#------------------------------------------------------------------------------ #$Date: 2021-11-05 02:01:28 +0200 (Fri, 05 Nov 2021) $ #$Revision: 270312 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/87/7708703.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708703 loop_ _publ_author_name 'Lahiri, Goutam Kumar' 'Bera, Sudip Kumar' _publ_section_title ; Structural and electronic forms of doubly oxido/Pz and triply oxido/(Pz)2 bridged mixed valent and isovalent diruthenium complexes (Pz=Pyrazolate) ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03076K _journal_year 2021 _chemical_formula_sum 'C24 H33 N2 O9 Ru2' _chemical_formula_weight 695.66 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _audit_update_record ; 2021-08-03 deposited with the CCDC. 2021-11-04 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 97.538(4) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 16.1406(8) _cell_length_b 17.1433(5) _cell_length_c 21.2754(10) _cell_measurement_reflns_used 9388 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 22.2120 _cell_measurement_theta_min 1.7410 _cell_volume 5836.1(4) _computing_cell_refinement 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.93a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 300(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Saxi-CrysAlisPro-abstract goniometer imported SAXI images' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0829 _diffrn_reflns_av_unetI/netI 0.0415 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_k_max 20 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 48389 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 24.994 _diffrn_reflns_theta_max 24.994 _diffrn_reflns_theta_min 1.741 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 1.084 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.37011 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.93a (Rigaku Oxford Diffraction, 2020) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'metallic pinkish pink' _exptl_crystal_density_diffrn 1.583 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 2808 _exptl_crystal_size_max 0.325 _exptl_crystal_size_mid 0.246 _exptl_crystal_size_min 0.132 _refine_diff_density_max 2.400 _refine_diff_density_min -1.753 _refine_diff_density_rms 0.151 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.116 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 397 _refine_ls_number_reflns 5113 _refine_ls_number_restraints 38 _refine_ls_restrained_S_all 1.112 _refine_ls_R_factor_all 0.1395 _refine_ls_R_factor_gt 0.1104 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0750P)^2^+162.1742P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2494 _refine_ls_wR_factor_ref 0.2736 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3751 _reflns_number_total 5113 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03076k2.cif _cod_data_source_block shelx _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 7708703 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.720 _shelx_estimated_absorpt_t_max 0.870 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL gkl_sb_2b_re_autored_a.res in C2/c CELL 0.71073 16.1406 17.1433 21.2754 90.000 97.538 90.000 ZERR 8.00 0.0008 0.0005 0.0010 0.000 0.004 0.000 LATT 7 SYMM - X, Y, 1/2 - Z SFAC C H N O RU UNIT 192 264 16 72 16 MERG 2 OMIT -3.00 50.00 OMIT 2 0 0 OMIT 0 0 2 OMIT 0 2 0 OMIT 1 1 4 OMIT -2 0 2 OMIT -14 2 3 OMIT 1 1 12 ISOR 0.001 0.001 N1 N2 ISOR 0.01 0.02 C21 C22 C23 C24 MORE -1 DFIX 1.450 0.020 C23 C24 DFIX 1.450 0.020 C23A C24A FMAP 2 PLAN 20 SIZE 0.132 0.246 0.325 ACTA BOND BOND $H CONF LIST 4 L.S. 20 TEMP 27.00 WGHT 0.075000 162.174210 FVAR 0.16977 0.55530 RU1 5 0.486022 0.726954 0.579117 11.00000 0.06553 0.04312 = 0.14167 -0.00671 0.02656 0.00362 RU2 5 0.509295 0.791838 0.433890 11.00000 0.06652 0.06708 = 0.10236 -0.02704 -0.01337 0.01774 O1 4 0.541101 0.770067 0.517975 11.00000 0.05953 0.05265 = 0.08390 -0.00620 0.00349 0.00351 O2 4 0.432647 0.828987 0.595906 11.00000 0.06105 0.04917 = 0.12887 -0.00961 0.01190 0.00506 O3 4 0.584602 0.743337 0.649610 11.00000 0.08396 0.05736 = 0.10218 -0.00480 0.02121 0.00668 O4 4 0.421288 0.683164 0.645457 11.00000 0.09961 0.05462 = 0.15644 -0.00939 0.05466 -0.00987 O5 4 0.533591 0.619648 0.565054 11.00000 0.07477 0.05186 = 0.14360 -0.00810 0.03839 0.00814 O6 4 0.561071 0.693488 0.405802 11.00000 0.05183 0.07984 = 0.12903 -0.05360 -0.01551 0.01875 O7 4 0.613527 0.856224 0.425462 11.00000 0.07499 0.06785 = 0.08503 -0.00455 -0.00016 0.01260 O8 4 0.465081 0.812347 0.341298 11.00000 0.07952 0.11276 = 0.08418 -0.03496 -0.00860 0.02651 O9 4 0.456995 0.892402 0.457244 11.00000 0.07490 0.07074 = 0.08886 -0.01844 -0.02045 0.02439 C2 1 0.464772 0.878330 0.635723 11.00000 0.07622 0.04952 = 0.10987 0.00490 0.03291 0.00602 C4 1 0.594111 0.805156 0.681379 11.00000 0.08943 0.08027 = 0.07549 0.01158 0.02754 0.00892 C12 1 0.638705 0.688494 0.403534 11.00000 0.07728 0.07817 = 0.10913 -0.03479 -0.01764 0.02318 C13 1 0.697833 0.746673 0.412618 11.00000 0.07346 0.08573 = 0.11315 -0.02959 -0.00419 0.01414 AFIX 43 H13 2 0.753338 0.731261 0.414403 11.00000 -1.20000 AFIX 0 C14 1 0.683423 0.826357 0.419441 11.00000 0.08938 0.07461 = 0.07486 -0.01055 -0.00488 0.00996 C15 1 0.754585 0.880711 0.420626 11.00000 0.08497 0.09335 = 0.15967 -0.01989 0.02000 -0.00601 AFIX 137 H15A 2 0.791325 0.862928 0.391615 11.00000 -1.50000 H15B 2 0.784485 0.882719 0.462688 11.00000 -1.50000 H15C 2 0.734208 0.931821 0.408347 11.00000 -1.50000 AFIX 0 C20 1 0.381230 1.009020 0.452561 11.00000 0.10633 0.08111 = 0.10920 -0.00678 0.02297 0.03330 AFIX 137 H20A 2 0.349119 0.994502 0.485641 11.00000 -1.50000 H20B 2 0.347660 1.040793 0.421959 11.00000 -1.50000 H20C 2 0.429632 1.037890 0.470406 11.00000 -1.50000 AFIX 0 C16 1 0.378228 0.858450 0.252214 11.00000 0.08741 0.14461 = 0.07746 -0.00309 0.00551 -0.01437 AFIX 137 H16A 2 0.424280 0.858967 0.227879 11.00000 -1.50000 H16B 2 0.341636 0.901401 0.239579 11.00000 -1.50000 H16C 2 0.348054 0.810341 0.244942 11.00000 -1.50000 AFIX 0 C8 1 0.475807 0.555404 0.649859 11.00000 0.09353 0.05888 = 0.12139 -0.00275 0.01074 -0.00896 AFIX 43 H8 2 0.478522 0.508930 0.672585 11.00000 -1.20000 AFIX 0 C17 1 0.410954 0.865784 0.322110 11.00000 0.05961 0.09339 = 0.09228 -0.00148 -0.00932 0.00333 C9 1 0.522368 0.559593 0.599408 11.00000 0.08816 0.03779 = 0.13488 -0.01362 -0.00362 -0.00015 C3 1 0.540623 0.869670 0.672897 11.00000 0.10820 0.06145 = 0.10231 0.00138 0.03662 0.01257 AFIX 43 H3 2 0.559358 0.913678 0.696087 11.00000 -1.20000 AFIX 0 C1 1 0.415827 0.952883 0.638433 11.00000 0.09800 0.05264 = 0.15345 -0.00883 0.01605 0.01446 AFIX 137 H1A 2 0.445167 0.994839 0.621199 11.00000 -1.50000 H1B 2 0.409412 0.964357 0.681695 11.00000 -1.50000 H1C 2 0.361735 0.946926 0.614130 11.00000 -1.50000 AFIX 0 C5 1 0.669974 0.808280 0.730700 11.00000 0.13480 0.10364 = 0.09846 -0.00294 -0.00155 0.01443 AFIX 137 H5A 2 0.655791 0.788959 0.770275 11.00000 -1.50000 H5B 2 0.688992 0.861226 0.735962 11.00000 -1.50000 H5C 2 0.713517 0.776648 0.717316 11.00000 -1.50000 AFIX 0 C10 1 0.569372 0.487801 0.582417 11.00000 0.08735 0.06497 = 0.15517 -0.01656 0.01140 0.01072 AFIX 137 H10A 2 0.539265 0.463318 0.545743 11.00000 -1.50000 H10B 2 0.574723 0.451899 0.617343 11.00000 -1.50000 H10C 2 0.623927 0.502672 0.573392 11.00000 -1.50000 AFIX 0 C18 1 0.384060 0.923846 0.355675 11.00000 0.07655 0.08419 = 0.09068 0.00304 0.00077 0.00863 AFIX 43 H18 2 0.346158 0.958794 0.334433 11.00000 -1.20000 AFIX 0 C7 1 0.425908 0.613670 0.669449 11.00000 0.09102 0.06204 = 0.13055 -0.01461 0.01051 -0.00964 C19 1 0.408424 0.936425 0.420573 11.00000 0.06779 0.06927 = 0.11573 -0.01032 0.01119 0.01029 C6 1 0.369123 0.598313 0.718527 11.00000 0.13439 0.09763 = 0.11933 -0.00800 0.02839 -0.02018 AFIX 137 H6A 2 0.375097 0.639360 0.749485 11.00000 -1.50000 H6B 2 0.383662 0.549364 0.738968 11.00000 -1.50000 H6C 2 0.312273 0.596389 0.698533 11.00000 -1.50000 AFIX 0 C11 1 0.667332 0.606140 0.388466 11.00000 0.09335 0.09234 = 0.26314 -0.07060 0.00544 0.02760 AFIX 137 H11A 2 0.653379 0.570527 0.420280 11.00000 -1.50000 H11B 2 0.726719 0.606013 0.387964 11.00000 -1.50000 H11C 2 0.639833 0.590290 0.347713 11.00000 -1.50000 PART 1 AFIX 0 N1 3 0.389548 0.712663 0.496049 21.00000 0.03905 0.03918 = 0.03922 -0.00003 0.00519 0.00003 N2 3 0.408528 0.736870 0.435264 21.00000 0.05850 0.05854 = 0.05851 -0.00008 0.00766 -0.00006 C21 1 0.345337 0.716775 0.392424 21.00000 0.06455 0.06451 = 0.06367 -0.00132 0.00245 -0.00810 AFIX 43 H21 2 0.342408 0.729087 0.349618 21.00000 -1.20000 AFIX 0 C22 1 0.285346 0.676436 0.417281 21.00000 0.07255 0.07315 = 0.07248 0.00291 0.00891 -0.00311 AFIX 43 H22 2 0.236234 0.656004 0.395797 21.00000 -1.20000 AFIX 0 C23 1 0.313497 0.672046 0.483093 21.00000 0.05980 0.06020 = 0.06424 -0.00199 0.00121 0.00862 C24 1 0.277761 0.635745 0.535013 21.00000 0.06169 0.07546 = 0.08493 0.00893 0.00124 -0.01132 AFIX 33 H24A 2 0.226283 0.610437 0.518879 21.00000 -1.50000 H24B 2 0.316210 0.597903 0.555271 21.00000 -1.50000 H24C 2 0.267156 0.674890 0.565223 21.00000 -1.50000 PART 2 AFIX 0 N1A 3 0.398497 0.718450 0.462720 -21.00000 0.05304 0.06258 = 0.05405 -0.04058 -0.01459 0.01377 N2A 3 0.396468 0.698740 0.528212 -21.00000 0.07923 0.06271 = 0.07050 0.01513 -0.01473 -0.00463 C21A 1 0.323024 0.663507 0.530408 -21.00000 0.02430 0.07184 = 0.13946 -0.02360 -0.02458 -0.00865 AFIX 43 H21A 2 0.304724 0.644792 0.567238 -21.00000 -1.20000 AFIX 0 C22A 1 0.277390 0.658533 0.469994 -21.00000 0.10940 0.07544 = 0.14547 -0.03526 -0.05848 0.01742 AFIX 43 H22A 2 0.224943 0.636122 0.459407 -21.00000 -1.20000 AFIX 0 C23A 1 0.323322 0.691743 0.431386 -21.00000 0.12205 0.06752 = 0.10571 -0.00126 -0.02246 0.01783 C24A 1 0.309426 0.695875 0.362852 -21.00000 0.13007 0.13654 = 0.13118 0.04683 -0.05393 -0.04634 AFIX 33 H24D 2 0.354277 0.724271 0.347960 -21.00000 -1.50000 H24E 2 0.307304 0.644072 0.345579 -21.00000 -1.50000 H24F 2 0.257481 0.722023 0.349567 -21.00000 -1.50000 AFIX 0 HKLF 4 REM gkl_sb_2b_re_autored_a.res in C2/c REM R1 = 0.1104 for 3751 Fo > 4sig(Fo) and 0.1395 for all 5113 data REM 397 parameters refined using 38 restraints END WGHT 0.0741 162.6721 REM Highest difference peak 2.400, deepest hole -1.753, 1-sigma level 0.151 Q1 1 0.5000 0.6545 0.2500 10.50000 0.05 2.40 Q2 1 0.4761 0.7735 0.4636 11.00000 0.05 1.73 Q3 1 0.4757 0.7135 0.6192 11.00000 0.05 1.10 Q4 1 0.5139 0.7791 0.4122 11.00000 0.05 0.81 Q5 1 0.4412 0.7409 0.4911 11.00000 0.05 0.78 Q6 1 0.4535 0.6618 0.7191 11.00000 0.05 0.72 Q7 1 0.5228 0.7226 0.5100 11.00000 0.05 0.65 Q8 1 0.4611 0.8557 0.2115 11.00000 0.05 0.63 Q9 1 0.5752 0.7881 0.4362 11.00000 0.05 0.62 Q10 1 0.5477 0.7252 0.5897 11.00000 0.05 0.60 Q11 1 0.4902 0.7062 0.5581 11.00000 0.05 0.55 Q12 1 0.5403 0.6557 0.4494 11.00000 0.05 0.53 Q13 1 0.4224 0.7266 0.5673 11.00000 0.05 0.52 Q14 1 0.5364 0.7723 0.3694 11.00000 0.05 0.47 Q15 1 0.5613 0.8298 0.3712 11.00000 0.05 0.43 Q16 1 0.5355 0.7012 0.3052 11.00000 0.05 0.40 Q17 1 0.4373 0.7688 0.3697 11.00000 0.05 0.38 Q18 1 0.6023 0.8084 0.4960 11.00000 0.05 0.38 Q19 1 0.5812 0.7843 0.5588 11.00000 0.05 0.37 Q20 1 0.5371 0.7975 0.7774 11.00000 0.05 0.36 ; _shelx_res_checksum 65473 _shelx_hkl_file ; 0 0 2 0.17 1.19 0 0 -2 0.15 0.37 0 0 3 2.12 2.35 0 0 -3 2.24 2.06 0 0 -3 2.16 1.57 0 0 3 1.67 1.15 0 0 3 1.57 1.74 0 0 -3 4.09 2.40 0 0 -3 4.77 2.19 0 0 3 -0.26 0.34 0 0 -4 5145.11 86.95 0 0 4 5330.39 89.78 0 0 -4 5261.52 95.31 0 0 4 5085.28 78.04 0 0 -4 5088.55 79.11 0 0 4 5127.00 93.40 0 0 4 5366.91 93.38 0 0 -4 5239.88 89.64 0 0 5 15.04 6.15 0 0 -5 15.79 5.99 0 0 -5 10.55 4.50 0 0 5 10.28 5.09 0 0 -5 10.26 5.47 0 0 5 13.91 6.09 0 0 5 11.47 4.33 0 0 -5 13.05 4.37 0 0 6 9557.69 149.24 0 0 -6 9538.33 145.82 0 0 -6 9999.00 162.21 0 0 -6 9401.75 132.96 0 0 6 9381.49 155.14 0 0 6 9274.89 131.05 0 0 6 9775.48 153.49 0 0 -6 9790.84 150.91 0 0 7 15.43 7.68 0 0 -7 15.10 6.94 0 0 -7 12.72 5.59 0 0 7 12.85 7.22 0 0 7 15.31 5.77 0 0 -7 13.00 4.87 0 0 7 18.04 8.56 0 0 -7 14.67 6.05 0 0 -8 3950.39 109.78 0 0 8 4028.14 113.98 0 0 -8 4105.37 120.89 0 0 8 3803.31 97.63 0 0 8 3900.15 116.23 0 0 -8 3801.63 98.92 0 0 8 4161.40 116.58 0 0 -8 4074.64 113.28 0 0 -9 6.29 5.81 0 0 9 -0.60 2.91 0 0 -9 -1.79 5.78 0 0 9 8.71 6.37 0 0 9 6.48 5.88 0 0 9 6.88 4.22 0 0 -9 1.98 6.56 0 0 -9 7.00 4.14 0 0 -10 531.34 44.83 0 0 10 535.62 45.95 0 0 -10 556.57 50.06 0 0 10 518.80 40.13 0 0 -10 589.69 43.64 0 0 -10 549.92 46.85 0 0 11 1.66 2.46 0 0 -11 1.54 2.59 0 0 -11 0.39 3.44 0 0 11 2.90 3.31 0 0 11 6.97 7.07 0 0 11 3.87 5.12 0 0 -11 6.60 5.56 0 0 -12 1657.73 86.92 0 0 12 1646.70 89.87 0 0 12 1562.69 76.98 0 0 -12 1741.19 98.60 0 0 12 1689.17 93.16 0 0 -12 1602.49 79.56 0 0 -12 1587.20 88.30 0 0 12 1727.98 92.72 0 0 13 35.08 15.26 0 0 -13 44.88 17.68 0 0 -13 36.79 15.95 0 0 13 60.31 20.82 0 0 13 30.74 12.34 0 0 13 58.76 21.85 0 0 -13 37.38 15.24 0 0 -14 715.05 62.20 0 0 14 759.65 67.75 0 0 14 693.04 66.20 0 0 -14 723.08 57.91 0 0 14 696.59 64.28 0 0 -14 702.68 64.12 0 0 15 72.12 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0 -6 3 1998.37 53.39 0 -6 -3 1940.18 62.75 0 6 -3 2035.52 51.36 0 -6 -3 2048.46 80.72 0 6 3 2077.39 45.06 0 -6 3 1900.34 53.53 0 -6 -3 1908.10 46.98 0 6 3 2110.62 83.66 0 -6 3 1844.00 47.48 0 6 3 1953.77 59.88 0 -6 3 1984.83 55.52 0 6 -3 1737.46 37.35 0 6 -4 111.81 15.52 0 6 -4 120.82 13.27 0 -6 -4 109.61 17.04 0 6 4 102.89 14.93 0 -6 4 128.40 14.75 0 -6 -4 107.28 15.57 0 -6 -4 103.30 12.56 0 6 -4 110.55 9.50 0 -6 -4 116.77 19.99 0 -6 4 108.82 14.57 0 6 4 109.79 12.37 0 6 4 135.59 22.12 0 6 -4 112.27 10.92 0 -6 4 115.92 9.41 0 6 4 103.97 15.50 0 -6 4 131.55 15.54 0 -6 -5 123.39 18.79 0 6 -5 95.63 12.90 0 6 -5 92.67 14.93 0 -6 5 97.36 14.00 0 -6 -5 118.67 17.88 0 6 5 116.37 17.32 0 6 5 136.48 23.44 0 -6 -5 122.32 21.85 0 -6 5 83.69 14.55 0 6 5 119.55 14.80 0 -6 -5 106.01 14.97 0 -6 5 85.36 13.37 0 6 5 118.98 17.17 0 6 -5 88.74 11.14 0 6 -6 41.34 8.07 0 -6 -6 41.91 11.79 0 6 6 53.20 12.76 0 6 -6 40.91 8.77 0 -6 6 34.23 8.98 0 -6 -6 40.01 11.19 0 6 6 49.43 12.07 0 -6 -6 41.69 10.19 0 6 6 46.69 9.86 0 -6 6 51.33 12.28 0 -6 6 40.95 10.13 0 6 6 45.54 14.23 0 -6 -6 38.34 13.04 0 -6 -7 17.75 8.10 0 6 -7 10.28 4.51 0 6 7 22.07 8.91 0 -6 7 19.17 7.17 0 6 7 19.96 8.41 0 -6 -7 21.60 8.40 0 6 -7 17.74 5.92 0 -6 -7 24.51 9.01 0 6 7 20.26 7.05 0 -6 7 14.61 6.86 0 -6 -7 18.13 9.25 0 -6 7 24.70 8.20 0 6 -8 31.88 8.78 0 -6 -8 40.77 13.45 0 6 8 37.72 12.33 0 6 8 52.84 14.03 0 -6 8 32.84 10.97 0 -6 -8 48.86 13.13 0 6 8 44.11 14.95 0 -6 -8 37.84 11.70 0 -6 8 32.38 11.16 0 6 8 47.29 13.00 0 -6 8 37.90 11.08 0 6 9 467.34 44.51 0 6 -9 479.96 38.04 0 -6 -9 453.49 43.19 0 6 9 473.94 50.38 0 -6 -9 491.76 50.43 0 -6 -9 465.15 42.09 0 6 9 480.06 41.50 0 -6 9 409.73 40.64 0 -6 9 426.92 39.41 0 6 -9 423.60 35.19 0 6 10 35.74 12.86 0 -6 -10 36.10 13.15 0 6 -10 12.09 6.67 0 6 -10 10.22 6.07 0 -6 -10 15.64 9.02 0 -6 10 13.10 7.57 0 6 10 26.59 11.14 0 6 10 32.74 13.90 0 -6 -10 24.42 10.71 0 -6 10 13.09 8.86 0 6 10 25.69 10.17 0 -6 -10 31.22 12.00 0 -6 -11 917.51 72.78 0 -6 11 854.73 60.91 0 6 -11 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433.00 36.98 -8 2 7 381.11 41.64 -8 -2 7 403.71 39.37 8 2 -6 1405.56 62.11 8 -2 -6 1489.17 72.90 8 -2 -6 1613.77 59.52 8 -2 -6 1602.45 68.62 8 2 -6 1469.51 55.72 -8 2 6 1545.15 66.33 -8 -2 6 1451.66 75.05 8 2 -6 1522.74 67.29 -8 2 6 1591.63 82.86 -8 -2 6 1454.84 72.09 8 -2 -5 315.36 31.82 8 2 -5 296.61 24.35 -8 2 5 262.86 27.25 -8 -2 5 376.53 37.63 8 -2 -5 272.63 24.65 8 2 -5 362.16 33.67 8 -2 -5 228.42 29.31 -8 2 5 308.31 33.96 -8 2 5 285.91 35.65 8 2 -4 804.21 48.08 8 -2 -4 747.54 39.20 8 -2 -4 764.50 46.73 -8 2 4 760.08 43.47 -8 -2 4 722.59 50.80 8 2 -4 731.82 38.07 8 -2 -4 687.92 47.37 -8 2 4 766.28 52.30 -8 2 4 734.85 54.74 8 2 -3 525.85 38.78 8 2 -3 504.19 32.04 8 -2 -3 428.54 29.86 -8 -2 3 500.86 33.93 -8 2 3 413.80 37.64 8 -2 -3 421.96 35.08 -8 2 3 385.41 31.05 -8 -2 3 488.10 41.75 8 -2 -3 437.94 38.14 -8 -2 3 484.41 43.55 -8 2 3 433.44 39.94 -8 2 3 450.57 41.41 8 2 -2 -0.95 4.05 -8 -2 2 10.43 5.12 -8 -2 2 5.87 4.07 -8 2 2 16.83 5.14 -8 2 2 17.23 8.32 8 2 -2 17.01 6.45 8 -2 -2 20.19 7.48 -8 2 2 16.38 5.41 -8 -2 2 -1.41 4.96 -8 2 2 32.10 11.06 -8 2 2 25.43 9.04 8 2 -1 199.46 20.86 -8 2 1 196.22 24.80 -8 -2 1 225.41 22.63 8 -2 -1 175.69 22.63 -8 2 1 182.16 20.47 -8 -2 1 210.10 25.73 8 2 -1 227.98 29.36 -8 -2 1 207.16 27.88 -8 2 1 164.07 23.96 -8 -2 1 215.47 23.67 -8 2 1 162.99 24.37 -8 2 0 856.25 45.37 -8 -2 0 738.30 48.49 8 -2 0 775.41 47.98 -8 2 0 830.08 50.71 -8 -2 0 762.33 42.18 8 2 0 736.55 42.48 -8 -2 0 747.53 52.64 8 2 0 759.34 52.96 -8 2 0 814.55 53.17 -8 2 0 791.77 54.16 -8 -2 0 716.61 44.22 -8 -2 -1 410.27 31.87 -8 -2 -1 432.66 38.01 8 -2 1 425.88 36.82 -8 2 -1 451.20 33.72 -8 2 -1 442.87 36.88 8 2 1 377.38 32.59 -8 2 -1 462.69 40.43 8 2 1 416.23 40.44 -8 -2 -1 356.23 32.52 -8 2 -1 407.10 39.45 -8 -2 -2 1912.13 78.06 -8 -2 -2 1946.27 70.40 -8 2 -2 2029.42 80.47 8 -2 2 1940.93 80.34 8 2 2 1911.12 75.52 8 2 2 1952.45 89.20 8 -2 2 1956.59 85.91 -8 2 -2 1980.56 85.44 8 -2 2 1909.49 81.76 -8 -2 -2 1935.11 77.47 -8 -2 -3 617.03 46.50 -8 2 -3 536.12 42.98 -8 -2 -3 664.61 43.25 8 2 3 597.55 45.35 8 -2 3 493.11 44.11 -8 -2 -3 643.65 52.52 8 2 3 602.43 50.96 8 -2 3 518.27 45.84 -8 2 -3 469.79 44.78 -8 -2 -3 602.43 45.68 8 2 3 579.71 39.50 8 -2 3 471.62 42.76 -8 -2 -4 378.02 34.49 -8 2 -4 367.46 35.92 8 2 4 388.57 38.67 8 -2 4 360.33 38.45 -8 -2 -4 395.72 40.90 -8 2 -4 369.36 39.84 8 2 4 406.76 42.40 8 -2 4 380.59 39.05 -8 2 -4 357.95 40.27 -8 -2 -4 394.06 38.97 8 -2 4 350.33 38.30 8 2 4 373.36 33.49 8 2 5 418.65 41.73 -8 -2 -5 426.13 38.40 8 -2 5 319.40 39.25 -8 2 -5 349.63 40.32 -8 -2 -5 455.63 45.98 8 2 5 421.08 44.35 8 -2 5 354.46 39.99 -8 2 -5 312.65 39.08 8 -2 5 309.10 37.45 8 2 5 388.54 36.49 -8 2 -6 402.01 39.62 8 2 6 330.02 38.94 -8 -2 -6 371.68 37.47 -8 2 -6 430.76 46.52 -8 -2 -6 363.67 43.06 -8 -2 -6 375.65 43.80 8 2 6 377.09 42.06 8 -2 6 455.46 44.56 -8 2 -6 456.80 47.80 -8 -2 -6 376.26 41.70 8 -2 6 438.42 43.42 -8 2 -7 20.43 10.54 8 -2 7 6.52 8.00 -8 -2 -7 22.05 11.68 8 2 7 13.50 9.56 -8 -2 -7 2.92 3.92 8 2 7 17.20 11.55 8 -2 7 11.93 10.02 -8 -2 -7 19.21 12.16 -8 2 -7 13.48 8.05 8 2 7 12.22 8.57 8 -2 7 15.69 9.97 -8 2 -7 21.35 12.72 -8 -2 -7 14.03 8.95 8 -2 8 1070.94 77.35 8 2 8 1035.27 74.01 -8 2 -8 1048.38 69.24 -8 -2 -8 1058.09 69.42 8 2 8 1138.79 76.76 8 -2 8 1152.60 76.46 -8 -2 -8 1035.53 76.86 -8 2 -8 1165.45 80.55 -8 -2 -8 1040.56 76.21 -8 2 -8 1062.00 77.27 -8 -2 -8 1004.39 73.46 8 2 8 1041.71 66.48 8 -2 8 1101.12 74.89 -8 2 -9 89.41 22.95 -8 -2 -9 97.84 23.41 8 -2 9 93.93 24.78 8 2 9 91.63 22.22 8 2 9 126.09 27.45 8 -2 9 98.07 25.30 -8 -2 -9 72.56 22.85 -8 -2 -9 94.01 25.55 -8 2 -9 84.85 22.94 -8 2 -9 107.51 27.01 -8 -2 -9 88.39 23.28 8 -2 9 80.33 22.97 8 2 9 95.67 21.69 8 -2 10 339.96 46.43 -8 2 -10 341.35 42.45 -8 -2 -10 364.85 44.94 8 2 10 378.13 48.17 8 -2 10 372.51 46.77 -8 -2 -10 337.26 48.36 -8 2 -10 331.58 48.50 -8 -2 -10 338.58 48.15 -8 2 -10 311.32 40.23 8 2 10 378.25 44.96 -8 2 -10 323.41 47.39 -8 -2 -10 338.01 46.19 8 -2 10 309.94 43.53 -8 2 -11 148.31 29.66 -8 -2 -11 179.75 33.15 8 -2 11 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21 0.24 10.36 8 -4 -21 22.92 14.25 -8 4 20 6.93 9.59 -8 -4 20 30.07 16.85 8 -4 -20 12.46 9.76 8 4 -20 9.71 7.62 -8 -4 20 0.89 4.99 8 -4 -20 9.02 9.60 -8 4 19 3.83 5.06 -8 -4 19 2.40 6.36 8 4 -19 3.13 3.63 8 -4 -19 21.75 14.44 -8 -4 19 3.66 10.02 8 -4 -19 -7.66 9.23 -8 -4 18 -0.75 5.96 8 4 -18 -4.70 8.53 8 -4 -18 2.55 7.02 -8 4 18 -0.09 5.17 -8 -4 18 11.26 9.81 -8 4 18 -1.09 9.04 -8 4 18 6.11 9.53 -8 -4 18 7.14 9.10 8 -4 -18 -5.87 7.53 -8 -4 17 30.15 15.74 8 4 -17 52.56 18.12 8 -4 -17 43.12 16.23 -8 4 17 23.45 14.82 8 -4 -17 43.91 18.54 -8 -4 17 59.68 19.56 8 4 -17 39.85 18.03 -8 4 17 42.67 22.17 -8 4 17 54.94 22.23 -8 -4 17 46.70 16.68 8 -4 -17 47.06 17.74 8 4 -16 3.78 7.03 8 -4 -16 17.66 14.87 -8 4 16 4.91 10.32 -8 -4 16 -13.35 10.50 -8 -4 16 10.81 9.33 -8 4 16 11.41 11.99 8 4 -16 8.63 8.22 8 -4 -16 9.07 8.04 -8 4 16 -1.27 6.98 -8 -4 16 16.94 10.32 8 -4 -16 0.16 4.79 8 4 -15 25.29 11.19 8 -4 -15 42.72 18.95 -8 4 15 24.23 11.83 -8 -4 15 15.98 8.17 -8 -4 15 16.11 11.05 -8 4 15 40.31 19.65 8 -4 -15 27.26 10.89 8 4 -15 33.68 14.17 -8 4 15 33.79 16.47 -8 -4 15 24.73 10.91 8 -4 -15 13.82 9.95 8 4 -14 6.30 8.43 -8 4 14 19.46 10.71 8 -4 -14 32.32 16.13 -8 -4 14 6.53 4.82 -8 -4 14 3.66 6.80 8 4 -14 28.20 14.49 8 -4 -14 21.47 10.18 -8 4 14 -9.16 11.08 -8 -4 14 4.06 5.41 8 -4 -14 10.60 7.89 8 4 -13 9.57 9.26 -8 -4 13 15.70 8.72 -8 4 13 28.36 13.76 8 -4 -13 26.64 14.22 8 -4 -13 28.69 10.43 -8 -4 13 12.00 9.16 -8 4 13 27.07 15.89 -8 4 13 6.09 6.88 -8 -4 13 4.62 5.49 8 -4 -13 17.41 10.04 -8 4 12 212.28 33.35 8 4 -12 174.04 28.47 -8 -4 12 235.35 29.93 8 -4 -12 218.45 36.74 -8 4 12 186.00 34.68 8 -4 -12 203.34 26.52 8 4 -12 208.47 33.19 -8 -4 12 214.65 32.08 -8 -4 12 197.80 29.56 -8 4 12 190.09 36.14 8 -4 -12 184.70 32.59 8 4 -11 93.98 20.15 -8 -4 11 104.21 19.28 -8 4 11 60.67 17.38 8 -4 -11 64.70 20.02 8 4 -11 99.46 21.95 8 -4 -11 84.56 16.93 -8 4 11 72.18 21.38 -8 -4 11 75.81 18.35 -8 4 11 47.83 18.37 -8 -4 11 96.50 20.11 8 -4 -11 95.98 23.38 8 -4 -10 208.95 33.68 -8 4 10 199.33 31.64 8 4 -10 270.88 30.81 -8 -4 10 286.90 29.33 -8 4 10 201.05 34.33 -8 -4 10 245.62 30.48 8 -4 -10 218.45 24.67 8 4 -10 297.20 35.88 8 -4 -10 209.27 32.56 -8 -4 10 256.38 31.66 -8 4 10 208.65 36.08 8 -4 -9 380.41 43.64 -8 4 9 345.58 39.77 8 4 -9 387.76 34.96 -8 -4 9 397.33 33.15 -8 4 9 321.10 42.51 -8 -4 9 371.92 34.94 -8 -4 9 414.18 46.61 8 -4 -9 380.77 30.11 8 4 -9 418.42 41.37 -8 4 9 380.99 46.71 -8 -4 9 380.11 37.77 8 -4 -9 382.46 43.13 8 -4 -8 225.67 31.98 -8 -4 8 176.63 21.76 8 4 -8 169.79 22.16 -8 4 8 188.31 32.08 8 4 -8 175.33 18.91 8 -4 -8 190.27 19.79 8 4 -8 167.55 25.95 -8 -4 8 167.18 29.21 -8 4 8 224.83 34.68 8 -4 -8 185.47 29.10 -8 -4 8 160.33 24.46 8 4 -7 533.82 37.24 8 -4 -7 578.94 50.20 -8 4 7 564.49 52.91 8 -4 -7 578.21 45.55 8 4 -7 527.47 30.63 8 4 -7 558.12 44.94 8 -4 -7 586.54 33.60 -8 4 7 547.27 53.13 8 -4 -7 510.67 46.43 8 -4 -6 731.34 49.85 8 4 -6 704.23 49.20 8 -4 -6 750.55 36.55 8 -4 -6 716.61 53.76 -8 -4 6 735.33 56.03 -8 4 6 784.44 52.35 -8 4 6 685.75 57.45 8 -4 -6 711.11 53.67 8 -4 -5 208.55 19.01 8 -4 -5 253.64 29.76 -8 4 5 220.73 22.32 -8 -4 5 286.08 34.71 8 4 -5 296.24 32.11 8 -4 -5 209.31 28.73 -8 -4 5 278.94 34.10 -8 4 5 220.42 27.93 -8 4 5 231.67 32.89 8 4 -4 734.95 49.06 8 -4 -4 783.66 50.52 -8 4 4 685.36 37.29 -8 -4 4 702.64 52.94 8 -4 -4 700.88 51.87 8 4 -4 601.61 33.60 -8 4 4 727.07 50.09 -8 -4 4 738.62 55.70 -8 4 4 696.02 55.66 8 4 -3 2009.15 79.90 8 -4 -3 1982.87 79.02 -8 4 3 1741.31 57.36 -8 -4 3 1914.08 85.68 8 4 -3 1775.81 56.35 8 -4 -3 1831.31 81.53 -8 4 3 1913.96 80.55 -8 4 3 1888.30 89.15 -8 4 3 1861.82 86.20 8 4 -2 35.67 16.26 -8 -4 2 30.48 9.72 -8 4 2 2.20 4.10 -8 -4 2 46.08 18.30 8 -4 -2 55.99 16.22 -8 4 2 10.86 2.72 -8 4 2 47.53 15.91 -8 4 2 71.20 19.43 8 -4 -1 573.73 42.93 8 4 -1 595.17 44.58 -8 -4 1 532.08 31.69 -8 -4 1 646.78 47.69 -8 4 1 462.30 30.37 8 4 -1 568.47 33.65 8 4 -1 557.10 46.00 8 -4 -1 467.07 39.70 -8 4 1 463.09 39.27 -8 4 1 524.04 46.33 -8 -4 1 572.26 34.65 -8 4 1 515.16 46.86 -8 4 0 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16.96 14.62 -22 4 6 14.00 15.26 -22 -4 6 2.08 12.01 22 -4 -5 -0.12 11.05 -22 4 5 -5.44 16.03 -22 -4 5 7.85 13.03 22 -4 -4 0.12 13.97 -22 4 4 -9.79 15.66 -22 -4 4 34.06 23.33 22 -4 -3 4.72 13.14 -22 4 3 -0.29 9.64 22 -4 -2 26.12 24.11 -22 4 2 -3.39 10.46 22 -4 -1 15.33 24.04 -22 4 1 -4.21 13.84 22 -4 0 54.29 32.25 -22 4 0 -20.22 22.87 22 -4 1 36.61 23.78 -22 -4 -1 38.39 27.37 22 -4 2 34.83 24.83 -22 -4 -2 32.92 25.86 22 -4 3 34.60 22.89 -22 -4 -3 -26.27 22.82 22 -4 4 19.14 15.00 -22 -4 -4 61.67 34.89 22 -4 5 13.82 13.77 22 -4 6 -14.89 19.15 22 -4 8 40.02 30.68 22 -4 9 -11.57 15.64 22 -4 10 -4.65 18.80 22 6 -19 -5.66 12.54 22 6 -18 -7.68 11.51 22 -6 -17 9.29 15.62 -22 -6 15 -9.60 12.94 22 -6 -14 -4.55 12.14 -22 -6 14 8.60 12.92 22 -6 -13 0.12 16.14 -22 -6 13 55.41 26.92 22 -6 -12 13.00 13.32 22 -6 -11 16.11 17.56 22 -6 -10 -30.30 20.97 22 -6 -9 -38.33 22.53 -22 -6 9 -8.80 11.78 22 -6 -8 -9.48 17.01 -22 6 8 11.83 18.66 -22 -6 8 13.57 17.05 22 -6 -7 -3.44 13.41 -22 6 7 24.27 21.95 -22 -6 7 20.39 17.68 22 -6 -6 -7.19 13.85 -22 6 6 13.06 15.78 -22 -6 6 6.18 13.86 22 -6 -5 8.65 11.29 -22 6 5 29.97 22.84 -22 -6 5 36.75 23.06 22 -6 -4 3.72 10.58 -22 6 4 1.01 11.25 -22 -6 4 9.13 11.73 22 -6 -3 -28.77 21.77 -22 6 3 2.62 12.40 -22 -6 3 -2.98 10.57 22 -6 -2 -10.29 17.72 -22 6 2 2.52 15.74 -22 -6 2 -32.11 24.26 22 -6 -1 -27.66 22.23 -22 6 1 9.67 16.21 22 -6 0 -3.25 10.27 -22 6 0 -16.42 16.16 22 -6 1 29.05 24.29 22 -6 2 36.07 25.78 -22 -6 -2 -1.00 9.75 -22 -6 -3 22.15 25.31 -22 -6 -4 8.45 16.48 22 -6 5 -13.30 20.75 22 -6 6 -17.85 21.06 22 -6 7 -22.58 24.42 22 8 -17 -0.14 25.12 -22 -8 15 -7.76 15.41 22 -8 -14 -2.22 11.97 -22 -8 14 24.96 19.26 22 -8 -13 -56.76 31.49 22 -8 -12 -0.13 13.73 22 -8 -11 2.93 11.80 -22 -8 11 64.42 30.55 -22 -8 10 13.84 14.33 -22 -8 9 -8.98 13.40 -22 8 8 19.85 19.98 -22 -8 8 32.22 22.95 -22 8 7 -20.01 14.73 -22 -8 7 -15.19 15.05 -22 8 6 4.44 12.41 -22 -8 6 36.43 21.33 -22 8 5 39.86 37.13 -22 -8 5 25.93 18.73 -22 8 4 0.29 11.35 -22 -8 4 24.31 24.03 -22 8 3 -20.43 18.37 -22 -8 3 -24.93 23.79 -22 8 2 -6.02 15.97 -22 -8 2 -29.68 20.40 22 -8 -1 44.06 28.71 -22 8 1 15.38 25.07 -22 -8 1 45.34 28.09 22 -8 0 46.40 25.10 22 -8 1 55.13 36.73 22 -8 2 35.61 28.55 -22 -8 -2 87.57 37.49 22 -8 3 15.32 21.69 -22 -8 -3 23.45 20.24 -22 -8 -4 33.40 24.37 -22 -10 11 -38.73 23.54 -22 -10 10 15.10 18.35 -22 -10 9 40.43 23.28 -22 -10 8 -7.92 12.10 -22 -10 7 9.51 14.34 -22 10 6 17.42 19.86 -22 -10 6 -3.95 11.53 -22 10 5 4.68 12.33 -22 -10 5 48.27 27.11 -22 10 4 -2.08 12.54 -22 -10 4 -19.41 20.34 -22 10 3 -11.41 18.99 -22 -10 3 -15.39 12.49 -22 -10 2 25.22 22.14 -22 -10 -2 51.13 28.71 -22 -10 -3 -14.95 19.00 -22 -12 -3 -16.09 21.45 23 1 -21 -52.92 27.34 -23 -1 6 -6.02 11.00 -23 -1 5 -14.68 17.18 -23 -1 4 -10.12 13.49 23 -1 -2 -30.99 18.66 23 -1 -1 25.06 22.86 23 -1 0 12.65 14.32 23 -1 1 8.30 10.81 23 -1 2 -29.50 22.62 23 -1 3 -2.97 12.84 23 -1 4 12.91 15.07 23 -1 5 54.33 32.46 23 -1 6 16.73 24.19 23 3 -20 -26.82 21.92 23 -3 -11 6.85 14.23 23 -3 -10 34.20 20.91 -23 -3 10 5.76 12.30 23 -3 -9 -23.25 19.16 -23 -3 9 5.91 14.21 23 -3 -8 40.59 22.73 -23 -3 8 1.43 9.72 23 -3 -7 -37.48 22.90 -23 -3 7 -6.71 14.78 23 -3 -6 -59.56 27.29 -23 -3 6 4.87 10.14 23 -3 -5 -34.90 22.64 -23 -3 5 3.93 13.80 23 -3 -4 -31.42 21.54 -23 -3 4 19.83 20.77 23 -3 -3 38.05 23.06 -23 -3 3 6.38 16.15 23 -3 -2 6.24 15.39 -23 -3 2 -9.01 15.11 23 -3 -1 -2.78 14.39 -23 -3 1 -33.26 27.08 23 -3 0 17.51 18.19 23 -3 1 23.09 22.25 23 -3 2 -52.34 26.79 23 -3 3 11.22 21.64 23 -3 4 21.09 38.15 23 -3 5 -14.77 19.07 23 -3 7 40.23 27.77 23 -3 8 -54.03 37.95 23 -5 -13 6.97 16.88 23 -5 -12 13.48 20.46 23 -5 -11 11.79 14.97 -23 -5 11 5.27 12.00 23 -5 -10 -44.81 26.19 -23 -5 10 8.04 16.93 23 -5 -9 16.91 14.55 -23 -5 9 26.58 20.14 23 -5 -8 -7.61 15.14 -23 -5 8 22.46 19.09 23 -5 -7 -4.72 17.09 -23 -5 7 -20.22 23.67 23 -5 -6 -16.85 18.09 -23 -5 6 56.82 30.46 23 -5 -5 -37.09 22.85 -23 -5 5 4.42 12.46 23 -5 -4 -17.63 17.89 -23 -5 4 32.95 25.50 23 -5 -3 31.55 22.36 -23 -5 3 19.14 16.01 23 -5 -2 0.95 13.90 -23 -5 2 -27.03 24.97 23 -5 -1 0.14 13.55 -23 -5 1 3.71 10.07 23 -5 0 4.81 14.95 -23 -5 0 10.25 18.33 23 -5 1 20.64 16.61 23 -5 4 14.86 21.19 23 -5 5 -8.12 16.72 23 -5 6 -33.14 27.99 23 -7 -14 -0.13 13.53 23 -7 -13 12.19 15.02 23 -7 -12 12.48 16.45 -23 -7 12 71.29 35.12 23 -7 -11 21.65 20.57 -23 -7 11 -9.81 17.64 23 -7 -10 -1.43 11.47 -23 -7 10 17.13 18.55 23 -7 -9 4.55 12.77 -23 -7 9 28.15 23.33 -23 -7 8 -13.08 16.24 -23 -7 7 4.04 15.24 -23 -7 6 -10.13 17.20 -23 -7 5 19.05 20.99 -23 -7 4 30.42 24.75 23 -7 -3 0.14 15.39 -23 -7 3 -25.76 23.00 23 -7 -2 70.70 30.43 -23 -7 2 -36.69 25.00 23 -7 -1 0.58 11.75 -23 -7 1 22.42 19.60 23 -7 0 -23.33 21.02 -23 -7 0 42.36 30.40 23 -7 1 5.43 12.42 23 -7 2 10.23 19.09 -23 -9 11 -14.71 18.54 -23 -9 10 29.04 24.89 -23 -9 9 -34.29 23.54 -23 -9 8 11.90 15.33 -23 -9 7 7.75 11.95 -23 -9 6 15.96 17.19 -23 -9 5 17.02 17.04 -23 -9 4 -69.93 33.99 -23 -9 3 -16.40 16.87 -23 -9 2 32.58 26.33 -23 -9 1 36.97 24.34 -23 -9 0 -5.18 17.81 24 -4 -7 9.48 17.55 24 -4 -6 22.99 23.17 24 -4 -5 -25.04 17.13 24 -4 -4 7.52 12.52 24 -4 -3 19.61 21.18 24 -4 -2 -0.14 19.68 24 -4 -1 -65.91 30.52 24 -4 3 35.69 27.58 24 -4 4 -29.13 27.49 24 -6 -9 -20.88 23.02 24 -6 -8 -0.14 14.65 24 -6 -7 1.78 14.02 24 -6 -6 31.40 25.73 24 -6 -5 -0.14 17.04 24 -6 -4 20.45 24.78 24 -6 -3 10.17 21.95 24 -6 -2 54.46 30.98 24 -6 -1 0.15 16.11 24 -6 0 -31.64 24.16 0 0 0 0.00 0.00 TITL GKL_SB_2B_RE_autored in C2/m REM C2/m (#12 in standard setting) CELL 0.71073 16.140594 17.143331 21.275391 90.0000 97.5376 90.0000 ZERR 25.00 0.000761 0.000451 0.000977 0.0000 0.0041 0.0000 LATT 7 SYMM -x, y,-z SFAC C H N O UNIT 275.00 250.00 25.00 25.00 REM CrysAlisPro recorded range (K): Min=300.0; max=300.0; aver:300.0 TEMP 27 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 25147 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ru1 Ru 0.48602(7) 0.72695(6) 0.57912(7) 0.0823(5) Uani 1 1 d . . . . . Ru2 Ru 0.50930(7) 0.79184(7) 0.43389(7) 0.0808(5) Uani 1 1 d . . . . . O1 O 0.5411(5) 0.7701(5) 0.5180(4) 0.066(2) Uani 1 1 d . . . . . O2 O 0.4326(6) 0.8290(5) 0.5959(5) 0.080(3) Uani 1 1 d . . . . . O3 O 0.5846(6) 0.7433(5) 0.6496(5) 0.080(3) Uani 1 1 d . . . . . O4 O 0.4213(7) 0.6832(6) 0.6455(6) 0.100(4) Uani 1 1 d . . . . . O5 O 0.5336(6) 0.6196(5) 0.5651(6) 0.088(3) Uani 1 1 d . . . . . O6 O 0.5611(6) 0.6935(6) 0.4058(5) 0.089(3) Uani 1 1 d . . . . . O7 O 0.6135(6) 0.8562(5) 0.4255(5) 0.077(3) Uani 1 1 d . . . . . O8 O 0.4651(6) 0.8123(7) 0.3413(5) 0.094(3) Uani 1 1 d . . . . . O9 O 0.4570(6) 0.8924(5) 0.4572(5) 0.081(3) Uani 1 1 d . . . . . C2 C 0.4648(10) 0.8783(8) 0.6357(8) 0.077(4) Uani 1 1 d . . . . . C4 C 0.5941(10) 0.8052(9) 0.6814(7) 0.080(4) Uani 1 1 d . . . . . C12 C 0.6387(10) 0.6885(9) 0.4035(8) 0.091(5) Uani 1 1 d . . . . . C13 C 0.6978(10) 0.7467(9) 0.4126(8) 0.092(5) Uani 1 1 d . . . . . H13 H 0.7533 0.7313 0.4144 0.111 Uiso 1 1 calc R U . . . C14 C 0.6834(10) 0.8264(9) 0.4194(7) 0.081(4) Uani 1 1 d . . . . . C15 C 0.7546(11) 0.8807(11) 0.4206(10) 0.112(6) Uani 1 1 d . . . . . H15A H 0.7913 0.8629 0.3916 0.168 Uiso 1 1 calc R U . . . H15B H 0.7845 0.8827 0.4627 0.168 Uiso 1 1 calc R U . . . H15C H 0.7342 0.9318 0.4083 0.168 Uiso 1 1 calc R U . . . C20 C 0.3812(11) 1.0090(9) 0.4526(8) 0.098(5) Uani 1 1 d . . . . . H20A H 0.3491 0.9945 0.4856 0.147 Uiso 1 1 calc R U . . . H20B H 0.3477 1.0408 0.4220 0.147 Uiso 1 1 calc R U . . . H20C H 0.4296 1.0379 0.4704 0.147 Uiso 1 1 calc R U . . . C16 C 0.3782(11) 0.8585(12) 0.2522(7) 0.104(6) Uani 1 1 d . . . . . H16A H 0.4243 0.8590 0.2279 0.155 Uiso 1 1 calc R U . . . H16B H 0.3416 0.9014 0.2396 0.155 Uiso 1 1 calc R U . . . H16C H 0.3481 0.8103 0.2449 0.155 Uiso 1 1 calc R U . . . C8 C 0.4758(11) 0.5554(9) 0.6499(9) 0.092(5) Uani 1 1 d . . . . . H8 H 0.4785 0.5089 0.6726 0.110 Uiso 1 1 calc R U . . . C17 C 0.4110(9) 0.8658(10) 0.3221(8) 0.083(4) Uani 1 1 d . . . . . C9 C 0.5224(10) 0.5596(8) 0.5994(9) 0.089(5) Uani 1 1 d . . . . . C3 C 0.5406(11) 0.8697(9) 0.6729(8) 0.089(5) Uani 1 1 d . . . . . H3 H 0.5594 0.9137 0.6961 0.106 Uiso 1 1 calc R U . . . C1 C 0.4158(11) 0.9529(8) 0.6384(9) 0.101(6) Uani 1 1 d . . . . . H1A H 0.4452 0.9948 0.6212 0.152 Uiso 1 1 calc R U . . . H1B H 0.4094 0.9644 0.6817 0.152 Uiso 1 1 calc R U . . . H1C H 0.3617 0.9469 0.6141 0.152 Uiso 1 1 calc R U . . . C5 C 0.6700(13) 0.8083(11) 0.7307(9) 0.114(6) Uani 1 1 d . . . . . H5A H 0.6558 0.7890 0.7703 0.171 Uiso 1 1 calc R U . . . H5B H 0.6890 0.8612 0.7360 0.171 Uiso 1 1 calc R U . . . H5C H 0.7135 0.7766 0.7173 0.171 Uiso 1 1 calc R U . . . C10 C 0.5694(10) 0.4878(9) 0.5824(10) 0.103(6) Uani 1 1 d . . . . . H10A H 0.5393 0.4633 0.5457 0.154 Uiso 1 1 calc R U . . . H10B H 0.5747 0.4519 0.6173 0.154 Uiso 1 1 calc R U . . . H10C H 0.6239 0.5027 0.5734 0.154 Uiso 1 1 calc R U . . . C18 C 0.3841(10) 0.9238(10) 0.3557(8) 0.085(4) Uani 1 1 d . . . . . H18 H 0.3462 0.9588 0.3344 0.102 Uiso 1 1 calc R U . . . C7 C 0.4259(11) 0.6137(9) 0.6694(9) 0.095(5) Uani 1 1 d . . . . . C19 C 0.4084(9) 0.9364(9) 0.4206(9) 0.084(4) Uani 1 1 d . . . . . C6 C 0.3691(13) 0.5983(11) 0.7185(9) 0.116(6) Uani 1 1 d . . . . . H6A H 0.3751 0.6394 0.7495 0.174 Uiso 1 1 calc R U . . . H6B H 0.3837 0.5494 0.7390 0.174 Uiso 1 1 calc R U . . . H6C H 0.3123 0.5964 0.6985 0.174 Uiso 1 1 calc R U . . . C11 C 0.6673(12) 0.6061(11) 0.3885(13) 0.151(10) Uani 1 1 d . . . . . H11A H 0.6534 0.5705 0.4203 0.227 Uiso 1 1 calc R U . . . H11B H 0.7267 0.6060 0.3880 0.227 Uiso 1 1 calc R U . . . H11C H 0.6398 0.5903 0.3477 0.227 Uiso 1 1 calc R U . . . N1 N 0.3895(14) 0.7127(14) 0.4960(16) 0.039(6) Uani 0.56(4) 1 d . U P A 1 N2 N 0.4085(16) 0.7369(15) 0.4353(14) 0.059(8) Uani 0.56(4) 1 d . U P A 1 C21 C 0.3453(18) 0.7168(16) 0.3924(18) 0.065(8) Uani 0.56(4) 1 d . U P A 1 H21 H 0.3424 0.7291 0.3496 0.078 Uiso 0.56(4) 1 calc R U P A 1 C22 C 0.285(2) 0.676(2) 0.4173(19) 0.073(12) Uani 0.56(4) 1 d . U P A 1 H22 H 0.2362 0.6560 0.3958 0.087 Uiso 0.56(4) 1 calc R U P A 1 C23 C 0.313(2) 0.6720(19) 0.4831(19) 0.062(9) Uani 0.56(4) 1 d D U P A 1 C24 C 0.278(2) 0.6357(17) 0.5350(13) 0.075(9) Uani 0.56(4) 1 d D U P A 1 H24A H 0.2263 0.6104 0.5189 0.112 Uiso 0.56(4) 1 calc R U P A 1 H24B H 0.3162 0.5979 0.5553 0.112 Uiso 0.56(4) 1 calc R U P A 1 H24C H 0.2672 0.6749 0.5652 0.112 Uiso 0.56(4) 1 calc R U P A 1 N1A N 0.3985(19) 0.718(2) 0.463(2) 0.058(12) Uani 0.44(4) 1 d . . P A 2 N2A N 0.3965(17) 0.6987(16) 0.528(2) 0.073(9) Uani 0.44(4) 1 d . . P A 2 C21A C 0.323(2) 0.664(2) 0.530(3) 0.082(14) Uani 0.44(4) 1 d . . P A 2 H21A H 0.3047 0.6448 0.5672 0.098 Uiso 0.44(4) 1 calc R U P A 2 C22A C 0.277(4) 0.659(3) 0.470(3) 0.12(3) Uani 0.44(4) 1 d . . P A 2 H22A H 0.2249 0.6361 0.4594 0.140 Uiso 0.44(4) 1 calc R U P A 2 C23A C 0.323(5) 0.692(3) 0.431(2) 0.102(18) Uani 0.44(4) 1 d D . P A 2 C24A C 0.309(4) 0.696(3) 0.363(2) 0.14(2) Uani 0.44(4) 1 d D . P A 2 H24D H 0.3543 0.7243 0.3480 0.208 Uiso 0.44(4) 1 calc R U P A 2 H24E H 0.3073 0.6441 0.3456 0.208 Uiso 0.44(4) 1 calc R U P A 2 H24F H 0.2575 0.7220 0.3496 0.208 Uiso 0.44(4) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.0655(7) 0.0431(6) 0.1417(13) -0.0067(6) 0.0266(7) 0.0036(5) Ru2 0.0665(7) 0.0671(7) 0.1024(10) -0.0270(6) -0.0134(6) 0.0177(6) O1 0.060(5) 0.053(5) 0.084(6) -0.006(4) 0.003(4) 0.004(4) O2 0.061(5) 0.049(5) 0.129(9) -0.010(5) 0.012(5) 0.005(4) O3 0.084(7) 0.057(5) 0.102(8) -0.005(5) 0.021(6) 0.007(5) O4 0.100(8) 0.055(6) 0.156(11) -0.009(6) 0.055(7) -0.010(5) O5 0.075(6) 0.052(5) 0.144(10) -0.008(6) 0.038(6) 0.008(5) O6 0.052(5) 0.080(6) 0.129(9) -0.054(6) -0.016(5) 0.019(5) O7 0.075(6) 0.068(6) 0.085(7) -0.005(5) 0.000(5) 0.013(5) O8 0.080(7) 0.113(8) 0.084(7) -0.035(6) -0.009(5) 0.027(6) O9 0.075(6) 0.071(6) 0.089(7) -0.018(5) -0.020(5) 0.024(5) C2 0.076(10) 0.050(7) 0.110(12) 0.005(8) 0.033(9) 0.006(7) C4 0.089(11) 0.080(10) 0.075(10) 0.012(8) 0.028(8) 0.009(8) C12 0.077(10) 0.078(10) 0.109(12) -0.035(9) -0.018(9) 0.023(8) C13 0.073(10) 0.086(10) 0.113(13) -0.030(9) -0.004(9) 0.014(8) C14 0.089(11) 0.075(9) 0.075(10) -0.011(7) -0.005(8) 0.010(8) C15 0.085(12) 0.093(12) 0.160(18) -0.020(12) 0.020(12) -0.006(10) C20 0.106(13) 0.081(10) 0.109(13) -0.007(9) 0.023(10) 0.033(9) C16 0.087(11) 0.145(16) 0.077(11) -0.003(11) 0.006(9) -0.014(11) C8 0.094(12) 0.059(9) 0.121(14) -0.003(9) 0.011(11) -0.009(8) C17 0.060(9) 0.093(11) 0.092(11) -0.001(9) -0.009(8) 0.003(8) C9 0.088(11) 0.038(7) 0.135(15) -0.014(8) -0.004(10) 0.000(7) C3 0.108(13) 0.061(9) 0.102(12) 0.001(8) 0.037(10) 0.013(8) C1 0.098(12) 0.053(8) 0.153(17) -0.009(9) 0.016(11) 0.014(8) C5 0.135(16) 0.104(13) 0.098(13) -0.003(11) -0.002(12) 0.014(12) C10 0.087(12) 0.065(9) 0.155(17) -0.017(10) 0.011(11) 0.011(8) C18 0.077(10) 0.084(10) 0.091(12) 0.003(9) 0.001(8) 0.009(8) C7 0.091(12) 0.062(9) 0.131(15) -0.015(9) 0.011(10) -0.010(8) C19 0.068(9) 0.069(9) 0.116(14) -0.010(9) 0.011(9) 0.010(7) C6 0.134(17) 0.098(13) 0.119(15) -0.008(11) 0.028(13) -0.020(12) C11 0.093(14) 0.092(13) 0.26(3) -0.071(16) 0.005(16) 0.028(11) N1 0.039(6) 0.039(6) 0.039(6) 0.0000(10) 0.0052(13) 0.0000(10) N2 0.059(8) 0.059(8) 0.059(8) -0.0001(10) 0.0077(14) -0.0001(10) C21 0.065(11) 0.065(11) 0.064(11) -0.001(8) 0.002(9) -0.008(8) C22 0.073(14) 0.073(14) 0.072(15) 0.003(9) 0.009(9) -0.003(9) C23 0.060(12) 0.060(12) 0.064(13) -0.002(9) 0.001(9) 0.009(8) C24 0.062(15) 0.075(14) 0.085(16) 0.009(12) 0.001(12) -0.011(12) N1A 0.053(15) 0.06(2) 0.05(2) -0.04(2) -0.015(16) 0.014(13) N2A 0.08(2) 0.063(16) 0.07(2) 0.015(15) -0.015(15) -0.005(13) C21A 0.024(17) 0.07(2) 0.14(4) -0.02(2) -0.025(18) -0.009(14) C22A 0.11(4) 0.08(3) 0.15(6) -0.04(3) -0.06(4) 0.02(3) C23A 0.12(5) 0.07(3) 0.11(5) 0.00(3) -0.02(4) 0.02(3) C24A 0.13(4) 0.14(4) 0.13(4) 0.05(3) -0.05(4) -0.05(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2A Ru1 O1 96.3(15) . . ? N2A Ru1 O2 90.7(9) . . ? O1 Ru1 O2 92.0(4) . . ? N2A Ru1 O4 82.4(15) . . ? O1 Ru1 O4 177.4(4) . . ? O2 Ru1 O4 85.7(4) . . ? N2A Ru1 O5 87.5(10) . . ? O1 Ru1 O5 91.9(4) . . ? O2 Ru1 O5 175.9(4) . . ? O4 Ru1 O5 90.4(4) . . ? N2A Ru1 O3 169.1(14) . . ? O1 Ru1 O3 93.5(4) . . ? O2 Ru1 O3 93.5(4) . . ? O4 Ru1 O3 87.9(5) . . ? O5 Ru1 O3 87.7(4) . . ? O1 Ru1 N1 80.4(8) . . ? O2 Ru1 N1 88.0(7) . . ? O4 Ru1 N1 98.3(8) . . ? O5 Ru1 N1 91.3(7) . . ? O3 Ru1 N1 173.8(8) . . ? O1 Ru2 N2 90.8(9) . . ? O1 Ru2 O6 92.6(4) . . ? N2 Ru2 O6 88.8(9) . . ? O1 Ru2 O9 90.4(4) . . ? N2 Ru2 O9 91.9(9) . . ? O6 Ru2 O9 177.0(5) . . ? O1 Ru2 O8 175.5(4) . . ? N2 Ru2 O8 84.7(10) . . ? O6 Ru2 O8 87.9(4) . . ? O9 Ru2 O8 89.2(4) . . ? O1 Ru2 O7 93.9(4) . . ? N2 Ru2 O7 175.0(9) . . ? O6 Ru2 O7 92.7(4) . . ? O9 Ru2 O7 86.3(4) . . ? O8 Ru2 O7 90.6(4) . . ? O1 Ru2 N1A 76.1(10) . . ? O6 Ru2 N1A 89.4(6) . . ? O9 Ru2 N1A 92.1(6) . . ? O8 Ru2 N1A 99.4(10) . . ? O7 Ru2 N1A 169.8(10) . . ? Ru1 O1 Ru2 132.6(5) . . ? C2 O2 Ru1 123.9(9) . . ? C4 O3 Ru1 122.4(10) . . ? C7 O4 Ru1 127.8(11) . . ? C9 O5 Ru1 123.8(10) . . ? C12 O6 Ru2 121.5(9) . . ? C14 O7 Ru2 123.3(10) . . ? C17 O8 Ru2 124.3(10) . . ? C19 O9 Ru2 126.8(10) . . ? O2 C2 C3 124.8(13) . . ? O2 C2 C1 115.1(14) . . ? C3 C2 C1 120.1(15) . . ? O3 C4 C3 124.6(16) . . ? O3 C4 C5 115.9(14) . . ? C3 C4 C5 119.5(16) . . ? O6 C12 C13 128.2(14) . . ? O6 C12 C11 113.5(15) . . ? C13 C12 C11 118.3(15) . . ? C12 C13 C14 127.0(15) . . ? C12 C13 H13 116.5 . . ? C14 C13 H13 116.5 . . ? O7 C14 C13 124.8(16) . . ? O7 C14 C15 116.5(14) . . ? C13 C14 C15 118.6(15) . . ? C14 C15 H15A 109.5 . . ? C14 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C14 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C19 C20 H20A 109.5 . . ? C19 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C19 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C17 C16 H16A 109.5 . . ? C17 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C17 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C7 C8 C9 126.2(16) . . ? C7 C8 H8 116.9 . . ? C9 C8 H8 116.9 . . ? O8 C17 C18 127.9(15) . . ? O8 C17 C16 112.6(15) . . ? C18 C17 C16 119.5(15) . . ? O5 C9 C8 127.5(14) . . ? O5 C9 C10 113.7(16) . . ? C8 C9 C10 118.7(15) . . ? C2 C3 C4 130.3(16) . . ? C2 C3 H3 114.9 . . ? C4 C3 H3 114.9 . . ? C2 C1 H1A 109.5 . . ? C2 C1 H1B 109.5 . . ? H1A C1 H1B 109.5 . . ? C2 C1 H1C 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? C4 C5 H5A 109.5 . . ? C4 C5 H5B 109.5 . . ? H5A C5 H5B 109.5 . . ? C4 C5 H5C 109.5 . . ? H5A C5 H5C 109.5 . . ? H5B C5 H5C 109.5 . . ? C9 C10 H10A 109.5 . . ? C9 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C9 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C17 C18 C19 125.1(15) . . ? C17 C18 H18 117.5 . . ? C19 C18 H18 117.5 . . ? O4 C7 C8 123.5(18) . . ? O4 C7 C6 115.3(15) . . ? C8 C7 C6 121.1(16) . . ? O9 C19 C18 125.5(14) . . ? O9 C19 C20 113.7(15) . . ? C18 C19 C20 120.7(15) . . ? C7 C6 H6A 109.5 . . ? C7 C6 H6B 109.5 . . ? H6A C6 H6B 109.5 . . ? C7 C6 H6C 109.5 . . ? H6A C6 H6C 109.5 . . ? H6B C6 H6C 109.5 . . ? C12 C11 H11A 109.5 . . ? C12 C11 H11B 109.5 . . ? H11A C11 H11B 109.5 . . ? C12 C11 H11C 109.5 . . ? H11A C11 H11C 109.5 . . ? H11B C11 H11C 109.5 . . ? C23 N1 N2 105(3) . . ? C23 N1 Ru1 136(3) . . ? N2 N1 Ru1 118.6(19) . . ? C21 N2 N1 108(3) . . ? C21 N2 Ru2 135(2) . . ? N1 N2 Ru2 117(2) . . ? N2 C21 C22 113(4) . . ? N2 C21 H21 123.5 . . ? C22 C21 H21 123.5 . . ? C21 C22 C23 105(4) . . ? C21 C22 H22 127.5 . . ? C23 C22 H22 127.5 . . ? N1 C23 C22 109(3) . . ? N1 C23 C24 119(5) . . ? C22 C23 C24 132(4) . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C23A N1A N2A 105(5) . . ? C23A N1A Ru2 135(5) . . ? N2A N1A Ru2 119.8(16) . . ? C21A N2A N1A 106(4) . . ? C21A N2A Ru1 140(4) . . ? N1A N2A Ru1 114(2) . . ? N2A C21A C22A 111(7) . . ? N2A C21A H21A 124.5 . . ? C22A C21A H21A 124.5 . . ? C23A C22A C21A 106(7) . . ? C23A C22A H22A 126.9 . . ? C21A C22A H22A 126.9 . . ? C22A C23A N1A 112(5) . . ? C22A C23A C24A 129(8) . . ? N1A C23A C24A 119(8) . . ? C23A C24A H24D 109.5 . . ? C23A C24A H24E 109.5 . . ? H24D C24A H24E 109.5 . . ? C23A C24A H24F 109.5 . . ? H24D C24A H24F 109.5 . . ? H24E C24A H24F 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ru1 N2A 1.76(3) . ? Ru1 O1 1.825(9) . ? Ru1 O2 2.003(9) . ? Ru1 O4 2.009(11) . ? Ru1 O5 2.031(9) . ? Ru1 O3 2.058(11) . ? Ru1 N1 2.21(3) . ? Ru2 O1 1.834(9) . ? Ru2 N2 1.88(2) . ? Ru2 O6 2.007(8) . ? Ru2 O9 2.010(9) . ? Ru2 O8 2.036(11) . ? Ru2 O7 2.040(10) . ? Ru2 N1A 2.33(5) . ? O2 C2 1.260(18) . ? O3 C4 1.256(18) . ? O4 C7 1.294(19) . ? O5 C9 1.289(19) . ? O6 C12 1.263(18) . ? O7 C14 1.261(17) . ? O8 C17 1.294(17) . ? O9 C19 1.278(17) . ? C2 C3 1.38(2) . ? C2 C1 1.508(18) . ? C4 C3 1.40(2) . ? C4 C5 1.51(2) . ? C12 C13 1.38(2) . ? C12 C11 1.53(2) . ? C13 C14 1.40(2) . ? C13 H13 0.9300 . ? C14 C15 1.48(2) . ? C15 H15A 0.9600 . ? C15 H15B 0.9600 . ? C15 H15C 0.9600 . ? C20 C19 1.51(2) . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C16 C17 1.52(2) . ? C16 H16A 0.9600 . ? C16 H16B 0.9600 . ? C16 H16C 0.9600 . ? C8 C7 1.38(2) . ? C8 C9 1.39(2) . ? C8 H8 0.9300 . ? C17 C18 1.33(2) . ? C9 C10 1.51(2) . ? C3 H3 0.9300 . ? C1 H1A 0.9600 . ? C1 H1B 0.9600 . ? C1 H1C 0.9600 . ? C5 H5A 0.9600 . ? C5 H5B 0.9600 . ? C5 H5C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C18 C19 1.40(2) . ? C18 H18 0.9300 . ? C7 C6 1.50(2) . ? C6 H6A 0.9600 . ? C6 H6B 0.9600 . ? C6 H6C 0.9600 . ? C11 H11A 0.9600 . ? C11 H11B 0.9600 . ? C11 H11C 0.9600 . ? N1 C23 1.41(5) . ? N1 N2 1.43(3) . ? N2 C21 1.32(5) . ? C21 C22 1.35(4) . ? C21 H21 0.9300 . ? C22 C23 1.42(6) . ? C22 H22 0.9300 . ? C23 C24 1.45(2) . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? N1A C23A 1.38(8) . ? N1A N2A 1.44(5) . ? N2A C21A 1.34(5) . ? C21A C22A 1.40(6) . ? C21A H21A 0.9300 . ? C22A C23A 1.31(10) . ? C22A H22A 0.9300 . ? C23A C24A 1.45(2) . ? C24A H24D 0.9600 . ? C24A H24E 0.9600 . ? C24A H24F 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N2A Ru1 O1 Ru2 8.7(11) . . . . ? O2 Ru1 O1 Ru2 -82.2(6) . . . . ? O5 Ru1 O1 Ru2 96.3(6) . . . . ? O3 Ru1 O1 Ru2 -175.8(6) . . . . ? N1 Ru1 O1 Ru2 5.4(8) . . . . ? N2 Ru2 O1 Ru1 -9.2(10) . . . . ? O6 Ru2 O1 Ru1 -98.0(6) . . . . ? O9 Ru2 O1 Ru1 82.8(6) . . . . ? O7 Ru2 O1 Ru1 169.1(6) . . . . ? N1A Ru2 O1 Ru1 -9.3(8) . . . . ? Ru1 O2 C2 C3 0(2) . . . . ? Ru1 O2 C2 C1 177.2(10) . . . . ? Ru1 O3 C4 C3 -1(2) . . . . ? Ru1 O3 C4 C5 -179.3(11) . . . . ? Ru2 O6 C12 C13 -7(3) . . . . ? Ru2 O6 C12 C11 173.3(14) . . . . ? O6 C12 C13 C14 -8(3) . . . . ? C11 C12 C13 C14 172.1(19) . . . . ? Ru2 O7 C14 C13 5(2) . . . . ? Ru2 O7 C14 C15 -173.8(12) . . . . ? C12 C13 C14 O7 9(3) . . . . ? C12 C13 C14 C15 -172.3(18) . . . . ? Ru2 O8 C17 C18 11(2) . . . . ? Ru2 O8 C17 C16 -169.8(10) . . . . ? Ru1 O5 C9 C8 2(2) . . . . ? Ru1 O5 C9 C10 -175.8(10) . . . . ? C7 C8 C9 O5 6(3) . . . . ? C7 C8 C9 C10 -176.3(16) . . . . ? O2 C2 C3 C4 -8(3) . . . . ? C1 C2 C3 C4 175.5(16) . . . . ? O3 C4 C3 C2 8(3) . . . . ? C5 C4 C3 C2 -173.4(17) . . . . ? O8 C17 C18 C19 -2(3) . . . . ? C16 C17 C18 C19 179.0(15) . . . . ? Ru1 O4 C7 C8 -3(3) . . . . ? Ru1 O4 C7 C6 180.0(12) . . . . ? C9 C8 C7 O4 -6(3) . . . . ? C9 C8 C7 C6 171.1(17) . . . . ? Ru2 O9 C19 C18 -2(2) . . . . ? Ru2 O9 C19 C20 -178.7(11) . . . . ? C17 C18 C19 O9 -3(3) . . . . ? C17 C18 C19 C20 173.4(16) . . . . ? C23 N1 N2 C21 4(3) . . . . ? Ru1 N1 N2 C21 174.6(17) . . . . ? C23 N1 N2 Ru2 -178.5(18) . . . . ? Ru1 N1 N2 Ru2 -8(3) . . . . ? O1 Ru2 N2 C21 -175(3) . . . . ? O6 Ru2 N2 C21 -82(3) . . . . ? O9 Ru2 N2 C21 95(3) . . . . ? O8 Ru2 N2 C21 6(3) . . . . ? O1 Ru2 N2 N1 9(2) . . . . ? O6 Ru2 N2 N1 102(2) . . . . ? O9 Ru2 N2 N1 -81(2) . . . . ? O8 Ru2 N2 N1 -170(2) . . . . ? N1 N2 C21 C22 -4(4) . . . . ? Ru2 N2 C21 C22 -180(3) . . . . ? N2 C21 C22 C23 1(4) . . . . ? N2 N1 C23 C22 -4(3) . . . . ? Ru1 N1 C23 C22 -171(2) . . . . ? N2 N1 C23 C24 177(3) . . . . ? Ru1 N1 C23 C24 9(4) . . . . ? C21 C22 C23 N1 2(4) . . . . ? C21 C22 C23 C24 -179(3) . . . . ? C23A N1A N2A C21A 0(3) . . . . ? Ru2 N1A N2A C21A 174(2) . . . . ? C23A N1A N2A Ru1 -180(3) . . . . ? Ru2 N1A N2A Ru1 -5(3) . . . . ? O1 Ru1 N2A C21A -180(4) . . . . ? O2 Ru1 N2A C21A -88(4) . . . . ? O4 Ru1 N2A C21A -2(4) . . . . ? O5 Ru1 N2A C21A 89(4) . . . . ? O3 Ru1 N2A C21A 25(8) . . . . ? O1 Ru1 N2A N1A 0(2) . . . . ? O2 Ru1 N2A N1A 91.7(19) . . . . ? O4 Ru1 N2A N1A 177(2) . . . . ? O5 Ru1 N2A N1A -92.0(19) . . . . ? O3 Ru1 N2A N1A -156(5) . . . . ? N1A N2A C21A C22A 1(4) . . . . ? Ru1 N2A C21A C22A -180(3) . . . . ? N2A C21A C22A C23A -1(5) . . . . ? C21A C22A C23A N1A 1(6) . . . . ? C21A C22A C23A C24A 173(5) . . . . ? N2A N1A C23A C22A 0(5) . . . . ? Ru2 N1A C23A C22A -174(3) . . . . ? N2A N1A C23A C24A -174(4) . . . . ? Ru2 N1A C23A C24A 13(6) . . . . ?