#------------------------------------------------------------------------------ #$Date: 2021-11-04 01:58:51 +0200 (Thu, 04 Nov 2021) $ #$Revision: 270276 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/86/7708691.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708691 loop_ _publ_author_name 'Zhang, Yue' 'Chen, Dian' 'Jin, Kai-Hang' 'Zang, Shuang-Quan' 'Wang, Qing-Lun' _publ_section_title ; Room-temperature phosphorescence of manganese-based metal halides ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03206B _journal_year 2021 _chemical_formula_moiety 'Cl6 Mn, 2(C4 H9 N5)' _chemical_formula_sum 'C8 H18 Cl6 Mn N10' _chemical_formula_weight 521.96 _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_Hall '-I 2y' _space_group_name_H-M_alt 'I 1 2/m 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-02-26 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-09-17 deposited with the CCDC. 2021-11-01 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 105.229(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 8.9461(3) _cell_length_b 9.6604(3) _cell_length_c 11.2084(3) _cell_measurement_reflns_used 1069 _cell_measurement_temperature 200.00(10) _cell_measurement_theta_max 72.4100 _cell_measurement_theta_min 5.6430 _cell_volume 934.65(5) _computing_cell_refinement 'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.27b (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 200.00(10) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.962 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 62.00 87.00 0.50 0.50 -- 0.00 57.00-180.00 50 2 \w -23.00 27.00 0.50 0.50 -- 0.00 38.00-120.00 100 3 \w -28.00 -2.00 0.50 0.50 -- 0.00 57.00-180.00 52 4 \w 53.00 81.00 0.50 0.50 -- 0.00 38.00-120.00 56 5 \w 63.00 187.00 0.50 0.70 -- 97.60 77.00 -60.00 248 6 \w 80.00 135.00 0.50 0.70 -- 97.60 77.00 0.00 110 7 \w 95.00 187.00 0.50 0.70 -- 97.60 61.00-120.00 184 8 \w 64.00 129.00 0.50 0.70 -- 97.60 -82.00 90.00 130 9 \w 139.00 181.00 0.50 0.70 -- 97.60 77.00 0.00 84 10 \w 10.00 74.00 0.50 0.70 -- 97.60 -77.00 90.00 128 11 \w 77.00 103.00 0.50 0.70 -- 97.60 45.00-120.00 52 12 \w 77.00 103.00 0.50 0.70 -- 97.60 61.00 150.00 52 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC12 (RINC): Kappa single' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0841774000 _diffrn_orient_matrix_UB_12 -0.1356628000 _diffrn_orient_matrix_UB_13 -0.0491084000 _diffrn_orient_matrix_UB_21 -0.0989806000 _diffrn_orient_matrix_UB_22 0.0777110000 _diffrn_orient_matrix_UB_23 -0.1134670000 _diffrn_orient_matrix_UB_31 0.1224475000 _diffrn_orient_matrix_UB_32 -0.0306774000 _diffrn_orient_matrix_UB_33 -0.0709000000 _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0284 _diffrn_reflns_av_unetI/netI 0.0408 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.962 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 1961 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.962 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.220 _diffrn_reflns_theta_min 5.656 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 13.802 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.51266 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.27b (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.855 _exptl_crystal_description block _exptl_crystal_F_000 526 _exptl_crystal_size_max 0.07 _exptl_crystal_size_mid 0.05 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.454 _refine_diff_density_min -0.531 _refine_diff_density_rms 0.101 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.029 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 65 _refine_ls_number_reflns 963 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.029 _refine_ls_R_factor_all 0.0384 _refine_ls_R_factor_gt 0.0375 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0750P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1024 _refine_ls_wR_factor_ref 0.1031 _reflns_Friedel_coverage 0.000 _reflns_number_gt 907 _reflns_number_total 963 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL hy_a.res in I2/m hy.res created by SHELXL-2016/4 at 16:10:36 on 26-Feb-2020 REM Old TITL hy_a.res in I2/m REM SHELXT solution in I2/m REM R1 0.082, Rweak 0.007, Alpha 0.024, Orientation as input REM Formula found by SHELXT: C16 N2 Mn Cl6 CELL 1.54184 8.9461 9.6604 11.2084 90 105.229 90 ZERR 2 0.0003 0.0003 0.0003 0 0.003 0 LATT 2 SYMM -X,+Y,-Z SFAC C H Cl Mn N UNIT 16 36 12 2 20 L.S. 4 0 0 PLAN 20 SIZE 0.05 0.07 0.05 BOND $H list 4 htab fmap 2 53 acta REM REM REM WGHT 0.075000 FVAR 0.44350 MN1 4 0.500000 0.500000 0.500000 10.25000 0.02617 0.02207 = 0.02050 0.00000 0.00437 0.00000 CL1 3 0.795370 0.500000 0.540338 10.50000 0.02817 0.03181 = 0.02635 0.00000 0.00688 0.00000 CL2 3 0.462396 0.310162 0.334298 11.00000 0.03173 0.02503 = 0.02316 -0.00299 0.00548 -0.00106 N1 5 0.755787 0.119928 0.516318 11.00000 0.03449 0.02167 = 0.02004 -0.00091 0.00573 0.00077 AFIX 43 H1 2 0.736439 0.196575 0.548333 11.00000 -1.20000 AFIX 0 N2 5 0.857694 0.245543 0.380776 11.00000 0.03674 0.02339 = 0.02178 0.00225 0.00901 0.00006 AFIX 93 H2A 2 0.840492 0.319408 0.417897 11.00000 -1.20000 H2B 2 0.898654 0.251297 0.319595 11.00000 -1.20000 AFIX 0 N3 5 0.653563 0.000000 0.654061 10.50000 0.04649 0.02599 = 0.02472 0.00000 0.01533 0.00000 AFIX 93 H3A 2 0.630746 -0.077094 0.683384 10.50000 -1.20000 H3B 2 0.631843 0.077094 0.684036 10.50000 -1.20000 AFIX 0 C1 1 0.821285 0.123530 0.417646 11.00000 0.02449 0.02500 = 0.01764 0.00163 0.00041 0.00134 C2 1 0.721525 0.000000 0.563578 10.50000 0.02608 0.02529 = 0.01751 0.00000 0.00010 0.00000 C3 1 0.849790 0.000000 0.365031 10.50000 0.03263 0.02524 = 0.01907 0.00000 0.00619 0.00000 AFIX 43 H3 2 0.887592 0.000000 0.295258 10.50000 -1.20000 AFIX 0 HKLF 4 REM hy_a.res in I2/m REM R1 = 0.0375 for 907 Fo > 4sig(Fo) and 0.0384 for all 963 data REM 65 parameters refined using 0 restraints END WGHT 0.0750 0.0000 REM Instructions for potential hydrogen bonds HTAB N1 CL1 EQIV $1 -x+1, y, -z+ HTAB N1 CL2_$1 HTAB N2 CL1 EQIV $2 -x+3/2, -y+1/2, -z+1/ HTAB N2 CL2_$2 EQIV $3 -x+1, -y, -z+ HTAB N3 CL2_$3 HTAB N3 CL2_$1 HTAB C3 CL2_$2 EQIV $4 -x+3/2, y-1/2, -z+1/ HTAB C3 CL2_$4 REM Highest difference peak 0.454, deepest hole -0.531, 1-sigma level 0.101 Q1 1 0.3543 0.5000 0.4959 10.50000 0.05 0.45 Q2 1 0.4892 0.3694 0.5338 11.00000 0.05 0.43 Q3 1 0.4607 0.4342 0.3597 11.00000 0.05 0.39 Q4 1 0.8407 0.4600 0.6648 11.00000 0.05 0.35 Q5 1 0.8632 0.5000 0.6576 10.50000 0.05 0.35 Q6 1 0.9157 0.5000 0.6407 10.50000 0.05 0.34 Q7 1 0.9245 0.0000 0.3434 10.50000 0.05 0.32 Q8 1 0.3382 0.4183 0.3217 11.00000 0.05 0.32 Q9 1 0.5187 0.2760 0.4620 11.00000 0.05 0.31 Q10 1 0.4865 0.1890 0.3058 11.00000 0.05 0.31 Q11 1 0.5983 0.3125 0.3425 11.00000 0.05 0.30 Q12 1 0.3241 0.3215 0.2648 11.00000 0.05 0.30 Q13 1 0.4400 0.1992 0.3934 11.00000 0.05 0.29 Q14 1 0.8091 0.3773 0.4950 11.00000 0.05 0.29 Q15 1 0.3204 0.3076 0.3022 11.00000 0.05 0.29 Q16 1 0.7832 0.0000 0.6970 10.50000 0.05 0.29 Q17 1 0.5993 0.3181 0.3980 11.00000 0.05 0.28 Q18 1 0.4875 0.0000 0.6008 10.50000 0.05 0.28 Q19 1 0.8281 -0.0287 0.3601 11.00000 0.05 0.27 Q20 1 0.6029 0.5000 0.6343 10.50000 0.05 0.26 REM The information below was added by Olex2. REM REM R1 = 0.0375 for 907 Fo > 4sig(Fo) and 0.0384 for all 1961 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.45, deepest hole -0.53 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0384 REM R1_gt = 0.0375 REM wR_ref = 0.1031 REM GOOF = 1.029 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 1961 REM Reflections_gt = 907 REM Parameters = n/a REM Hole = -0.53 REM Peak = 0.45 REM Flack = n/a ; _cod_data_source_file d1dt03206b2.cif _cod_data_source_block 3 _cod_database_code 7708691 _shelx_shelxl_version_number 2016/4 _chemical_oxdiff_usercomment ' ' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.545 _shelx_estimated_absorpt_t_min 0.445 _reflns_odcompleteness_completeness 99.78 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups, All N(H,H) groups 2. Others Fixed Sof: H3A(0.5) H3B(0.5) 3.a Aromatic/amide H refined with riding coordinates: N1(H1), C3(H3) 3.b X=CH2 refined with riding coordinates: N2(H2A,H2B), N3(H3A,H3B) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.695 _oxdiff_exptl_absorpt_empirical_full_min 0.675 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z+1/2' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z+1/2' 'x+1/2, -y+1/2, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Mn1 Mn 0.500000 0.500000 0.500000 0.0232(2) Uani 1 4 d S T P . . Cl1 Cl 0.79537(9) 0.500000 0.54034(7) 0.0288(3) Uani 1 2 d S T P . . Cl2 Cl 0.46240(6) 0.31016(6) 0.33430(5) 0.0270(2) Uani 1 1 d . . . . . N1 N 0.7558(2) 0.1199(2) 0.51632(18) 0.0257(5) Uani 1 1 d . . . . . H1 H 0.736439 0.196575 0.548333 0.031 Uiso 1 1 calc R . . . . N2 N 0.8577(2) 0.2455(2) 0.38078(19) 0.0271(5) Uani 1 1 d . . . . . H2A H 0.840492 0.319408 0.417897 0.032 Uiso 1 1 calc R . . . . H2B H 0.898654 0.251297 0.319595 0.032 Uiso 1 1 calc R . . . . N3 N 0.6536(4) 0.000000 0.6541(3) 0.0313(7) Uani 1 2 d S T P . . H3A H 0.630746 -0.077094 0.683384 0.038 Uiso 0.5 1 calc R . . . . H3B H 0.631843 0.077094 0.684036 0.038 Uiso 0.5 1 calc R . . . . C1 C 0.8213(2) 0.1235(3) 0.4176(2) 0.0233(5) Uani 1 1 d . . . . . C2 C 0.7215(4) 0.000000 0.5636(3) 0.0240(7) Uani 1 2 d S T P . . C3 C 0.8498(4) 0.000000 0.3650(3) 0.0258(7) Uani 1 2 d S T P . . H3 H 0.887592 0.000000 0.295258 0.031 Uiso 1 2 calc RS T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Mn1 0.0262(4) 0.0221(4) 0.0205(4) 0.000 0.0044(3) 0.000 Cl1 0.0282(4) 0.0318(5) 0.0264(4) 0.000 0.0069(3) 0.000 Cl2 0.0317(4) 0.0250(4) 0.0232(3) -0.0030(2) 0.0055(2) -0.0011(2) N1 0.0345(10) 0.0217(12) 0.0200(9) -0.0009(8) 0.0057(7) 0.0008(8) N2 0.0367(11) 0.0234(12) 0.0218(9) 0.0022(8) 0.0090(8) 0.0001(9) N3 0.0465(17) 0.0260(16) 0.0247(14) 0.000 0.0153(13) 0.000 C1 0.0245(10) 0.0250(14) 0.0176(10) 0.0016(9) 0.0004(8) 0.0013(9) C2 0.0261(15) 0.0253(18) 0.0175(14) 0.000 0.0001(11) 0.000 C3 0.0326(16) 0.0252(19) 0.0191(15) 0.000 0.0062(12) 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Mn Mn -0.5299 2.8052 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Cl1 Mn1 Cl1 180.0 . 5_666 ? Cl1 Mn1 Cl2 93.482(18) . 6_565 ? Cl1 Mn1 Cl2 93.481(18) 5_666 2_656 ? Cl1 Mn1 Cl2 93.481(18) 5_666 5_666 ? Cl1 Mn1 Cl2 86.518(18) 5_666 . ? Cl1 Mn1 Cl2 86.518(18) . 2_656 ? Cl1 Mn1 Cl2 86.519(17) 5_666 6_565 ? Cl1 Mn1 Cl2 93.482(18) . . ? Cl1 Mn1 Cl2 86.518(18) . 5_666 ? Cl2 Mn1 Cl2 88.88(3) 5_666 6_565 ? Cl2 Mn1 Cl2 88.88(3) . 2_656 ? Cl2 Mn1 Cl2 91.12(3) . 6_565 ? Cl2 Mn1 Cl2 180.0 6_565 2_656 ? Cl2 Mn1 Cl2 91.12(3) 5_666 2_656 ? Cl2 Mn1 Cl2 180.0 . 5_666 ? C1 N1 H1 119.1 . . ? C2 N1 H1 119.1 . . ? C2 N1 C1 121.8(2) . . ? H2A N2 H2B 120.0 . . ? C1 N2 H2A 120.0 . . ? C1 N2 H2B 120.0 . . ? H3A N3 H3B 120.0 . . ? C2 N3 H3A 120.0 . . ? C2 N3 H3B 120.0 . . ? N1 C1 C3 118.9(2) . . ? N2 C1 N1 117.7(2) . . ? N2 C1 C3 123.3(2) . . ? N1 C2 N1 119.3(3) 6 . ? N3 C2 N1 120.34(15) . 6 ? N3 C2 N1 120.34(15) . . ? C1 C3 C1 119.1(3) 6 . ? C1 C3 H3 120.4 . . ? C1 C3 H3 120.4 6 . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Mn1 Cl1 2.5611(8) . ? Mn1 Cl1 2.5611(8) 5_666 ? Mn1 Cl2 2.5686(6) 2_656 ? Mn1 Cl2 2.5686(6) 5_666 ? Mn1 Cl2 2.5686(6) 6_565 ? Mn1 Cl2 2.5686(6) . ? N1 H1 0.8600 . ? N1 C1 1.381(3) . ? N1 C2 1.342(3) . ? N2 H2A 0.8600 . ? N2 H2B 0.8600 . ? N2 C1 1.318(3) . ? N3 H3A 0.8600 . ? N3 H3B 0.8600 . ? N3 C2 1.312(4) . ? C1 C3 1.384(3) . ? C2 N1 1.342(3) 6 ? C3 C1 1.384(3) 6 ? C3 H3 0.9300 . ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma 0 0 2 2144.24 88.61 0 0 4 252.03 12.01 0 0 6 2225.94 93.76 0 0 -8 0.09 1.37 0 0 -10 99.69 7.15 0 0 -12 224.24 11.43 0 1 1 67.91 3.33 0 -1 1 71.02 3.31 0 1 1 64.76 3.14 0 1 -1 74.71 3.3 0 -1 3 314.18 14.21 0 -1 5 694.79 31.34 0 -1 5 718.87 31.64 0 1 -7 97.78 6.12 0 1 -9 26.08 3.31 0 -1 -11 3.02 2.19 0 1 -11 3.32 1.79 0 1 -11 5.61 2.93 0 1 -13 14.66 1.78 0 -2 0 146.09 6.61 0 2 2 2812.6 116.03 0 2 2 2835.59 116.5 0 -2 4 1800.53 75.04 0 2 4 1766.2 75.22 0 2 -6 11.47 1.93 0 2 -8 41.65 4.04 0 -2 -10 6.49 2.25 0 2 -10 3.54 2.47 0 2 -12 80.63 5.46 0 2 -12 75.03 4.83 0 -3 -1 432.91 18.85 0 -3 -1 455.43 19.16 0 3 3 6746.73 274.89 0 3 3 6591.94 275.65 0 -3 -3 6701.05 274.89 0 3 5 47.05 4.08 0 3 -7 51.55 4.57 0 3 9 677.46 29.98 0 3 -9 657.92 30.76 0 3 -9 648.06 30.56 0 3 -11 3.23 2.26 0 3 -11 5.32 2.63 0 -4 0 1836.88 76.7 0 -4 0 1857.06 76.76 0 4 -2 122.56 6.67 0 4 -4 44.43 3.64 0 4 -6 187.34 10.42 0 4 -6 185.44 10.49 0 4 -8 59.86 5.65 0 4 8 56.77 4.87 0 4 -8 62.07 5.63 0 4 -10 80.47 6.36 0 4 -10 84.04 6.46 0 4 10 81.73 5.52 0 4 -12 64.38 4.3 0 4 -12 70.8 4.45 0 -5 1 1902.4 81.9 0 5 -1 1925.21 82.34 0 -5 -1 2011.72 82.06 0 -5 -1 1993.92 81.64 0 5 -3 106.14 6.04 0 5 -3 80.96 6.01 0 5 -5 880.04 38.99 0 5 -5 890.65 39.72 0 5 -5 897.79 38.9 0 5 -7 239.53 13.41 0 5 -7 229.64 12.79 0 5 9 123.45 7.77 0 5 -9 114.52 7.97 0 5 -11 126.48 7.16 0 5 -11 129.83 7.63 0 -6 0 1845.79 77.48 0 6 0 1785.47 77.75 0 6 -2 149.95 9.75 0 -6 2 181.4 10.18 0 6 2 161.47 9.38 0 6 -4 75.5 6 0 6 -4 78.77 5.88 0 6 -6 571.35 27.44 0 6 8 72.74 5.84 0 6 -8 69.66 5.57 0 6 -8 72.6 6.48 0 6 10 121.93 6.83 0 6 -10 111.8 6.62 0 7 1 8.69 3.25 0 -7 1 9.82 2.57 0 7 3 796.73 36.09 0 7 -3 786.49 36.94 0 -7 3 839.7 37.81 0 7 -5 58.73 5.53 0 7 -5 57.49 5.41 0 7 -7 4.6 2.86 0 7 9 108.36 6.65 0 7 -9 101.16 7.12 0 8 0 422.2 22.29 0 8 -2 1249.66 57.32 0 -8 2 1275.65 57.22 0 8 2 1303.87 56.63 0 8 -4 257 14.59 0 -8 4 261.38 15.27 0 8 -6 101.38 6.57 0 8 -6 80.99 6.47 0 8 -8 169.7 9.84 0 8 8 181.21 9.75 0 9 -1 3.86 4.65 0 9 1 5.44 4.01 0 9 -3 295.02 16.05 0 -9 3 254.26 15.3 0 9 3 275.67 14.5 0 9 -5 40.35 4.69 0 9 7 1.58 1.48 0 10 0 822.95 38.11 0 10 -2 51.19 6.42 0 10 2 50.9 5.12 0 10 4 13.81 2.23 0 10 -4 15.37 3.38 0 10 6 299.69 14.15 0 11 1 284.55 13.49 0 11 -1 241.46 13.62 0 11 -3 2.3 2.3 1 0 -13 361.14 16.23 1 0 -11 223.35 12.13 1 0 -9 5.37 2.47 1 0 -7 4666.05 193.07 -1 0 5 4207.97 174.26 -1 0 5 4191.02 173.6 -1 0 3 663.25 28.39 1 0 -1 846.72 33.6 -1 0 1 781.6 33.53 1 0 1 283.14 12.16 1 0 3 672.64 29.34 1 0 5 395.43 18.87 -1 0 -7 126.91 7.33 -1 0 -9 782.58 34.68 -1 0 -11 267.15 13.72 1 -1 -12 149.43 8.19 1 1 -12 152.57 8.69 1 -1 -10 85.48 6.32 1 1 -10 92.1 6.98 1 1 -10 87.72 6.15 1 1 -8 136.25 8.11 -1 -1 6 603.25 28.99 -1 -1 6 649.38 28.46 -1 1 4 237.87 10.77 -1 1 2 390.86 16.25 1 -1 0 1060.28 43.96 -1 -1 -2 65.23 3.57 1 1 2 61.43 3.59 1 -1 2 53.48 3.89 1 1 4 65.92 4.73 1 -1 4 73.19 5 1 1 6 195.65 9.72 -1 1 -6 187.52 9.93 -1 -1 -6 187.42 9.69 -1 1 -8 22.41 3 -1 1 -10 30.79 3.64 -1 1 -12 150.36 8.13 -1 -1 -12 144.24 7.67 1 2 -13 14.54 1.91 1 2 -11 63.28 5.68 1 2 -11 67.84 5.16 1 -2 -9 1194.51 52.09 1 2 -9 1209.34 52.57 1 2 -7 119.8 7.39 -1 -2 5 162.41 8.99 1 2 -3 3937.17 161.08 -1 2 3 3894.19 160.06 -1 -2 1 404.66 17.48 1 -2 -1 403.11 16.77 1 2 1 100.7 5.17 -1 -2 -1 113.42 5.4 1 2 3 38.54 2.91 -1 -2 -3 39.25 2.84 1 -2 3 34.87 2.77 -1 2 -5 398.23 18.92 1 -2 5 429.66 19.97 1 2 7 14.1 2.14 -1 2 -7 13.04 2.47 -1 2 -9 307.16 15.71 -1 -2 -11 3.58 1.75 -1 2 -11 5.32 2.08 1 3 -12 9.28 1.94 1 3 -10 1217.5 53.73 1 3 -10 1231.9 53.86 1 3 -8 1047.07 47.2 1 3 -8 1086.65 47.31 1 3 -6 12.98 2.34 1 3 -6 5.7 1.99 -1 3 4 2105.16 92.92 -1 3 4 2256.22 91.49 1 3 -2 450.43 19.38 -1 -3 2 419.04 19.19 -1 -3 0 1191.61 49.86 1 3 2 1002.64 42.37 1 3 4 119.34 7.2 -1 -3 -4 124.18 6.69 1 3 4 113.63 6.58 1 3 6 612.36 27.5 1 3 8 126.39 7.78 -1 3 -8 124.28 8.16 -1 3 -10 3.98 2.85 -1 3 -10 4.64 2.57 -1 3 -12 140.49 7.4 -1 3 -12 148.16 7.67 1 4 -11 4.41 2.39 1 4 -11 3.44 2.56 1 4 -9 10.23 3.14 -1 4 9 11.14 2.34 1 4 -9 8.51 3.15 1 4 -7 344.25 17.52 1 4 -5 1065.04 44.5 1 4 -5 974.48 44.66 -1 -4 3 759.29 20.4 1 4 -3 798.81 20.76 -1 -4 1 136.66 6.8 1 -4 -1 127.45 6.05 -1 -4 -1 45.2 3.04 -1 -4 -1 46.57 3.22 -1 4 -1 37.12 2.63 1 4 3 2.92 1.04 -1 -4 -3 2.79 1.11 -1 4 -5 35.21 3.52 1 4 7 19.62 2.89 -1 4 -9 58.42 5.59 -1 4 -9 59.31 5.61 1 4 9 66.7 5.19 -1 4 -11 332.11 16.27 -1 4 -11 356.32 16.57 1 5 -12 368.79 16.02 1 5 -12 331.38 15.49 1 5 -10 100.28 7.23 -1 5 10 96.48 6.26 1 5 -10 95.08 6.71 1 5 -8 416.45 20.79 1 5 -6 1884.94 80.97 1 5 -6 1877.27 80.22 1 5 -4 18.01 2.72 1 5 -4 17.05 2.73 -1 -5 2 3.72 1.14 1 5 -2 4.61 1.99 1 5 -2 4.89 1.37 -1 -5 0 1121.73 45.19 -1 -5 0 1058.46 44.74 -1 5 0 980.82 44.48 1 -5 0 1078.16 44.37 -1 5 0 1022.99 45.66 -1 5 -2 189.46 10.31 -1 5 -4 17.9 2.62 -1 5 -4 20.56 2.8 -1 5 -6 450.29 21.91 -1 5 -6 477.57 22.5 1 5 8 196.47 11.1 -1 5 -8 197.31 11.61 -1 5 -8 188.21 11.18 -1 5 -10 110.37 6.81 -1 5 -10 101.87 7.1 1 5 10 114.2 6.64 1 6 -11 96.17 5.79 1 6 -11 81.99 4.9 -1 6 9 9.43 2.29 1 6 -9 8.99 3.45 1 6 -9 10.3 2.49 1 6 -7 705.41 30.49 1 6 -7 577.53 28.54 1 6 -5 315.96 16.51 1 6 -5 349.37 17.39 -1 6 3 12.26 2.53 1 6 -3 15.82 2.46 1 6 -3 16.26 3.29 -1 -6 1 1222.49 51.78 -1 6 1 1134.07 51.43 1 6 1 59.12 4.84 -1 -6 -1 54.04 4.62 -1 6 -1 50.16 5.01 1 6 3 669.37 30.67 -1 6 -3 681.41 31.58 -1 6 -3 726.42 31.01 -1 6 -5 46.41 4.52 -1 6 -5 52.89 4.92 -1 6 -7 37.02 4.72 1 6 7 36.28 4.12 1 6 9 55.91 4.6 -1 6 -9 53.44 4.95 -1 6 -9 48.48 4.11 -1 7 10 207.1 10.18 1 7 -10 201.35 10.79 1 7 -8 105.17 8 1 7 -6 18.71 3.28 1 7 -6 13.39 3.47 1 7 -4 599.22 27.45 1 7 -4 569.81 27.81 1 7 -2 212.5 13.17 -1 7 2 242.73 13.15 -1 -7 2 224 13.5 -1 -7 0 19.94 3.47 1 7 0 21.81 4.09 -1 7 0 16.72 3.88 1 7 2 109.4 7.61 -1 7 -2 114.58 8.49 -1 7 -4 4.74 2.01 -1 7 -4 10.13 3.47 1 7 6 85.27 6.82 -1 7 -6 96.12 7.09 1 7 8 81.8 5.96 -1 7 -8 78.34 6.21 1 7 10 59.82 3.7 -1 7 -10 60.27 4.03 -1 8 9 559.17 24.66 1 8 -9 540.26 25.01 -1 -8 7 83.48 7.01 1 8 -7 67.81 5.89 -1 -8 5 279.79 16.3 1 8 -5 272.76 14.62 1 8 -5 255.54 14.14 1 8 -3 943.29 43.87 -1 -8 3 958.23 44.82 -1 8 3 962.31 42.9 1 8 -1 217.17 14.26 -1 -8 1 247.87 14.52 -1 8 1 238.27 14.2 1 8 1 16.49 4.34 1 8 3 627.02 28.83 -1 8 -3 618.16 30.07 1 8 5 180.12 10.34 -1 8 -5 183.06 10.3 -1 8 -7 187.83 10.52 1 8 9 69.64 4.17 -1 8 -9 60.2 4.05 1 9 -8 58.72 3.99 -1 -9 6 9.57 2.72 1 9 -6 5.8 2.26 -1 -9 4 163.05 11.14 1 9 -4 161.97 10.58 -1 -9 2 145.1 10.65 -1 9 2 141.46 9.86 -1 9 0 5.06 4.25 1 9 0 7.36 4.71 -1 9 -2 21.44 5.24 1 9 2 15.04 2.54 1 9 2 20.16 3.99 1 9 4 2.65 1.8 -1 9 -4 3.09 3.39 1 9 6 4.61 1.94 -1 10 7 285.1 13.21 1 10 -5 123.43 7.36 -1 10 5 113.22 6.89 1 10 -3 2.21 3.62 -1 10 3 2.56 2.29 1 10 -1 354.06 19.71 -1 10 1 399.01 19.6 1 10 1 25.98 4.27 1 10 3 231.54 12.64 -1 10 -3 319.97 14.88 1 10 5 22.75 2.43 -1 10 -5 19.42 2.62 1 11 -4 3.03 1.8 -1 11 2 2.4 1.88 1 11 0 156.91 8.97 -1 11 0 146.33 8.87 -1 11 -2 30.06 3.68 1 11 2 19.86 2.34 -1 11 -4 1.98 1.39 2 0 -12 409.15 19.19 2 0 -10 43.9 4.69 2 0 -8 18.75 2.98 -2 0 6 234.94 11.62 -2 0 6 239.2 12.74 -2 0 4 1555.88 65.47 -2 0 2 208.36 9.22 2 0 -2 209.91 9.37 2 0 0 90.87 4.41 -2 0 0 84.42 4.09 2 0 2 9999 410.31 2 0 4 21.25 2.53 -2 0 -6 2760.58 115.67 -2 0 -8 2.07 1.87 -2 0 -10 109.81 6.69 -2 0 -12 409.47 18.32 2 1 -13 366.87 16.66 2 1 -11 290.32 15.26 2 -1 -11 296.11 14.79 2 1 -9 8.97 3.03 2 -1 -9 7.34 2.49 2 1 -9 9.19 2.4 2 1 -7 310.67 15.52 2 -1 -7 318.47 15.39 2 1 -7 309.81 15.58 -2 1 5 102.72 5.34 -2 -1 5 108.15 6.52 -2 1 5 108.74 6.46 -2 -1 3 653.89 26.78 -2 1 3 654.64 26.78 2 1 -3 634.76 26.86 -2 1 3 601.63 25.93 2 -1 -1 358.28 15.48 -2 1 1 358.53 15.62 -2 -1 1 393.1 16.07 2 1 -1 381.26 15.98 2 -1 1 2555.65 104.69 -2 -1 -1 2524.43 105.14 -2 -1 -3 284.79 13.87 2 -1 3 282.02 14.54 2 1 3 316.82 14.12 2 1 5 505.06 22.28 -2 1 -5 502.29 22.61 -2 -1 -5 461.51 22.29 -2 1 -7 336.69 16.79 2 1 7 339.66 16.47 -2 -1 -7 343.54 16.5 -2 1 -9 85.56 6.18 -2 -1 -9 83.45 5.54 -2 1 -11 219.12 11.31 -2 -1 -11 205.98 10.86 -2 1 -11 214.02 10.66 2 2 -12 19.86 3.1 2 2 -10 539.17 25.27 2 2 -10 510.1 24.8 2 2 -8 330.28 16.32 2 2 -8 300.83 16.21 2 2 -6 130.46 7.98 -2 2 6 152.07 8.58 -2 -2 4 223.19 10.89 -2 2 2 73.03 3.57 -2 -2 2 76.96 4.21 -2 2 2 70.53 3.56 -2 -2 0 1560.63 67.5 2 -2 0 1657.55 67.13 2 2 2 873.95 36.59 2 -2 2 869.37 35.96 2 -2 2 790.84 36.94 -2 -2 -4 398.41 18.9 2 -2 4 454.95 19.85 2 2 4 391.21 19.11 2 2 4 384.08 19.21 2 -2 4 403.53 18.97 2 2 6 28.12 3.03 -2 -2 -6 30.63 3.29 -2 2 -6 28.94 3.39 2 2 8 673.02 30.04 -2 2 -8 649.09 30.35 -2 2 -10 432.48 20.56 2 3 -13 4.32 1.36 2 3 -11 75.81 5.83 2 3 -9 259.31 14.15 2 3 -9 244.82 14.16 2 3 -7 396.45 19.78 2 3 -7 412.06 19.97 2 3 -5 12.08 2.02 2 3 -5 10.14 1.95 -2 3 5 8.14 1.54 -2 -3 5 10.96 1.94 2 3 -3 227.92 10.54 -2 3 3 194.65 9.4 -2 -3 3 206.62 10.19 -2 -3 1 2618.97 106.18 2 -3 -1 2532.26 105.26 2 3 1 3.67 1.09 2 -3 1 3.13 1.33 2 -3 3 720.4 31.28 2 3 3 679.31 30.58 -2 -3 -3 691.52 30.52 -2 -3 -5 312.99 14.93 -2 3 -5 308.08 15.31 2 3 5 300.12 15.03 -2 3 -7 210.91 12.18 2 3 7 242.41 12.29 2 3 9 931.52 41.06 -2 3 -9 930.62 41.46 -2 3 -11 12.82 2.25 -2 3 -11 11.84 2.34 2 4 -12 158.35 8.49 2 4 -12 160.08 8.6 2 4 -10 529.11 25.27 2 4 -10 530.26 25.45 2 4 -8 302.77 16.18 2 4 -8 300.86 16.29 2 4 -6 16.21 2.73 2 4 -4 4.21 1.57 -2 -4 2 714.6 31.15 2 -4 0 81.31 4.97 -2 -4 0 93.93 5.33 -2 -4 0 82.96 5.06 2 -4 2 2.35 1.32 2 4 2 4.41 1.3 -2 4 -4 746.47 31.64 -2 4 -4 673.41 30.9 -2 4 -6 783.26 35.26 2 4 6 777.38 34.9 2 4 8 129.41 8.25 -2 4 -10 97.9 6.52 -2 4 -10 107.73 6.88 2 4 10 98.41 6.11 2 5 -11 25.86 3.41 2 5 -11 25.98 3.07 2 5 -9 364.27 18.82 2 5 -9 346.02 18.01 2 5 -7 327.08 17.76 2 5 -7 335.06 17.13 2 5 -5 20.04 3.21 2 5 -5 19.07 2.94 2 5 -5 15.58 2.46 2 5 -3 1395.65 59.31 2 5 -3 1375.99 59.9 -2 -5 1 96.22 5.92 2 5 -1 105.39 6.71 -2 -5 -1 17.72 2.38 2 5 1 13.97 2.28 -2 5 -3 460.03 20.45 -2 5 -3 402.32 19.7 -2 5 -5 384.35 18.86 2 5 7 237.5 12.76 -2 5 -7 234.8 12.78 -2 5 -7 232.54 13.11 -2 5 -9 3.22 2.02 -2 5 -9 0.24 2.56 2 5 9 2.66 1.78 -2 5 -11 228.17 10.89 2 6 -12 86.84 4.79 2 6 -10 2.29 1.8 -2 6 10 1.74 1.39 2 6 -8 155.53 9.43 2 6 -8 162.72 10.82 2 6 -6 342.47 16.94 2 6 -6 329.67 16.68 2 6 -6 362.76 18.59 2 6 -4 239.36 12.3 -2 6 4 196.51 11.23 2 6 -4 222.4 12.33 2 6 -2 19.6 3.53 -2 6 2 15.55 3 2 6 -2 17.17 2.37 -2 -6 2 15.63 2.9 -2 -6 0 141.15 9.06 -2 6 0 141.59 9.28 2 6 0 163.61 9.26 2 6 2 72.68 5.43 -2 6 -2 84.96 6.5 2 6 4 114.93 7.6 -2 6 -4 121.39 7.84 -2 6 -4 115.25 7.42 -2 6 -6 495.12 23.94 -2 6 -8 6.87 2.84 2 6 8 5.53 2.21 2 6 10 218.7 10.65 -2 6 -10 226.03 11.01 2 7 -9 137.27 8.96 2 7 -7 17.03 3.99 2 7 -5 10.23 3.05 2 7 -5 5.36 3.19 -2 -7 3 32.44 4.64 -2 7 3 33.45 4.24 2 7 -3 31.62 3.65 2 7 -3 37.82 5.2 -2 -7 1 57.09 5.58 2 7 -1 51.47 5.56 -2 7 1 46.28 5.38 2 7 1 202.93 11.11 2 7 1 168.99 9.94 -2 7 -1 192.36 11.76 2 7 3 476.62 22.43 -2 7 -3 496.58 23.69 2 7 3 469.21 22.88 -2 7 -5 3.7 2.64 2 7 5 3.41 2.37 -2 7 -5 0.4 1.93 -2 7 -7 84.59 6.4 2 7 9 253.84 12.12 -2 7 -9 242.98 12.18 -2 8 10 233.39 10.32 2 8 -10 203.46 10.76 -2 -8 8 8.39 2.76 2 8 -8 4.81 2.37 2 8 -6 405.23 19.41 2 8 -6 388.31 19.95 -2 -8 6 393.88 21.47 2 8 -4 266.53 15.08 -2 -8 4 254.98 15.86 2 8 -4 255.86 13.79 -2 8 4 267.26 14.01 -2 8 2 21.6 4.71 -2 -8 2 21.26 4.26 -2 8 0 820.62 41.44 2 8 0 978.01 41.81 -2 8 -2 8.46 4.29 2 8 2 6.76 2.13 2 8 2 10.5 3.15 -2 8 -4 30.09 4.78 2 8 4 33.37 4.07 -2 8 -6 0.86 1.66 2 8 6 0.12 1.87 -2 8 -8 405.18 18.39 -2 9 9 51.59 3.29 2 9 -7 2.57 1.64 -2 -9 7 3.74 2.1 -2 -9 5 7.28 3.12 2 9 -5 6.36 3.22 -2 9 3 2.75 3.03 -2 -9 3 4.07 3.06 2 9 -3 6.17 4.68 -2 9 1 4.15 4.13 2 9 -1 4.52 4.41 2 9 1 231.73 13.58 -2 9 -3 277.2 14.76 2 9 3 240.99 13.32 -2 9 -5 4.66 2.28 2 9 5 3.37 1.87 2 9 7 72.15 4.56 2 10 -6 105.54 5.96 2 10 -4 162.32 9.83 -2 10 2 14.91 3.5 -2 10 0 48.42 5.76 2 10 0 65.86 6.18 -2 10 -2 117.6 8.19 2 10 2 92.2 6.43 2 10 4 15.23 1.98 -2 10 -4 18.2 3 2 11 -3 140.66 8.25 -2 11 1 41.39 3.97 2 11 -1 45.64 4.28 2 11 1 1.32 1.61 -2 11 -3 73.34 4.87 3 0 -13 106.82 5.72 3 0 -11 117.59 7.66 3 0 -9 254.87 13.93 3 0 -7 415.94 19.79 -3 0 5 811.64 34.63 -3 0 3 1154.15 48.3 3 0 -1 6410.27 263.2 -3 0 -1 2923.21 121.27 3 0 3 101.67 5.96 -3 0 -5 1556.26 66.59 3 0 5 1550.75 66.47 -3 0 -7 182.02 10.63 3 0 7 184.53 10.28 -3 0 -9 17.01 2.79 -3 0 -11 372.03 17.23 3 -1 -12 27.31 2.74 3 1 -12 26.28 3.16 3 -1 -10 97.14 6.8 3 1 -10 93.39 7.2 3 -1 -8 7.08 2.18 3 1 -8 4.54 2.41 3 1 -8 4.39 2.14 -3 -1 6 585.45 26.31 3 1 -6 578.79 26.24 -3 1 6 596.15 27.07 3 1 -6 582.29 26.37 -3 1 4 81.08 4.09 -3 -1 4 91.42 4.92 3 -1 -2 679.56 29.47 -3 -1 2 721.9 30.29 3 1 -2 710.88 30.17 3 1 -2 740.01 30.32 -3 -1 0 1508.2 62.86 3 1 0 1495.82 63 -3 1 0 1518.77 63.14 3 -1 2 114.81 5.81 3 1 4 621.1 26.25 -3 -1 -4 612.99 26.17 3 -1 4 562.6 26.07 -3 1 -6 608.01 28.98 3 1 6 645.23 28.86 -3 -1 -6 624.77 28.93 -3 1 -8 6.21 2.61 3 1 8 6.61 1.91 -3 -1 -8 6.33 2.19 -3 1 -10 4.58 1.96 3 2 -13 41.14 3.15 3 2 -11 20.47 2.96 3 2 -11 24.58 3.79 3 2 -9 106.08 7.74 3 2 -9 91.5 7.25 3 2 -7 508.52 24.05 3 2 -7 513.19 24.27 3 2 -5 128.59 7.33 -3 -2 5 128.13 7.29 -3 2 5 130.78 7.29 -3 -2 3 2278.79 97.01 3 2 -3 2393.44 97.4 3 -2 -1 113.4 5.66 3 2 -1 128.32 6.56 -3 -2 1 131.42 6.78 -3 -2 -1 399.98 18.65 3 -2 1 420.12 17.59 -3 -2 -3 2714.16 110.41 3 2 3 2592.85 110.58 3 2 3 2636.95 110.08 3 -2 3 2601.6 109.45 -3 -2 -5 175.74 10.31 3 2 5 196.8 10.42 -3 2 -7 272.31 14.52 -3 -2 -7 253.46 13.76 -3 -2 -7 284.09 14.54 3 2 7 287.94 14.38 3 2 9 192.39 10.7 -3 2 -9 217.1 11.43 -3 2 -11 80.61 4.85 -3 2 -11 80.18 4.56 3 3 -12 83.96 5.61 3 3 -12 79 5.22 3 3 -10 87.81 6.87 3 3 -8 225.17 12.83 3 3 -8 218.94 13.01 3 3 -6 400.48 18.45 3 3 -6 358.97 18.53 -3 -3 4 1247.39 52.03 3 3 -4 1178.58 52.25 -3 -3 2 386.1 17.7 -3 -3 0 170.49 8.57 3 3 0 161.9 8.67 3 -3 2 2833.66 119.49 3 3 2 2780.37 118.76 3 3 2 2942.27 119.2 3 3 4 234.79 12.45 -3 3 -4 251.63 13.12 -3 -3 -6 4.42 2.15 -3 3 -6 3.5 2.35 3 3 6 1.68 1.81 -3 3 -8 583.36 26.84 3 3 8 560.24 26.57 -3 3 -10 24.35 3.14 -3 3 -10 28.14 3.16 3 4 -13 2.6 0.92 3 4 -11 17.92 3.03 3 4 -11 14.9 2.91 3 4 -9 104.13 8.01 3 4 -9 119.67 8.57 3 4 -7 275.52 14.5 3 4 -7 258.15 14.79 3 4 -5 31.17 3.23 3 4 -5 33.1 3.39 3 4 -3 4.03 1.42 3 4 -3 7.47 2.28 3 4 -1 160.15 9.18 -3 -4 1 168.73 9.04 -3 -4 -1 747.1 31.22 3 4 1 659.26 30.83 3 -4 1 720.67 31.25 3 4 1 691.5 30.92 -3 4 -3 452.16 20.6 3 4 3 413.6 20.22 -3 4 -5 269.38 14.2 -3 -4 -5 279.34 13.98 3 4 5 258.44 13.86 -3 4 -7 213.73 12 3 4 7 209.81 11.73 3 4 9 33.73 3.47 -3 4 -9 31.62 3.59 -3 4 -11 31.47 2.42 3 5 -12 75.33 4.56 3 5 -12 76.1 4.75 3 5 -10 444.03 21.19 3 5 -10 440.57 21.92 3 5 -8 29.28 4.16 3 5 -8 42.32 5.46 3 5 -6 193.68 10.45 3 5 -6 176.42 11.09 3 5 -6 170.49 9.91 3 5 -4 233.52 12.61 3 5 -4 215.86 11.32 3 5 -4 242.58 12.4 3 5 -2 715.12 35.39 3 5 -2 853.83 34.98 3 5 0 2299.81 98.3 -3 -5 0 2325.07 98.39 3 5 0 2370.42 97.7 3 5 2 2.53 1.39 3 5 2 2.73 1.76 -3 5 -4 418.93 20.19 3 5 4 432.16 20.25 -3 5 -4 404.16 19.94 3 5 6 682.69 31.91 -3 5 -6 716.54 32.2 3 5 8 53.93 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