4 0.70 2.40 -22 -4 -4 7.00 2.60 22 -4 4 6.20 3.00 22 4 -4 5.90 2.30 -22 5 -4 13.90 4.80 -22 -5 4 9.00 2.70 -22 5 4 8.60 4.20 22 5 -4 17.60 3.60 -22 -5 -4 14.00 3.00 22 5 -4 10.80 2.90 -22 -6 4 17.20 3.10 -22 6 -4 18.60 5.00 -22 6 4 17.40 4.90 22 6 -4 14.50 2.60 -22 -6 -4 19.90 4.00 22 6 -4 21.60 4.10 -22 7 -4 26.10 5.40 22 7 4 27.60 4.00 -22 -7 4 32.20 4.30 -22 7 -4 36.20 5.70 -22 7 4 34.60 7.00 -22 -7 -4 33.70 4.20 22 7 -4 31.50 3.60 22 7 -4 30.40 4.40 -22 -8 4 19.60 3.70 -22 8 -4 21.20 5.20 22 8 -4 23.70 3.90 -22 8 4 24.60 5.70 -22 -8 -4 17.60 2.90 -22 9 -4 88.09 8.40 -22 -9 4 75.49 5.70 -22 9 -4 76.49 6.70 -22 9 4 85.39 8.60 -22 -9 -4 74.69 5.50 22 9 -4 86.49 5.80 -22 10 -4 9.40 4.00 22 10 4 7.30 2.40 -22 10 4 4.60 4.00 -22 -10 -4 10.30 2.20 22 10 -4 5.40 2.40 22 11 4 68.09 4.90 22 11 -4 75.29 5.30 22 12 4 10.50 2.60 22 12 -4 16.10 2.70 22 13 -4 26.30 3.20 -23 0 -4 -0.60 2.60 23 0 -4 -0.20 2.20 23 0 -4 1.30 2.10 23 0 4 -0.20 2.20 23 0 4 0.40 2.40 23 1 4 1.00 2.10 23 -1 -4 1.00 2.20 23 1 4 1.70 2.50 23 -1 -4 0.80 2.30 23 1 -4 0.90 2.30 23 -1 4 2.60 2.50 -23 -1 -4 -2.20 2.50 23 1 -4 -2.40 1.70 23 -1 4 -3.30 2.20 23 -2 -4 11.00 2.80 -23 -2 4 7.40 3.00 23 2 4 16.50 3.30 23 2 4 9.40 2.30 23 2 -4 7.20 2.10 23 -2 4 9.90 2.90 -23 -2 -4 8.70 3.00 23 2 -4 8.50 2.70 23 -3 -4 7.00 2.70 -23 -3 4 4.90 2.80 23 3 4 6.60 1.90 23 -3 4 8.50 3.10 23 3 -4 4.20 2.40 23 3 -4 7.00 1.80 -23 -3 -4 8.60 2.80 -23 -4 4 3.90 2.60 23 -4 -4 1.70 2.50 23 -4 4 1.30 2.70 23 4 -4 0.00 2.00 -23 -4 -4 1.40 2.50 23 5 4 18.70 3.30 -23 -5 4 13.20 3.00 23 -5 4 23.20 4.00 23 5 -4 22.50 3.40 23 5 -4 25.20 3.80 -23 -5 -4 18.60 3.20 -23 -6 4 11.40 2.70 23 6 4 11.50 2.80 -23 6 -4 16.60 4.70 -23 6 4 17.00 5.00 -23 -6 -4 11.70 2.80 23 6 -4 15.40 3.00 23 6 -4 18.70 3.60 -23 -7 4 28.60 4.30 -23 7 -4 33.00 6.00 -23 7 -4 37.70 5.60 23 7 4 24.60 3.60 -23 -7 -4 26.00 4.10 -23 7 4 28.00 6.00 23 7 -4 26.10 3.50 23 7 -4 31.40 4.30 -23 8 -4 12.80 3.60 -23 -8 4 23.90 4.20 -23 8 -4 18.80 4.90 23 8 -4 15.60 2.90 -23 -8 -4 20.70 3.80 -23 8 4 27.90 5.60 23 8 -4 18.50 3.10 -23 -9 4 5.10 2.30 -23 9 -4 4.60 2.80 -23 9 -4 5.50 4.00 23 9 -4 3.50 2.30 -23 9 4 5.10 4.30 -23 -9 -4 6.90 2.30 -23 -10 -4 8.10 2.20 23 10 -4 6.80 2.50 23 11 -4 21.20 3.60 23 12 -4 5.70 2.10 23 13 -4 -0.40 1.90 24 0 4 27.10 4.20 24 0 -4 35.40 4.10 24 0 4 29.70 4.90 24 0 -4 35.40 4.80 24 -1 -4 2.50 2.40 24 -1 -4 6.20 2.50 24 1 4 0.50 2.10 24 1 4 4.80 2.80 24 1 -4 4.30 2.50 -24 -1 -4 1.30 2.90 24 1 -4 2.50 1.90 24 -1 4 2.30 2.40 24 -1 4 2.60 2.40 24 2 4 116.99 6.70 24 -2 -4 120.19 7.40 24 2 4 121.69 8.20 24 -2 4 123.99 7.70 24 2 -4 120.99 6.60 24 2 -4 147.89 8.10 -24 -2 -4 114.69 8.40 24 3 4 62.49 5.60 24 -3 -4 66.09 5.50 24 3 4 53.99 3.80 -24 -3 4 44.00 5.30 24 3 -4 48.40 3.70 24 3 -4 59.19 5.20 24 -3 4 49.00 5.40 -24 -3 -4 48.60 5.80 -24 -4 4 75.69 6.40 24 4 4 77.89 6.30 -24 -4 -4 74.89 6.60 24 4 -4 98.89 6.20 24 -4 4 78.39 6.50 24 -5 -4 9.60 3.10 24 5 4 12.30 2.80 -24 -5 4 11.40 3.00 24 5 -4 18.00 3.50 -24 -5 -4 6.20 2.80 24 -5 4 17.60 3.50 24 5 -4 14.20 2.90 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2 4 81.09 6.40 26 2 -4 81.69 6.20 26 -2 4 80.49 6.00 26 2 -4 81.89 4.90 -26 -2 -4 83.39 7.20 26 -3 -4 56.59 5.10 26 3 4 37.50 4.80 26 -3 4 46.70 5.00 26 3 -4 42.60 4.70 -26 -3 -4 46.50 6.00 26 4 4 37.80 4.50 26 -4 4 38.50 4.90 26 4 -4 39.20 4.50 26 4 -4 49.50 4.50 -26 -4 -4 37.10 5.80 26 5 4 34.10 4.20 26 -5 -4 41.00 4.90 26 5 -4 41.20 4.50 26 5 -4 46.70 4.20 26 -5 4 43.50 5.00 -26 -5 -4 37.30 5.60 26 -6 -4 97.49 6.40 26 6 4 67.19 5.50 -26 6 -4 91.69 7.20 26 6 -4 81.19 5.30 -26 -6 -4 80.79 6.60 26 6 -4 84.59 5.80 26 -6 4 83.69 6.30 -26 7 -4 19.50 3.80 26 7 4 17.60 3.30 -26 7 4 19.30 5.50 26 7 -4 19.40 3.00 26 7 -4 19.60 3.50 -26 -7 -4 17.70 3.30 26 8 4 21.50 3.10 26 8 -4 26.90 2.90 -26 -8 -4 27.80 4.50 26 8 -4 25.00 3.60 26 9 -4 9.20 2.40 26 10 -4 18.00 3.30 26 11 -4 16.60 3.00 27 0 -4 0.10 2.10 27 0 -4 -2.40 1.80 27 0 4 0.20 2.00 27 0 4 -0.20 2.30 27 1 4 5.30 2.00 27 1 4 7.40 2.80 27 -1 -4 6.80 2.40 27 -1 -4 9.40 2.40 27 -1 4 5.80 2.60 27 -1 4 2.70 2.30 27 1 -4 9.90 2.60 27 1 -4 7.50 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3.80 4.20 -6 15 7 -4.90 6.00 6 15 -7 5.00 3.10 -6 16 -7 0.10 1.80 -6 16 -7 3.50 2.50 7 0 -7 0.60 4.40 7 -1 -7 84.19 13.30 7 1 -7 74.59 10.60 7 -2 -7 138.09 17.70 7 2 -7 177.98 13.10 7 -3 -7 2.00 6.50 7 -3 7 -5.70 5.30 7 -4 -7 198.28 21.80 7 -4 7 186.48 20.50 7 -5 -7 15.80 8.60 7 -5 7 24.10 9.20 7 -6 -7 14.30 10.20 -7 6 7 25.60 4.20 7 -6 7 20.10 8.70 -7 7 7 47.30 5.50 7 7 -7 43.10 7.10 7 -8 -7 8.00 3.10 7 8 -7 2.20 4.20 7 -8 7 4.50 2.50 -7 8 7 5.00 2.90 -7 9 -7 4.80 6.10 7 -9 -7 7.90 3.50 7 9 -7 -1.60 4.90 -7 9 7 7.10 2.90 7 -9 7 4.10 2.80 -7 9 7 5.30 3.60 7 -10 -7 13.80 4.50 -7 10 -7 18.10 7.60 -7 10 -7 11.00 3.50 -7 10 -7 12.70 3.20 7 10 -7 12.30 6.20 7 -10 7 11.70 3.40 -7 10 7 25.80 13.70 7 10 -7 11.30 3.10 -7 10 7 11.10 3.00 -7 11 -7 57.19 5.40 7 -11 -7 67.79 9.00 -7 11 -7 65.09 6.70 -7 11 -7 60.49 12.70 -7 11 7 59.39 20.00 7 -11 7 62.39 7.00 7 11 -7 53.79 6.10 7 11 -7 58.59 5.50 -7 11 7 58.99 6.40 -7 12 -7 22.30 9.50 -7 12 -7 26.30 4.50 7 -12 -7 26.90 6.10 -7 12 -7 27.70 4.50 7 12 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0.20 2.10 12 0 -7 17.10 7.30 12 -1 -7 34.40 9.00 12 1 -7 24.90 6.90 12 -2 -7 21.20 8.60 12 -3 -7 15.20 8.80 12 -3 7 13.60 8.20 12 -4 -7 21.30 9.40 -12 4 7 24.50 4.80 12 -4 7 25.50 10.30 -12 5 7 14.00 3.90 -12 6 7 85.99 7.60 12 -7 -7 5.20 4.00 12 -7 7 6.40 3.60 -12 7 7 6.20 3.80 12 -8 -7 1.50 4.20 12 -8 7 3.00 3.80 -12 8 7 5.50 3.90 12 -9 -7 33.40 6.20 -12 9 -7 40.00 5.80 -12 9 -7 40.60 5.70 -12 9 -7 49.70 5.20 -12 9 7 36.00 5.70 12 9 -7 50.79 5.30 12 -9 7 48.20 8.10 -12 9 7 39.10 6.20 -12 10 -7 86.69 13.80 -12 10 -7 68.89 6.80 12 -10 -7 63.89 10.30 -12 10 -7 55.09 6.50 -12 10 -7 69.19 6.10 12 -10 7 68.39 9.30 12 10 -7 67.49 5.50 12 10 -7 65.19 6.40 -12 10 7 65.99 7.20 -12 10 7 65.69 6.80 -12 11 -7 4.20 3.40 12 -11 -7 3.60 6.20 -12 11 -7 1.00 3.00 12 11 7 -1.10 2.30 -12 11 -7 -0.50 2.50 12 11 -7 4.40 3.10 12 -11 7 6.00 5.70 -12 11 7 -0.20 3.30 -12 11 7 3.60 3.30 12 11 -7 4.20 2.50 -12 12 -7 0.90 3.00 12 -12 -7 -3.70 6.20 -12 12 -7 2.40 2.70 12 12 -7 3.80 2.60 -12 12 7 2.30 2.90 12 -12 7 5.80 5.80 -12 13 -7 13.10 3.50 -12 13 -7 5.90 2.70 12 -13 -7 8.60 6.40 -12 13 7 13.30 3.40 12 -13 7 12.00 6.30 12 13 -7 10.00 2.90 -12 14 -7 17.30 3.40 -12 14 -7 17.40 3.10 -12 14 7 52.79 20.40 -12 14 7 26.60 4.50 -12 15 -7 15.60 2.80 -12 15 -7 13.70 2.90 13 0 -7 -6.70 4.20 13 0 7 1.60 2.60 13 1 7 19.50 3.90 13 -1 -7 14.10 7.50 13 -1 7 20.50 4.30 13 2 7 167.38 9.10 13 -2 -7 152.28 19.30 13 -2 7 181.28 10.10 13 -3 -7 64.89 14.70 13 3 7 63.29 4.70 13 -3 7 62.59 6.30 -13 3 7 61.09 6.30 13 -3 7 91.89 16.60 13 4 7 26.30 3.40 -13 4 7 28.70 5.10 13 -4 7 33.90 5.10 -13 5 7 29.80 5.60 -13 6 7 29.60 6.00 -13 7 7 35.90 6.50 -13 8 7 16.20 4.70 -13 9 -7 17.40 4.20 -13 9 -7 23.00 4.00 13 -9 -7 18.10 5.90 -13 9 -7 20.70 3.40 -13 9 7 21.10 3.80 13 -9 7 16.20 5.40 -13 9 7 15.50 4.60 13 -10 -7 9.90 6.40 -13 10 -7 3.40 3.20 -13 10 -7 4.90 2.90 -13 10 -7 0.70 6.90 -13 10 -7 8.10 3.80 13 10 -7 9.40 2.80 -13 10 7 6.90 3.30 13 -10 7 5.10 5.50 -13 10 7 10.80 4.20 13 -11 -7 44.80 10.50 -13 11 -7 25.40 5.00 -13 11 -7 21.60 4.40 13 11 7 26.50 4.50 -13 11 -7 27.70 5.80 13 11 -7 26.00 4.30 13 -11 7 38.90 9.50 -13 11 7 29.60 5.10 -13 11 7 21.60 4.10 13 -12 -7 21.60 7.10 -13 12 -7 22.20 4.30 -13 12 -7 25.80 5.10 13 12 7 21.20 3.80 -13 12 7 31.90 5.60 13 12 -7 16.70 3.30 -13 13 -7 -0.40 2.90 -13 13 -7 -0.60 2.40 -13 13 7 -1.50 2.70 13 13 -7 0.10 2.30 -13 14 -7 7.20 2.80 -13 14 -7 0.80 2.30 13 14 -7 9.30 2.90 -13 15 -7 14.30 2.70 -13 15 -7 16.90 2.70 14 0 -7 14.40 6.80 14 0 7 12.50 3.20 14 1 7 574.74 25.40 14 -1 -7 516.65 39.00 14 -1 7 566.44 25.80 14 2 7 529.45 24.10 14 -2 -7 508.15 39.40 14 -2 7 551.74 25.00 14 3 7 21.30 3.40 14 -3 7 19.30 4.10 -14 3 7 24.00 4.50 14 -4 7 163.28 10.30 -14 4 7 170.38 10.70 -14 5 7 133.89 9.80 -14 6 7 55.49 6.90 -14 7 7 41.10 6.90 -14 8 -7 15.30 3.60 -14 8 -7 14.40 4.00 -14 8 7 9.00 4.40 -14 9 -7 16.10 3.70 -14 9 -7 14.90 4.20 -14 9 -7 13.60 3.20 -14 9 7 17.50 3.70 14 9 -7 19.80 3.20 -14 9 7 6.80 4.40 -14 10 -7 36.00 5.10 -14 10 -7 30.70 5.80 -14 10 -7 34.60 9.80 -14 10 -7 29.30 5.60 14 10 -7 30.80 4.40 -14 10 7 24.00 4.30 -14 10 7 28.40 5.40 -14 11 -7 13.50 3.40 -14 11 -7 8.80 3.70 -14 11 -7 14.60 4.00 14 11 7 18.60 3.20 -14 11 7 14.30 4.30 14 11 -7 15.00 3.10 -14 11 7 13.20 3.60 14 12 7 3.00 3.10 -14 12 -7 4.90 2.90 -14 12 -7 7.00 3.20 -14 12 -7 3.30 3.20 -14 12 7 1.90 2.80 14 12 -7 4.40 2.70 -14 13 -7 7.50 2.90 -14 13 -7 3.90 3.00 -14 13 7 11.80 3.20 14 13 -7 6.90 2.60 -14 14 -7 15.00 2.90 -14 14 -7 11.30 2.90 14 14 -7 17.60 3.20 -14 15 -7 -0.20 1.90 15 0 7 -0.50 2.50 15 1 7 11.50 3.00 15 -1 -7 1.30 6.20 15 -1 7 12.60 3.30 15 2 7 77.79 5.70 15 -2 7 71.69 6.70 15 3 7 48.50 4.40 15 -3 7 52.99 5.80 -15 3 7 42.20 5.80 -15 -4 7 50.49 4.00 -15 4 7 27.60 5.60 -15 -4 -7 34.90 4.10 15 -4 7 36.80 5.50 -15 -4 -7 43.40 3.60 -15 -5 7 3.30 1.80 -15 5 7 3.90 3.60 -15 6 7 60.99 7.20 -15 7 7 11.50 4.60 -15 8 -7 27.80 4.90 -15 8 -7 30.10 5.60 -15 8 -7 41.40 6.00 -15 8 7 45.30 7.20 -15 8 7 37.40 6.10 -15 9 -7 1.50 3.40 -15 9 -7 3.70 2.60 -15 9 -7 3.40 3.20 -15 9 7 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9 -7 4.60 2.30 -25 -9 -7 0.60 2.20 -25 10 -7 20.30 4.10 25 10 -7 19.30 3.50 25 11 -7 5.20 2.10 26 0 7 47.30 5.20 26 0 -7 49.90 4.40 26 0 -7 36.00 4.70 26 0 7 45.40 4.50 26 1 7 73.09 6.10 26 -1 -7 65.39 5.70 26 1 7 72.89 5.10 26 -1 -7 74.69 5.50 26 1 -7 74.79 4.90 26 -1 7 64.89 6.00 26 -1 7 71.19 5.50 26 1 -7 69.99 5.80 26 -2 -7 17.80 3.00 26 2 7 18.30 3.40 26 2 7 20.30 3.00 26 2 -7 17.90 3.00 26 -2 7 20.20 3.40 26 2 -7 22.60 4.10 -26 -2 -7 18.90 4.20 26 3 7 46.90 5.20 26 -3 -7 64.69 5.40 26 3 -7 41.00 4.60 26 -3 7 42.70 5.10 -26 -3 -7 41.00 6.40 26 -4 -7 33.10 4.60 26 4 7 20.70 4.20 26 4 -7 32.50 3.80 26 4 -7 29.50 4.40 26 -4 7 24.90 4.60 -26 -4 -7 29.50 5.40 26 5 7 8.30 2.50 26 5 -7 2.90 2.40 -26 -5 -7 1.10 2.90 26 -5 7 4.60 2.70 26 5 -7 4.30 2.00 26 -6 -7 26.00 4.80 26 6 7 25.30 3.70 -26 6 -7 39.90 5.60 26 6 -7 25.20 3.30 26 6 -7 28.70 4.10 26 -6 7 27.20 4.60 -26 -6 -7 27.60 5.10 -26 7 -7 19.10 3.70 26 7 7 14.70 2.40 26 7 -7 12.40 2.60 26 7 -7 17.20 2.80 -26 -7 -7 13.30 3.10 -26 8 -7 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18.80 5 3 -8 146.69 10.90 5 -4 -8 33.70 11.00 5 4 -8 32.80 5.20 5 -4 8 37.60 9.50 -5 5 -8 73.79 13.10 5 -5 -8 74.89 15.80 -5 5 8 70.59 7.90 5 -5 8 67.89 13.80 5 5 -8 68.49 7.50 5 -6 -8 199.88 23.40 -5 6 8 186.88 10.20 5 6 -8 176.38 12.30 5 -6 8 219.48 21.60 -5 6 8 164.78 13.00 5 7 8 95.89 12.20 -5 7 8 99.69 10.80 5 7 -8 90.49 9.20 -5 7 8 93.49 6.70 5 8 8 4.80 5.90 5 -8 -8 5.60 2.80 -5 8 8 9.60 5.60 5 8 -8 1.80 4.00 5 -8 8 11.30 2.80 -5 8 8 5.10 2.60 -5 8 8 32.10 12.20 5 9 8 66.99 15.70 -5 9 -8 56.09 10.60 5 -9 -8 56.99 6.40 5 9 8 55.99 12.00 -5 9 8 59.79 10.80 5 9 -8 53.49 9.40 -5 9 8 71.29 15.50 -5 9 8 37.50 4.70 5 -9 8 57.39 5.60 5 -10 -8 28.30 6.30 -5 10 -8 22.20 3.90 -5 10 -8 29.70 8.40 5 10 8 33.00 15.70 5 10 8 21.50 9.30 -5 10 8 31.10 16.70 5 -10 8 21.30 4.80 5 10 -8 25.30 7.10 5 10 -8 27.50 4.80 -5 10 8 18.70 8.40 5 -11 -8 29.80 7.20 -5 11 -8 34.30 4.30 -5 11 -8 37.50 5.70 -5 11 -8 26.20 8.90 -5 11 8 38.60 10.80 -5 11 8 17.20 6.70 5 11 -8 35.90 5.20 -5 11 8 27.00 5.60 5 11 -8 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6.70 3.40 7 -12 8 1.80 3.70 -7 12 8 3.80 2.90 7 12 -8 -1.10 2.70 7 12 -8 1.40 2.50 -7 12 8 2.50 5.40 -7 13 -8 2.80 2.40 7 -13 -8 7.60 5.80 -7 13 -8 0.40 3.00 7 -13 8 2.00 4.20 7 13 -8 -0.40 2.80 7 13 -8 -1.60 2.80 -7 13 8 4.30 2.90 -7 13 8 -0.70 6.00 7 -14 -8 29.80 6.30 -7 14 -8 26.80 4.30 -7 14 -8 22.80 4.90 -7 14 8 7.30 7.50 7 -14 8 20.60 5.30 7 14 -8 24.40 4.90 -7 15 -8 1.40 2.90 -7 15 -8 9.90 2.50 -7 15 -8 3.00 2.70 7 -15 -8 4.40 5.20 -7 15 8 1.30 6.00 7 -15 8 5.20 4.50 -7 16 -8 18.80 3.30 -7 16 -8 16.70 2.90 8 0 -8 454.45 31.30 8 -1 -8 14.90 7.20 8 1 -8 12.20 5.70 8 -2 -8 79.59 14.60 8 2 -8 84.39 9.50 8 -3 -8 13.10 7.60 8 -4 -8 162.78 20.60 8 -4 8 194.38 21.30 8 -5 -8 24.30 10.10 -8 5 8 32.30 5.30 8 -5 8 18.10 8.80 8 -6 -8 18.20 11.20 8 -6 8 16.40 8.90 -8 6 8 23.30 4.30 8 -7 -8 67.49 6.80 -8 7 8 82.69 6.90 8 -7 8 72.59 6.30 8 -8 -8 4.30 3.30 8 -8 8 2.60 2.60 -8 8 8 3.20 2.80 8 -9 -8 189.78 12.60 -8 9 8 168.18 10.70 -8 9 8 186.38 27.00 8 -9 8 186.88 11.90 -8 10 -8 16.30 3.80 -8 10 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91.39 18.10 -9 5 8 88.69 7.20 9 -5 8 68.49 16.20 9 -6 -8 8.30 9.30 -9 6 8 4.20 3.30 9 -6 8 13.90 9.00 9 -7 -8 22.90 4.10 -9 7 8 33.20 5.60 9 -7 8 29.10 5.00 9 -8 -8 25.30 6.20 -9 8 8 31.90 5.30 9 -8 8 30.70 5.30 9 -9 -8 56.39 7.70 -9 9 8 53.49 6.00 9 -9 8 55.89 6.70 -9 10 -8 13.70 3.60 -9 10 -8 0.90 6.60 -9 10 -8 8.30 2.80 9 -10 -8 10.10 4.90 -9 10 -8 13.50 3.70 -9 10 8 43.40 17.50 9 10 -8 11.70 3.30 -9 10 8 9.30 3.40 9 -10 8 17.60 4.30 -9 10 8 14.80 3.60 -9 11 -8 7.70 3.30 -9 11 -8 5.30 3.00 9 11 8 -6.10 2.80 9 -11 -8 9.10 5.30 -9 11 -8 11.60 8.20 -9 11 -8 4.10 2.50 9 11 -8 7.10 3.20 -9 11 8 2.90 2.80 -9 11 8 5.90 3.40 9 11 -8 2.10 2.60 9 -11 8 3.70 4.10 -9 11 8 7.50 5.50 -9 12 -8 9.00 2.90 9 -12 -8 15.30 6.50 -9 12 -8 10.00 3.60 -9 12 8 10.40 3.30 9 12 -8 12.70 3.40 -9 12 8 11.20 6.20 9 12 -8 9.90 2.90 9 -12 8 11.80 5.00 9 -13 -8 3.50 6.20 -9 13 -8 3.30 2.50 -9 13 -8 1.50 3.10 9 13 -8 4.80 3.00 -9 13 8 1.60 2.80 9 -13 8 1.30 5.00 9 13 -8 -1.50 2.60 -9 13 8 1.30 6.30 -9 14 -8 5.70 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3.60 -10 12 -8 15.70 3.30 -10 12 -8 17.40 4.00 10 -12 -8 17.40 6.70 10 12 -8 13.90 3.20 10 -12 8 21.40 6.00 -10 12 8 16.60 3.80 10 12 -8 16.00 3.60 -10 12 8 75.69 24.50 -10 13 -8 3.50 3.30 -10 13 -8 1.90 2.40 10 -13 -8 3.40 6.20 -10 13 8 2.90 2.90 10 13 -8 0.10 2.50 10 13 -8 0.50 2.80 10 -13 8 3.10 5.50 -10 13 8 6.70 6.40 -10 14 -8 38.00 4.60 -10 14 -8 34.60 5.10 10 -14 -8 35.00 6.90 -10 14 8 56.29 24.30 10 -14 8 39.00 9.60 -10 15 -8 15.20 3.10 -10 15 -8 16.70 2.80 -10 16 -8 5.80 2.00 11 0 -8 -0.20 5.00 11 -1 -8 38.60 9.90 11 1 -8 19.90 6.40 11 -2 -8 140.99 18.80 11 -3 -8 95.19 17.60 11 -4 -8 9.30 8.60 -11 4 8 12.50 3.60 11 -4 8 14.00 9.00 -11 5 8 113.09 8.70 -11 6 8 17.70 4.30 11 -7 -8 20.00 4.50 11 -7 8 18.70 3.90 -11 7 8 24.80 4.90 11 -8 -8 11.10 4.50 -11 8 8 15.40 4.30 -11 9 -8 125.79 8.70 -11 9 -8 127.29 8.80 -11 9 -8 114.59 8.30 11 -9 -8 125.19 11.00 11 -9 8 123.19 10.30 11 9 -8 126.89 8.30 -11 9 8 161.68 23.30 -11 9 8 115.69 9.20 -11 9 8 125.79 8.80 -11 10 -8 44.30 10.50 -11 10 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4.30 -12 6 8 8.80 4.00 12 -7 -8 17.20 4.60 -12 7 8 11.70 4.30 12 -8 -8 26.70 5.60 12 -8 8 28.00 6.80 -12 8 8 35.40 6.30 -12 9 -8 2.40 2.90 12 -9 -8 7.00 5.30 -12 9 -8 6.80 2.80 -12 9 -8 6.80 3.40 12 -9 8 6.20 4.70 -12 9 8 12.00 3.50 12 9 -8 8.10 2.90 -12 9 8 6.80 3.90 -12 10 -8 5.70 3.50 -12 10 -8 4.60 2.70 -12 10 -8 6.30 3.40 12 -10 -8 7.50 6.00 -12 10 -8 7.20 7.00 12 -10 8 8.40 5.50 12 10 -8 7.80 3.10 -12 10 8 5.00 3.20 -12 10 8 12.30 4.20 12 10 -8 6.00 2.50 12 -11 -8 -1.90 6.00 -12 11 -8 10.60 3.60 -12 11 -8 5.10 2.70 -12 11 -8 2.00 3.10 12 11 -8 0.90 3.00 -12 11 8 3.30 3.40 12 -11 8 7.00 5.80 -12 11 8 2.90 2.90 12 11 -8 7.80 2.60 -12 12 -8 3.90 3.20 -12 12 -8 0.30 2.50 12 -12 -8 5.90 6.50 12 -12 8 0.40 5.80 12 12 -8 7.00 2.70 -12 12 8 2.80 3.10 -12 13 -8 10.90 2.90 12 -13 -8 2.90 6.30 -12 13 -8 6.00 3.30 12 13 -8 12.40 2.80 12 -13 8 6.00 6.30 -12 13 8 11.90 3.20 -12 13 8 57.99 22.10 -12 14 -8 3.50 2.50 -12 14 -8 5.50 2.70 -12 14 8 1.60 5.20 -12 15 -8 -0.90 2.30 -12 15 -8 0.00 2.00 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9 33.70 6.80 -5 16 -9 7.60 1.90 -5 16 -9 2.10 2.30 6 0 -9 27.40 8.30 6 -1 -9 329.47 26.90 6 1 -9 347.97 25.00 6 -2 -9 25.40 9.50 6 2 -9 26.20 6.40 6 -3 -9 13.10 8.10 6 -4 -9 27.70 9.90 6 -5 -9 65.59 15.90 6 -5 9 71.49 14.50 6 -6 -9 119.09 19.80 6 -6 9 124.79 18.20 -6 6 9 142.09 8.60 -6 7 9 23.30 4.50 6 -8 -9 23.40 5.30 -6 8 9 48.70 12.70 6 -8 9 29.10 4.70 -6 8 9 23.90 4.50 6 -9 -9 34.90 6.40 6 9 9 74.89 17.70 -6 9 9 35.50 4.90 6 -9 9 42.60 5.50 -6 9 9 68.49 16.90 6 -10 -9 57.09 7.70 -6 10 -9 51.89 4.80 -6 10 -9 52.89 5.80 -6 10 -9 54.29 5.20 6 10 9 60.59 21.20 -6 10 -9 49.50 10.60 -6 10 9 56.99 19.90 -6 10 9 40.10 5.70 6 10 -9 55.09 5.70 -6 10 9 38.90 4.80 6 -10 9 55.69 6.30 6 -11 -9 104.89 10.40 -6 11 -9 103.89 7.00 6 11 9 82.29 26.20 -6 11 -9 116.49 8.60 -6 11 -9 103.99 14.90 -6 11 9 118.59 8.10 6 -11 9 106.69 9.00 -6 11 9 97.49 26.80 6 11 -9 115.09 8.00 6 11 -9 118.69 7.10 -6 12 -9 37.80 4.70 6 -12 -9 42.80 8.70 -6 12 -9 36.50 6.10 6 12 -9 44.80 5.70 6 -12 9 36.20 6.50 -6 12 9 40.30 5.60 6 12 -9 33.30 4.80 -6 13 -9 6.40 3.30 -6 13 -9 7.00 2.60 6 -13 -9 5.80 5.80 6 -13 9 4.00 4.00 6 13 -9 8.90 3.20 -6 13 9 -1.50 6.50 -6 13 9 8.60 3.10 -6 14 -9 17.70 3.00 -6 14 -9 19.00 3.60 6 -14 -9 13.00 5.90 -6 -14 9 17.10 3.80 -6 14 9 7.50 7.40 6 14 -9 17.30 3.60 6 -14 9 15.30 4.90 -6 15 -9 5.20 2.30 -6 15 -9 6.10 2.80 6 -15 -9 4.20 5.30 6 -15 9 5.10 4.50 6 15 -9 8.70 3.10 -6 15 9 1.10 6.10 -6 16 -9 1.30 2.30 -6 16 -9 4.00 1.90 7 0 -9 -0.90 4.90 7 -1 -9 38.80 9.60 7 1 -9 53.49 10.40 7 -2 -9 -0.20 6.10 7 2 -9 2.70 4.20 7 -3 -9 96.59 17.00 7 -4 -9 92.39 17.10 7 -5 -9 147.19 21.20 -7 5 9 168.98 9.90 7 -5 9 151.28 19.60 7 -6 -9 0.70 7.40 7 -6 9 2.60 7.20 -7 6 9 4.80 3.10 7 -7 -9 13.40 3.50 -7 7 9 18.30 3.80 7 -7 9 16.00 3.20 7 -8 -9 6.80 3.50 7 -8 9 8.90 2.90 -7 8 9 14.10 3.50 7 -9 -9 8.30 4.00 -7 9 9 45.20 15.70 7 -9 9 12.40 3.30 -7 9 9 8.00 3.10 -7 10 -9 22.40 4.10 -7 10 -9 27.80 8.80 -7 10 -9 20.50 4.30 7 -10 -9 31.40 7.30 -7 10 -9 18.60 3.20 -7 10 9 19.50 4.10 -7 10 9 26.80 4.10 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77.49 6.80 8 -7 9 73.19 6.40 8 -8 -9 281.17 16.80 -8 8 9 301.07 15.40 8 -8 9 289.57 16.80 -8 8 9 287.77 37.30 8 -9 -9 -0.20 3.70 -8 9 9 2.10 3.00 -8 9 9 35.70 14.30 8 -9 9 3.50 3.10 -8 10 -9 282.17 14.70 -8 10 -9 267.97 13.60 8 -10 -9 267.07 16.80 -8 10 -9 264.87 14.10 -8 10 -9 263.07 21.60 8 10 -9 279.17 14.10 -8 10 9 239.98 13.90 8 -10 9 271.57 16.40 -8 10 9 259.37 14.40 -8 10 9 262.77 38.30 -8 11 -9 24.80 4.50 -8 11 -9 27.40 4.50 8 -11 -9 21.10 5.80 -8 11 -9 31.40 9.60 -8 11 9 49.40 22.00 -8 11 9 19.00 3.80 8 11 -9 24.10 5.00 8 -11 9 15.40 4.60 8 11 -9 30.80 4.50 -8 12 -9 36.60 4.90 -8 12 -9 38.30 5.90 8 -12 -9 26.80 6.80 -8 12 9 32.40 5.60 8 12 -9 26.30 4.60 8 12 -9 34.70 5.70 8 -12 9 51.59 8.10 -8 12 9 58.59 27.70 8 -13 -9 7.50 6.20 -8 13 -9 6.10 2.60 -8 13 -9 9.70 3.50 -8 13 9 8.30 3.10 8 13 -9 7.50 3.10 8 -13 9 6.90 5.00 8 13 -9 5.90 3.10 -8 13 9 1.50 6.50 -8 14 -9 7.20 3.00 8 -14 -9 2.00 6.00 -8 14 -9 4.10 2.50 8 14 -9 8.40 3.20 -8 14 9 1.80 6.90 8 -14 9 8.30 5.20 -8 15 -9 10.10 2.50 -8 15 -9 10.50 3.00 -8 16 -9 11.00 2.20 9 0 -9 -0.60 5.40 9 -1 -9 38.70 9.90 9 1 -9 44.00 10.10 9 -2 -9 14.70 7.90 9 2 -9 11.00 4.80 9 -3 -9 51.89 12.80 9 -4 -9 48.10 13.40 9 -5 -9 168.88 24.10 -9 5 9 208.38 12.00 9 -5 9 194.38 23.10 -9 6 9 44.90 5.90 9 -7 -9 5.40 3.40 -9 7 9 6.00 3.40 9 -7 9 5.70 3.00 9 -8 -9 30.60 6.60 -9 8 9 50.39 6.00 9 -8 9 44.80 6.00 -9 9 -9 26.50 5.20 9 -9 -9 24.00 5.10 9 -9 9 37.90 6.20 -9 9 9 29.60 5.40 9 9 -9 24.10 4.90 -9 10 -9 35.90 9.80 -9 10 -9 46.90 5.80 -9 10 -9 55.59 6.40 -9 10 -9 51.09 5.40 9 -10 -9 59.69 8.80 -9 10 9 45.30 5.80 -9 10 9 78.19 21.20 -9 10 9 44.40 6.00 9 -10 9 58.59 7.80 9 10 -9 58.89 5.90 -9 11 -9 3.40 3.10 9 -11 -9 2.50 5.60 -9 11 -9 11.90 8.10 -9 11 -9 4.10 2.50 -9 11 -9 4.20 3.20 -9 11 9 3.80 3.00 9 11 -9 5.60 2.60 9 11 -9 4.20 3.10 -9 11 9 8.50 5.70 9 -11 9 5.20 4.20 -9 11 9 1.70 2.90 9 -12 -9 14.60 6.40 -9 12 -9 11.60 2.90 -9 12 -9 13.30 3.80 -9 12 9 13.00 3.70 -9 12 9 49.10 25.90 9 12 -9 13.10 3.50 9 -12 9 12.80 5.30 9 12 -9 17.20 3.10 -9 13 -9 9.80 2.80 -9 13 -9 14.70 3.80 9 -13 -9 7.10 6.30 9 -13 9 14.20 5.80 -9 13 9 7.90 3.20 9 13 -9 13.70 3.50 -9 13 9 5.40 6.60 9 13 -9 13.40 3.10 -9 14 -9 5.00 2.50 9 -14 -9 -3.50 5.60 -9 14 -9 7.50 3.00 9 -14 9 7.40 5.20 -9 14 9 3.20 6.00 -9 15 -9 12.00 2.50 -9 15 -9 15.00 3.10 -9 16 -9 7.00 1.90 10 0 -9 257.97 22.40 10 -1 -9 0.90 6.40 10 1 -9 -2.80 4.20 10 -2 -9 256.47 25.10 10 -3 -9 128.49 19.20 10 -4 -9 73.99 16.90 -10 4 9 57.19 6.30 10 -5 -9 99.19 20.10 10 -5 9 111.79 20.80 -10 5 9 91.39 7.90 -10 6 9 47.00 6.50 10 -8 -9 27.50 5.30 -10 8 9 47.20 6.00 10 -8 9 33.80 6.10 10 -9 -9 3.50 4.70 -10 9 -9 4.00 3.10 -10 9 9 1.20 3.20 10 9 -9 4.90 2.80 10 -9 9 2.30 3.60 -10 10 -9 25.70 5.20 -10 10 -9 27.20 4.80 10 -10 -9 23.80 6.20 -10 10 -9 23.50 8.50 -10 10 -9 31.80 5.70 10 10 -9 28.70 4.20 -10 10 9 23.50 4.60 10 10 -9 25.00 5.10 -10 10 9 26.30 5.20 10 -10 9 40.50 7.30 -10 11 -9 22.80 4.20 -10 11 -9 13.50 8.20 -10 11 -9 19.50 4.00 -10 11 -9 24.90 4.80 10 -11 -9 22.30 6.50 -10 11 9 21.20 4.00 -10 11 9 25.70 5.50 10 -11 9 26.30 5.60 10 11 -9 28.00 4.50 10 11 -9 18.70 3.70 -10 12 -9 11.30 3.70 -10 12 -9 12.30 3.10 10 -12 -9 12.10 6.60 -10 12 9 59.99 26.50 10 12 -9 13.20 3.50 10 12 -9 16.10 3.10 -10 12 9 17.40 3.90 10 -12 9 17.30 6.10 10 -13 -9 17.70 7.00 -10 13 -9 16.10 3.80 -10 13 -9 19.40 3.30 10 13 -9 18.50 3.80 10 13 -9 20.20 3.40 -10 13 9 13.30 3.40 -10 13 9 66.49 27.90 10 -13 9 24.00 6.30 10 -14 -9 12.10 6.20 -10 14 -9 3.40 2.80 -10 14 -9 5.10 2.40 -10 14 9 4.80 5.80 10 -14 9 -0.10 5.40 -10 15 -9 2.40 2.10 -10 15 -9 1.20 2.50 11 0 -9 2.80 5.50 11 -1 -9 101.99 15.70 11 1 -9 79.09 11.40 11 -2 -9 122.09 18.00 11 -3 -9 531.05 39.90 11 3 9 485.95 22.70 11 4 9 49.40 4.20 11 -4 -9 27.30 11.10 -11 4 9 46.70 5.90 -11 5 9 95.09 8.00 -11 6 9 38.10 6.20 11 -7 -9 13.00 4.30 -11 7 9 16.00 4.40 11 -7 9 11.10 3.70 11 -8 -9 11.60 4.70 -11 8 9 13.20 4.20 -11 9 -9 91.59 6.90 11 -9 -9 84.89 10.40 -11 9 -9 87.69 7.50 -11 9 9 96.19 8.20 -11 9 9 84.29 7.30 11 -9 9 102.79 9.20 11 9 -9 98.89 7.10 -11 10 -9 61.59 13.10 -11 10 -9 68.59 6.70 11 -10 -9 54.19 10.10 -11 10 -9 66.79 6.70 -11 10 -9 63.49 5.90 -11 10 9 50.09 6.60 11 10 -9 59.59 5.20 11 -10 9 65.29 9.00 11 10 -9 58.89 6.20 -11 10 9 60.69 6.40 -11 11 -9 7.10 3.50 -11 11 -9 1.70 2.70 11 -11 -9 8.40 6.40 -11 11 -9 -1.90 3.10 -11 11 9 6.40 3.30 11 -11 9 7.40 5.50 11 11 -9 7.80 3.10 11 11 -9 9.10 2.70 -11 11 9 11.90 3.50 11 -12 -9 5.20 6.50 -11 12 -9 -0.20 3.00 -11 12 -9 -1.60 2.50 11 12 -9 2.70 2.40 11 12 -9 0.00 2.80 11 -12 9 6.30 6.00 -11 12 9 -0.90 2.90 -11 13 -9 29.00 5.00 -11 13 -9 32.80 5.70 11 -13 -9 34.30 7.30 11 13 -9 37.70 4.50 -11 13 9 35.00 5.40 -11 13 9 70.29 24.00 11 -13 9 45.90 9.50 -11 14 -9 8.60 2.70 -11 14 -9 12.10 3.10 -11 14 -9 25.10 11.00 11 -14 -9 10.30 5.80 -11 14 9 5.90 6.00 -11 15 -9 5.40 2.20 -11 15 -9 5.20 2.60 12 0 -9 39.30 9.70 12 0 9 41.60 5.20 12 -1 -9 73.09 14.30 12 1 9 86.19 6.20 12 -1 9 94.79 6.80 12 1 -9 71.99 11.90 12 2 9 125.89 7.40 12 -2 -9 98.79 17.20 12 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7.10 -9 11 -10 31.50 9.60 -9 11 -10 21.70 4.10 -9 11 -10 22.00 3.80 9 -11 -10 24.90 6.40 -9 11 -10 24.70 4.90 9 11 -10 23.40 4.40 9 -11 10 34.40 7.40 9 11 -10 24.70 4.10 -9 11 10 24.90 4.50 -9 11 10 68.29 24.90 -9 11 10 27.40 5.50 9 -12 -10 10.10 6.50 -9 12 -10 10.40 2.90 -9 12 -10 8.90 3.60 9 12 -10 10.60 2.70 -9 12 10 6.00 6.20 9 12 -10 8.40 3.20 -9 12 10 12.00 3.60 9 -12 10 12.10 5.20 -9 13 -10 24.50 4.60 9 -13 -10 32.10 7.40 -9 13 -10 34.90 5.60 9 13 -10 36.00 5.30 9 -13 10 38.40 9.50 -9 13 10 62.19 26.40 9 13 -10 31.00 4.90 -9 14 -10 3.50 2.90 9 -14 -10 -5.10 5.80 -9 14 -10 4.70 2.40 -9 14 10 3.20 6.30 9 -14 10 3.90 5.00 -9 15 -10 29.10 4.40 -9 15 -10 30.10 4.10 10 0 -10 41.70 10.20 10 -1 -10 -3.90 5.40 10 1 -10 5.10 5.80 10 -2 -10 484.65 37.50 10 -3 -10 456.65 37.10 10 -4 -10 260.27 27.30 10 4 10 232.78 11.60 -10 4 10 224.78 13.00 -10 5 10 79.59 7.30 -10 6 10 482.65 23.70 10 -7 -10 14.30 4.40 -10 7 10 23.60 4.70 10 -7 10 21.70 5.30 10 -8 -10 81.39 9.10 10 -8 10 104.19 8.70 -10 8 10 106.09 8.50 -10 9 -10 33.30 5.60 10 -9 -10 34.10 8.40 -10 9 -10 39.80 4.80 -10 9 10 20.40 4.90 10 9 -10 30.30 4.90 -10 9 10 36.10 5.40 10 -9 10 40.80 7.00 10 -10 -10 88.49 10.80 -10 10 -10 109.09 7.90 -10 10 -10 102.89 8.00 -10 10 -10 66.79 12.90 -10 10 -10 91.29 7.10 10 10 -10 91.09 7.30 -10 10 10 86.59 7.90 -10 10 10 93.49 7.60 10 -10 10 92.79 9.70 10 10 -10 96.39 6.30 -10 10 10 117.29 25.50 -10 11 -10 5.20 2.80 -10 11 -10 8.40 3.40 -10 11 -10 10.00 3.40 10 -11 -10 6.40 6.00 -10 11 10 8.50 3.40 10 11 -10 5.80 2.70 10 11 -10 7.60 3.20 10 -11 10 8.40 5.20 -10 11 10 8.20 3.40 10 -12 -10 47.00 11.20 -10 12 -10 22.60 4.40 -10 12 -10 32.60 4.90 -10 12 10 35.30 5.80 10 -12 10 54.39 9.90 10 12 -10 28.10 5.10 10 12 -10 34.60 4.60 -10 12 10 72.59 26.60 10 -13 -10 3.30 6.60 -10 13 -10 2.30 3.10 -10 13 -10 7.00 2.60 10 13 -10 9.40 3.40 10 -13 10 3.20 5.60 -10 13 10 5.70 5.80 10 13 -10 3.50 2.70 10 -14 -10 27.90 6.60 -10 14 -10 35.20 5.10 -10 14 -10 39.10 4.50 10 -14 10 34.30 6.40 -10 15 -10 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13.70 2.90 -11 11 10 70.09 24.70 11 -12 -10 3.00 6.60 -11 12 -10 5.70 2.80 -11 12 -10 5.00 3.30 11 12 -10 12.80 2.90 -11 12 10 5.20 3.20 11 12 -10 6.60 3.20 11 -12 10 9.20 6.10 -11 13 -10 11.90 2.90 -11 13 -10 10.10 3.40 11 -13 -10 11.00 6.60 -11 13 10 5.40 5.90 11 13 -10 9.40 2.90 11 -13 10 20.10 6.20 -11 14 -10 0.40 2.20 -11 14 -10 1.50 2.60 -11 14 10 1.30 5.90 -11 15 -10 7.20 2.60 -11 15 -10 7.80 2.20 12 0 -10 11.30 6.70 12 0 10 20.80 4.40 12 1 10 286.07 14.20 12 -1 -10 263.17 25.50 12 -1 10 278.27 14.40 12 -2 -10 17.90 9.30 12 2 10 25.40 4.10 12 -2 10 29.60 5.00 12 3 10 39.40 4.50 12 -3 10 39.90 5.50 -12 3 10 46.20 6.10 12 4 10 23.40 3.60 -12 4 10 29.80 5.80 12 -4 10 27.20 5.00 -12 5 10 129.69 9.90 -12 6 10 42.60 6.70 -12 7 10 72.49 8.00 12 -8 -10 4.10 5.40 -12 8 -10 1.50 2.80 -12 8 10 2.80 3.70 12 8 -10 5.10 2.70 12 -9 -10 29.00 6.80 -12 9 -10 45.70 5.40 -12 9 -10 42.10 5.70 12 9 -10 40.60 5.40 -12 9 10 35.90 5.60 -12 9 10 34.00 6.70 12 -9 10 58.89 9.20 -12 10 -10 8.30 3.00 -12 10 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16.80 7.00 -7 12 -15 18.30 3.20 7 12 -15 15.40 3.30 7 -12 15 12.80 5.60 -7 12 15 10.70 8.60 -7 -12 -15 17.60 4.10 7 12 -15 16.00 3.70 -7 13 -15 31.60 4.40 -7 -13 15 36.10 5.00 -7 13 -15 27.60 5.00 7 -13 -15 22.80 7.00 7 -13 15 40.80 8.60 -7 13 15 13.10 8.70 -7 -13 -15 30.20 6.10 7 13 -15 33.60 5.20 -7 14 -15 1.60 2.10 -7 14 -15 0.00 2.60 7 14 -15 1.60 2.70 -7 14 15 3.30 7.10 -7 15 -15 11.30 2.10 -7 15 -15 11.40 2.50 8 0 15 294.27 15.40 8 0 -15 275.37 27.80 8 1 15 79.59 6.90 -8 1 15 68.39 7.30 8 1 -15 76.19 15.00 8 -1 15 76.39 7.20 8 2 15 279.07 15.10 8 -2 15 288.07 15.70 -8 2 15 297.77 15.90 -8 -2 -15 341.07 33.90 8 3 15 47.60 5.50 -8 3 15 45.90 6.40 8 -3 15 52.99 6.50 8 4 15 294.97 15.00 -8 -4 -15 281.87 16.70 -8 4 15 321.27 16.50 8 5 15 26.40 4.50 -8 5 15 28.20 5.30 -8 -5 -15 30.50 4.90 8 -6 -15 110.09 9.90 8 6 15 123.49 7.60 -8 -6 -15 118.69 8.50 -8 6 15 136.19 9.70 -8 6 15 93.89 25.00 8 -7 -15 10.20 4.70 8 -7 15 13.10 4.10 -8 -7 -15 12.10 3.40 -8 7 15 11.70 4.20 -8 8 -15 139.69 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4.30 3.20 -9 11 -15 -1.80 2.90 9 -11 -15 -2.80 6.30 9 11 -15 1.00 2.90 -9 11 15 1.20 6.50 -9 -11 -15 9.10 3.40 9 11 -15 3.90 1.90 9 -11 15 0.60 5.90 9 -12 -15 20.70 7.40 -9 12 -15 33.10 4.80 -9 12 -15 34.30 5.70 -9 -12 -15 37.50 5.90 9 12 -15 35.00 5.30 9 12 -15 34.80 3.70 -9 -13 15 18.00 4.10 -9 13 -15 9.40 2.70 -9 13 -15 15.70 3.50 -9 13 15 6.10 7.20 -9 -13 -15 14.40 3.40 -9 14 -15 6.50 2.30 -9 14 -15 4.60 2.60 -9 15 -15 0.70 1.80 10 0 15 186.18 11.30 10 1 15 246.88 13.70 10 -1 15 251.07 14.20 10 2 15 21.20 4.00 10 -2 15 9.30 4.00 -10 2 15 17.30 4.60 -10 -2 -15 19.60 4.50 -10 -2 -15 18.50 3.60 10 3 15 135.29 8.80 10 -3 15 137.19 9.80 -10 3 15 129.69 10.00 -10 -3 -15 134.19 9.40 -10 -3 -15 138.89 7.90 10 4 15 2.60 2.80 -10 4 15 7.00 4.10 -10 4 15 6.40 4.40 -10 -4 -15 3.40 2.60 10 5 15 86.29 6.30 -10 5 15 82.19 8.20 -10 5 15 49.50 21.20 -10 -5 -15 87.59 7.00 -10 6 15 55.49 22.70 -10 6 15 100.69 9.00 -10 -6 -15 96.89 7.60 -10 7 -15 19.20 3.70 -10 7 15 12.70 4.60 -10 -7 -15 24.30 5.20 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14 -15 14.50 2.80 -11 14 -15 13.70 2.60 12 0 15 207.48 12.20 12 1 15 186.48 10.90 -12 -1 -15 159.08 9.10 -12 -1 -15 173.68 11.40 12 -1 15 174.18 11.00 12 2 15 73.09 6.70 12 -2 15 78.09 7.50 -12 -2 -15 70.09 5.70 -12 -2 -15 84.89 7.10 -12 2 15 89.99 8.80 12 3 15 154.28 9.90 -12 -3 -15 162.28 10.80 -12 3 15 155.98 11.40 -12 -3 -15 167.28 8.90 12 -3 15 163.88 10.90 12 4 15 112.19 7.90 -12 -4 -15 124.69 7.40 -12 4 15 99.89 9.60 -12 -4 -15 125.39 8.90 12 5 15 41.80 4.70 -12 5 15 48.70 7.20 -12 -5 -15 32.60 5.50 -12 -5 -15 46.70 5.00 -12 6 -15 68.69 6.40 -12 6 15 57.99 8.20 -12 -6 -15 64.79 6.60 -12 7 -15 100.59 7.30 -12 -7 -15 99.79 8.10 -12 7 15 97.39 9.40 12 7 -15 93.59 5.90 -12 7 15 51.79 22.10 -12 8 -15 19.60 3.90 -12 8 -15 22.00 4.70 -12 8 15 14.00 5.10 -12 -8 -15 20.60 4.00 12 8 -15 20.60 3.70 -12 9 -15 -3.50 2.90 -12 9 -15 2.10 2.80 -12 9 15 -5.00 4.70 -12 9 15 2.40 4.20 12 9 -15 0.80 1.90 -12 -9 -15 2.20 3.00 -12 10 -15 3.60 3.30 -12 10 -15 5.90 2.80 -12 10 15 12.30 4.40 -12 -10 -15 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16.00 4.80 5 5 -27 17.00 3.40 -5 5 27 12.00 5.80 5 6 27 15.20 4.30 5 6 27 8.60 3.30 5 6 -27 11.80 3.10 -5 6 27 15.20 5.30 5 7 27 -0.90 2.60 -5 7 27 8.70 4.70 5 7 -27 3.90 2.60 5 8 -27 36.60 4.70 -5 9 -27 12.90 2.70 5 9 -27 11.00 2.70 -5 10 -27 8.20 2.40 5 10 -27 8.40 2.20 5 11 -27 13.10 2.30 6 0 27 94.19 10.80 6 0 27 105.79 9.60 6 1 27 241.58 14.10 6 1 27 229.08 16.00 6 -1 27 248.58 14.30 -6 1 27 251.27 17.20 6 -1 27 223.08 16.00 6 2 27 7.80 4.70 6 2 27 18.60 6.00 -6 2 27 14.80 6.20 6 -2 27 9.20 5.60 6 3 27 72.89 8.80 6 3 27 49.40 7.50 -6 3 27 50.99 9.60 6 4 27 24.00 4.60 6 4 27 37.40 7.20 -6 4 27 30.30 6.90 6 5 27 117.99 8.20 6 5 27 127.99 9.90 -6 5 27 132.59 11.70 6 5 -27 110.49 8.10 6 6 27 2.10 3.40 6 6 27 2.40 3.00 -6 6 27 9.30 5.00 6 6 -27 3.90 2.70 6 7 27 80.59 5.50 6 7 -27 73.79 6.40 -6 7 27 105.09 9.40 6 8 -27 14.40 2.90 -6 9 -27 27.90 4.40 6 9 -27 30.90 4.30 -6 10 -27 10.60 2.50 6 10 -27 8.60 2.30 6 11 -27 25.10 3.10 7 0 27 -1.90 4.10 7 0 27 4.40 5.00 7 1 27 3.60 4.20 7 1 27 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157.78 11.60 0 7 28 0.40 3.10 0 7 28 -3.90 3.60 0 7 -28 -1.00 2.30 0 8 28 190.28 9.30 0 8 -28 183.48 10.20 0 9 -28 -0.40 2.20 0 10 -28 270.27 13.30 -1 0 28 -4.90 5.30 1 0 28 -0.10 5.50 1 1 28 13.00 6.40 -1 1 28 8.10 6.00 1 2 28 29.70 7.30 -1 2 28 17.40 6.80 1 3 28 26.80 6.90 -1 3 28 46.90 9.30 1 4 28 57.99 8.90 -1 4 28 26.40 6.80 1 5 28 18.90 5.60 -1 5 28 9.50 5.40 1 6 28 17.10 4.10 1 6 28 15.30 5.00 -1 6 28 3.60 4.60 1 7 28 7.50 3.40 -1 7 -28 4.20 2.60 1 7 -28 5.20 2.60 -1 7 28 11.50 4.60 -1 8 -28 7.70 2.60 1 8 28 25.80 3.80 1 8 -28 8.20 2.70 -1 8 28 11.70 3.10 -1 9 -28 24.20 4.00 1 9 -28 24.00 4.10 -1 10 -28 2.60 2.10 1 10 -28 1.50 2.20 2 0 28 0.30 4.80 -2 0 28 4.10 5.70 2 0 28 5.90 6.00 2 1 28 4.20 5.70 -2 1 28 1.50 5.60 2 -1 28 -1.50 5.20 2 2 28 17.70 6.40 -2 2 28 12.00 6.20 2 3 28 39.40 7.50 -2 3 28 34.80 7.70 2 4 28 8.20 5.30 -2 4 28 9.80 5.80 2 5 28 15.60 5.30 2 5 28 15.80 4.50 -2 5 28 22.40 6.10 2 6 28 33.40 6.60 2 6 28 31.40 5.60 -2 6 28 28.30 6.10 2 6 -28 18.80 3.50 2 7 28 17.10 3.50 2 7 -28 20.80 4.50 -2 7 28 20.90 5.50 -2 8 -28 3.30 2.50 -2 8 28 1.00 3.00 2 8 -28 -0.70 2.30 -2 9 -28 1.00 2.20 2 9 -28 3.70 2.30 -2 10 -28 4.20 2.10 2 10 -28 0.80 2.00 3 0 28 5.90 5.00 3 0 28 2.20 5.30 3 1 28 10.00 6.10 3 1 28 8.00 5.00 -3 1 28 10.40 6.10 3 -1 28 22.60 6.70 3 2 28 18.80 5.20 3 2 28 13.40 5.90 -3 2 28 23.50 7.10 3 3 28 18.20 6.20 3 3 28 12.90 4.90 -3 3 28 17.70 6.70 3 4 28 5.40 4.10 3 4 28 0.40 4.60 -3 4 28 1.10 5.40 3 5 28 5.30 4.50 3 5 28 2.50 3.70 -3 5 28 -0.20 5.00 3 6 28 14.30 4.50 3 6 28 12.60 3.80 3 6 -28 17.90 3.40 -3 6 28 27.50 5.90 3 7 28 5.60 2.90 3 7 -28 7.00 2.70 -3 8 -28 20.10 4.10 3 8 -28 25.20 4.30 -3 9 -28 0.90 2.10 3 9 -28 2.40 2.10 -3 10 -28 6.40 2.20 3 10 -28 7.80 2.20 4 0 28 7.50 5.70 4 0 28 6.40 5.00 4 1 28 345.87 18.60 4 1 28 362.86 21.50 -4 1 28 379.56 22.00 4 -1 28 356.06 21.30 4 2 28 18.40 6.50 4 2 28 14.90 5.10 -4 2 28 23.20 6.90 4 3 28 77.19 8.60 4 3 28 79.79 10.00 -4 3 28 102.89 11.40 4 4 28 86.79 9.50 4 4 28 74.39 8.10 -4 4 28 96.59 10.80 4 5 28 31.30 6.00 4 5 28 25.20 5.50 -4 5 28 31.00 6.50 4 6 28 44.00 5.50 4 6 28 43.10 6.50 -4 6 28 54.99 8.40 4 6 -28 45.90 5.50 4 7 28 80.69 5.70 4 7 -28 71.39 6.10 4 8 -28 30.00 4.50 -4 9 -28 16.50 2.90 4 9 -28 17.40 3.70 -4 10 -28 24.90 3.80 4 10 -28 27.90 3.70 5 0 28 1.60 4.80 5 0 28 2.80 5.30 5 1 28 18.10 5.30 5 1 28 8.40 5.50 5 -1 28 4.80 5.50 -5 1 28 9.20 6.30 5 2 28 4.20 4.50 5 2 28 3.10 5.00 -5 2 28 1.70 5.40 5 3 28 13.80 4.80 5 3 28 19.00 5.60 -5 3 28 14.70 6.20 5 4 28 44.50 6.80 5 4 28 41.00 7.50 -5 4 28 59.49 9.40 5 5 28 3.60 4.10 5 5 28 3.20 3.30 -5 5 28 1.10 5.00 5 5 -28 1.90 2.60 5 6 28 4.60 3.70 5 6 28 7.50 3.10 5 6 -28 4.40 2.80 -5 6 28 12.20 5.10 5 7 28 6.60 2.70 5 7 -28 2.80 2.50 5 8 -28 38.70 4.70 -5 9 -28 2.30 2.20 5 9 -28 1.10 2.20 -5 10 -28 26.80 3.80 5 10 -28 27.40 3.50 6 0 28 6.20 5.50 6 0 28 13.80 5.00 6 1 28 12.10 4.80 6 1 28 16.90 6.30 6 -1 28 8.10 4.80 6 -1 28 19.80 6.50 -6 1 28 16.60 6.40 6 2 28 5.10 5.20 6 2 28 7.80 4.60 6 -2 28 6.80 5.40 -6 2 28 3.10 5.70 6 3 28 55.69 8.60 6 3 28 61.79 7.50 -6 3 28 54.09 9.80 6 4 28 5.10 4.40 6 4 28 0.70 3.50 -6 4 28 0.30 5.10 6 5 28 17.30 4.70 6 5 28 10.50 3.50 -6 5 28 18.60 6.20 6 5 -28 16.90 3.40 6 6 28 8.70 3.60 6 6 28 11.40 3.30 6 6 -28 11.40 3.10 -6 6 28 15.50 5.40 6 7 -28 6.30 2.50 6 8 -28 7.80 2.50 6 9 -28 1.90 2.10 -6 9 28 2.70 2.40 6 10 -28 15.30 3.20 7 0 28 -5.20 4.70 7 0 28 -0.80 4.10 7 1 28 12.30 4.80 7 1 28 17.40 6.00 7 -1 28 26.30 6.50 7 -1 28 14.00 5.00 7 2 28 6.30 5.30 7 2 28 7.40 4.20 -7 2 28 -3.60 5.40 7 -2 28 -2.70 5.00 7 3 28 3.80 4.60 7 3 28 -2.90 3.50 -7 3 28 9.80 5.80 7 4 28 81.79 8.50 7 4 28 75.29 7.00 -7 4 28 96.49 10.60 7 5 28 16.90 3.70 7 5 28 17.40 4.70 -7 5 28 13.00 5.90 7 5 -28 20.70 3.40 7 6 28 38.90 4.60 7 6 -28 24.60 4.70 -7 6 28 26.10 6.10 7 7 -28 4.20 2.50 7 8 -28 22.00 4.10 7 9 -28 9.80 2.50 7 10 -28 19.70 3.30 8 0 28 50.79 8.00 8 0 28 65.29 9.40 8 1 28 246.88 16.00 8 1 28 238.68 13.70 8 -1 28 241.08 16.10 8 -1 28 215.98 13.80 8 2 28 40.00 8.10 8 2 28 35.70 6.90 -8 2 28 45.20 9.10 8 -2 28 51.29 8.80 8 3 28 216.18 12.40 8 3 28 220.78 14.30 8 4 28 24.90 5.60 8 4 28 21.70 4.30 -8 4 28 29.70 6.60 8 5 28 171.98 9.70 8 5 28 170.68 11.10 -8 5 28 216.78 14.10 8 5 -28 173.38 10.40 8 6 28 5.10 2.60 8 6 -28 0.90 2.30 8 7 -28 99.79 6.90 8 8 -28 7.60 2.50 8 9 -28 49.60 4.70 8 10 -28 21.90 3.20 9 0 28 -2.00 4.60 9 0 28 0.30 3.80 9 1 28 -3.40 4.00 9 1 28 2.20 4.90 9 -1 28 3.00 4.20 9 -1 28 6.80 5.20 9 2 28 57.69 7.30 9 2 28 45.60 7.90 9 -2 28 59.49 7.80 9 -2 28 66.09 9.20 -9 2 28 58.19 9.30 9 3 28 26.90 4.70 9 3 28 20.20 5.30 -9 3 28 23.90 6.40 9 4 28 6.70 4.20 9 4 28 9.00 3.60 9 4 -28 7.50 3.10 -9 4 28 13.90 5.70 9 5 28 29.40 4.70 9 5 28 34.00 5.40 9 5 -28 36.80 4.90 -9 5 28 47.90 8.30 9 6 28 3.60 2.20 9 6 -28 2.00 2.30 9 7 -28 7.50 2.60 9 8 -28 11.20 2.70 9 9 -28 -0.60 2.00 9 10 -28 14.70 3.00 10 0 28 -1.10 4.50 10 0 28 2.10 4.00 10 1 28 17.00 4.70 10 1 28 18.50 5.50 10 -1 28 27.60 5.20 10 -1 28 13.80 5.80 10 2 28 14.50 4.90 10 2 28 11.90 4.20 10 -2 28 7.20 5.10 10 -2 28 9.50 4.40 10 3 28 17.90 3.90 10 3 28 20.90 5.10 -10 3 28 17.50 5.80 10 4 28 3.90 3.70 10 4 28 3.70 3.10 -10 4 28 9.20 5.00 10 4 -28 10.10 2.90 10 5 28 8.70 2.80 -10 5 28 9.70 5.80 10 5 -28 11.90 2.80 10 6 -28 10.40 2.80 10 7 -28 0.60 2.20 10 8 -28 7.30 2.40 10 9 -28 3.60 2.00 11 0 28 -1.60 3.80 11 0 28 -2.00 4.30 11 1 28 1.70 4.50 11 1 28 6.70 3.90 11 -1 28 -0.80 3.80 11 -1 28 3.80 4.60 11 2 28 -1.40 3.90 11 2 28 1.70 3.40 11 -2 28 5.20 4.00 11 -2 28 11.10 5.00 11 3 28 5.40 4.00 11 3 28 11.90 3.60 -11 3 28 3.80 5.00 11 -3 28 12.20 5.00 11 4 28 18.60 3.40 11 4 28 19.80 4.20 11 4 -28 18.90 3.40 -11 4 28 23.50 6.10 11 5 28 13.90 2.70 11 5 -28 13.30 2.90 11 6 -28 6.90 2.60 11 7 -28 -0.10 2.10 11 8 -28 -1.40 2.00 11 9 -28 5.90 2.00 12 0 28 45.20 6.40 12 0 28 41.80 7.50 12 1 28 5.00 3.70 12 1 28 2.20 4.00 12 -1 28 -1.80 3.50 12 -1 28 6.20 4.50 12 2 28 30.60 5.60 12 2 28 40.70 6.40 12 -2 28 41.70 7.40 12 -2 28 47.40 6.60 12 3 28 5.90 3.10 12 3 28 7.40 3.70 12 -3 28 6.60 3.80 -12 3 28 3.80 5.30 12 -3 28 13.10 4.80 12 4 28 41.30 4.60 12 4 -28 39.20 5.00 12 5 28 10.60 2.30 12 5 -28 12.00 2.80 12 6 -28 70.69 5.70 12 7 -28 7.50 2.40 12 8 -28 67.49 5.20 12 9 -28 11.10 2.10 13 0 28 -6.00 3.50 13 0 28 1.10 3.20 13 1 28 17.80 4.70 13 1 28 14.40 3.70 13 -1 28 14.60 4.90 13 -1 28 11.60 3.80 13 2 28 11.60 4.30 13 2 28 17.30 3.60 13 -2 28 16.30 4.00 13 -2 28 16.90 4.90 13 3 28 6.10 2.80 13 -3 28 8.50 3.60 13 4 28 10.10 2.60 13 4 -28 8.70 2.70 13 5 -28 9.50 2.70 13 6 -28 1.30 2.20 13 7 -28 1.70 2.10 13 8 -28 -2.20 1.80 14 0 28 0.10 3.00 14 0 28 0.70 3.70 14 1 28 0.80 2.90 14 1 28 1.60 3.60 14 -1 28 2.20 4.00 14 -1 28 4.50 3.40 14 2 28 6.80 2.90 14 -2 28 1.90 3.10 14 3 28 0.00 2.30 14 -3 28 -1.20 2.80 14 4 28 17.30 2.70 14 4 -28 14.00 2.90 14 5 -28 13.20 2.80 14 6 -28 29.00 4.10 14 7 -28 0.40 2.00 14 8 -28 8.50 2.20 15 0 28 -1.90 2.80 15 1 28 5.20 2.80 15 -1 28 4.60 3.10 15 2 28 -1.60 2.40 15 -2 28 -2.60 2.70 15 3 28 1.90 2.50 15 -3 28 3.50 3.10 15 4 28 18.10 3.10 15 4 -28 15.10 2.90 15 -4 28 28.70 5.00 15 5 -28 2.30 2.20 15 6 -28 -0.60 2.00 15 7 -28 10.60 2.30 15 8 -28 2.20 1.80 16 0 28 60.19 5.80 16 1 28 40.80 4.90 16 -1 28 44.90 5.30 16 2 28 37.60 4.40 16 -2 28 41.40 5.50 16 3 28 10.60 2.40 16 -3 28 12.30 3.40 16 -4 28 35.70 4.90 16 4 -28 24.90 4.30 16 5 -28 1.50 2.10 16 6 -28 35.60 4.10 16 7 -28 0.60 1.80 17 0 28 0.50 2.50 17 1 28 2.10 2.40 17 -1 28 -1.40 2.60 17 2 28 7.10 2.50 17 -2 28 14.20 3.30 17 3 28 3.90 1.90 17 -3 28 2.70 2.90 17 -4 28 2.70 2.90 17 4 -28 5.40 2.40 17 -5 28 26.40 4.50 17 5 -28 27.10 3.90 17 6 -28 4.60 1.90 18 0 28 42.50 4.60 18 1 28 4.40 2.50 18 -1 28 6.80 2.80 18 2 28 11.30 2.30 18 -2 28 16.90 3.40 18 3 28 14.40 2.40 18 -3 28 23.30 4.30 18 -4 28 4.50 2.80 18 4 -28 4.00 2.20 18 5 -28 4.00 2.00 18 -5 28 3.40 2.50 18 6 -28 14.70 3.20 19 0 28 -3.10 2.20 19 1 28 11.00 2.40 19 -1 28 6.80 2.70 19 2 28 15.30 2.20 19 -2 28 15.90 3.00 19 -3 28 -1.70 2.40 19 4 -28 30.90 3.90 19 -4 28 34.40 4.20 20 0 28 8.30 2.30 20 1 28 27.30 3.20 20 -1 28 23.40 3.70 20 2 28 19.80 2.60 20 -2 28 19.60 3.70 20 -3 28 98.79 6.00 20 -4 28 17.10 2.90 21 0 28 1.40 1.80 21 1 28 1.80 1.60 21 -1 28 3.30 2.00 21 -2 28 6.00 2.20 21 -3 28 3.90 2.20 0 0 29 -0.80 5.30 0 1 29 211.68 15.80 0 2 29 3.80 5.50 0 3 29 173.28 13.90 0 4 29 1.30 5.00 0 5 29 26.30 6.20 0 6 29 4.50 4.30 0 6 29 2.30 3.60 0 7 29 19.10 3.70 0 7 -29 11.10 2.90 0 8 -29 0.00 2.30 0 9 -29 19.50 3.90 0 10 -29 2.20 1.90 -1 0 29 0.40 5.40 1 0 29 -2.60 5.60 1 1 29 8.40 6.10 -1 1 29 4.40 6.00 1 2 29 14.80 6.50 -1 2 29 12.20 6.10 1 3 29 61.69 9.90 -1 3 29 57.49 9.70 1 4 29 68.69 9.40 -1 4 29 47.10 8.70 1 5 29 48.40 6.70 1 5 29 51.29 8.00 -1 5 29 41.00 7.20 1 6 29 11.90 3.80 1 6 29 15.60 4.90 -1 6 29 18.10 5.30 1 7 29 8.80 3.20 1 7 -29 9.50 2.80 -1 7 29 11.30 3.60 -1 8 -29 -0.10 2.30 1 8 -29 2.20 2.30 -1 8 29 3.30 2.40 -1 9 -29 5.00 2.30 1 9 -29 9.90 2.50 -1 10 -29 6.70 2.10 1 10 -29 7.50 2.10 2 0 29 160.28 13.50 2 0 29 142.89 11.70 -2 0 29 158.38 13.90 2 1 29 39.50 6.40 2 1 29 40.60 7.80 2 -1 29 46.30 8.20 -2 1 29 48.10 9.80 2 2 29 87.69 10.60 2 2 29 78.09 9.00 -2 2 29 64.69 10.60 2 3 29 26.80 5.70 2 3 29 53.59 9.00 -2 3 29 37.90 7.70 2 4 29 46.00 7.20 2 4 29 44.20 8.10 -2 4 29 30.30 6.80 2 5 29 17.30 5.20 2 5 29 18.80 4.40 -2 5 29 9.70 5.10 2 6 29 72.79 6.90 -2 6 29 86.59 9.00 2 7 29 8.00 3.00 -2 7 29 5.30 3.50 2 7 -29 5.70 2.60 -2 8 -29 85.89 6.50 -2 8 29 90.29 6.20 2 8 -29 99.09 6.40 -2 9 -29 -1.30 2.00 2 9 -29 2.00 2.20 2 10 -29 79.19 5.30 3 0 29 -1.40 4.80 3 0 29 -0.60 5.60 3 1 29 7.30 4.90 3 1 29 2.30 5.60 3 -1 29 9.10 5.60 -3 1 29 -11.00 4.60 3 2 29 9.60 4.90 3 2 29 9.20 5.60 -3 2 29 -1.60 5.70 3 3 29 6.50 4.60 3 3 29 -2.20 4.90 -3 3 29 5.50 5.70 3 4 29 26.10 6.00 3 4 29 32.00 5.30 -3 4 29 23.90 6.60 3 5 29 1.40 4.20 3 5 29 -0.10 3.50 -3 5 29 -3.60 4.70 3 6 29 3.80 3.20 -3 6 29 -5.10 4.30 3 6 -29 -4.60 2.20 3 7 29 13.60 3.10 3 7 -29 20.60 4.30 -3 8 29 18.60 3.30 3 8 -29 13.90 2.90 -3 9 -29 3.20 2.10 3 9 -29 1.40 2.10 3 10 -29 -0.30 1.90 4 0 29 146.49 12.50 4 0 29 119.89 10.80 4 1 29 10.20 5.10 4 1 29 16.50 6.20 -4 1 29 5.80 6.00 4 -1 29 20.50 7.00 4 2 29 45.90 8.90 4 2 29 42.20 7.80 -4 2 29 28.70 7.40 4 3 29 30.20 5.40 4 3 29 27.60 6.30 -4 3 29 19.50 6.70 4 4 29 16.40 5.10 4 4 29 6.60 4.30 -4 4 29 14.20 6.10 4 5 29 1.50 3.50 4 5 29 0.50 3.90 -4 5 29 -8.80 4.20 4 6 29 21.60 3.70 4 6 -29 22.40 4.50 4 7 29 0.90 2.40 4 7 -29 0.00 2.30 -4 8 29 10.70 3.10 4 8 -29 9.10 2.60 4 9 -29 11.30 2.50 4 10 -29 21.60 3.40 5 0 29 -0.80 4.20 5 0 29 7.10 5.50 5 1 29 12.40 4.70 5 1 29 5.00 5.50 5 -1 29 5.90 4.70 5 -1 29 10.20 5.80 -5 1 29 19.50 7.10 5 2 29 17.30 5.00 5 2 29 18.30 6.20 -5 2 29 33.60 7.20 5 3 29 9.90 4.30 5 3 29 4.70 4.90 -5 3 29 12.50 5.90 5 4 29 73.69 7.30 5 4 29 67.89 8.50 -5 4 29 86.49 10.40 5 5 29 0.50 3.90 5 5 29 0.20 3.10 -5 5 29 0.90 5.00 5 6 29 8.90 3.10 5 6 -29 7.70 2.70 5 7 -29 28.20 4.40 5 8 -29 3.40 2.40 5 9 -29 13.00 2.50 5 10 -29 4.90 2.00 6 0 29 12.50 5.00 6 0 29 12.70 6.10 6 1 29 114.29 9.90 6 1 29 130.29 11.80 -6 1 29 146.29 12.90 6 -1 29 117.89 10.10 6 -1 29 133.89 12.10 6 2 29 19.60 4.90 6 2 29 25.10 6.20 6 -2 29 7.90 5.90 -6 2 29 21.50 6.90 6 3 29 130.59 11.20 6 3 29 134.69 9.80 -6 3 29 155.18 13.10 6 4 29 6.90 3.50 6 4 29 2.10 4.40 -6 4 29 -4.70 4.70 6 5 29 64.89 7.20 6 5 29 58.59 6.20 -6 5 29 64.89 9.20 6 6 29 1.50 2.70 6 6 -29 4.10 2.60 6 7 -29 27.00 4.40 6 8 -29 12.00 2.80 6 9 -29 9.00 2.30 7 0 29 -1.70 4.30 7 0 29 -7.60 4.60 7 1 29 7.40 4.40 7 1 29 12.10 5.70 7 -1 29 11.70 4.90 7 -1 29 13.60 5.80 7 2 29 11.80 4.30 7 2 29 9.30 5.30 -7 2 29 12.60 6.00 7 -2 29 16.00 5.80 7 3 29 9.30 4.00 7 3 29 7.90 4.70 -7 3 29 8.60 5.70 7 4 29 3.70 3.50 7 4 29 1.70 4.20 -7 4 29 -7.10 4.60 7 5 29 5.30 3.20 -7 5 29 12.60 5.60 7 5 -29 6.20 2.70 7 6 29 11.60 2.80 7 6 -29 3.10 2.60 7 7 -29 8.80 2.70 7 8 -29 4.10 2.30 7 9 -29 30.10 3.80 8 0 29 241.98 14.10 8 0 29 246.38 16.20 8 1 29 28.30 6.40 8 1 29 31.70 5.50 8 -1 29 27.80 5.50 8 -1 29 35.10 7.10 8 2 29 104.19 10.20 8 2 29 106.19 9.00 -8 2 29 128.19 11.90 8 -2 29 114.79 10.90 8 3 29 0.60 3.60 8 3 29 7.40 4.60 -8 3 29 7.00 5.40 8 4 29 64.59 7.30 8 4 29 60.19 6.50 -8 4 29 70.59 9.50 8 5 29 1.90 2.70 8 5 -29 1.70 2.40 8 6 29 75.19 5.00 8 6 -29 73.89 6.00 8 7 -29 7.40 2.60 8 8 -29 75.39 5.60 8 9 -29 8.50 2.10 9 0 29 3.90 4.30 9 0 29 0.00 4.70 9 1 29 1.80 4.00 9 1 29 5.90 4.80 9 -1 29 7.60 5.20 9 -1 29 2.80 4.30 9 2 29 9.00 4.80 9 2 29 5.20 3.90 9 -2 29 7.20 4.20 -9 2 29 10.50 5.80 9 -2 29 6.90 5.20 9 3 29 2.20 3.60 9 3 29 3.10 4.20 -9 3 29 2.90 5.30 9 4 29 30.90 5.00 9 4 29 12.40 4.20 9 5 29 24.00 4.30 9 5 -29 24.90 4.40 9 6 -29 10.30 2.70 9 7 -29 30.80 4.40 9 8 -29 20.60 3.80 9 9 -29 8.20 2.20 10 0 29 5.60 4.10 10 0 29 -0.40 4.70 10 1 29 93.89 9.50 10 1 29 94.69 8.10 10 -1 29 110.69 10.20 10 -1 29 80.89 8.30 10 2 29 46.80 6.30 10 2 29 33.10 6.10 10 -2 29 29.30 5.20 10 -2 29 28.20 5.90 10 3 29 101.69 8.50 10 3 29 76.29 6.90 -10 3 29 99.79 10.90 10 4 29 -0.50 2.80 10 5 29 60.59 4.70 10 5 -29 47.60 5.30 10 6 -29 17.30 3.10 10 7 -29 38.10 4.50 10 8 -29 15.50 2.60 10 9 -29 22.10 3.20 11 0 29 -4.40 3.60 11 0 29 3.80 4.30 11 1 29 8.10 4.50 11 1 29 3.20 3.70 11 -1 29 3.50 4.00 11 -1 29 3.50 4.70 11 2 29 7.10 3.50 11 2 29 2.10 3.70 11 -2 29 1.00 4.40 11 -2 29 2.30 3.70 11 3 29 0.20 3.00 11 4 29 7.30 2.80 11 5 29 3.90 2.20 11 5 -29 -0.50 2.20 11 6 -29 8.80 2.60 11 7 -29 -2.00 2.00 11 8 -29 7.20 2.10 12 0 29 6.20 4.40 12 0 29 8.20 3.60 12 1 29 48.30 5.80 12 -1 29 34.20 6.00 12 2 29 12.90 3.50 12 -2 29 17.90 4.10 12 3 29 10.80 3.10 12 -3 29 13.60 3.90 12 4 29 7.00 2.60 12 5 29 54.49 4.10 12 5 -29 64.99 5.40 12 6 -29 4.30 2.30 12 7 -29 44.50 4.60 12 8 -29 6.60 2.10 13 0 29 4.10 3.30 13 1 29 2.70 3.00 13 -1 29 1.60 3.30 13 2 29 34.40 4.90 13 -2 29 45.00 5.70 13 3 29 -0.40 2.40 13 -3 29 7.70 3.50 13 4 29 20.50 3.50 13 4 -29 19.40 3.20 13 5 -29 8.70 2.50 13 6 -29 15.70 2.70 13 7 -29 4.60 2.10 13 8 -29 2.10 1.80 14 0 29 38.60 5.30 14 1 29 4.00 2.90 14 -1 29 5.10 3.30 14 2 29 11.60 3.00 14 -2 29 7.10 3.30 14 3 29 2.40 2.40 14 -3 29 3.50 3.10 14 4 29 18.70 3.10 14 4 -29 24.50 4.30 14 -4 29 16.30 4.00 14 5 -29 4.50 2.20 14 6 -29 18.90 3.80 14 7 -29 17.00 3.40 15 0 29 -1.70 2.70 15 1 29 9.40 3.00 15 -1 29 7.30 3.10 15 2 29 20.20 3.30 15 -2 29 20.50 3.70 15 3 29 8.00 2.50 15 -3 29 14.80 3.60 15 4 -29 0.50 2.10 15 -4 29 -5.90 2.40 15 5 -29 14.20 2.60 15 6 -29 26.30 3.80 15 7 -29 1.10 1.90 16 0 29 16.80 3.40 16 1 29 21.70 4.10 16 -1 29 17.00 3.60 16 2 29 3.20 2.30 16 -2 29 -0.70 2.80 16 3 29 15.10 2.40 16 -3 29 17.20 3.40 16 -4 29 5.20 2.90 16 4 -29 5.80 2.30 16 5 -29 59.79 4.80 16 6 -29 28.60 3.60 17 0 29 0.40 2.50 17 1 29 -1.10 2.30 17 -1 29 7.30 2.90 17 2 29 3.20 2.20 17 -2 29 2.60 2.80 17 3 29 8.50 1.80 17 -3 29 9.00 3.00 17 4 -29 21.80 3.70 17 -4 29 18.50 3.40 17 5 -29 -1.80 1.70 18 0 29 27.70 4.20 18 1 29 21.00 3.50 18 -1 29 22.30 3.40 18 2 29 24.60 3.10 18 -2 29 20.30 3.40 18 -3 29 16.40 3.10 18 -4 29 33.30 4.20 19 0 29 1.00 2.10 19 1 29 6.90 2.10 19 -1 29 5.00 2.40 19 2 29 -0.50 1.50 19 -2 29 -0.10 2.20 19 -3 29 3.10 2.30 20 0 29 53.99 3.90 20 1 29 13.30 2.50 20 -1 29 6.70 2.10 20 -2 29 19.50 3.30 0 0 30 11.80 6.10 0 1 30 -5.10 5.40 0 2 30 10.00 5.90 0 3 30 -6.10 4.90 0 4 30 27.30 6.60 0 5 30 -1.10 4.40 0 5 30 -2.30 3.80 0 6 30 31.80 4.60 0 7 30 -1.70 2.80 0 8 -30 10.70 2.60 0 9 -30 0.70 1.90 -1 0 30 10.20 6.30 1 0 30 6.10 5.10 1 0 30 -4.70 5.30 1 1 30 1.70 4.70 1 1 30 5.20 5.60 -1 1 30 -1.40 5.50 1 2 30 4.30 4.70 1 2 30 -4.20 4.90 -1 2 30 0.50 5.60 1 3 30 7.20 4.70 1 3 30 16.60 6.10 -1 3 30 8.30 6.00 1 4 30 12.90 5.60 1 4 30 8.50 4.50 -1 4 30 9.20 5.50 1 5 30 8.50 4.00 1 5 30 -1.00 4.60 -1 5 30 9.50 5.30 1 6 30 6.40 3.70 -1 6 30 4.60 3.60 1 7 30 2.90 2.70 -1 7 30 0.10 3.10 1 8 -30 6.20 2.40 -1 9 -30 -0.60 1.90 1 9 -30 -1.60 1.90 -2 0 30 63.59 10.60 2 0 30 62.39 8.70 2 0 30 53.49 9.80 2 1 30 75.89 9.20 2 1 30 77.69 10.60 2 -1 30 95.09 11.00 -2 1 30 86.99 10.90 2 2 30 19.80 6.50 2 2 30 17.30 5.30 -2 2 30 22.50 6.70 2 3 30 52.59 7.70 2 3 30 54.69 8.90 -2 3 30 47.10 9.40 2 4 30 5.90 5.00 2 4 30 10.70 4.50 -2 4 30 5.40 5.40 2 5 30 47.60 6.50 2 6 30 13.00 3.50 2 7 30 28.10 4.40 2 7 -30 36.70 4.50 -2 7 30 47.80 5.50 2 8 -30 -1.10 2.10 -2 8 30 6.90 2.50 2 9 -30 31.60 3.80 3 0 30 -4.90 4.60 3 0 30 -4.30 4.40 3 1 30 6.10 4.90 3 1 30 5.80 5.40 3 -1 30 -1.20 5.10 -3 1 30 1.50 5.60 3 2 30 13.90 5.30 3 2 30 14.20 6.00 -3 2 30 15.80 6.70 3 3 30 9.50 5.30 3 3 30 4.20 4.40 -3 3 30 5.80 5.70 3 4 30 23.90 5.60 3 4 30 12.90 4.50 -3 4 30 17.00 6.30 3 5 30 0.40 3.50 3 6 30 14.40 3.40 3 7 30 3.90 2.40 3 7 -30 3.30 2.40 -3 7 30 7.00 3.40 3 8 -30 6.80 2.40 -3 8 30 3.80 2.40 3 9 -30 12.10 2.40 4 0 30 10.90 5.00 4 0 30 16.00 6.20 4 1 30 13.30 5.10 4 1 30 11.00 5.80 -4 1 30 15.00 6.40 4 -1 30 2.00 5.50 4 2 30 16.20 5.80 4 2 30 9.00 4.80 -4 2 30 13.00 6.20 4 3 30 41.30 8.10 4 3 30 36.60 6.80 -4 3 30 45.40 9.00 4 4 30 0.90 4.30 4 4 30 -1.20 3.60 -4 4 30 0.50 5.00 4 5 30 -1.40 3.10 4 6 30 49.40 5.30 4 7 -30 14.60 2.90 -4 8 30 5.90 2.80 4 8 -30 4.90 2.30 4 9 -30 16.30 3.30 5 0 30 -4.40 4.10 5 0 30 8.70 5.50 5 1 30 12.00 5.80 5 1 30 19.20 5.10 5 -1 30 16.90 6.30 5 -1 30 11.20 4.70 -5 1 30 19.70 6.80 5 2 30 8.50 4.40 5 2 30 11.30 5.40 -5 2 30 3.30 5.50 5 3 30 40.70 7.80 5 3 30 15.60 4.50 -5 3 30 9.10 5.90 5 4 30 15.00 4.00 5 4 30 8.90 4.70 -5 4 30 13.50 5.60 5 5 30 10.10 3.60 5 6 30 32.50 4.60 5 6 -30 26.20 4.40 5 7 -30 33.30 4.60 -5 8 30 15.10 3.20 5 8 -30 7.00 2.50 5 9 -30 16.00 3.20 6 0 30 159.18 11.10 6 1 30 7.00 5.30 6 1 30 5.40 4.20 6 -1 30 7.50 4.90 6 -1 30 -0.30 4.90 6 2 30 104.89 10.40 6 2 30 117.49 9.00 -6 2 30 93.09 11.00 6 3 30 18.30 4.50 6 3 30 22.10 5.60 -6 3 30 15.80 6.10 6 4 30 40.30 7.20 6 4 30 40.00 6.00 6 5 30 11.60 3.50 6 6 30 85.69 5.60 6 6 -30 79.79 6.20 6 7 -30 6.30 2.50 6 8 -30 24.70 4.00 -6 8 30 31.30 4.50 6 9 -30 1.80 1.90 7 0 30 1.80 5.00 7 0 30 -3.30 4.20 7 1 30 0.20 4.10 7 1 30 4.40 5.10 7 -1 30 -1.70 4.10 7 -1 30 -2.00 4.60 7 2 30 11.50 4.40 7 2 30 6.30 5.00 7 -2 30 7.40 5.50 -7 2 30 8.00 5.80 7 3 30 2.90 3.60 7 3 30 -0.40 4.20 -7 3 30 1.00 4.90 7 4 30 17.50 4.10 7 5 30 1.60 2.90 7 6 30 6.50 2.30 7 6 -30 8.50 2.70 7 7 -30 5.60 2.40 7 8 -30 0.30 2.00 8 0 30 10.40 4.70 8 0 30 -3.70 4.70 8 1 30 22.30 4.90 8 1 30 20.90 5.70 8 -1 30 24.20 5.40 8 -1 30 26.90 6.40 8 2 30 66.39 8.50 8 2 30 68.09 7.50 8 -2 30 69.29 7.80 8 3 30 11.60 4.00 8 3 30 25.40 5.60 8 4 30 1.60 3.20 8 5 30 9.80 3.00 8 6 -30 24.20 4.40 8 7 -30 12.30 2.70 8 8 -30 0.30 2.00 9 0 30 -1.40 3.90 9 0 30 0.00 4.50 9 1 30 9.30 4.80 9 1 30 -1.70 3.70 9 -1 30 -6.40 4.20 9 -1 30 5.20 4.00 9 2 30 7.20 3.80 9 2 30 14.30 4.90 9 -2 30 9.90 4.30 9 3 30 43.10 5.70 9 4 30 12.20 3.40 9 5 30 11.30 2.70 9 5 -30 13.50 2.90 9 6 -30 22.90 4.20 9 7 -30 33.50 4.20 9 8 -30 0.70 1.90 10 0 30 48.40 6.60 10 1 30 6.70 3.80 10 -1 30 8.40 4.10 10 2 30 29.20 4.50 10 -2 30 21.40 4.70 10 3 30 -2.00 3.00 10 4 30 40.20 4.80 10 5 30 5.30 2.20 10 5 -30 10.20 2.70 10 6 -30 43.20 4.80 10 7 -30 10.70 2.50 10 8 -30 32.90 3.80 11 0 30 -6.70 3.20 11 1 30 8.70 3.80 11 -1 30 1.90 3.60 11 2 30 8.60 3.40 11 -2 30 5.00 3.60 11 3 30 15.00 3.30 11 -3 30 11.30 3.80 11 4 30 -0.50 2.30 11 5 30 20.10 2.90 11 5 -30 14.00 2.90 11 6 -30 2.30 2.20 11 7 -30 7.80 2.20 12 0 30 10.20 3.60 12 1 30 25.00 4.20 12 -1 30 27.60 5.40 12 2 30 15.60 3.40 12 -2 30 15.20 3.80 12 3 30 34.50 4.40 12 -3 30 25.90 4.30 12 4 30 27.80 3.70 12 5 -30 21.30 4.10 12 6 -30 0.80 2.10 12 7 -30 16.40 3.40 13 0 30 1.20 3.00 13 1 30 2.00 2.90 13 -1 30 2.60 3.20 13 2 30 10.70 2.90 13 -2 30 3.00 3.30 13 3 30 1.10 2.40 13 -3 30 0.40 3.00 13 4 30 5.60 2.10 13 5 -30 0.50 2.00 13 6 -30 5.00 2.10 14 0 30 17.00 3.60 14 1 30 56.99 5.30 14 -1 30 55.19 5.70 14 2 30 4.60 2.60 14 -2 30 2.00 3.10 14 3 30 18.50 3.60 14 -3 30 33.80 5.00 14 4 30 4.70 2.00 14 -4 30 3.20 2.90 14 5 -30 33.40 4.10 14 6 -30 6.40 2.10 15 0 30 1.00 2.70 15 1 30 11.10 3.00 15 -1 30 11.60 3.40 15 2 30 4.00 2.40 15 -2 30 -1.80 2.90 15 3 30 2.40 2.00 15 -3 30 6.70 3.10 15 -4 30 30.30 4.70 15 5 -30 11.30 2.40 16 0 30 8.60 2.70 16 1 30 0.30 2.40 16 -1 30 6.10 2.80 16 2 30 1.00 2.00 16 -2 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6.30 4.80 2 1 31 3.50 5.40 -2 1 31 6.40 5.60 2 2 31 43.00 8.80 2 2 31 54.89 8.10 -2 2 31 57.59 9.60 2 3 31 8.10 4.50 2 3 31 10.60 5.50 -2 3 31 3.00 5.60 2 4 31 29.30 5.10 2 5 31 2.90 3.50 2 6 31 -1.10 2.90 -2 6 31 9.00 4.00 2 7 31 -0.40 2.30 -2 7 31 2.50 2.90 2 8 -31 -2.40 1.90 3 0 31 -0.80 5.00 3 0 31 4.90 4.60 3 1 31 -1.80 5.00 3 1 31 -0.70 4.40 -3 1 31 8.80 6.00 3 -1 31 -5.50 4.80 3 2 31 7.40 4.60 3 2 31 0.30 5.10 -3 2 31 6.90 5.70 3 3 31 8.60 5.30 3 3 31 9.90 4.40 3 4 31 5.00 3.70 3 5 31 17.10 3.80 3 6 31 20.60 3.50 -3 6 31 22.80 4.30 -3 7 31 19.30 3.70 3 8 -31 0.70 1.90 4 0 31 47.70 7.90 4 0 31 75.09 9.60 4 1 31 22.80 5.10 4 1 31 27.90 6.40 -4 1 31 23.80 6.80 4 -1 31 21.00 6.60 4 -1 31 25.70 5.40 4 2 31 60.59 9.10 4 2 31 66.29 7.60 -4 2 31 69.29 9.90 4 3 31 13.50 4.40 4 4 31 37.70 6.00 4 5 31 7.00 3.40 4 6 31 7.90 3.00 4 7 -31 29.30 4.10 -4 7 31 29.40 5.00 4 8 -31 1.20 2.00 5 0 31 -4.60 4.50 5 0 31 -0.70 4.20 5 1 31 5.90 4.20 5 1 31 7.00 5.30 5 -1 31 -3.40 4.30 5 2 31 -4.50 3.80 5 2 31 5.80 5.10 5 3 31 1.00 3.60 5 4 31 17.50 4.00 5 5 31 42.20 5.40 5 6 31 5.80 2.50 5 7 -31 10.30 2.60 -5 7 31 11.00 3.40 5 8 -31 4.40 2.00 6 0 31 4.20 4.40 6 0 31 2.50 5.40 6 1 31 5.00 5.50 6 1 31 0.90 4.10 6 -1 31 4.00 4.40 6 2 31 28.90 5.00 6 3 31 -2.50 3.50 6 4 31 -0.60 3.30 6 5 31 5.20 3.00 6 6 31 13.90 2.50 6 7 -31 22.40 3.90 6 8 -31 4.90 2.10 7 0 31 8.10 4.40 7 1 31 4.60 4.20 7 -1 31 7.00 4.40 7 2 31 6.70 4.10 7 3 31 9.90 4.00 7 4 31 -2.60 3.00 7 5 31 2.10 2.70 7 6 -31 20.10 4.00 7 7 -31 23.70 4.00 8 0 31 81.29 7.90 8 1 31 6.40 4.20 8 -1 31 16.10 4.50 8 2 31 82.19 7.30 8 -2 31 68.19 7.60 8 3 31 13.20 3.80 8 4 31 100.39 6.90 8 5 31 -6.00 2.10 8 6 -31 47.30 4.70 8 7 -31 4.10 2.20 9 0 31 1.20 3.80 9 1 31 4.00 3.70 9 -1 31 5.70 4.00 9 2 31 33.80 5.80 9 -2 31 26.20 4.80 9 3 31 11.10 3.60 9 4 31 3.40 2.80 9 5 31 9.50 2.30 9 6 -31 7.30 2.40 9 7 -31 19.50 3.60 10 0 31 66.19 6.90 10 1 31 18.40 4.10 10 -1 31 16.60 4.30 10 2 31 52.79 6.10 10 -2 31 51.19 6.40 10 3 31 7.20 3.10 10 4 31 8.20 2.70 10 5 31 8.50 2.00 10 6 -31 11.10 2.50 11 0 31 -5.00 3.10 11 1 31 1.00 3.20 11 -1 31 0.40 3.40 11 2 31 0.30 2.80 11 -2 31 -1.10 3.20 11 3 31 6.00 2.70 11 -3 31 7.20 3.50 11 4 31 8.50 2.40 11 6 -31 3.30 2.10 12 0 31 18.50 3.80 12 1 31 -5.40 2.70 12 -1 31 0.30 3.00 12 2 31 34.80 4.60 12 -2 31 35.30 5.40 12 3 31 -0.30 2.40 12 -3 31 1.60 3.10 12 4 31 37.70 3.70 13 0 31 -0.10 2.90 13 1 31 -1.70 2.80 13 -1 31 2.40 3.10 13 2 31 8.20 2.80 13 -2 31 0.40 2.90 13 3 31 4.30 2.30 13 -3 31 9.20 3.20 13 -4 31 4.10 3.00 14 0 31 30.30 4.70 14 1 31 3.90 2.60 14 -1 31 0.60 2.80 14 2 31 14.00 2.90 14 -2 31 15.00 3.40 14 3 31 2.00 2.00 14 -3 31 -4.30 2.70 14 -4 31 50.69 5.00 15 0 31 0.30 2.70 15 1 31 9.50 2.80 15 -1 31 8.60 2.90 15 2 31 0.80 2.20 15 -2 31 9.60 3.10 15 3 31 0.70 1.60 15 -3 31 -0.50 2.50 16 0 31 1.40 2.40 16 1 31 39.30 4.00 16 -1 31 41.40 4.50 16 2 31 3.10 1.80 16 -2 31 -3.80 2.30 16 -3 31 51.09 5.00 17 0 31 1.50 2.10 17 1 31 -0.70 1.80 17 -1 31 0.90 2.30 17 -2 31 3.60 2.40 0 0 32 49.00 8.10 0 1 32 -2.30 4.20 0 2 32 43.70 7.50 0 3 32 0.20 4.20 0 4 32 38.40 6.70 0 5 32 -6.70 3.60 0 6 32 43.80 5.20 0 7 32 -2.00 2.20 1 0 32 -0.70 4.60 1 1 32 6.30 4.80 -1 1 32 0.60 4.40 1 2 32 4.30 4.50 -1 2 32 9.60 4.60 1 3 32 9.80 4.60 -1 3 32 15.50 4.70 1 4 32 9.80 4.20 -1 4 32 6.10 4.30 1 5 32 9.40 3.60 -1 5 32 9.40 4.00 1 6 32 1.70 2.90 -1 6 32 3.60 3.10 -1 7 32 6.00 2.40 2 0 32 2.80 4.30 2 1 32 17.70 4.90 -2 1 32 24.10 5.40 2 2 32 4.90 4.40 -2 2 32 9.90 4.80 2 3 32 18.70 4.80 -2 3 32 23.00 5.20 2 4 32 8.50 3.90 -2 4 32 10.70 4.50 2 5 32 1.60 3.20 -2 5 32 0.20 3.80 2 6 32 1.10 2.70 -2 6 32 6.20 3.40 -2 7 32 11.00 2.70 3 0 32 4.90 4.40 3 1 32 8.60 4.40 3 -1 32 5.10 4.60 3 2 32 0.60 4.00 3 3 32 8.00 4.00 3 4 32 10.30 3.80 3 5 32 14.90 3.70 -3 5 32 32.00 5.90 3 6 32 1.00 2.50 -3 6 32 2.80 3.40 -3 7 32 9.80 2.70 4 0 32 4.30 4.10 4 1 32 9.40 4.40 4 -1 32 7.20 4.80 4 2 32 20.20 4.70 4 3 32 7.10 3.80 4 4 32 9.80 3.80 4 5 32 4.30 3.10 4 6 32 7.20 2.50 -4 6 32 8.70 3.60 -4 7 32 14.40 3.10 5 0 32 0.60 4.10 5 1 32 5.30 4.30 5 -1 32 6.60 4.50 5 2 32 -0.50 3.90 5 3 32 4.90 3.80 5 4 32 6.60 3.60 5 5 32 36.40 4.80 5 6 32 3.30 2.00 -5 6 32 4.30 3.50 -5 7 32 1.10 2.70 6 0 32 52.09 7.30 6 1 32 10.70 4.50 6 -1 32 10.70 4.50 6 2 32 28.60 4.90 6 3 32 5.20 3.70 6 4 32 30.50 5.40 6 5 32 27.90 4.20 -6 7 32 49.20 5.00 7 0 32 -5.30 3.70 7 1 32 10.40 4.40 7 -1 32 15.20 4.40 7 2 32 6.80 3.90 7 -2 32 3.20 4.00 7 3 32 -2.50 3.20 7 4 32 1.60 2.90 7 5 32 18.10 2.80 -7 7 32 1.30 2.90 8 0 32 9.80 4.20 8 1 32 5.30 3.90 8 -1 32 -0.90 3.80 8 2 32 18.60 4.20 8 -2 32 15.10 4.40 8 3 32 13.20 3.60 8 4 32 9.20 3.00 8 5 32 13.00 2.30 -8 7 32 14.70 3.50 9 0 32 2.10 3.70 9 1 32 7.20 3.80 9 -1 32 5.50 4.00 9 2 32 28.30 5.30 9 -2 32 26.50 4.60 9 3 32 3.50 2.90 9 4 32 14.10 2.90 10 0 32 28.70 5.60 10 1 32 28.80 5.20 10 -1 32 27.10 4.50 10 2 32 8.60 3.30 10 -2 32 19.70 4.00 10 3 32 13.20 3.00 10 -3 32 17.00 3.70 10 4 32 40.70 4.00 11 0 32 0.00 3.10 11 1 32 3.70 3.10 11 -1 32 -0.30 3.10 11 2 32 12.10 3.00 11 -2 32 13.50 3.70 11 3 32 2.80 2.40 11 -3 32 3.90 3.10 11 4 32 23.70 3.30 12 0 32 25.90 4.90 12 1 32 6.00 2.80 12 -1 32 0.40 2.90 12 2 32 3.50 2.60 12 -2 32 10.10 3.40 12 3 32 4.50 2.30 12 -3 32 2.70 3.00 13 0 32 0.50 2.70 13 1 32 5.10 2.70 13 -1 32 5.80 3.00 13 2 32 2.70 2.50 13 -2 32 4.80 3.00 13 3 32 0.10 1.90 13 -3 32 -0.20 2.80 14 0 32 4.20 2.70 14 1 32 11.60 2.70 14 -1 32 8.40 3.00 14 2 32 3.20 2.10 14 -2 32 1.20 2.60 14 -3 32 1.90 2.50 15 0 32 3.90 2.40 15 1 32 15.90 2.70 15 -1 32 21.50 4.00 15 2 32 6.00 2.00 15 -2 32 9.60 2.80 16 0 32 29.10 3.70 16 1 32 13.70 2.50 16 -1 32 11.70 2.70 0 0 33 2.70 4.30 0 1 33 61.99 8.00 0 2 33 -0.50 4.10 0 3 33 45.70 7.10 0 4 33 -1.40 3.60 0 5 33 2.30 3.20 0 6 33 2.30 2.70 1 0 33 -0.10 4.00 -1 0 33 2.10 4.50 1 1 33 5.00 4.20 -1 1 33 -1.90 4.20 1 2 33 6.00 4.20 -1 2 33 1.10 4.10 1 3 33 6.40 4.10 -1 3 33 9.40 4.40 1 4 33 40.40 5.90 -1 4 33 33.60 6.30 1 5 33 14.40 3.40 -1 5 33 10.90 3.70 1 6 33 35.90 4.20 -1 6 33 22.20 4.30 2 0 33 24.20 5.00 2 1 33 -3.30 3.90 -2 1 33 -1.80 4.10 2 2 33 15.40 4.50 -2 2 33 13.20 4.70 2 3 33 14.70 4.30 -2 3 33 27.70 5.00 2 4 33 14.70 3.70 -2 4 33 2.90 4.00 2 5 33 3.20 3.10 -2 5 33 4.50 3.60 2 6 33 2.70 2.30 -2 6 33 4.20 2.90 3 0 33 -0.40 3.80 3 1 33 -0.90 3.80 -3 1 33 3.00 4.20 3 -1 33 1.20 4.10 3 2 33 -3.20 3.60 -3 2 33 3.50 4.30 3 3 33 3.30 3.60 -3 3 33 5.00 4.30 3 4 33 13.00 3.70 -3 4 33 18.20 4.50 3 5 33 45.30 5.20 -3 5 33 42.90 6.20 3 6 33 3.80 2.30 -3 6 33 -2.10 2.80 4 0 33 24.90 5.10 4 1 33 4.90 4.20 -4 1 33 12.20 4.60 4 -1 33 6.50 4.40 4 2 33 35.00 6.50 -4 2 33 36.70 7.00 4 3 33 0.60 3.60 -4 3 33 -4.10 4.00 4 4 33 4.30 3.40 -4 4 33 3.10 4.00 4 5 33 15.10 3.20 -4 5 33 20.00 4.20 -4 6 33 0.80 3.00 5 0 33 -1.20 3.90 5 1 33 2.50 4.00 5 -1 33 -1.70 3.90 5 2 33 1.90 3.80 5 3 33 7.10 3.60 5 4 33 4.70 3.10 5 5 33 28.40 4.10 -5 5 33 30.20 5.60 -5 6 33 1.80 3.00 6 0 33 61.39 7.20 6 1 33 8.80 4.10 6 -1 33 9.50 4.30 6 2 33 1.00 3.60 6 -2 33 4.30 4.00 6 3 33 40.70 5.50 6 4 33 3.20 3.00 6 5 33 14.80 2.60 -6 5 33 21.00 4.30 -6 6 33 12.10 3.30 7 0 33 -3.80 3.60 7 1 33 9.10 3.90 7 -1 33 4.20 3.80 7 2 33 22.10 4.20 7 -2 33 23.80 4.70 7 3 33 -1.60 3.00 7 4 33 3.00 2.70 7 5 33 34.40 3.30 -7 6 33 4.70 3.10 8 0 33 12.50 4.10 8 1 33 23.10 4.30 8 -1 33 19.00 4.30 8 2 33 4.60 3.40 8 -2 33 11.80 3.90 8 3 33 18.20 3.30 8 4 33 16.70 2.90 -8 6 33 -2.70 2.90 9 0 33 1.20 3.30 9 1 33 4.60 3.30 9 -1 33 4.90 3.50 9 2 33 18.40 3.60 9 -2 33 19.70 3.90 9 3 33 6.60 2.80 9 -3 33 2.00 3.10 9 4 33 0.60 2.10 10 0 33 7.30 3.40 10 1 33 -1.10 2.90 10 -1 33 -0.10 3.10 10 2 33 1.00 2.60 10 -2 33 -3.00 2.90 10 3 33 4.70 2.30 10 -3 33 6.90 3.10 10 4 33 4.60 2.00 11 0 33 -0.40 2.80 11 1 33 2.70 2.80 11 -1 33 3.20 3.00 11 2 33 7.40 2.70 11 -2 33 6.80 3.10 11 3 33 2.90 2.10 11 -3 33 7.00 2.80 12 0 33 17.10 3.20 12 1 33 33.40 4.20 12 -1 33 33.20 4.60 12 2 33 23.80 3.60 12 -2 33 12.50 3.20 12 3 33 16.00 2.90 13 0 33 3.20 2.70 13 1 33 1.50 2.40 13 -1 33 6.50 2.90 13 2 33 6.50 2.10 13 -2 33 11.40 3.00 14 0 33 8.00 2.40 14 1 33 25.40 3.50 14 -1 33 29.30 3.90 0 0 34 15.00 4.50 0 1 34 2.30 3.70 0 2 34 2.80 3.80 0 3 34 -0.30 3.50 0 4 34 -3.20 3.20 0 5 34 -2.10 2.80 1 0 34 3.00 3.80 -1 0 34 -1.70 3.90 1 1 34 6.20 4.00 -1 1 34 4.80 4.10 1 2 34 1.80 3.90 -1 2 34 8.50 4.10 1 3 34 1.00 3.40 -1 3 34 -6.10 3.50 1 4 34 12.10 3.50 -1 4 34 11.00 3.60 1 5 34 17.30 3.30 -1 5 34 19.10 3.40 -2 0 34 9.80 4.40 2 0 34 9.20 4.20 2 1 34 9.20 4.10 2 -1 34 9.80 4.40 -2 1 34 16.80 4.70 2 2 34 43.10 6.30 -2 2 34 41.70 6.60 2 3 34 9.60 3.90 -2 3 34 11.30 4.20 2 4 34 12.60 3.60 -2 4 34 15.30 4.00 2 5 34 8.70 2.90 -2 5 34 2.50 3.10 3 0 34 3.80 4.00 3 1 34 1.50 3.90 3 -1 34 4.10 4.20 -3 1 34 2.20 4.10 3 2 34 6.40 3.90 -3 2 34 5.10 4.00 3 3 34 3.50 3.60 -3 3 34 9.70 4.00 3 4 34 13.70 3.50 -3 4 34 13.90 4.00 3 5 34 1.60 2.40 -3 5 34 -0.80 3.10 4 0 34 40.50 6.60 4 1 34 17.60 4.30 4 -1 34 16.40 4.50 -4 1 34 13.50 4.40 4 2 34 7.10 3.80 -4 2 34 10.50 4.30 4 3 34 4.40 3.60 -4 3 34 -1.20 3.80 4 4 34 11.90 3.20 -4 4 34 4.40 3.70 4 5 34 4.20 2.40 -4 5 34 4.60 3.30 5 0 34 -1.90 3.70 5 1 34 4.60 3.90 -5 1 34 6.00 4.10 5 -1 34 1.30 3.70 5 2 34 0.50 3.40 -5 2 34 -1.10 3.80 5 -2 34 -7.70 3.40 5 3 34 15.90 3.70 -5 3 34 14.80 4.20 5 4 34 -1.50 2.50 -5 4 34 2.20 3.50 -5 5 34 5.40 3.30 6 0 34 56.79 6.50 6 1 34 2.60 3.50 6 -1 34 4.90 3.80 -6 1 34 7.70 3.90 6 2 34 21.30 4.00 6 -2 34 9.10 3.90 -6 2 34 15.60 4.50 6 3 34 24.90 4.60 -6 3 34 24.70 4.60 6 4 34 10.60 2.70 -6 4 34 5.70 3.60 -6 5 34 -0.10 3.00 7 0 34 2.50 3.60 7 1 34 18.50 4.00 -7 1 34 11.50 4.20 7 -1 34 18.10 4.20 7 2 34 13.80 3.50 7 -2 34 13.80 3.80 -7 2 34 11.40 4.20 7 3 34 13.20 3.10 -7 3 34 4.70 3.80 7 4 34 3.00 2.20 -7 4 34 0.20 3.40 -7 5 34 2.60 3.10 8 0 34 0.10 3.20 8 1 34 5.50 3.20 8 -1 34 12.70 3.60 8 2 34 9.60 3.10 8 -2 34 7.50 3.20 8 3 34 28.90 4.00 -8 4 34 10.80 3.70 9 0 34 3.90 3.10 9 1 34 9.40 3.10 9 -1 34 2.80 2.90 9 2 34 3.60 2.50 9 -2 34 2.50 2.80 9 3 34 11.20 2.40 10 0 34 27.30 4.60 10 1 34 4.40 2.60 10 -1 34 5.50 2.90 10 2 34 0.20 2.30 10 -2 34 1.00 2.70 11 0 34 2.40 2.50 11 1 34 14.40 2.80 11 -1 34 11.60 2.90 11 2 34 4.30 2.20 12 0 34 5.70 2.50 12 1 34 9.70 2.60 0 0 35 4.80 3.70 0 1 35 24.30 4.50 0 2 35 -3.60 3.10 0 3 35 9.10 3.50 0 4 35 3.60 3.00 -1 0 35 6.30 3.80 1 0 35 3.10 3.70 1 1 35 2.80 3.80 1 -1 35 0.80 3.80 -1 1 35 -3.20 3.40 1 2 35 5.70 3.60 -1 2 35 4.30 3.60 1 3 35 -0.90 3.10 -1 3 35 -1.40 3.20 1 4 35 10.90 3.10 -1 4 35 9.20 3.20 2 0 35 0.10 3.60 -2 0 35 3.00 3.70 2 1 35 6.70 3.90 -2 1 35 2.00 3.50 2 -1 35 4.10 3.90 2 2 35 4.50 3.60 -2 2 35 2.10 3.60 2 3 35 8.10 3.40 -2 3 35 2.50 3.30 2 4 35 8.30 3.00 -2 4 35 11.20 3.30 -3 0 35 -2.60 3.40 3 0 35 -1.90 3.60 3 1 35 2.50 3.70 -3 1 35 4.00 3.70 3 -1 35 0.40 3.50 3 2 35 6.00 3.50 -3 2 35 2.50 3.50 3 3 35 4.50 3.10 -3 3 35 7.80 3.60 3 4 35 4.40 2.70 -3 4 35 5.00 3.10 4 0 35 91.49 7.30 4 1 35 1.30 3.40 4 -1 35 -0.60 3.40 -4 1 35 2.70 3.70 4 2 35 22.00 3.90 -4 2 35 25.50 4.50 4 3 35 1.30 2.80 -4 3 35 6.40 3.60 4 4 35 15.20 3.00 -4 4 35 8.90 3.30 5 0 35 -0.60 3.30 5 1 35 -1.40 3.20 5 -1 35 1.90 3.40 -5 1 35 4.80 3.70 5 2 35 3.20 3.10 -5 2 35 -3.10 3.40 5 3 35 2.60 2.80 -5 3 35 4.10 3.60 6 0 35 3.30 3.20 6 1 35 51.79 5.60 -6 1 35 45.40 6.40 6 -1 35 46.00 5.60 6 2 35 7.40 3.20 -6 2 35 2.20 3.50 6 3 35 30.60 4.20 -6 3 35 27.50 4.30 7 0 35 -0.70 2.80 7 1 35 -2.20 2.70 7 -1 35 6.30 3.10 7 2 35 4.70 2.60 8 0 35 21.50 3.50 8 1 35 13.70 3.00 8 -1 35 5.60 3.00 8 2 35 2.40 2.30 9 0 35 -3.60 2.40 9 1 35 14.60 2.90 0 1 36 1.00 3.30 0 2 36 12.10 3.60 1 1 36 -7.00 3.00 1 2 36 6.90 3.30 2 1 36 30.80 5.20 2 2 36 2.10 3.10 3 1 36 1.30 3.10 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 45681 _olex2_date_sample_data_collection 2021-03-10 _olex2_date_sample_submission 2021-03-05 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a mylar loop in perfluoroether oil' _olex2_submission_original_sample_id MEM054_150K _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.60035(3) 0.75842(6) 0.42259(3) 0.0228(2) Uani 1 1 d . . . . . Cu2 Cu 0.65898(3) 1.24110(6) 0.59874(3) 0.0213(2) Uani 1 1 d . . . . . P2 P 0.67359(5) 0.79639(10) 0.44214(6) 0.0216(3) Uani 1 1 d . . . . . P3 P 0.58518(5) 1.20464(10) 0.57662(6) 0.0209(3) Uani 1 1 d . . . . . P4 P 0.66866(5) 1.23739(11) 0.67407(6) 0.0228(3) Uani 1 1 d . . . . . P1 P 0.58342(5) 0.74807(11) 0.34845(6) 0.0253(4) Uani 1 1 d . . . . . O2 O 0.59675(13) 1.1043(3) 0.65781(15) 0.0226(9) Uani 1 1 d . . . . . O1 O 0.65524(14) 0.8864(3) 0.36113(16) 0.0249(9) Uani 1 1 d . . . . . N4 N 0.69236(16) 1.3561(3) 0.56838(18) 0.0212(11) Uani 1 1 d . . . . . N1 N 0.56251(17) 0.6490(3) 0.45063(19) 0.0235(11) Uani 1 1 d . . . . . O3 O 0.8410(2) 1.1095(4) 0.1632(2) 0.0546(15) Uani 1 1 d . . . . . N2 N 0.54069(17) 0.8311(4) 0.44581(19) 0.0232(11) Uani 1 1 d . . . . . N3 N 0.71644(16) 1.1756(4) 0.56923(19) 0.0233(11) Uani 1 1 d . . . . . C78 C 0.57217(19) 0.9501(4) 0.6370(2) 0.0241(13) Uani 1 1 d . . . . . C88 C 0.6512(2) 0.9456(5) 0.7357(2) 0.0296(14) Uani 1 1 d . . . . . H88 H 0.647594 0.884985 0.747684 0.036 Uiso 1 1 calc R U . . . C76 C 0.57046(18) 1.0813(4) 0.5855(2) 0.0222(13) Uani 1 1 d . . . . . C56 C 0.7493(2) 1.2360(4) 0.5555(2) 0.0216(12) Uani 1 1 d . . . . . C68 C 0.5228(2) 1.2328(5) 0.4557(3) 0.0339(16) Uani 1 1 d . . . . . H68 H 0.492252 1.230766 0.443914 0.041 Uiso 1 1 calc R U . . . C77 C 0.57933(18) 1.0434(4) 0.6260(2) 0.0236(14) Uani 1 1 d . . . . . C39 C 0.6255(2) 0.9158(4) 0.3285(2) 0.0236(13) Uani 1 1 d . . . . . C5 C 0.5189(2) 0.6723(5) 0.4616(2) 0.0259(14) Uani 1 1 d . . . . . C97 C 0.6245(2) 1.3072(5) 0.7025(2) 0.0292(14) Uani 1 1 d . . . . . C86 C 0.6933(2) 1.0902(5) 0.7341(2) 0.0294(14) Uani 1 1 d . . . . . H86 H 0.718002 1.127857 0.744615 0.035 Uiso 1 1 calc R U . . . C55 C 0.7927(2) 1.2054(5) 0.5415(2) 0.0284(14) Uani 1 1 d . . . . . H55 H 0.815571 1.248476 0.531724 0.034 Uiso 1 1 calc R U . . . C61 C 0.6776(2) 1.4442(5) 0.5652(2) 0.0263(14) Uani 1 1 d . . . . . C57 C 0.7364(2) 1.3355(4) 0.5553(2) 0.0216(12) Uani 1 1 d . . . . . C30 C 0.6665(2) 1.0743(5) 0.3293(3) 0.0314(15) Uani 1 1 d . . . . . C69 C 0.5302(2) 1.2186(5) 0.4999(2) 0.0288(14) Uani 1 1 d . . . . . H69 H 0.504401 1.206647 0.518596 0.035 Uiso 1 1 calc R U . . . C40 C 0.6862(2) 0.7821(4) 0.5006(2) 0.0252(13) Uani 1 1 d . . . . . C10 C 0.5313(2) 0.9235(5) 0.4420(2) 0.0283(14) Uani 1 1 d . . . . . C66 C 0.6056(3) 1.2527(5) 0.4455(3) 0.0319(15) Uani 1 1 d . . . . . H66 H 0.631408 1.264598 0.426810 0.038 Uiso 1 1 calc R U . . . C1 C 0.5752(2) 0.5581(5) 0.4527(3) 0.0304(15) Uani 1 1 d . . . . . C34 C 0.7057(2) 0.9817(4) 0.4602(2) 0.0281(14) Uani 1 1 d . . . . . H34 H 0.714193 0.961879 0.488955 0.034 Uiso 1 1 calc R U . . . C29 C 0.6322(2) 1.0035(5) 0.3089(2) 0.0283(14) Uani 1 1 d . . . . . C54 C 0.8020(2) 1.1099(5) 0.5421(3) 0.0349(16) Uani 1 1 d . . . . . H54 H 0.831633 1.087068 0.533404 0.042 Uiso 1 1 calc R U . . . C25 C 0.5906(2) 0.8549(4) 0.3156(2) 0.0255(14) Uani 1 1 d . . . . . C83 C 0.6204(2) 0.9758(4) 0.7030(2) 0.0266(13) Uani 1 1 d . . . . . C116 C 0.2725(2) 1.1684(4) 0.4271(2) 0.0277(13) Uani 1 1 d . . . . . H116 H 0.283973 1.178294 0.456049 0.033 Uiso 1 1 calc R U . . . C67 C 0.5610(3) 1.2503(5) 0.4282(3) 0.0343(15) Uani 1 1 d . . . . . H67 H 0.556342 1.260535 0.397666 0.041 Uiso 1 1 calc R U . . . C91 C 0.7240(2) 1.2771(4) 0.6967(2) 0.0282(14) Uani 1 1 d . . . . . C35 C 0.68687(19) 0.9189(4) 0.4301(2) 0.0258(14) Uani 1 1 d . . . . . C46 C 0.7226(2) 0.7365(5) 0.4155(2) 0.0268(14) Uani 1 1 d . . . . . C42 C 0.7395(2) 0.7706(5) 0.5616(3) 0.0320(16) Uani 1 1 d . . . . . H42 H 0.770358 0.769866 0.572776 0.038 Uiso 1 1 calc R U . . . C43 C 0.7024(2) 0.7592(5) 0.5901(3) 0.0320(15) Uani 1 1 d . . . . . H43 H 0.707985 0.751715 0.620692 0.038 Uiso 1 1 calc R U . . . C139 C 0.3718(2) 0.7172(5) 0.5547(3) 0.0344(16) Uani 1 1 d . . . . . C47 C 0.7334(2) 0.6435(5) 0.4276(3) 0.0315(15) Uani 1 1 d . . . . . H47 H 0.716868 0.614817 0.451055 0.038 Uiso 1 1 calc R U . . . C100 C 0.5546(3) 1.4188(6) 0.7384(3) 0.0425(18) Uani 1 1 d . . . . . H100 H 0.530455 1.456771 0.749942 0.051 Uiso 1 1 calc R U . . . C79 C 0.5561(2) 0.8936(4) 0.6031(3) 0.0291(14) Uani 1 1 d . . . . . H79 H 0.551259 0.829319 0.608780 0.035 Uiso 1 1 calc R U . . . C11 C 0.5693(2) 0.9861(5) 0.4274(3) 0.0339(16) Uani 1 1 d . . . . . H11A H 0.575265 0.976422 0.395965 0.051 Uiso 1 1 calc R U . . . H11B H 0.597589 0.972368 0.444173 0.051 Uiso 1 1 calc R U . . . H11C H 0.560172 1.050953 0.432400 0.051 Uiso 1 1 calc R U . . . C41 C 0.7320(2) 0.7830(5) 0.5172(2) 0.0282(15) Uani 1 1 d . . . . . H41 H 0.757547 0.792044 0.497910 0.034 Uiso 1 1 calc R U . . . C26 C 0.5641(2) 0.8775(5) 0.2792(3) 0.0325(15) Uani 1 1 d . . . . . H26 H 0.540042 0.836961 0.269533 0.039 Uiso 1 1 calc R U . . . C36 C 0.6743(2) 0.9520(4) 0.3888(2) 0.0241(13) Uani 1 1 d . . . . . C9 C 0.4876(2) 0.9581(5) 0.4522(3) 0.0317(15) Uani 1 1 d . . . . . H9 H 0.481335 1.022736 0.449206 0.038 Uiso 1 1 calc R U . . . C145 C 0.4384(2) 0.6897(5) 0.6147(3) 0.0320(15) Uani 1 1 d . . . . . C45 C 0.6490(2) 0.7693(5) 0.5298(2) 0.0281(14) Uani 1 1 d . . . . . H45 H 0.618026 0.767941 0.518926 0.034 Uiso 1 1 calc R U . . . C64 C 0.5749(2) 1.2214(4) 0.5179(2) 0.0225(13) Uani 1 1 d . . . . . C48 C 0.7673(2) 0.5944(5) 0.4059(3) 0.0394(19) Uani 1 1 d . . . . . H48 H 0.773830 0.532110 0.414393 0.047 Uiso 1 1 calc R U . . . C38 C 0.6432(3) 1.1702(5) 0.3298(3) 0.0409(17) Uani 1 1 d . . . . . H38A H 0.637926 1.191093 0.299510 0.061 Uiso 1 1 calc R U . . . H38B H 0.663339 1.214709 0.345016 0.061 Uiso 1 1 calc R U . . . H38C H 0.613295 1.165999 0.345223 0.061 Uiso 1 1 calc R U . . . C71 C 0.5209(2) 1.3512(5) 0.5837(3) 0.0339(16) Uani 1 1 d . . . . . H71 H 0.537657 1.377191 0.559702 0.041 Uiso 1 1 calc R U . . . C146 C 0.4499(3) 0.6428(5) 0.6529(3) 0.0412(17) Uani 1 1 d . . . . . H146 H 0.426924 0.636154 0.675121 0.049 Uiso 1 1 calc R U . . . C121 C 0.3519(2) 1.3312(5) 0.3764(3) 0.0365(17) Uani 1 1 d . . . . . C87 C 0.6865(2) 1.0015(5) 0.7510(3) 0.0329(15) Uani 1 1 d . . . . . H87 H 0.706550 0.979118 0.773506 0.039 Uiso 1 1 calc R U . . . C2 C 0.5444(3) 0.4893(5) 0.4657(3) 0.0361(16) Uani 1 1 d . . . . . H2 H 0.554099 0.426216 0.467313 0.043 Uiso 1 1 calc R U . . . C82 C 0.5791(2) 0.9217(5) 0.6846(2) 0.0283(14) Uani 1 1 d . . . . . C114 C 0.3767(2) 1.1396(5) 0.4705(3) 0.0334(15) Uani 1 1 d . . . . . H114 H 0.365055 1.084835 0.456912 0.040 Uiso 1 1 calc R U . . . C81 C 0.5538(2) 1.0218(5) 0.5525(2) 0.0269(14) Uani 1 1 d . . . . . H81 H 0.547124 1.045434 0.524010 0.032 Uiso 1 1 calc R U . . . C75 C 0.5100(2) 1.2284(5) 0.6360(3) 0.0320(14) Uani 1 1 d . . . . . H75 H 0.518933 1.170376 0.648429 0.038 Uiso 1 1 calc R U . . . C70 C 0.53476(18) 1.2651(4) 0.6010(2) 0.0243(13) Uani 1 1 d . . . . . C28 C 0.6054(2) 1.0219(5) 0.2713(3) 0.0346(16) Uani 1 1 d . . . . . H28 H 0.610082 1.078449 0.255646 0.041 Uiso 1 1 calc R U . . . C119 C 0.2367(2) 1.1399(5) 0.3441(3) 0.0359(16) Uani 1 1 d . . . . . H119 H 0.224576 1.129650 0.315402 0.043 Uiso 1 1 calc R U . . . C127 C 0.3490(2) 0.6995(5) 0.6417(3) 0.0333(15) Uani 1 1 d . . . . . C148 C 0.5285(2) 0.6132(5) 0.6278(3) 0.0425(19) Uani 1 1 d . . . . . H148 H 0.558707 0.588606 0.632654 0.051 Uiso 1 1 calc R U . . . C120 C 0.2822(2) 1.1700(5) 0.3495(3) 0.0324(15) Uani 1 1 d . . . . . H120 H 0.300577 1.181350 0.324058 0.039 Uiso 1 1 calc R U . . . C13 C 0.5213(2) 0.7205(5) 0.3463(2) 0.0355(16) Uani 1 1 d . . . . . C149 C 0.5181(2) 0.6574(5) 0.5892(3) 0.0403(19) Uani 1 1 d . . . . . H149 H 0.540956 0.662350 0.566708 0.048 Uiso 1 1 calc R U . . . C85 C 0.6632(2) 1.1240(4) 0.7010(2) 0.0256(13) Uani 1 1 d . . . . . C80 C 0.5470(2) 0.9275(5) 0.5619(2) 0.0300(15) Uani 1 1 d . . . . . H80 H 0.536120 0.886731 0.539602 0.036 Uiso 1 1 calc R U . . . C101 C 0.5882(3) 1.4560(5) 0.7109(3) 0.0410(17) Uani 1 1 d . . . . . H101 H 0.587690 1.520751 0.704523 0.049 Uiso 1 1 calc R U . . . C53 C 0.7683(2) 1.0503(5) 0.5554(2) 0.0287(14) Uani 1 1 d . . . . . H53 H 0.774112 0.985194 0.555344 0.034 Uiso 1 1 calc R U . . . C31 C 0.6801(2) 1.0438(4) 0.3751(2) 0.0270(14) Uani 1 1 d . . . . . C74 C 0.4717(3) 1.2768(6) 0.6531(3) 0.0407(17) Uani 1 1 d . . . . . H74 H 0.454732 1.251296 0.677067 0.049 Uiso 1 1 calc R U . . . C115 C 0.3022(2) 1.1842(4) 0.3912(3) 0.0303(15) Uani 1 1 d . . . . . C117 C 0.2265(2) 1.1385(5) 0.4215(3) 0.0326(15) Uani 1 1 d . . . . . H117 H 0.207533 1.127923 0.446646 0.039 Uiso 1 1 calc R U . . . C4 C 0.4861(3) 0.6060(5) 0.4743(3) 0.0400(18) Uani 1 1 d . . . . . H4 H 0.455252 0.623976 0.481387 0.048 Uiso 1 1 calc R U . . . C52 C 0.7252(2) 1.0832(4) 0.5690(2) 0.0232(13) Uani 1 1 d . . . . . C118 C 0.2088(2) 1.1246(5) 0.3810(3) 0.0364(17) Uani 1 1 d . . . . . H118 H 0.177488 1.104640 0.377567 0.044 Uiso 1 1 calc R U . . . C113 C 0.3948(2) 1.1321(6) 0.5127(3) 0.0363(17) Uani 1 1 d . . . . . H113 H 0.395453 1.073457 0.527162 0.044 Uiso 1 1 calc R U . . . C151 C 0.8081(3) 1.1105(6) 0.1873(3) 0.0442(19) Uani 1 1 d . . . . . C129 C 0.2856(3) 0.5946(6) 0.6630(3) 0.047(2) Uani 1 1 d . . . . . H129 H 0.265487 0.544758 0.655212 0.057 Uiso 1 1 calc R U . . . C60 C 0.7069(2) 1.5157(5) 0.5510(3) 0.0324(15) Uani 1 1 d . . . . . H60 H 0.695626 1.577686 0.548975 0.039 Uiso 1 1 calc R U . . . C98 C 0.5917(2) 1.2691(5) 0.7312(3) 0.0342(15) Uani 1 1 d . . . . . H98 H 0.593226 1.204968 0.738576 0.041 Uiso 1 1 calc R U . . . C110 C 0.3932(2) 1.3007(5) 0.4687(3) 0.0333(15) Uani 1 1 d . . . . . H110 H 0.393584 1.359059 0.453932 0.040 Uiso 1 1 calc R U . . . C62 C 0.6281(2) 1.4646(5) 0.5770(3) 0.0334(15) Uani 1 1 d . . . . . H62A H 0.626777 1.520455 0.595406 0.050 Uiso 1 1 calc R U . . . H62B H 0.614979 1.411733 0.593119 0.050 Uiso 1 1 calc R U . . . H62C H 0.610081 1.474948 0.550007 0.050 Uiso 1 1 calc R U . . . C32 C 0.6998(2) 1.1046(5) 0.4057(3) 0.0318(15) Uani 1 1 d . . . . . H32 H 0.704973 1.167793 0.397929 0.038 Uiso 1 1 calc R U . . . C58 C 0.7676(2) 1.4052(5) 0.5418(2) 0.0272(14) Uani 1 1 d . . . . . H58 H 0.798655 1.389792 0.533969 0.033 Uiso 1 1 calc R U . . . C84 C 0.6276(2) 1.0661(4) 0.6879(2) 0.0243(13) Uani 1 1 d . . . . . C59 C 0.7526(2) 1.4952(5) 0.5400(3) 0.0345(16) Uani 1 1 d . . . . . H59 H 0.773239 1.543382 0.531273 0.041 Uiso 1 1 calc R U . . . C122 C 0.3233(3) 1.3954(5) 0.3971(3) 0.0422(19) Uani 1 1 d . . . . . H122 H 0.308854 1.376863 0.423763 0.051 Uiso 1 1 calc R U . . . C92 C 0.7282(3) 1.3174(6) 0.7381(3) 0.0432(18) Uani 1 1 d . . . . . H92 H 0.701078 1.331694 0.754570 0.052 Uiso 1 1 calc R U . . . C33 C 0.7119(2) 1.0739(5) 0.4474(3) 0.0339(16) Uani 1 1 d . . . . . H33 H 0.724723 1.116910 0.467781 0.041 Uiso 1 1 calc R U . . . C89 C 0.5863(3) 0.8155(5) 0.6898(3) 0.0355(16) Uani 1 1 d . . . . . H89A H 0.587459 0.799712 0.721199 0.053 Uiso 1 1 calc R U . . . H89B H 0.615534 0.797263 0.675738 0.053 Uiso 1 1 calc R U . . . H89C H 0.560385 0.782349 0.675922 0.053 Uiso 1 1 calc R U . . . C27 C 0.5728(2) 0.9602(5) 0.2567(3) 0.0362(17) Uani 1 1 d . . . . . H27 H 0.555687 0.973889 0.230744 0.043 Uiso 1 1 calc R U . . . C112 C 0.4118(2) 1.2104(6) 0.5336(3) 0.0398(18) Uani 1 1 d . . . . . H112 H 0.423683 1.206905 0.562687 0.048 Uiso 1 1 calc R U . . . C63 C 0.6879(2) 1.0197(4) 0.5843(3) 0.0331(16) Uani 1 1 d . . . . . H63A H 0.677219 1.039193 0.613480 0.050 Uiso 1 1 calc R U . . . H63B H 0.700005 0.956015 0.585886 0.050 Uiso 1 1 calc R U . . . H63C H 0.661829 1.021835 0.563534 0.050 Uiso 1 1 calc R U . . . C103 C 0.3937(2) 1.1605(5) 0.3688(2) 0.0338(15) Uani 1 1 d . . . . . C19 C 0.6117(5) 0.6645(7) 0.3120(4) 0.0687(12) Uani 1 1 d . . . . . C111 C 0.4110(2) 1.2955(6) 0.5106(3) 0.0363(17) Uani 1 1 d . . . . . H111 H 0.422857 1.349976 0.524264 0.044 Uiso 1 1 calc R U . . . C109 C 0.3745(2) 1.2232(5) 0.4467(2) 0.0298(14) Uani 1 1 d . . . . . C130 C 0.2811(2) 0.6372(6) 0.7028(3) 0.046(2) Uani 1 1 d . . . . . H130 H 0.258100 0.616887 0.723095 0.055 Uiso 1 1 calc R U . . . C8 C 0.4533(2) 0.8989(5) 0.4668(3) 0.0365(16) Uani 1 1 d . . . . . H8 H 0.423508 0.922508 0.474361 0.044 Uiso 1 1 calc R U . . . C90 C 0.5351(2) 0.9503(6) 0.7104(3) 0.0373(17) Uani 1 1 d . . . . . H90A H 0.508102 0.916973 0.698632 0.056 Uiso 1 1 calc R U . . . H90B H 0.530174 1.017509 0.707393 0.056 Uiso 1 1 calc R U . . . H90C H 0.539107 0.934667 0.741562 0.056 Uiso 1 1 calc R U . . . C44 C 0.6572(2) 0.7586(4) 0.5743(3) 0.0320(16) Uani 1 1 d . . . . . H44 H 0.631908 0.750919 0.594072 0.038 Uiso 1 1 calc R U . . . C3 C 0.4993(3) 0.5138(5) 0.4764(3) 0.0414(19) Uani 1 1 d . . . . . H3 H 0.477561 0.467515 0.485017 0.050 Uiso 1 1 calc R U . . . C102 C 0.6218(3) 1.4017(5) 0.6928(3) 0.0383(17) Uani 1 1 d . . . . . H102 H 0.643732 1.428543 0.673163 0.046 Uiso 1 1 calc R U . . . C99 C 0.5569(3) 1.3242(6) 0.7488(3) 0.0423(18) Uani 1 1 d . . . . . H99 H 0.534477 1.297595 0.768104 0.051 Uiso 1 1 calc R U . . . C147 C 0.4942(3) 0.6044(7) 0.6601(3) 0.050(2) Uani 1 1 d . . . . . H147 H 0.500864 0.572810 0.686854 0.060 Uiso 1 1 calc R U . . . C140 C 0.3563(2) 0.7861(6) 0.5249(3) 0.0394(17) Uani 1 1 d . . . . . H140 H 0.353851 0.848459 0.534971 0.047 Uiso 1 1 calc R U . . . C126 C 0.3718(3) 1.3612(7) 0.3369(3) 0.054(2) Uani 1 1 d . . . . . H126 H 0.391170 1.320457 0.320522 0.065 Uiso 1 1 calc R U . . . C128 C 0.3200(2) 0.6246(5) 0.6335(3) 0.0388(17) Uani 1 1 d . . . . . H128 H 0.323554 0.591764 0.606578 0.047 Uiso 1 1 calc R U . . . C137 C 0.4359(3) 0.9966(5) 0.6245(3) 0.045(2) Uani 1 1 d . . . . . H137 H 0.465383 1.025989 0.626874 0.053 Uiso 1 1 calc R U . . . C14 C 0.5079(4) 0.6280(7) 0.3498(3) 0.059(3) Uani 1 1 d . . . . . H14 H 0.530314 0.579866 0.346567 0.071 Uiso 1 1 calc R U . . . C7 C 0.4626(2) 0.8054(5) 0.4703(3) 0.0296(14) Uani 1 1 d . . . . . H7 H 0.439266 0.763284 0.480105 0.036 Uiso 1 1 calc R U . . . C49 C 0.7923(3) 0.6352(6) 0.3714(3) 0.0450(19) Uani 1 1 d . . . . . H49 H 0.815683 0.601011 0.356344 0.054 Uiso 1 1 calc R U . . . C93 C 0.7717(3) 1.3370(6) 0.7556(3) 0.056(2) Uani 1 1 d . . . . . H93 H 0.774357 1.361266 0.784583 0.067 Uiso 1 1 calc R U . . . C6 C 0.5067(2) 0.7737(5) 0.4593(2) 0.0255(13) Uani 1 1 d . . . . . C65 C 0.6124(2) 1.2378(4) 0.4901(2) 0.0284(14) Uani 1 1 d . . . . . H65 H 0.642985 1.238769 0.501841 0.034 Uiso 1 1 calc R U . . . C51 C 0.7481(2) 0.7753(5) 0.3812(3) 0.0324(15) Uani 1 1 d . . . . . H51 H 0.741558 0.837289 0.372274 0.039 Uiso 1 1 calc R U . . . C104 C 0.3845(3) 1.0720(6) 0.3517(3) 0.0482(19) Uani 1 1 d . . . . . H104 H 0.353613 1.048657 0.352980 0.058 Uiso 1 1 calc R U . . . C73 C 0.4584(2) 1.3611(5) 0.6355(3) 0.0428(18) Uani 1 1 d . . . . . H73 H 0.432223 1.392998 0.647087 0.051 Uiso 1 1 calc R U . . . C106 C 0.4646(3) 1.0481(9) 0.3317(3) 0.065(3) Uani 1 1 d . . . . . H106 H 0.488342 1.010017 0.319454 0.078 Uiso 1 1 calc R U . . . C18 C 0.4883(3) 0.7896(7) 0.3516(3) 0.0453(19) Uani 1 1 d . . . . . H18 H 0.496923 0.853233 0.349537 0.054 Uiso 1 1 calc R U . . . C134 C 0.3519(2) 0.9091(5) 0.6165(3) 0.0407(18) Uani 1 1 d . . . . . H134 H 0.322331 0.880385 0.613056 0.049 Uiso 1 1 calc R U . . . C150 C 0.4736(2) 0.6954(5) 0.5827(3) 0.0368(17) Uani 1 1 d . . . . . H150 H 0.467093 0.726062 0.555731 0.044 Uiso 1 1 calc R U . . . C133 C 0.3914(2) 0.8531(5) 0.6135(3) 0.0342(15) Uani 1 1 d . . . . . C136 C 0.3959(3) 1.0485(5) 0.6281(3) 0.0400(17) Uani 1 1 d . . . . . H136 H 0.397368 1.113639 0.633300 0.048 Uiso 1 1 calc R U . . . C138 C 0.4333(2) 0.9008(5) 0.6174(3) 0.0361(16) Uani 1 1 d . . . . . H138 H 0.461463 0.866599 0.615202 0.043 Uiso 1 1 calc R U . . . C144 C 0.3747(2) 0.6279(6) 0.5367(3) 0.0419(19) Uani 1 1 d . . . . . H144 H 0.385910 0.579009 0.554923 0.050 Uiso 1 1 calc R U . . . C37 C 0.7113(3) 1.0799(6) 0.3006(3) 0.0403(18) Uani 1 1 d . . . . . H37A H 0.726677 1.019065 0.300259 0.060 Uiso 1 1 calc R U . . . H37B H 0.732418 1.126502 0.313008 0.060 Uiso 1 1 calc R U . . . H37C H 0.702931 1.097661 0.270474 0.060 Uiso 1 1 calc R U . . . C72 C 0.4830(2) 1.3992(5) 0.6011(3) 0.0382(17) Uani 1 1 d . . . . . H72 H 0.474201 1.457776 0.589257 0.046 Uiso 1 1 calc R U . . . C105 C 0.4186(4) 1.0176(7) 0.3329(4) 0.063(3) Uani 1 1 d . . . . . H105 H 0.410743 0.958767 0.320702 0.076 Uiso 1 1 calc R U . . . C50 C 0.7825(3) 0.7262(6) 0.3597(3) 0.0428(19) Uani 1 1 d . . . . . H50 H 0.799584 0.755079 0.336689 0.051 Uiso 1 1 calc R U . . . C132 C 0.3435(3) 0.7403(5) 0.6828(3) 0.0415(18) Uani 1 1 d . . . . . H132 H 0.363193 0.790646 0.690725 0.050 Uiso 1 1 calc R U . . . C96 C 0.7634(2) 1.2606(6) 0.6724(3) 0.0418(19) Uani 1 1 d . . . . . H96 H 0.760822 1.233545 0.644023 0.050 Uiso 1 1 calc R U . . . C108 C 0.4407(3) 1.1882(7) 0.3670(3) 0.0468(19) Uani 1 1 d . . . . . H108 H 0.448968 1.246884 0.379083 0.056 Uiso 1 1 calc R U . . . C141 C 0.3445(2) 0.7667(8) 0.4818(3) 0.052(2) Uani 1 1 d . . . . . H141 H 0.334587 0.815668 0.463040 0.063 Uiso 1 1 calc R U . . . C107 C 0.4749(3) 1.1347(8) 0.3486(3) 0.057(2) Uani 1 1 d . . . . . H107 H 0.505921 1.157293 0.347529 0.068 Uiso 1 1 calc R U . . . C135 C 0.3532(3) 1.0036(5) 0.6241(3) 0.0432(19) Uani 1 1 d . . . . . H135 H 0.325125 1.037982 0.626578 0.052 Uiso 1 1 calc R U . . . C12 C 0.6243(3) 0.5353(5) 0.4403(4) 0.050(2) Uani 1 1 d . . . . . H12A H 0.645526 0.561821 0.462222 0.075 Uiso 1 1 calc R U . . . H12B H 0.631216 0.561631 0.411324 0.075 Uiso 1 1 calc R U . . . H12C H 0.628209 0.467617 0.439411 0.075 Uiso 1 1 calc R U . . . C131 C 0.3100(3) 0.7099(6) 0.7132(3) 0.047(2) Uani 1 1 d . . . . . H131 H 0.307379 0.739678 0.741049 0.056 Uiso 1 1 calc R U . . . C20 C 0.6560(5) 0.6346(7) 0.3221(4) 0.0687(12) Uani 1 1 d . . . . . H20 H 0.669616 0.652990 0.349259 0.082 Uiso 1 1 calc R U . . . C94 C 0.8113(3) 1.3212(6) 0.7308(3) 0.054(2) Uani 1 1 d . . . . . H94 H 0.840954 1.336399 0.742456 0.065 Uiso 1 1 calc R U . . . C123 C 0.3142(3) 1.4839(6) 0.3821(4) 0.059(3) Uani 1 1 d . . . . . H123 H 0.294493 1.524566 0.398194 0.071 Uiso 1 1 calc R U . . . C152 C 0.8086(3) 1.1636(8) 0.2294(4) 0.063(2) Uani 1 1 d . . . . . H15A H 0.840693 1.180247 0.236894 0.094 Uiso 1 1 calc R U . . . H15B H 0.795402 1.125119 0.252924 0.094 Uiso 1 1 calc R U . . . H15C H 0.790045 1.220381 0.226121 0.094 Uiso 1 1 calc R U . . . C95 C 0.8078(3) 1.2833(8) 0.6892(4) 0.063(3) Uani 1 1 d . . . . . H95 H 0.834890 1.272751 0.671988 0.075 Uiso 1 1 calc R U . . . C125 C 0.3630(4) 1.4534(8) 0.3212(4) 0.073(4) Uani 1 1 d . . . . . H125 H 0.377508 1.473789 0.294844 0.087 Uiso 1 1 calc R U . . . C142 C 0.3470(3) 0.6761(9) 0.4657(3) 0.059(3) Uani 1 1 d . . . . . H142 H 0.338531 0.662578 0.436108 0.071 Uiso 1 1 calc R U . . . C124 C 0.3342(4) 1.5123(7) 0.3432(4) 0.066(3) Uani 1 1 d . . . . . H124 H 0.328047 1.572630 0.331804 0.079 Uiso 1 1 calc R U . . . B2 B 0.3876(2) 0.7397(5) 0.6059(3) 0.0308(17) Uani 1 1 d . . . . . C143 C 0.3620(3) 0.6064(7) 0.4936(4) 0.055(2) Uani 1 1 d . . . . . H143 H 0.363658 0.543990 0.483453 0.066 Uiso 1 1 calc R U . . . B1 B 0.3554(3) 1.2240(5) 0.3957(3) 0.0304(16) Uani 1 1 d . . . . . C17 C 0.4421(3) 0.7646(10) 0.3601(4) 0.072(3) Uani 1 1 d . . . . . H17 H 0.419634 0.812518 0.363669 0.086 Uiso 1 1 calc R U . . . C24 C 0.5909(5) 0.6380(7) 0.2722(4) 0.0687(12) Uani 1 1 d . . . . . H24 H 0.560815 0.660068 0.264669 0.082 Uiso 1 1 calc R U . . . C15 C 0.4610(5) 0.6058(10) 0.3582(3) 0.079(4) Uani 1 1 d . . . . . H15 H 0.451697 0.542549 0.360443 0.095 Uiso 1 1 calc R U . . . C153 C 0.7643(3) 1.0587(8) 0.1764(4) 0.066(3) Uani 1 1 d . . . . . H15D H 0.739221 1.103308 0.170614 0.099 Uiso 1 1 calc R U . . . H15E H 0.755607 1.018993 0.201328 0.099 Uiso 1 1 calc R U . . . H15F H 0.769352 1.020122 0.150293 0.099 Uiso 1 1 calc R U . . . C16 C 0.4284(4) 0.6760(12) 0.3633(4) 0.083(4) Uani 1 1 d . . . . . H16 H 0.396708 0.661338 0.368969 0.100 Uiso 1 1 calc R U . . . C21 C 0.6811(5) 0.5786(7) 0.2938(4) 0.0687(12) Uani 1 1 d . . . . . H21 H 0.711359 0.557586 0.301640 0.082 Uiso 1 1 calc R U . . . C22 C 0.6621(5) 0.5540(7) 0.2548(4) 0.0687(12) Uani 1 1 d . . . . . H22 H 0.680120 0.519742 0.234200 0.082 Uiso 1 1 calc R U . . . C23 C 0.6149(5) 0.5790(7) 0.2438(4) 0.0687(12) Uani 1 1 d . . . . . H23 H 0.600580 0.555671 0.217910 0.082 Uiso 1 1 calc R U . . . C154 C 0.5412(9) 0.367(2) 0.3005(11) 0.110(5) Uiso 0.4 1 d D . P . . C155 C 0.5312(14) 0.290(3) 0.2698(12) 0.110(5) Uiso 0.4 1 d D . P . . H15G H 0.525281 0.233083 0.285413 0.166 Uiso 0.4 1 d R U P . . H15H H 0.503991 0.307413 0.253483 0.166 Uiso 0.4 1 d R U P . . H15I H 0.556741 0.280973 0.249893 0.166 Uiso 0.4 1 d R U P . . O4 O 0.5099(9) 0.3816(19) 0.3253(9) 0.110(5) Uiso 0.4 1 d D . P . . C156 C 0.5851(10) 0.383(3) 0.3243(14) 0.110(5) Uiso 0.4 1 d D . P . . H15J H 0.598346 0.329005 0.337680 0.166 Uiso 0.4 1 d R U P . . H15K H 0.603006 0.400165 0.298820 0.166 Uiso 0.4 1 d R U P . . H15L H 0.585566 0.433915 0.345030 0.166 Uiso 0.4 1 d R U P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.0216(4) 0.0227(4) 0.0241(5) -0.0008(4) 0.0022(4) -0.0022(3) Cu2 0.0204(3) 0.0230(4) 0.0204(5) -0.0006(4) 0.0007(3) -0.0016(3) P2 0.0223(6) 0.0200(7) 0.0226(9) 0.0009(6) 0.0015(6) -0.0019(5) P3 0.0199(6) 0.0227(7) 0.0201(9) -0.0005(6) 0.0002(6) -0.0015(5) P4 0.0252(6) 0.0255(8) 0.0177(9) -0.0009(6) -0.0017(6) -0.0048(6) P1 0.0278(7) 0.0250(8) 0.0230(10) -0.0025(6) 0.0007(6) -0.0016(6) O2 0.0258(18) 0.022(2) 0.020(2) 0.0002(17) -0.0059(16) -0.0027(16) O1 0.0281(19) 0.023(2) 0.024(3) -0.0006(18) -0.0028(17) 0.0007(16) N4 0.019(2) 0.020(2) 0.024(3) 0.000(2) 0.001(2) -0.0013(19) N1 0.027(2) 0.019(2) 0.025(3) 0.001(2) 0.001(2) -0.003(2) O3 0.055(3) 0.054(3) 0.055(4) 0.014(3) 0.013(3) 0.011(3) N2 0.025(2) 0.024(3) 0.021(3) -0.004(2) 0.001(2) -0.001(2) N3 0.023(2) 0.025(3) 0.022(3) 0.000(2) -0.002(2) -0.004(2) C78 0.021(2) 0.025(3) 0.026(4) -0.001(3) 0.001(2) -0.004(2) C88 0.031(3) 0.031(3) 0.028(4) 0.007(3) 0.000(3) 0.003(3) C76 0.016(2) 0.026(3) 0.024(4) 0.002(2) -0.001(2) -0.001(2) C56 0.026(3) 0.026(3) 0.013(3) -0.001(2) -0.002(2) 0.001(2) C68 0.035(3) 0.035(4) 0.032(5) -0.006(3) -0.008(3) 0.006(3) C77 0.020(2) 0.022(3) 0.029(4) -0.007(3) 0.004(2) -0.003(2) C39 0.025(3) 0.024(3) 0.023(4) -0.001(3) 0.006(2) 0.007(2) C5 0.024(3) 0.027(3) 0.027(4) -0.006(3) -0.002(3) -0.004(2) C97 0.035(3) 0.033(3) 0.019(4) 0.002(3) -0.003(3) 0.007(3) C86 0.029(3) 0.033(3) 0.026(4) 0.001(3) -0.003(3) -0.002(3) C55 0.024(3) 0.027(3) 0.034(4) 0.003(3) 0.003(3) 0.000(2) C61 0.029(3) 0.027(3) 0.023(4) -0.001(3) -0.003(2) -0.003(3) C57 0.023(2) 0.022(3) 0.019(4) -0.003(2) 0.000(2) 0.001(2) C30 0.035(3) 0.030(3) 0.029(4) 0.007(3) 0.012(3) -0.001(3) C69 0.023(3) 0.032(3) 0.032(4) -0.005(3) -0.001(3) 0.004(2) C40 0.024(3) 0.019(3) 0.032(4) 0.007(3) -0.003(3) -0.001(2) C10 0.029(3) 0.026(3) 0.030(4) -0.004(3) 0.001(3) 0.003(3) C66 0.039(3) 0.033(4) 0.023(4) -0.001(3) 0.008(3) 0.002(3) C1 0.028(3) 0.026(3) 0.038(5) 0.000(3) 0.002(3) -0.001(3) C34 0.032(3) 0.025(3) 0.028(4) -0.003(3) -0.001(3) -0.001(3) C29 0.026(3) 0.030(3) 0.028(4) 0.002(3) 0.008(3) 0.003(3) C54 0.026(3) 0.035(4) 0.043(5) 0.004(3) 0.007(3) 0.008(3) C25 0.026(3) 0.028(3) 0.023(4) -0.001(3) 0.004(2) 0.008(2) C83 0.029(3) 0.024(3) 0.027(4) 0.001(3) 0.003(3) -0.001(2) C116 0.031(3) 0.027(3) 0.025(4) -0.001(3) -0.001(3) 0.006(2) C67 0.055(4) 0.029(3) 0.019(4) -0.001(3) 0.000(3) 0.004(3) C91 0.038(3) 0.023(3) 0.024(4) 0.004(3) -0.007(3) -0.010(3) C35 0.021(2) 0.025(3) 0.032(4) -0.002(3) 0.001(2) 0.000(2) C46 0.025(3) 0.026(3) 0.029(4) 0.001(3) -0.001(3) -0.002(2) C42 0.030(3) 0.026(3) 0.040(5) 0.001(3) -0.006(3) 0.001(3) C43 0.042(3) 0.029(3) 0.025(4) 0.000(3) -0.006(3) 0.003(3) C139 0.017(3) 0.045(4) 0.041(5) 0.003(3) 0.001(3) -0.004(3) C47 0.027(3) 0.027(3) 0.040(5) 0.004(3) -0.003(3) -0.004(2) C100 0.047(4) 0.045(4) 0.036(5) -0.005(3) 0.005(3) 0.013(3) C79 0.030(3) 0.022(3) 0.035(4) -0.006(3) 0.000(3) -0.003(2) C11 0.038(3) 0.025(3) 0.039(5) -0.004(3) 0.012(3) 0.000(3) C41 0.021(3) 0.031(3) 0.033(4) 0.004(3) 0.000(2) -0.001(2) C26 0.027(3) 0.037(4) 0.033(4) -0.004(3) 0.000(3) 0.002(3) C36 0.024(3) 0.023(3) 0.025(4) -0.006(3) 0.005(2) 0.001(2) C9 0.036(3) 0.027(3) 0.032(4) -0.004(3) 0.001(3) 0.002(3) C145 0.031(3) 0.028(3) 0.038(5) -0.008(3) 0.000(3) -0.006(3) C45 0.022(3) 0.033(3) 0.030(4) 0.003(3) 0.004(2) 0.001(2) C64 0.023(2) 0.021(3) 0.024(4) -0.004(2) -0.001(2) 0.004(2) C48 0.031(3) 0.022(3) 0.066(6) -0.005(3) -0.005(3) 0.003(3) C38 0.056(4) 0.027(3) 0.039(5) 0.004(3) -0.005(4) 0.001(3) C71 0.030(3) 0.029(3) 0.043(5) -0.004(3) -0.004(3) 0.002(3) C146 0.039(3) 0.046(4) 0.038(5) -0.006(3) 0.001(3) 0.008(3) C121 0.032(3) 0.036(4) 0.041(5) 0.003(3) -0.010(3) -0.010(3) C87 0.032(3) 0.030(3) 0.037(4) 0.006(3) -0.004(3) 0.002(3) C2 0.041(3) 0.023(3) 0.044(5) 0.003(3) 0.001(3) -0.002(3) C82 0.033(3) 0.026(3) 0.026(4) 0.001(3) 0.005(3) -0.001(3) C114 0.031(3) 0.040(4) 0.029(4) -0.005(3) 0.002(3) 0.007(3) C81 0.027(3) 0.029(3) 0.025(4) -0.004(3) -0.004(3) -0.004(2) C75 0.031(3) 0.036(3) 0.030(4) -0.007(3) 0.000(3) 0.003(3) C70 0.021(2) 0.030(3) 0.022(4) -0.009(3) -0.003(3) -0.001(2) C28 0.035(3) 0.032(3) 0.037(5) 0.008(3) 0.006(3) 0.009(3) C119 0.041(3) 0.029(3) 0.037(5) -0.005(3) -0.012(3) 0.001(3) C127 0.029(3) 0.031(3) 0.040(5) 0.007(3) -0.006(3) 0.004(3) C148 0.032(3) 0.041(4) 0.055(6) -0.014(4) -0.004(3) 0.008(3) C120 0.038(3) 0.032(3) 0.027(4) -0.001(3) -0.002(3) 0.003(3) C13 0.037(3) 0.051(4) 0.018(4) -0.001(3) -0.001(3) -0.017(3) C149 0.028(3) 0.030(3) 0.063(6) -0.008(3) -0.004(3) 0.004(3) C85 0.027(3) 0.025(3) 0.025(4) 0.000(3) 0.004(2) 0.001(2) C80 0.037(3) 0.028(3) 0.024(4) -0.008(3) 0.000(3) -0.005(3) C101 0.048(4) 0.035(4) 0.040(5) 0.003(3) 0.000(3) 0.006(3) C53 0.031(3) 0.023(3) 0.032(4) -0.001(3) -0.001(3) 0.006(3) C31 0.026(3) 0.024(3) 0.031(4) 0.001(3) 0.004(3) 0.003(2) C74 0.039(3) 0.052(4) 0.032(5) -0.005(4) 0.009(3) 0.002(3) C115 0.032(3) 0.024(3) 0.035(4) 0.001(3) 0.000(3) 0.002(3) C117 0.027(3) 0.030(3) 0.040(5) 0.000(3) 0.005(3) -0.002(2) C4 0.034(3) 0.034(4) 0.051(5) -0.004(3) 0.011(3) -0.007(3) C52 0.025(3) 0.024(3) 0.020(4) -0.003(2) -0.002(2) 0.001(2) C118 0.031(3) 0.029(3) 0.049(5) -0.005(3) -0.003(3) 0.000(3) C113 0.030(3) 0.050(4) 0.030(5) 0.005(3) 0.002(3) 0.010(3) C151 0.046(4) 0.042(4) 0.045(5) 0.019(4) 0.001(4) 0.014(3) C129 0.047(4) 0.051(5) 0.044(6) 0.014(4) -0.010(4) -0.027(4) C60 0.039(3) 0.021(3) 0.037(5) -0.003(3) -0.002(3) -0.004(3) C98 0.041(3) 0.034(3) 0.028(4) -0.003(3) 0.008(3) -0.002(3) C110 0.024(3) 0.045(4) 0.031(4) -0.006(3) 0.004(3) -0.004(3) C62 0.031(3) 0.029(3) 0.040(5) 0.004(3) 0.002(3) 0.004(3) C32 0.035(3) 0.026(3) 0.034(4) 0.002(3) -0.001(3) 0.004(3) C58 0.024(3) 0.027(3) 0.030(4) 0.001(3) 0.004(3) -0.003(2) C84 0.025(3) 0.031(3) 0.017(4) 0.000(3) -0.002(2) 0.002(2) C59 0.035(3) 0.025(3) 0.043(5) 0.001(3) 0.007(3) -0.010(3) C122 0.040(3) 0.032(4) 0.055(6) 0.002(3) -0.012(4) -0.003(3) C92 0.047(4) 0.046(4) 0.037(5) -0.005(3) -0.014(3) -0.004(3) C33 0.038(3) 0.024(3) 0.040(5) -0.008(3) -0.003(3) -0.005(3) C89 0.051(4) 0.028(3) 0.028(4) 0.005(3) -0.006(3) -0.004(3) C27 0.031(3) 0.045(4) 0.033(4) 0.006(3) -0.004(3) 0.014(3) C112 0.023(3) 0.064(5) 0.032(5) 0.000(4) -0.001(3) 0.005(3) C63 0.034(3) 0.020(3) 0.045(5) -0.001(3) 0.006(3) 0.000(3) C103 0.038(3) 0.046(4) 0.017(4) 0.003(3) -0.004(3) 0.010(3) C19 0.111(3) 0.053(2) 0.042(2) -0.0036(17) 0.013(2) 0.036(2) C111 0.024(3) 0.053(4) 0.032(5) -0.010(3) 0.002(3) -0.007(3) C109 0.024(3) 0.038(4) 0.028(4) -0.005(3) 0.003(2) 0.000(3) C130 0.035(3) 0.054(5) 0.048(6) 0.022(4) 0.004(3) 0.004(3) C8 0.027(3) 0.042(4) 0.040(5) -0.003(3) 0.002(3) 0.003(3) C90 0.031(3) 0.049(4) 0.032(5) 0.001(3) 0.006(3) -0.010(3) C44 0.034(3) 0.026(3) 0.036(5) 0.000(3) 0.009(3) 0.002(3) C3 0.037(3) 0.032(4) 0.055(6) -0.001(3) 0.010(3) -0.013(3) C102 0.048(4) 0.036(4) 0.031(5) 0.001(3) -0.003(3) -0.001(3) C99 0.044(4) 0.050(4) 0.033(5) 0.000(3) 0.010(3) -0.003(3) C147 0.054(4) 0.064(5) 0.033(5) -0.005(4) -0.006(4) 0.028(4) C140 0.026(3) 0.056(5) 0.036(5) 0.004(4) 0.002(3) 0.000(3) C126 0.057(5) 0.066(5) 0.038(5) 0.014(4) -0.011(4) -0.022(4) C128 0.040(3) 0.044(4) 0.032(5) 0.008(3) -0.007(3) -0.014(3) C137 0.041(4) 0.033(4) 0.060(6) 0.003(3) -0.002(3) -0.010(3) C14 0.067(5) 0.072(6) 0.039(6) 0.015(4) -0.023(4) -0.041(5) C7 0.025(3) 0.031(3) 0.033(4) -0.001(3) 0.001(3) 0.000(2) C49 0.040(4) 0.041(4) 0.053(6) -0.008(4) 0.012(4) 0.004(3) C93 0.072(6) 0.046(5) 0.050(6) -0.012(4) -0.020(5) -0.017(4) C6 0.025(3) 0.028(3) 0.023(4) -0.002(3) -0.001(2) -0.003(2) C65 0.030(3) 0.027(3) 0.028(4) 0.000(3) 0.001(3) -0.002(3) C51 0.034(3) 0.030(3) 0.033(5) 0.004(3) 0.006(3) 0.005(3) C104 0.053(4) 0.055(5) 0.037(5) -0.007(4) 0.000(4) 0.011(4) C73 0.034(3) 0.046(4) 0.049(5) -0.018(4) 0.004(3) 0.013(3) C106 0.056(5) 0.104(8) 0.033(5) -0.007(5) 0.002(4) 0.044(5) C18 0.034(3) 0.076(6) 0.026(5) -0.007(4) 0.002(3) -0.010(4) C134 0.031(3) 0.040(4) 0.052(5) -0.001(3) -0.005(3) 0.002(3) C150 0.028(3) 0.039(4) 0.044(5) 0.000(3) 0.002(3) -0.003(3) C133 0.033(3) 0.041(4) 0.029(4) -0.001(3) 0.002(3) -0.001(3) C136 0.049(4) 0.035(4) 0.035(5) 0.004(3) 0.002(3) 0.001(3) C138 0.030(3) 0.035(4) 0.043(5) 0.001(3) -0.001(3) -0.003(3) C144 0.030(3) 0.052(5) 0.044(5) -0.014(4) 0.003(3) -0.006(3) C37 0.038(3) 0.046(4) 0.036(5) 0.006(3) 0.008(3) -0.011(3) C72 0.036(3) 0.031(3) 0.047(5) -0.010(3) -0.012(3) 0.008(3) C105 0.079(6) 0.064(6) 0.046(6) -0.014(5) -0.001(5) 0.026(5) C50 0.040(4) 0.044(4) 0.044(5) 0.002(4) 0.017(3) 0.006(3) C132 0.047(4) 0.032(4) 0.045(5) -0.006(3) 0.010(3) -0.006(3) C96 0.033(3) 0.067(5) 0.025(4) -0.003(4) 0.000(3) -0.017(3) C108 0.038(4) 0.077(6) 0.026(5) -0.003(4) -0.003(3) 0.001(4) C141 0.019(3) 0.093(7) 0.044(6) 0.008(5) -0.002(3) -0.002(4) C107 0.039(4) 0.103(8) 0.030(5) -0.003(5) 0.002(3) 0.016(4) C135 0.041(4) 0.036(4) 0.052(6) 0.002(3) -0.002(3) 0.003(3) C12 0.037(3) 0.026(3) 0.088(7) 0.007(4) 0.018(4) 0.004(3) C131 0.059(4) 0.042(4) 0.040(5) -0.003(3) 0.016(4) 0.004(4) C20 0.111(3) 0.053(2) 0.042(2) -0.0036(17) 0.013(2) 0.036(2) C94 0.048(4) 0.066(5) 0.049(6) 0.006(4) -0.021(4) -0.027(4) C123 0.053(5) 0.038(4) 0.086(8) 0.003(5) -0.027(5) -0.008(4) C152 0.057(5) 0.080(7) 0.052(7) 0.003(5) 0.007(4) -0.011(5) C95 0.035(4) 0.104(8) 0.050(6) 0.014(5) -0.008(4) -0.024(4) C125 0.088(7) 0.076(7) 0.053(7) 0.032(6) -0.017(6) -0.047(7) C142 0.029(3) 0.113(9) 0.036(5) -0.017(5) 0.005(3) -0.014(4) C124 0.072(6) 0.039(5) 0.088(9) 0.007(5) -0.028(6) -0.018(5) B2 0.024(3) 0.033(4) 0.035(5) -0.005(3) 0.000(3) -0.006(3) C143 0.036(4) 0.068(6) 0.060(7) -0.022(5) 0.007(4) -0.017(4) B1 0.032(3) 0.030(4) 0.030(5) -0.002(3) -0.001(3) -0.004(3) C17 0.034(4) 0.140(11) 0.042(6) -0.016(6) -0.002(4) -0.016(5) C24 0.111(3) 0.053(2) 0.042(2) -0.0036(17) 0.013(2) 0.036(2) C15 0.089(8) 0.113(9) 0.036(6) 0.027(6) -0.026(5) -0.070(8) C153 0.057(5) 0.086(7) 0.055(7) 0.004(5) 0.006(5) -0.002(5) C16 0.049(5) 0.151(12) 0.050(7) 0.013(7) -0.012(5) -0.058(8) C21 0.111(3) 0.053(2) 0.042(2) -0.0036(17) 0.013(2) 0.036(2) C22 0.111(3) 0.053(2) 0.042(2) -0.0036(17) 0.013(2) 0.036(2) C23 0.111(3) 0.053(2) 0.042(2) -0.0036(17) 0.013(2) 0.036(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P2 Cu1 P1 118.00(7) . . ? N1 Cu1 P2 124.05(16) . . ? N1 Cu1 P1 103.83(16) . . ? N1 Cu1 N2 79.3(2) . . ? N2 Cu1 P2 123.14(15) . . ? N2 Cu1 P1 100.66(16) . . ? P3 Cu2 P4 113.47(7) . . ? N4 Cu2 P3 118.06(15) . . ? N4 Cu2 P4 113.25(16) . . ? N3 Cu2 P3 120.11(15) . . ? N3 Cu2 P4 108.54(16) . . ? N3 Cu2 N4 78.9(2) . . ? C40 P2 Cu1 114.5(2) . . ? C40 P2 C35 105.1(3) . . ? C40 P2 C46 102.9(3) . . ? C35 P2 Cu1 111.92(19) . . ? C35 P2 C46 101.6(3) . . ? C46 P2 Cu1 119.1(2) . . ? C76 P3 Cu2 112.98(18) . . ? C76 P3 C70 102.3(3) . . ? C64 P3 Cu2 114.0(2) . . ? C64 P3 C76 103.5(3) . . ? C64 P3 C70 101.7(3) . . ? C70 P3 Cu2 120.2(2) . . ? C97 P4 Cu2 111.8(2) . . ? C91 P4 Cu2 118.2(2) . . ? C91 P4 C97 104.8(3) . . ? C91 P4 C85 100.6(3) . . ? C85 P4 Cu2 117.0(2) . . ? C85 P4 C97 102.5(3) . . ? C25 P1 Cu1 116.8(2) . . ? C13 P1 Cu1 104.8(2) . . ? C13 P1 C25 105.7(3) . . ? C19 P1 Cu1 122.7(4) . . ? C19 P1 C25 99.7(4) . . ? C19 P1 C13 105.7(5) . . ? C84 O2 C77 116.0(5) . . ? C39 O1 C36 118.5(5) . . ? C61 N4 Cu2 128.6(4) . . ? C61 N4 C57 118.7(5) . . ? C57 N4 Cu2 112.2(4) . . ? C5 N1 Cu1 113.6(4) . . ? C5 N1 C1 118.7(5) . . ? C1 N1 Cu1 127.0(4) . . ? C10 N2 Cu1 127.6(4) . . ? C6 N2 Cu1 112.8(4) . . ? C6 N2 C10 118.8(5) . . ? C56 N3 Cu2 113.3(4) . . ? C56 N3 C52 120.0(5) . . ? C52 N3 Cu2 126.0(4) . . ? C77 C78 C82 118.0(6) . . ? C79 C78 C77 115.5(6) . . ? C79 C78 C82 126.3(6) . . ? C83 C88 H88 119.1 . . ? C87 C88 H88 119.1 . . ? C87 C88 C83 121.8(6) . . ? C77 C76 P3 118.2(5) . . ? C77 C76 C81 117.7(6) . . ? C81 C76 P3 124.0(5) . . ? N3 C56 C55 121.3(6) . . ? N3 C56 C57 116.5(5) . . ? C55 C56 C57 122.1(6) . . ? C69 C68 H68 120.4 . . ? C69 C68 C67 119.1(7) . . ? C67 C68 H68 120.4 . . ? O2 C77 C78 119.1(6) . . ? C76 C77 O2 116.1(5) . . ? C76 C77 C78 124.8(6) . . ? O1 C39 C29 119.7(6) . . ? O1 C39 C25 117.3(6) . . ? C25 C39 C29 123.0(6) . . ? N1 C5 C4 121.9(6) . . ? N1 C5 C6 116.7(6) . . ? C4 C5 C6 121.3(6) . . ? C98 C97 P4 123.2(5) . . ? C102 C97 P4 118.2(6) . . ? C102 C97 C98 118.5(7) . . ? C87 C86 H86 120.2 . . ? C87 C86 C85 119.6(6) . . ? C85 C86 H86 120.2 . . ? C56 C55 H55 120.7 . . ? C56 C55 C54 118.6(6) . . ? C54 C55 H55 120.7 . . ? N4 C61 C60 121.8(6) . . ? N4 C61 C62 118.0(6) . . ? C60 C61 C62 120.2(6) . . ? N4 C57 C56 116.5(5) . . ? N4 C57 C58 121.6(6) . . ? C58 C57 C56 121.9(5) . . ? C29 C30 C37 109.7(6) . . ? C38 C30 C29 108.5(6) . . ? C38 C30 C37 108.7(6) . . ? C31 C30 C29 110.1(5) . . ? C31 C30 C38 111.4(6) . . ? C31 C30 C37 108.4(6) . . ? C68 C69 H69 119.3 . . ? C68 C69 C64 121.3(6) . . ? C64 C69 H69 119.3 . . ? C41 C40 P2 122.2(5) . . ? C45 C40 P2 118.6(5) . . ? C45 C40 C41 119.1(6) . . ? N2 C10 C11 118.2(5) . . ? N2 C10 C9 120.7(6) . . ? C9 C10 C11 121.1(6) . . ? C67 C66 H66 120.1 . . ? C67 C66 C65 119.8(7) . . ? C65 C66 H66 120.1 . . ? N1 C1 C2 121.9(6) . . ? N1 C1 C12 116.9(6) . . ? C2 C1 C12 121.2(6) . . ? C35 C34 H34 120.6 . . ? C33 C34 H34 120.6 . . ? C33 C34 C35 118.8(7) . . ? C39 C29 C30 120.5(6) . . ? C28 C29 C39 116.0(6) . . ? C28 C29 C30 123.5(6) . . ? C55 C54 H54 120.4 . . ? C53 C54 C55 119.1(6) . . ? C53 C54 H54 120.4 . . ? C39 C25 P1 116.9(5) . . ? C26 C25 P1 124.6(5) . . ? C26 C25 C39 118.5(6) . . ? C88 C83 C82 126.6(6) . . ? C84 C83 C88 115.3(6) . . ? C84 C83 C82 118.0(6) . . ? C115 C116 H116 119.0 . . ? C117 C116 H116 119.0 . . ? C117 C116 C115 122.0(7) . . ? C68 C67 H67 119.9 . . ? C66 C67 C68 120.3(7) . . ? C66 C67 H67 119.9 . . ? C92 C91 P4 123.3(6) . . ? C96 C91 P4 117.6(5) . . ? C96 C91 C92 119.0(7) . . ? C34 C35 P2 124.7(5) . . ? C36 C35 P2 117.0(5) . . ? C36 C35 C34 118.2(6) . . ? C47 C46 P2 119.6(5) . . ? C51 C46 P2 123.1(5) . . ? C51 C46 C47 117.1(6) . . ? C43 C42 H42 119.8 . . ? C41 C42 H42 119.8 . . ? C41 C42 C43 120.4(6) . . ? C42 C43 H43 119.7 . . ? C42 C43 C44 120.5(7) . . ? C44 C43 H43 119.7 . . ? C140 C139 B2 123.6(7) . . ? C144 C139 C140 114.4(8) . . ? C144 C139 B2 122.0(7) . . ? C46 C47 H47 119.5 . . ? C48 C47 C46 121.0(7) . . ? C48 C47 H47 119.5 . . ? C101 C100 H100 120.6 . . ? C101 C100 C99 118.7(7) . . ? C99 C100 H100 120.6 . . ? C78 C79 H79 118.9 . . ? C80 C79 C78 122.2(6) . . ? C80 C79 H79 118.9 . . ? C10 C11 H11A 109.5 . . ? C10 C11 H11B 109.5 . . ? C10 C11 H11C 109.5 . . ? H11A C11 H11B 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C40 C41 H41 120.1 . . ? C42 C41 C40 119.7(6) . . ? C42 C41 H41 120.1 . . ? C25 C26 H26 120.2 . . ? C25 C26 C27 119.5(6) . . ? C27 C26 H26 120.2 . . ? O1 C36 C35 114.9(6) . . ? O1 C36 C31 120.8(6) . . ? C35 C36 C31 124.3(6) . . ? C10 C9 H9 120.0 . . ? C8 C9 C10 120.0(6) . . ? C8 C9 H9 120.0 . . ? C146 C145 C150 115.9(6) . . ? C146 C145 B2 124.0(6) . . ? C150 C145 B2 120.1(7) . . ? C40 C45 H45 119.9 . . ? C44 C45 C40 120.2(6) . . ? C44 C45 H45 119.9 . . ? C69 C64 P3 121.9(5) . . ? C65 C64 P3 119.4(5) . . ? C65 C64 C69 118.7(6) . . ? C47 C48 H48 119.7 . . ? C47 C48 C49 120.6(7) . . ? C49 C48 H48 119.7 . . ? C30 C38 H38A 109.5 . . ? C30 C38 H38B 109.5 . . ? C30 C38 H38C 109.5 . . ? H38A C38 H38B 109.5 . . ? H38A C38 H38C 109.5 . . ? H38B C38 H38C 109.5 . . ? C70 C71 H71 119.5 . . ? C72 C71 H71 119.5 . . ? C72 C71 C70 121.1(7) . . ? C145 C146 H146 118.7 . . ? C145 C146 C147 122.6(8) . . ? C147 C146 H146 118.7 . . ? C122 C121 C126 115.2(8) . . ? C122 C121 B1 119.7(7) . . ? C126 C121 B1 124.7(8) . . ? C88 C87 C86 120.9(7) . . ? C88 C87 H87 119.5 . . ? C86 C87 H87 119.5 . . ? C1 C2 H2 120.5 . . ? C3 C2 C1 119.0(6) . . ? C3 C2 H2 120.5 . . ? C78 C82 C83 108.4(5) . . ? C78 C82 C89 112.4(6) . . ? C78 C82 C90 107.8(6) . . ? C83 C82 C89 111.1(6) . . ? C83 C82 C90 108.4(6) . . ? C90 C82 C89 108.6(6) . . ? C113 C114 H114 118.0 . . ? C113 C114 C109 124.0(7) . . ? C109 C114 H114 118.0 . . ? C76 C81 H81 120.3 . . ? C80 C81 C76 119.4(7) . . ? C80 C81 H81 120.3 . . ? C70 C75 H75 120.0 . . ? C70 C75 C74 119.9(7) . . ? C74 C75 H75 120.0 . . ? C71 C70 P3 119.2(6) . . ? C75 C70 P3 122.2(5) . . ? C75 C70 C71 118.6(6) . . ? C29 C28 H28 119.4 . . ? C27 C28 C29 121.2(7) . . ? C27 C28 H28 119.4 . . ? C120 C119 H119 120.1 . . ? C120 C119 C118 119.7(7) . . ? C118 C119 H119 120.1 . . ? C128 C127 C132 114.9(7) . . ? C128 C127 B2 123.9(7) . . ? C132 C127 B2 121.2(6) . . ? C149 C148 H148 120.3 . . ? C149 C148 C147 119.5(7) . . ? C147 C148 H148 120.3 . . ? C119 C120 H120 118.8 . . ? C119 C120 C115 122.5(7) . . ? C115 C120 H120 118.8 . . ? C14 C13 P1 118.3(7) . . ? C18 C13 P1 120.7(6) . . ? C18 C13 C14 119.2(8) . . ? C148 C149 H149 120.1 . . ? C148 C149 C150 119.9(7) . . ? C150 C149 H149 120.1 . . ? C86 C85 P4 124.9(5) . . ? C84 C85 P4 118.2(5) . . ? C84 C85 C86 117.0(6) . . ? C79 C80 C81 120.4(6) . . ? C79 C80 H80 119.8 . . ? C81 C80 H80 119.8 . . ? C100 C101 H101 119.4 . . ? C102 C101 C100 121.2(7) . . ? C102 C101 H101 119.4 . . ? C54 C53 H53 119.6 . . ? C54 C53 C52 120.8(6) . . ? C52 C53 H53 119.6 . . ? C36 C31 C30 121.3(6) . . ? C36 C31 C32 116.1(7) . . ? C32 C31 C30 122.5(6) . . ? C75 C74 H74 119.7 . . ? C73 C74 C75 120.6(8) . . ? C73 C74 H74 119.7 . . ? C116 C115 C120 115.4(6) . . ? C116 C115 B1 124.0(7) . . ? C120 C115 B1 120.5(6) . . ? C116 C117 H117 119.6 . . ? C118 C117 C116 120.8(7) . . ? C118 C117 H117 119.6 . . ? C5 C4 H4 120.5 . . ? C3 C4 C5 119.0(7) . . ? C3 C4 H4 120.5 . . ? N3 C52 C53 120.2(6) . . ? N3 C52 C63 117.9(5) . . ? C53 C52 C63 121.9(6) . . ? C119 C118 H118 120.2 . . ? C117 C118 C119 119.6(6) . . ? C117 C118 H118 120.2 . . ? C114 C113 H113 120.2 . . ? C112 C113 C114 119.5(7) . . ? C112 C113 H113 120.2 . . ? O3 C151 C152 121.6(8) . . ? O3 C151 C153 121.7(9) . . ? C152 C151 C153 116.8(8) . . ? C130 C129 H129 120.1 . . ? C130 C129 C128 119.8(7) . . ? C128 C129 H129 120.1 . . ? C61 C60 H60 120.4 . . ? C59 C60 C61 119.3(6) . . ? C59 C60 H60 120.4 . . ? C97 C98 H98 119.8 . . ? C99 C98 C97 120.4(7) . . ? C99 C98 H98 119.8 . . ? C111 C110 H110 118.7 . . ? C111 C110 C109 122.5(7) . . ? C109 C110 H110 118.7 . . ? C61 C62 H62A 109.5 . . ? C61 C62 H62B 109.5 . . ? C61 C62 H62C 109.5 . . ? H62A C62 H62B 109.5 . . ? H62A C62 H62C 109.5 . . ? H62B C62 H62C 109.5 . . ? C31 C32 H32 119.6 . . ? C33 C32 C31 120.8(6) . . ? C33 C32 H32 119.6 . . ? C57 C58 H58 120.5 . . ? C59 C58 C57 119.0(6) . . ? C59 C58 H58 120.5 . . ? O2 C84 C83 119.4(5) . . ? C85 C84 O2 115.3(6) . . ? C85 C84 C83 125.3(6) . . ? C60 C59 H59 120.3 . . ? C58 C59 C60 119.4(6) . . ? C58 C59 H59 120.3 . . ? C121 C122 H122 117.3 . . ? C123 C122 C121 125.3(10) . . ? C123 C122 H122 117.3 . . ? C91 C92 H92 119.6 . . ? C93 C92 C91 120.7(8) . . ? C93 C92 H92 119.6 . . ? C34 C33 H33 119.1 . . ? C32 C33 C34 121.8(7) . . ? C32 C33 H33 119.1 . . ? C82 C89 H89A 109.5 . . ? C82 C89 H89B 109.5 . . ? C82 C89 H89C 109.5 . . ? H89A C89 H89B 109.5 . . ? H89A C89 H89C 109.5 . . ? H89B C89 H89C 109.5 . . ? C26 C27 H27 119.4 . . ? C28 C27 C26 121.3(7) . . ? C28 C27 H27 119.4 . . ? C113 C112 H112 120.8 . . ? C113 C112 C111 118.3(7) . . ? C111 C112 H112 120.8 . . ? C52 C63 H63A 109.5 . . ? C52 C63 H63B 109.5 . . ? C52 C63 H63C 109.5 . . ? H63A C63 H63B 109.5 . . ? H63A C63 H63C 109.5 . . ? H63B C63 H63C 109.5 . . ? C104 C103 C108 115.0(7) . . ? C104 C103 B1 124.2(7) . . ? C108 C103 B1 120.3(7) . . ? C20 C19 P1 118.7(9) . . ? C20 C19 C24 120.2(9) . . ? C24 C19 P1 120.8(9) . . ? C110 C111 C112 120.9(7) . . ? C110 C111 H111 119.6 . . ? C112 C111 H111 119.6 . . ? C114 C109 C110 114.7(7) . . ? C114 C109 B1 120.4(6) . . ? C110 C109 B1 124.7(6) . . ? C129 C130 H130 120.3 . . ? C129 C130 C131 119.3(7) . . ? C131 C130 H130 120.3 . . ? C9 C8 H8 120.3 . . ? C9 C8 C7 119.5(6) . . ? C7 C8 H8 120.3 . . ? C82 C90 H90A 109.5 . . ? C82 C90 H90B 109.5 . . ? C82 C90 H90C 109.5 . . ? H90A C90 H90B 109.5 . . ? H90A C90 H90C 109.5 . . ? H90B C90 H90C 109.5 . . ? C43 C44 H44 120.1 . . ? C45 C44 C43 119.9(7) . . ? C45 C44 H44 120.1 . . ? C2 C3 H3 120.3 . . ? C4 C3 C2 119.4(7) . . ? C4 C3 H3 120.3 . . ? C97 C102 H102 119.5 . . ? C101 C102 C97 121.0(8) . . ? C101 C102 H102 119.5 . . ? C100 C99 H99 119.9 . . ? C98 C99 C100 120.1(7) . . ? C98 C99 H99 119.9 . . ? C146 C147 H147 120.2 . . ? C148 C147 C146 119.6(8) . . ? C148 C147 H147 120.2 . . ? C139 C140 H140 118.5 . . ? C141 C140 C139 122.9(9) . . ? C141 C140 H140 118.5 . . ? C121 C126 H126 120.0 . . ? C121 C126 C125 120.0(10) . . ? C125 C126 H126 120.0 . . ? C127 C128 C129 123.3(8) . . ? C127 C128 H128 118.3 . . ? C129 C128 H128 118.3 . . ? C136 C137 H137 119.9 . . ? C136 C137 C138 120.2(7) . . ? C138 C137 H137 119.9 . . ? C13 C14 H14 120.1 . . ? C13 C14 C15 119.7(12) . . ? C15 C14 H14 120.1 . . ? C8 C7 H7 120.7 . . ? C8 C7 C6 118.6(6) . . ? C6 C7 H7 120.7 . . ? C48 C49 H49 120.6 . . ? C50 C49 C48 118.9(7) . . ? C50 C49 H49 120.6 . . ? C92 C93 H93 120.1 . . ? C94 C93 C92 119.9(9) . . ? C94 C93 H93 120.1 . . ? N2 C6 C5 116.1(5) . . ? N2 C6 C7 122.5(6) . . ? C7 C6 C5 121.4(6) . . ? C66 C65 C64 120.8(6) . . ? C66 C65 H65 119.6 . . ? C64 C65 H65 119.6 . . ? C46 C51 H51 119.1 . . ? C50 C51 C46 121.9(7) . . ? C50 C51 H51 119.1 . . ? C103 C104 H104 118.8 . . ? C105 C104 C103 122.4(9) . . ? C105 C104 H104 118.8 . . ? C74 C73 H73 119.9 . . ? C72 C73 C74 120.2(6) . . ? C72 C73 H73 119.9 . . ? C105 C106 H106 120.7 . . ? C107 C106 H106 120.7 . . ? C107 C106 C105 118.5(8) . . ? C13 C18 H18 120.3 . . ? C13 C18 C17 119.3(10) . . ? C17 C18 H18 120.3 . . ? C133 C134 H134 118.1 . . ? C135 C134 H134 118.1 . . ? C135 C134 C133 123.8(7) . . ? C145 C150 H150 118.8 . . ? C149 C150 C145 122.5(8) . . ? C149 C150 H150 118.8 . . ? C134 C133 B2 121.7(6) . . ? C138 C133 C134 114.5(7) . . ? C138 C133 B2 123.8(6) . . ? C137 C136 H136 120.7 . . ? C137 C136 C135 118.6(7) . . ? C135 C136 H136 120.7 . . ? C137 C138 H138 118.5 . . ? C133 C138 C137 123.1(7) . . ? C133 C138 H138 118.5 . . ? C139 C144 H144 118.2 . . ? C143 C144 C139 123.6(9) . . ? C143 C144 H144 118.2 . . ? C30 C37 H37A 109.5 . . ? C30 C37 H37B 109.5 . . ? C30 C37 H37C 109.5 . . ? H37A C37 H37B 109.5 . . ? H37A C37 H37C 109.5 . . ? H37B C37 H37C 109.5 . . ? C71 C72 H72 120.2 . . ? C73 C72 C71 119.6(7) . . ? C73 C72 H72 120.2 . . ? C104 C105 C106 120.5(10) . . ? C104 C105 H105 119.7 . . ? C106 C105 H105 119.7 . . ? C49 C50 H50 119.8 . . ? C51 C50 C49 120.5(8) . . ? C51 C50 H50 119.8 . . ? C127 C132 H132 118.7 . . ? C127 C132 C131 122.6(7) . . ? C131 C132 H132 118.7 . . ? C91 C96 H96 119.5 . . ? C91 C96 C95 120.9(8) . . ? C95 C96 H96 119.5 . . ? C103 C108 H108 118.4 . . ? C107 C108 C103 123.1(9) . . ? C107 C108 H108 118.4 . . ? C140 C141 H141 119.7 . . ? C140 C141 C142 120.7(9) . . ? C142 C141 H141 119.7 . . ? C106 C107 H107 119.8 . . ? C108 C107 C106 120.4(9) . . ? C108 C107 H107 119.8 . . ? C134 C135 C136 119.8(7) . . ? C134 C135 H135 120.1 . . ? C136 C135 H135 120.1 . . ? C1 C12 H12A 109.5 . . ? C1 C12 H12B 109.5 . . ? C1 C12 H12C 109.5 . . ? H12A C12 H12B 109.5 . . ? H12A C12 H12C 109.5 . . ? H12B C12 H12C 109.5 . . ? C130 C131 C132 120.0(8) . . ? C130 C131 H131 120.0 . . ? C132 C131 H131 120.0 . . ? C19 C20 H20 119.2 . . ? C19 C20 C21 121.7(12) . . ? C21 C20 H20 119.2 . . ? C93 C94 H94 119.8 . . ? C95 C94 C93 120.3(7) . . ? C95 C94 H94 119.8 . . ? C122 C123 H123 120.7 . . ? C122 C123 C124 118.6(11) . . ? C124 C123 H123 120.7 . . ? C151 C152 H15A 109.5 . . ? C151 C152 H15B 109.5 . . ? C151 C152 H15C 109.5 . . ? H15A C152 H15B 109.5 . . ? H15A C152 H15C 109.5 . . ? H15B C152 H15C 109.5 . . ? C96 C95 H95 120.5 . . ? C94 C95 C96 119.1(9) . . ? C94 C95 H95 120.5 . . ? C126 C125 H125 119.3 . . ? C124 C125 C126 121.4(10) . . ? C124 C125 H125 119.3 . . ? C141 C142 H142 120.8 . . ? C143 C142 C141 118.4(9) . . ? C143 C142 H142 120.8 . . ? C123 C124 H124 120.3 . . ? C125 C124 C123 119.5(9) . . ? C125 C124 H124 120.3 . . ? C139 B2 C127 111.3(5) . . ? C145 B2 C139 108.1(6) . . ? C145 B2 C127 109.6(6) . . ? C133 B2 C139 110.0(6) . . ? C133 B2 C145 110.5(5) . . ? C133 B2 C127 107.2(6) . . ? C144 C143 H143 120.0 . . ? C142 C143 C144 119.9(9) . . ? C142 C143 H143 120.0 . . ? C115 B1 C121 103.9(5) . . ? C115 B1 C103 112.9(6) . . ? C115 B1 C109 112.9(6) . . ? C103 B1 C121 112.4(6) . . ? C109 B1 C121 111.2(6) . . ? C109 B1 C103 103.8(5) . . ? C18 C17 H17 118.8 . . ? C16 C17 C18 122.5(12) . . ? C16 C17 H17 118.8 . . ? C19 C24 H24 120.4 . . ? C23 C24 C19 119.2(11) . . ? C23 C24 H24 120.4 . . ? C14 C15 H15 119.9 . . ? C16 C15 C14 120.2(10) . . ? C16 C15 H15 119.9 . . ? C151 C153 H15D 109.5 . . ? C151 C153 H15E 109.5 . . ? C151 C153 H15F 109.5 . . ? H15D C153 H15E 109.5 . . ? H15D C153 H15F 109.5 . . ? H15E C153 H15F 109.5 . . ? C17 C16 C15 119.0(9) . . ? C17 C16 H16 120.5 . . ? C15 C16 H16 120.5 . . ? C20 C21 H21 120.5 . . ? C22 C21 C20 119.1(12) . . ? C22 C21 H21 120.5 . . ? C21 C22 H22 119.4 . . ? C21 C22 C23 121.2(9) . . ? C23 C22 H22 119.4 . . ? C24 C23 C22 118.4(11) . . ? C24 C23 H23 120.8 . . ? C22 C23 H23 120.8 . . ? O4 C154 C155 113(2) . . ? O4 C154 C156 108(2) . . ? C156 C154 C155 127(2) . . ? C154 C155 H15G 111.1 . . ? C154 C155 H15H 106.8 . . ? C154 C155 H15I 110.5 . . ? H15G C155 H15H 109.5 . . ? H15G C155 H15I 109.5 . . ? H15H C155 H15I 109.5 . . ? C154 C156 H15J 114.5 . . ? C154 C156 H15K 95.9 . . ? C154 C156 H15L 117.0 . . ? H15J C156 H15K 109.5 . . ? H15J C156 H15L 109.5 . . ? H15K C156 H15L 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cu1 P2 2.2551(16) . ? Cu1 P1 2.309(2) . ? Cu1 N1 2.094(5) . ? Cu1 N2 2.129(5) . ? Cu2 P3 2.2868(16) . ? Cu2 P4 2.306(2) . ? Cu2 N4 2.123(5) . ? Cu2 N3 2.102(5) . ? P2 C40 1.825(7) . ? P2 C35 1.838(6) . ? P2 C46 1.839(7) . ? P3 C76 1.843(6) . ? P3 C64 1.824(7) . ? P3 C70 1.846(6) . ? P4 C97 1.835(7) . ? P4 C91 1.824(6) . ? P4 C85 1.831(7) . ? P1 C25 1.843(7) . ? P1 C13 1.831(7) . ? P1 C19 1.826(9) . ? O2 C77 1.397(8) . ? O2 C84 1.387(8) . ? O1 C39 1.376(8) . ? O1 C36 1.378(8) . ? N4 C61 1.338(9) . ? N4 C57 1.359(8) . ? N1 C5 1.341(8) . ? N1 C1 1.357(9) . ? O3 C151 1.197(11) . ? N2 C10 1.360(9) . ? N2 C6 1.343(9) . ? N3 C56 1.350(8) . ? N3 C52 1.352(9) . ? C78 C77 1.397(9) . ? C78 C79 1.391(10) . ? C78 C82 1.514(10) . ? C88 H88 0.9500 . ? C88 C83 1.400(10) . ? C88 C87 1.376(10) . ? C76 C77 1.368(10) . ? C76 C81 1.402(9) . ? C56 C55 1.389(9) . ? C56 C57 1.477(9) . ? C68 H68 0.9500 . ? C68 C69 1.375(11) . ? C68 C67 1.403(11) . ? C39 C29 1.407(10) . ? C39 C25 1.388(9) . ? C5 C4 1.394(10) . ? C5 C6 1.500(9) . ? C97 C98 1.396(10) . ? C97 C102 1.392(11) . ? C86 H86 0.9500 . ? C86 C87 1.388(10) . ? C86 C85 1.412(10) . ? C55 H55 0.9500 . ? C55 C54 1.399(10) . ? C61 C60 1.396(10) . ? C61 C62 1.497(9) . ? C57 C58 1.407(9) . ? C30 C29 1.545(10) . ? C30 C38 1.532(10) . ? C30 C31 1.511(11) . ? C30 C37 1.558(9) . ? C69 H69 0.9500 . ? C69 C64 1.397(9) . ? C40 C41 1.411(9) . ? C40 C45 1.402(9) . ? C10 C11 1.483(9) . ? C10 C9 1.389(9) . ? C66 H66 0.9500 . ? C66 C67 1.384(11) . ? C66 C65 1.388(11) . ? C1 C2 1.385(10) . ? C1 C12 1.497(9) . ? C34 H34 0.9500 . ? C34 C35 1.395(10) . ? C34 C33 1.393(10) . ? C29 C28 1.404(11) . ? C54 H54 0.9500 . ? C54 C53 1.357(10) . ? C25 C26 1.383(10) . ? C83 C82 1.525(9) . ? C83 C84 1.392(9) . ? C116 H116 0.9500 . ? C116 C115 1.403(10) . ? C116 C117 1.402(9) . ? C67 H67 0.9500 . ? C91 C92 1.390(11) . ? C91 C96 1.374(11) . ? C35 C36 1.388(10) . ? C46 C47 1.421(10) . ? C46 C51 1.391(11) . ? C42 H42 0.9500 . ? C42 C43 1.382(11) . ? C42 C41 1.378(11) . ? C43 H43 0.9500 . ? C43 C44 1.386(10) . ? C139 C140 1.413(12) . ? C139 C144 1.398(11) . ? C139 B2 1.654(12) . ? C47 H47 0.9500 . ? C47 C48 1.372(11) . ? C100 H100 0.9500 . ? C100 C101 1.385(12) . ? C100 C99 1.397(12) . ? C79 H79 0.9500 . ? C79 C80 1.368(11) . ? C11 H11A 0.9800 . ? C11 H11B 0.9800 . ? C11 H11C 0.9800 . ? C41 H41 0.9500 . ? C26 H26 0.9500 . ? C26 C27 1.393(11) . ? C36 C31 1.394(9) . ? C9 H9 0.9500 . ? C9 C8 1.375(11) . ? C145 C146 1.382(12) . ? C145 C150 1.405(11) . ? C145 B2 1.650(9) . ? C45 H45 0.9500 . ? C45 C44 1.382(12) . ? C64 C65 1.388(10) . ? C48 H48 0.9500 . ? C48 C49 1.400(13) . ? C38 H38A 0.9800 . ? C38 H38B 0.9800 . ? C38 H38C 0.9800 . ? C71 H71 0.9500 . ? C71 C70 1.401(10) . ? C71 C72 1.395(10) . ? C146 H146 0.9500 . ? C146 C147 1.406(11) . ? C121 C122 1.386(12) . ? C121 C126 1.397(13) . ? C121 B1 1.651(11) . ? C87 H87 0.9500 . ? C2 H2 0.9500 . ? C2 C3 1.381(11) . ? C82 C89 1.548(10) . ? C82 C90 1.544(9) . ? C114 H114 0.9500 . ? C114 C113 1.388(11) . ? C114 C109 1.403(11) . ? C81 H81 0.9500 . ? C81 C80 1.399(10) . ? C75 H75 0.9500 . ? C75 C70 1.384(11) . ? C75 C74 1.403(11) . ? C28 H28 0.9500 . ? C28 C27 1.365(11) . ? C119 H119 0.9500 . ? C119 C120 1.389(10) . ? C119 C118 1.397(12) . ? C127 C128 1.385(10) . ? C127 C132 1.391(12) . ? C127 B2 1.658(11) . ? C148 H148 0.9500 . ? C148 C149 1.369(13) . ? C148 C147 1.395(13) . ? C120 H120 0.9500 . ? C120 C115 1.407(11) . ? C13 C14 1.388(12) . ? C13 C18 1.382(13) . ? C149 H149 0.9500 . ? C149 C150 1.404(10) . ? C85 C84 1.377(9) . ? C80 H80 0.9500 . ? C101 H101 0.9500 . ? C101 C102 1.359(12) . ? C53 H53 0.9500 . ? C53 C52 1.388(9) . ? C31 C32 1.398(11) . ? C74 H74 0.9500 . ? C74 C73 1.379(13) . ? C115 B1 1.638(10) . ? C117 H117 0.9500 . ? C117 C118 1.347(12) . ? C4 H4 0.9500 . ? C4 C3 1.379(11) . ? C52 C63 1.483(9) . ? C118 H118 0.9500 . ? C113 H113 0.9500 . ? C113 C112 1.380(12) . ? C151 C152 1.491(15) . ? C151 C153 1.500(14) . ? C129 H129 0.9500 . ? C129 C130 1.362(14) . ? C129 C128 1.402(12) . ? C60 H60 0.9500 . ? C60 C59 1.388(10) . ? C98 H98 0.9500 . ? C98 C99 1.384(11) . ? C110 H110 0.9500 . ? C110 C111 1.375(11) . ? C110 C109 1.406(10) . ? C62 H62A 0.9800 . ? C62 H62B 0.9800 . ? C62 H62C 0.9800 . ? C32 H32 0.9500 . ? C32 C33 1.384(11) . ? C58 H58 0.9500 . ? C58 C59 1.365(10) . ? C59 H59 0.9500 . ? C122 H122 0.9500 . ? C122 C123 1.376(12) . ? C92 H92 0.9500 . ? C92 C93 1.389(12) . ? C33 H33 0.9500 . ? C89 H89A 0.9800 . ? C89 H89B 0.9800 . ? C89 H89C 0.9800 . ? C27 H27 0.9500 . ? C112 H112 0.9500 . ? C112 C111 1.409(12) . ? C63 H63A 0.9800 . ? C63 H63B 0.9800 . ? C63 H63C 0.9800 . ? C103 C104 1.400(12) . ? C103 C108 1.410(11) . ? C103 B1 1.647(10) . ? C19 C20 1.379(18) . ? C19 C24 1.401(18) . ? C111 H111 0.9500 . ? C109 B1 1.645(11) . ? C130 H130 0.9500 . ? C130 C131 1.373(13) . ? C8 H8 0.9500 . ? C8 C7 1.375(11) . ? C90 H90A 0.9800 . ? C90 H90B 0.9800 . ? C90 H90C 0.9800 . ? C44 H44 0.9500 . ? C3 H3 0.9500 . ? C102 H102 0.9500 . ? C99 H99 0.9500 . ? C147 H147 0.9500 . ? C140 H140 0.9500 . ? C140 C141 1.380(13) . ? C126 H126 0.9500 . ? C126 C125 1.430(15) . ? C128 H128 0.9500 . ? C137 H137 0.9500 . ? C137 C136 1.376(11) . ? C137 C138 1.394(11) . ? C14 H14 0.9500 . ? C14 C15 1.411(16) . ? C7 H7 0.9500 . ? C7 C6 1.389(9) . ? C49 H49 0.9500 . ? C49 C50 1.385(12) . ? C93 H93 0.9500 . ? C93 C94 1.382(15) . ? C65 H65 0.9500 . ? C51 H51 0.9500 . ? C51 C50 1.380(11) . ? C104 H104 0.9500 . ? C104 C105 1.379(13) . ? C73 H73 0.9500 . ? C73 C72 1.374(13) . ? C106 H106 0.9500 . ? C106 C105 1.393(16) . ? C106 C107 1.379(16) . ? C18 H18 0.9500 . ? C18 C17 1.401(12) . ? C134 H134 0.9500 . ? C134 C133 1.395(10) . ? C134 C135 1.379(11) . ? C150 H150 0.9500 . ? C133 C138 1.392(10) . ? C133 B2 1.649(10) . ? C136 H136 0.9500 . ? C136 C135 1.392(11) . ? C138 H138 0.9500 . ? C144 H144 0.9500 . ? C144 C143 1.395(14) . ? C37 H37A 0.9800 . ? C37 H37B 0.9800 . ? C37 H37C 0.9800 . ? C72 H72 0.9500 . ? C105 H105 0.9500 . ? C50 H50 0.9500 . ? C132 H132 0.9500 . ? C132 C131 1.403(12) . ? C96 H96 0.9500 . ? C96 C95 1.411(11) . ? C108 H108 0.9500 . ? C108 C107 1.369(13) . ? C141 H141 0.9500 . ? C141 C142 1.394(15) . ? C107 H107 0.9500 . ? C135 H135 0.9500 . ? C12 H12A 0.9800 . ? C12 H12B 0.9800 . ? C12 H12C 0.9800 . ? C131 H131 0.9500 . ? C20 H20 0.9500 . ? C20 C21 1.382(14) . ? C94 H94 0.9500 . ? C94 C95 1.381(15) . ? C123 H123 0.9500 . ? C123 C124 1.376(18) . ? C152 H15A 0.9800 . ? C152 H15B 0.9800 . ? C152 H15C 0.9800 . ? C95 H95 0.9500 . ? C125 H125 0.9500 . ? C125 C124 1.358(18) . ? C142 H142 0.9500 . ? C142 C143 1.382(16) . ? C124 H124 0.9500 . ? C143 H143 0.9500 . ? C17 H17 0.9500 . ? C17 C16 1.34(2) . ? C24 H24 0.9500 . ? C24 C23 1.393(14) . ? C15 H15 0.9500 . ? C15 C16 1.39(2) . ? C153 H15D 0.9800 . ? C153 H15E 0.9800 . ? C153 H15F 0.9800 . ? C16 H16 0.9500 . ? C21 H21 0.9500 . ? C21 C22 1.353(17) . ? C22 H22 0.9500 . ? C22 C23 1.441(18) . ? C23 H23 0.9500 . ? C154 C155 1.476(7) . ? C154 O4 1.19(2) . ? C154 C156 1.475(7) . ? C155 H15G 0.9598 . ? C155 H15H 0.9601 . ? C155 H15I 0.9599 . ? C156 H15J 0.9600 . ? C156 H15K 0.9600 . ? C156 H15L 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Cu1 P2 C40 C41 166.1(5) . . . . ? Cu1 P2 C40 C45 -13.5(6) . . . . ? Cu1 P2 C35 C34 129.0(5) . . . . ? Cu1 P2 C35 C36 -46.7(5) . . . . ? Cu1 P2 C46 C47 -75.1(6) . . . . ? Cu1 P2 C46 C51 99.9(6) . . . . ? Cu1 P1 C25 C39 32.2(5) . . . . ? Cu1 P1 C25 C26 -148.4(5) . . . . ? Cu1 P1 C13 C14 -84.8(7) . . . . ? Cu1 P1 C13 C18 79.9(6) . . . . ? Cu1 P1 C19 C20 -27.8(11) . . . . ? Cu1 P1 C19 C24 158.4(8) . . . . ? Cu1 N1 C5 C4 169.8(6) . . . . ? Cu1 N1 C5 C6 -9.7(8) . . . . ? Cu1 N1 C1 C2 -169.6(6) . . . . ? Cu1 N1 C1 C12 10.7(10) . . . . ? Cu1 N2 C10 C11 -12.0(10) . . . . ? Cu1 N2 C10 C9 169.2(5) . . . . ? Cu1 N2 C6 C5 8.1(7) . . . . ? Cu1 N2 C6 C7 -171.4(6) . . . . ? Cu2 P3 C76 C77 49.2(5) . . . . ? Cu2 P3 C76 C81 -126.0(4) . . . . ? Cu2 P3 C64 C69 -168.5(5) . . . . ? Cu2 P3 C64 C65 11.3(6) . . . . ? Cu2 P3 C70 C71 84.4(6) . . . . ? Cu2 P3 C70 C75 -95.6(5) . . . . ? Cu2 P4 C97 C98 116.2(6) . . . . ? Cu2 P4 C97 C102 -59.5(6) . . . . ? Cu2 P4 C91 C92 150.2(5) . . . . ? Cu2 P4 C91 C96 -33.9(7) . . . . ? Cu2 P4 C85 C86 136.3(5) . . . . ? Cu2 P4 C85 C84 -42.7(6) . . . . ? Cu2 N4 C61 C60 168.6(5) . . . . ? Cu2 N4 C61 C62 -12.0(9) . . . . ? Cu2 N4 C57 C56 12.4(7) . . . . ? Cu2 N4 C57 C58 -168.3(5) . . . . ? Cu2 N3 C56 C55 169.9(5) . . . . ? Cu2 N3 C56 C57 -11.3(7) . . . . ? Cu2 N3 C52 C53 -168.4(5) . . . . ? Cu2 N3 C52 C63 10.8(9) . . . . ? P2 C40 C41 C42 -179.1(5) . . . . ? P2 C40 C45 C44 -179.7(5) . . . . ? P2 C35 C36 O1 -2.9(7) . . . . ? P2 C35 C36 C31 177.2(5) . . . . ? P2 C46 C47 C48 174.8(6) . . . . ? P2 C46 C51 C50 -175.3(6) . . . . ? P3 C76 C77 O2 3.3(7) . . . . ? P3 C76 C77 C78 -176.8(5) . . . . ? P3 C76 C81 C80 175.1(5) . . . . ? P3 C64 C65 C66 -178.7(5) . . . . ? P4 C97 C98 C99 -174.7(6) . . . . ? P4 C97 C102 C101 176.3(6) . . . . ? P4 C91 C92 C93 172.9(7) . . . . ? P4 C91 C96 C95 -175.5(7) . . . . ? P4 C85 C84 O2 -5.6(8) . . . . ? P4 C85 C84 C83 175.8(5) . . . . ? P1 C25 C26 C27 -179.7(5) . . . . ? P1 C13 C14 C15 165.7(7) . . . . ? P1 C13 C18 C17 -165.2(7) . . . . ? P1 C19 C20 C21 -173.6(9) . . . . ? P1 C19 C24 C23 175.7(9) . . . . ? O1 C39 C29 C30 -11.6(9) . . . . ? O1 C39 C29 C28 169.9(6) . . . . ? O1 C39 C25 P1 7.7(7) . . . . ? O1 C39 C25 C26 -171.8(6) . . . . ? O1 C36 C31 C30 -1.0(9) . . . . ? O1 C36 C31 C32 180.0(5) . . . . ? N4 C61 C60 C59 -0.2(11) . . . . ? N4 C57 C58 C59 -2.9(11) . . . . ? N1 C5 C4 C3 1.3(12) . . . . ? N1 C5 C6 N2 0.9(9) . . . . ? N1 C5 C6 C7 -179.6(7) . . . . ? N1 C1 C2 C3 0.9(13) . . . . ? N2 C10 C9 C8 0.5(11) . . . . ? N3 C56 C55 C54 -0.3(11) . . . . ? N3 C56 C57 N4 -0.9(9) . . . . ? N3 C56 C57 C58 179.8(6) . . . . ? C78 C79 C80 C81 0.0(10) . . . . ? C88 C83 C82 C78 -149.4(7) . . . . ? C88 C83 C82 C89 -25.4(10) . . . . ? C88 C83 C82 C90 93.9(8) . . . . ? C88 C83 C84 O2 -175.4(6) . . . . ? C88 C83 C84 C85 3.2(10) . . . . ? C76 P3 C64 C69 68.3(6) . . . . ? C76 P3 C64 C65 -111.9(5) . . . . ? C76 P3 C70 C71 -149.5(5) . . . . ? C76 P3 C70 C75 30.5(6) . . . . ? C76 C81 C80 C79 0.8(10) . . . . ? C56 N3 C52 C53 1.1(10) . . . . ? C56 N3 C52 C63 -179.7(6) . . . . ? C56 C55 C54 C53 1.4(11) . . . . ? C56 C57 C58 C59 176.3(7) . . . . ? C68 C69 C64 P3 179.0(5) . . . . ? C68 C69 C64 C65 -0.8(10) . . . . ? C77 O2 C84 C83 -37.3(8) . . . . ? C77 O2 C84 C85 144.1(6) . . . . ? C77 C78 C79 C80 -1.2(9) . . . . ? C77 C78 C82 C83 -37.8(7) . . . . ? C77 C78 C82 C89 -161.0(6) . . . . ? C77 C78 C82 C90 79.3(7) . . . . ? C77 C76 C81 C80 -0.2(9) . . . . ? C39 O1 C36 C35 154.0(5) . . . . ? C39 O1 C36 C31 -26.2(8) . . . . ? C39 C29 C28 C27 4.1(10) . . . . ? C39 C25 C26 C27 -0.3(10) . . . . ? C5 N1 C1 C2 0.1(11) . . . . ? C5 N1 C1 C12 -179.7(7) . . . . ? C5 C4 C3 C2 -0.3(14) . . . . ? C97 P4 C91 C92 25.0(7) . . . . ? C97 P4 C91 C96 -159.1(6) . . . . ? C97 P4 C85 C86 -101.1(6) . . . . ? C97 P4 C85 C84 80.0(6) . . . . ? C97 C98 C99 C100 -0.6(12) . . . . ? C86 C85 C84 O2 175.4(6) . . . . ? C86 C85 C84 C83 -3.2(10) . . . . ? C55 C56 C57 N4 177.9(6) . . . . ? C55 C56 C57 C58 -1.3(10) . . . . ? C55 C54 C53 C52 -1.3(12) . . . . ? C61 N4 C57 C56 -174.3(6) . . . . ? C61 N4 C57 C58 4.9(10) . . . . ? C61 C60 C59 C58 2.2(12) . . . . ? C57 N4 C61 C60 -3.4(10) . . . . ? C57 N4 C61 C62 176.0(6) . . . . ? C57 C56 C55 C54 -179.1(7) . . . . ? C57 C58 C59 C60 -0.7(12) . . . . ? C30 C29 C28 C27 -174.4(6) . . . . ? C30 C31 C32 C33 -180.0(6) . . . . ? C69 C68 C67 C66 0.3(10) . . . . ? C69 C64 C65 C66 1.1(10) . . . . ? C40 P2 C35 C34 4.1(6) . . . . ? C40 P2 C35 C36 -171.6(5) . . . . ? C40 P2 C46 C47 52.9(6) . . . . ? C40 P2 C46 C51 -132.2(6) . . . . ? C40 C45 C44 C43 -1.0(10) . . . . ? C10 N2 C6 C5 178.3(6) . . . . ? C10 N2 C6 C7 -1.2(10) . . . . ? C10 C9 C8 C7 -1.1(12) . . . . ? C1 N1 C5 C4 -1.2(10) . . . . ? C1 N1 C5 C6 179.3(6) . . . . ? C1 C2 C3 C4 -0.8(13) . . . . ? C34 C35 C36 O1 -178.9(5) . . . . ? C34 C35 C36 C31 1.2(9) . . . . ? C29 C39 C25 P1 -174.3(5) . . . . ? C29 C39 C25 C26 6.3(9) . . . . ? C29 C30 C31 C36 19.2(8) . . . . ? C29 C30 C31 C32 -161.8(6) . . . . ? C29 C28 C27 C26 1.5(11) . . . . ? C54 C53 C52 N3 0.0(11) . . . . ? C54 C53 C52 C63 -179.1(7) . . . . ? C25 P1 C13 C14 151.2(7) . . . . ? C25 P1 C13 C18 -44.1(7) . . . . ? C25 P1 C19 C20 103.1(9) . . . . ? C25 P1 C19 C24 -70.7(10) . . . . ? C25 C39 C29 C30 170.4(6) . . . . ? C25 C39 C29 C28 -8.1(9) . . . . ? C25 C26 C27 C28 -3.5(11) . . . . ? C83 C88 C87 C86 -0.8(11) . . . . ? C116 C115 B1 C121 -108.6(7) . . . . ? C116 C115 B1 C103 129.4(7) . . . . ? C116 C115 B1 C109 12.0(9) . . . . ? C116 C117 C118 C119 0.3(10) . . . . ? C67 C68 C69 C64 0.1(10) . . . . ? C67 C66 C65 C64 -0.7(10) . . . . ? C91 P4 C97 C98 -114.6(6) . . . . ? C91 P4 C97 C102 69.7(6) . . . . ? C91 P4 C85 C86 6.8(7) . . . . ? C91 P4 C85 C84 -172.1(5) . . . . ? C91 C92 C93 C94 3.6(14) . . . . ? C91 C96 C95 C94 1.1(15) . . . . ? C35 P2 C40 C41 -70.7(6) . . . . ? C35 P2 C40 C45 109.7(5) . . . . ? C35 P2 C46 C47 161.5(6) . . . . ? C35 P2 C46 C51 -23.5(7) . . . . ? C35 C34 C33 C32 0.0(10) . . . . ? C35 C36 C31 C30 178.8(6) . . . . ? C35 C36 C31 C32 -0.2(9) . . . . ? C46 P2 C40 C41 35.3(6) . . . . ? C46 P2 C40 C45 -144.3(5) . . . . ? C46 P2 C35 C34 -102.8(6) . . . . ? C46 P2 C35 C36 81.4(5) . . . . ? C46 C47 C48 C49 0.4(11) . . . . ? C46 C51 C50 C49 1.0(13) . . . . ? C42 C43 C44 C45 0.1(10) . . . . ? C43 C42 C41 C40 -1.3(10) . . . . ? C139 C140 C141 C142 0.7(10) . . . . ? C139 C144 C143 C142 2.2(11) . . . . ? C47 C46 C51 C50 -0.2(11) . . . . ? C47 C48 C49 C50 0.4(12) . . . . ? C100 C101 C102 C97 -2.2(12) . . . . ? C79 C78 C77 O2 -178.1(5) . . . . ? C79 C78 C77 C76 1.9(9) . . . . ? C79 C78 C82 C83 147.0(6) . . . . ? C79 C78 C82 C89 23.8(9) . . . . ? C79 C78 C82 C90 -95.9(7) . . . . ? C11 C10 C9 C8 -178.3(8) . . . . ? C41 C40 C45 C44 0.7(10) . . . . ? C41 C42 C43 C44 1.0(10) . . . . ? C36 O1 C39 C29 32.3(8) . . . . ? C36 O1 C39 C25 -149.6(6) . . . . ? C36 C31 C32 C33 -1.0(9) . . . . ? C9 C8 C7 C6 0.5(12) . . . . ? C145 C146 C147 C148 -0.2(13) . . . . ? C45 C40 C41 C42 0.5(10) . . . . ? C64 P3 C76 C77 173.1(4) . . . . ? C64 P3 C76 C81 -2.2(5) . . . . ? C64 P3 C70 C71 -42.6(6) . . . . ? C64 P3 C70 C75 137.4(6) . . . . ? C48 C49 C50 C51 -1.0(13) . . . . ? C38 C30 C29 C39 -135.2(6) . . . . ? C38 C30 C29 C28 43.2(9) . . . . ? C38 C30 C31 C36 139.6(6) . . . . ? C38 C30 C31 C32 -41.4(8) . . . . ? C146 C145 C150 C149 -1.1(10) . . . . ? C146 C145 B2 C139 -138.2(7) . . . . ? C146 C145 B2 C127 -16.6(9) . . . . ? C146 C145 B2 C133 101.4(8) . . . . ? C121 C122 C123 C124 0.8(13) . . . . ? C121 C126 C125 C124 -2.1(14) . . . . ? C87 C88 C83 C82 -177.8(7) . . . . ? C87 C88 C83 C84 -1.1(10) . . . . ? C87 C86 C85 P4 -177.8(6) . . . . ? C87 C86 C85 C84 1.1(10) . . . . ? C82 C78 C77 O2 6.2(8) . . . . ? C82 C78 C77 C76 -173.8(5) . . . . ? C82 C78 C79 C80 174.1(6) . . . . ? C82 C83 C84 O2 1.7(9) . . . . ? C82 C83 C84 C85 -179.8(6) . . . . ? C114 C113 C112 C111 -1.3(10) . . . . ? C114 C109 B1 C121 175.1(6) . . . . ? C114 C109 B1 C115 58.8(8) . . . . ? C114 C109 B1 C103 -63.8(7) . . . . ? C81 C76 C77 O2 178.8(5) . . . . ? C81 C76 C77 C78 -1.3(8) . . . . ? C75 C74 C73 C72 -0.7(12) . . . . ? C70 P3 C76 C77 -81.5(5) . . . . ? C70 P3 C76 C81 103.3(5) . . . . ? C70 P3 C64 C69 -37.6(6) . . . . ? C70 P3 C64 C65 142.2(5) . . . . ? C70 C71 C72 C73 -0.7(11) . . . . ? C70 C75 C74 C73 -0.2(11) . . . . ? C119 C120 C115 C116 -1.7(10) . . . . ? C119 C120 C115 B1 -177.4(6) . . . . ? C127 C132 C131 C130 0.0(13) . . . . ? C148 C149 C150 C145 -0.3(11) . . . . ? C120 C119 C118 C117 -0.6(10) . . . . ? C120 C115 B1 C121 66.7(8) . . . . ? C120 C115 B1 C103 -55.3(9) . . . . ? C120 C115 B1 C109 -172.7(6) . . . . ? C13 P1 C25 C39 148.2(5) . . . . ? C13 P1 C25 C26 -32.4(6) . . . . ? C13 P1 C19 C20 -147.5(9) . . . . ? C13 P1 C19 C24 38.7(11) . . . . ? C13 C14 C15 C16 -0.5(14) . . . . ? C13 C18 C17 C16 0.1(15) . . . . ? C149 C148 C147 C146 -1.3(13) . . . . ? C85 P4 C97 C98 -9.9(7) . . . . ? C85 P4 C97 C102 174.4(6) . . . . ? C85 P4 C91 C92 -81.1(6) . . . . ? C85 P4 C91 C96 94.8(6) . . . . ? C85 C86 C87 C88 0.8(11) . . . . ? C101 C100 C99 C98 -1.2(13) . . . . ? C31 C30 C29 C39 -13.0(8) . . . . ? C31 C30 C29 C28 165.4(6) . . . . ? C31 C32 C33 C34 1.0(10) . . . . ? C74 C75 C70 P3 -179.5(6) . . . . ? C74 C75 C70 C71 0.5(10) . . . . ? C74 C73 C72 C71 1.1(12) . . . . ? C115 C116 C117 C118 -0.7(10) . . . . ? C117 C116 C115 C120 1.3(9) . . . . ? C117 C116 C115 B1 176.9(6) . . . . ? C4 C5 C6 N2 -178.6(7) . . . . ? C4 C5 C6 C7 0.9(11) . . . . ? C52 N3 C56 C55 -0.9(10) . . . . ? C52 N3 C56 C57 177.9(6) . . . . ? C118 C119 C120 C115 1.4(11) . . . . ? C113 C114 C109 C110 1.2(9) . . . . ? C113 C114 C109 B1 176.3(6) . . . . ? C113 C112 C111 C110 0.8(10) . . . . ? C129 C130 C131 C132 0.7(12) . . . . ? C98 C97 C102 C101 0.4(11) . . . . ? C110 C109 B1 C121 -10.3(9) . . . . ? C110 C109 B1 C115 -126.6(7) . . . . ? C110 C109 B1 C103 110.7(7) . . . . ? C62 C61 C60 C59 -179.5(7) . . . . ? C84 O2 C77 C78 33.2(7) . . . . ? C84 O2 C77 C76 -146.8(5) . . . . ? C84 C83 C82 C78 34.0(8) . . . . ? C84 C83 C82 C89 158.0(6) . . . . ? C84 C83 C82 C90 -82.7(8) . . . . ? C122 C121 C126 C125 1.5(11) . . . . ? C122 C121 B1 C115 61.5(8) . . . . ? C122 C121 B1 C103 -176.1(6) . . . . ? C122 C121 B1 C109 -60.2(8) . . . . ? C122 C123 C124 C125 -1.2(13) . . . . ? C92 C91 C96 C95 0.5(13) . . . . ? C92 C93 C94 C95 -1.9(15) . . . . ? C33 C34 C35 P2 -176.8(5) . . . . ? C33 C34 C35 C36 -1.1(9) . . . . ? C103 C104 C105 C106 2.2(16) . . . . ? C103 C108 C107 C106 -1.6(15) . . . . ? C19 P1 C25 C39 -102.3(6) . . . . ? C19 P1 C25 C26 77.1(7) . . . . ? C19 P1 C13 C14 46.0(8) . . . . ? C19 P1 C13 C18 -149.2(7) . . . . ? C19 C20 C21 C22 1.3(18) . . . . ? C19 C24 C23 C22 -5.5(16) . . . . ? C111 C110 C109 C114 -1.8(9) . . . . ? C111 C110 C109 B1 -176.6(6) . . . . ? C109 C114 C113 C112 0.3(10) . . . . ? C109 C110 C111 C112 0.8(10) . . . . ? C130 C129 C128 C127 -3.2(12) . . . . ? C8 C7 C6 N2 0.6(11) . . . . ? C8 C7 C6 C5 -178.9(7) . . . . ? C102 C97 C98 C99 1.0(11) . . . . ? C99 C100 C101 C102 2.6(13) . . . . ? C147 C148 C149 C150 1.5(11) . . . . ? C140 C139 C144 C143 -2.1(10) . . . . ? C140 C139 B2 C145 -130.7(6) . . . . ? C140 C139 B2 C127 108.8(7) . . . . ? C140 C139 B2 C133 -9.9(8) . . . . ? C140 C141 C142 C143 -0.7(11) . . . . ? C126 C121 C122 C123 -1.0(11) . . . . ? C126 C121 B1 C115 -110.7(8) . . . . ? C126 C121 B1 C103 11.7(10) . . . . ? C126 C121 B1 C109 127.6(7) . . . . ? C126 C125 C124 C123 1.9(15) . . . . ? C128 C127 C132 C131 -2.2(11) . . . . ? C128 C127 B2 C139 27.0(9) . . . . ? C128 C127 B2 C145 -92.6(8) . . . . ? C128 C127 B2 C133 147.4(7) . . . . ? C128 C129 C130 C131 0.8(12) . . . . ? C137 C136 C135 C134 -0.2(13) . . . . ? C14 C13 C18 C17 -0.5(12) . . . . ? C14 C15 C16 C17 0.0(16) . . . . ? C93 C94 C95 C96 -0.4(15) . . . . ? C6 N2 C10 C11 179.4(7) . . . . ? C6 N2 C10 C9 0.6(10) . . . . ? C6 C5 C4 C3 -179.3(8) . . . . ? C65 C66 C67 C68 0.0(10) . . . . ? C51 C46 C47 C48 -0.5(10) . . . . ? C104 C103 C108 C107 2.0(13) . . . . ? C104 C103 B1 C121 -129.8(8) . . . . ? C104 C103 B1 C115 -12.7(10) . . . . ? C104 C103 B1 C109 109.9(8) . . . . ? C18 C13 C14 C15 0.8(12) . . . . ? C18 C17 C16 C15 0.2(16) . . . . ? C134 C133 C138 C137 1.0(12) . . . . ? C134 C133 B2 C139 73.2(9) . . . . ? C134 C133 B2 C145 -167.5(7) . . . . ? C134 C133 B2 C127 -48.0(9) . . . . ? C150 C145 C146 C147 1.3(11) . . . . ? C150 C145 B2 C139 43.5(8) . . . . ? C150 C145 B2 C127 165.1(6) . . . . ? C150 C145 B2 C133 -76.9(8) . . . . ? C133 C134 C135 C136 1.7(14) . . . . ? C136 C137 C138 C133 0.3(14) . . . . ? C138 C137 C136 C135 -0.7(13) . . . . ? C138 C133 B2 C139 -106.8(8) . . . . ? C138 C133 B2 C145 12.5(10) . . . . ? C138 C133 B2 C127 132.0(7) . . . . ? C144 C139 C140 C141 0.6(9) . . . . ? C144 C139 B2 C145 46.5(8) . . . . ? C144 C139 B2 C127 -74.0(8) . . . . ? C144 C139 B2 C133 167.2(6) . . . . ? C37 C30 C29 C39 106.2(7) . . . . ? C37 C30 C29 C28 -75.4(8) . . . . ? C37 C30 C31 C36 -100.8(7) . . . . ? C37 C30 C31 C32 78.2(8) . . . . ? C72 C71 C70 P3 179.9(5) . . . . ? C72 C71 C70 C75 -0.1(10) . . . . ? C105 C106 C107 C108 1.4(15) . . . . ? C132 C127 C128 C129 3.8(11) . . . . ? C132 C127 B2 C139 -153.0(7) . . . . ? C132 C127 B2 C145 87.4(8) . . . . ? C132 C127 B2 C133 -32.6(9) . . . . ? C96 C91 C92 C93 -2.9(12) . . . . ? C108 C103 C104 C105 -2.2(13) . . . . ? C108 C103 B1 C121 58.9(9) . . . . ? C108 C103 B1 C115 176.0(7) . . . . ? C108 C103 B1 C109 -61.4(8) . . . . ? C141 C142 C143 C144 -0.7(11) . . . . ? C107 C106 C105 C104 -1.6(16) . . . . ? C135 C134 C133 C138 -2.0(12) . . . . ? C135 C134 C133 B2 178.0(8) . . . . ? C12 C1 C2 C3 -179.4(9) . . . . ? C20 C19 C24 C23 2.0(17) . . . . ? C20 C21 C22 C23 -5.0(17) . . . . ? B2 C139 C140 C141 178.0(6) . . . . ? B2 C139 C144 C143 -179.5(6) . . . . ? B2 C145 C146 C147 -177.1(7) . . . . ? B2 C145 C150 C149 177.4(7) . . . . ? B2 C127 C128 C129 -176.2(7) . . . . ? B2 C127 C132 C131 177.8(7) . . . . ? B2 C133 C138 C137 -179.0(8) . . . . ? B1 C121 C122 C123 -173.9(7) . . . . ? B1 C121 C126 C125 174.1(7) . . . . ? B1 C103 C104 C105 -173.9(9) . . . . ? B1 C103 C108 C107 174.0(8) . . . . ? C24 C19 C20 C21 0.2(18) . . . . ? C21 C22 C23 C24 7.2(17) . . . . ? loop_ _twin_individual_id _twin_individual_mass_fraction_refined 1 0.90(3) 2 0.10(3)