#------------------------------------------------------------------------------ #$Date: 2021-11-25 02:04:40 +0200 (Thu, 25 Nov 2021) $ #$Revision: 270870 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/89/7708922.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708922 loop_ _publ_author_name 'Gonzalez, Vanessa M.' 'Park, Gyeongjin' 'Yang, Mengxi' 'Gabba\"i, Fran\,cois P.' _publ_section_title ; Fluoride anion complexation and transport using a stibonium cation stabilized by an intramolecular PO \\rightarrow Sb pnictogen bond ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03370K _journal_year 2021 _chemical_formula_moiety 'C36 H29 F O P Sb' _chemical_formula_sum 'C36 H29 F O P Sb' _chemical_formula_weight 649.31 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-04-19 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-08-30 deposited with the CCDC. 2021-11-12 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 18.1724(19) _cell_length_b 11.1064(11) _cell_length_c 28.431(3) _cell_measurement_reflns_used 9924 _cell_measurement_temperature 110 _cell_measurement_theta_max 72.427 _cell_measurement_theta_min 3.109 _cell_volume 5738.2(10) _computing_cell_refinement 'SAINT V8.40A (?, 2016)' _computing_data_reduction 'SAINT V8.40A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 110.0 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0940 _diffrn_reflns_av_unetI/netI 0.0545 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 22 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 34 _diffrn_reflns_limit_l_min -35 _diffrn_reflns_number 33523 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 72.420 _diffrn_reflns_theta_min 3.109 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 8.426 _exptl_absorpt_correction_T_max 0.7536 _exptl_absorpt_correction_T_min 0.5186 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1075 before and 0.0630 after correction. The Ratio of minimum to maximum transmission is 0.6882. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.503 _exptl_crystal_description plate _exptl_crystal_F_000 2624 _exptl_crystal_size_max 0.24 _exptl_crystal_size_mid 0.12 _exptl_crystal_size_min 0.07 _refine_diff_density_max 1.560 _refine_diff_density_min -1.206 _refine_diff_density_rms 0.141 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.082 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 361 _refine_ls_number_reflns 5648 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.082 _refine_ls_R_factor_all 0.0743 _refine_ls_R_factor_gt 0.0533 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0334P)^2^+40.2473P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1150 _refine_ls_wR_factor_ref 0.1322 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4254 _reflns_number_total 5648 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03370k2.cif _cod_data_source_block test_j_0ma_a _cod_original_cell_volume 5738.1(10) _cod_database_code 7708922 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.590 _shelx_estimated_absorpt_t_min 0.237 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C5(H5), C3(H3), C26(H26), C18(H18), C30(H30), C4(H4), C12(H12), C17(H17), C36(H36), C6(H6), C32(H32), C24(H24), C27(H27), C23(H23), C14(H14), C20(H20), C10(H10), C35(H35), C22(H22), C34(H34), C29(H29), C11(H11), C33(H33), C8(H8), C21(H21), C16(H16), C28(H28), C9(H9), C15(H15) ; _shelx_res_file ; TITL test_j_0ma_a.res in Pbca test_j_0ma_a.res created by SHELXL-2018/3 at 11:09:16 on 19-Apr-2021 REM Old TITL test_j_0ma in Pbca REM SHELXT solution in Pbca REM R1 0.121, Rweak 0.001, Alpha 0.077, Orientation as input REM Formula found by SHELXT: C36 F O P Sb CELL 1.54178 18.1724 11.1064 28.4306 90 90 90 ZERR 8 0.0019 0.0011 0.0028 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H F O P Sb UNIT 288 232 8 8 8 8 L.S. 10 PLAN 20 SIZE 0.12 0.07 0.24 TEMP -163.15 BOND $H LIST 6 fmap 2 acta REM REM REM WGHT 0.033400 40.247303 FVAR 0.14903 SB1 6 0.477768 0.435200 0.626232 11.00000 0.02380 0.02026 = 0.01574 -0.00016 -0.00139 0.00074 P1 5 0.565337 0.291608 0.711823 11.00000 0.02233 0.02372 = 0.01900 0.00180 -0.00183 0.00018 F1 3 0.450058 0.548243 0.679390 11.00000 0.04200 0.03162 = 0.02019 -0.00441 0.00069 -0.00130 O1 4 0.577028 0.391069 0.675858 11.00000 0.02460 0.03102 = 0.02475 0.00672 -0.00200 -0.00265 C25 1 0.578965 0.337327 0.771976 11.00000 0.02932 0.02365 = 0.02138 0.00304 -0.00112 0.00039 C19 1 0.524346 0.301169 0.578332 11.00000 0.02780 0.02659 = 0.01730 -0.00465 -0.00186 0.00874 C1 1 0.429344 0.301299 0.672546 11.00000 0.02907 0.01957 = 0.01814 -0.00046 0.00443 0.00274 C5 1 0.324015 0.185352 0.697931 11.00000 0.02109 0.03199 = 0.02943 -0.00540 -0.00042 -0.00406 AFIX 43 H5 2 0.273820 0.163766 0.693926 11.00000 -1.20000 AFIX 0 C7 1 0.378961 0.481654 0.588376 11.00000 0.02291 0.02985 = 0.02526 0.00185 -0.00506 0.00076 C3 1 0.438729 0.161725 0.738266 11.00000 0.02539 0.02516 = 0.02187 0.00098 0.00020 0.00248 AFIX 43 H3 2 0.467465 0.125076 0.762229 11.00000 -1.20000 AFIX 0 C2 1 0.470920 0.245741 0.707168 11.00000 0.02841 0.01959 = 0.02019 -0.00107 0.00235 0.00500 C26 1 0.649855 0.340032 0.790935 11.00000 0.02541 0.03532 = 0.02794 0.00242 -0.00418 0.00152 AFIX 43 H26 2 0.690669 0.314194 0.772656 11.00000 -1.20000 AFIX 0 C13 1 0.544350 0.584707 0.604662 11.00000 0.03099 0.02442 = 0.02286 -0.00039 0.00333 -0.00094 C18 1 0.526325 0.643365 0.563103 11.00000 0.04475 0.03189 = 0.02145 0.00193 0.00159 0.00001 AFIX 43 H18 2 0.487893 0.612827 0.543847 11.00000 -1.20000 AFIX 0 C31 1 0.626905 0.168208 0.699593 11.00000 0.02246 0.02590 = 0.02536 -0.00294 -0.00396 0.00167 C30 1 0.520379 0.375318 0.798869 11.00000 0.03218 0.03146 = 0.02952 -0.00351 -0.00152 0.00174 AFIX 43 H30 2 0.472298 0.374499 0.785756 11.00000 -1.20000 AFIX 0 C4 1 0.364968 0.133255 0.733529 11.00000 0.03926 0.02786 = 0.02405 -0.00111 -0.00051 -0.00531 AFIX 43 H4 2 0.342529 0.078100 0.754662 11.00000 -1.20000 AFIX 0 C12 1 0.356171 0.417939 0.548865 11.00000 0.03979 0.03306 = 0.03079 -0.00301 -0.00912 0.00304 AFIX 43 H12 2 0.384566 0.351589 0.538127 11.00000 -1.20000 AFIX 0 C17 1 0.564099 0.746442 0.549463 11.00000 0.04715 0.03501 = 0.02778 0.00361 0.00016 0.00599 AFIX 43 H17 2 0.550346 0.786751 0.521333 11.00000 -1.20000 AFIX 0 C36 1 0.660419 0.162108 0.655446 11.00000 0.03039 0.04014 = 0.02856 -0.00245 -0.00087 0.00244 AFIX 43 H36 2 0.649992 0.221608 0.632384 11.00000 -1.20000 AFIX 0 C6 1 0.356341 0.269781 0.667799 11.00000 0.03304 0.02284 = 0.02647 -0.00176 -0.00280 0.00537 AFIX 43 H6 2 0.327571 0.305894 0.643729 11.00000 -1.20000 AFIX 0 C32 1 0.640141 0.077801 0.732729 11.00000 0.02725 0.03072 = 0.03184 -0.00100 -0.00139 -0.00347 AFIX 43 H32 2 0.616691 0.080286 0.762577 11.00000 -1.20000 AFIX 0 C24 1 0.498622 0.183322 0.579622 11.00000 0.03813 0.03183 = 0.02185 0.00149 0.00202 0.00034 AFIX 43 H24 2 0.458810 0.162455 0.599685 11.00000 -1.20000 AFIX 0 C27 1 0.660380 0.380677 0.836637 11.00000 0.03758 0.03550 = 0.03096 -0.00011 -0.01213 0.00261 AFIX 43 H27 2 0.708624 0.384343 0.849427 11.00000 -1.20000 AFIX 0 C23 1 0.531481 0.095750 0.551343 11.00000 0.05252 0.02694 = 0.02727 -0.00625 -0.00325 0.00682 AFIX 43 H23 2 0.513411 0.015500 0.551926 11.00000 -1.20000 AFIX 0 C14 1 0.600054 0.630353 0.631904 11.00000 0.04593 0.03250 = 0.03262 0.00837 -0.00887 -0.00222 AFIX 43 H14 2 0.612874 0.591559 0.660535 11.00000 -1.20000 AFIX 0 C20 1 0.581808 0.328560 0.549052 11.00000 0.04006 0.03320 = 0.02385 0.01058 0.00678 0.01033 AFIX 43 H20 2 0.599038 0.409253 0.547804 11.00000 -1.20000 AFIX 0 C10 1 0.251473 0.547274 0.539785 11.00000 0.02665 0.04844 = 0.04301 0.01251 -0.00853 -0.00388 AFIX 43 H10 2 0.208566 0.570644 0.523022 11.00000 -1.20000 AFIX 0 C35 1 0.709144 0.068818 0.645192 11.00000 0.03136 0.04731 = 0.03452 -0.01036 0.00002 0.00485 AFIX 43 H35 2 0.733020 0.065476 0.615495 11.00000 -1.20000 AFIX 0 C22 1 0.590120 0.124832 0.522483 11.00000 0.04974 0.02939 = 0.02985 -0.00464 0.00932 0.01299 AFIX 43 H22 2 0.612692 0.064502 0.503696 11.00000 -1.20000 AFIX 0 C34 1 0.722464 -0.019381 0.678899 11.00000 0.03647 0.03250 = 0.05421 -0.01173 -0.00669 0.00583 AFIX 43 H34 2 0.755914 -0.082827 0.672183 11.00000 -1.20000 AFIX 0 C29 1 0.530168 0.414622 0.844573 11.00000 0.04174 0.03384 = 0.02590 -0.00912 0.00874 -0.00114 AFIX 43 H29 2 0.489330 0.440486 0.862824 11.00000 -1.20000 AFIX 0 C11 1 0.292785 0.449723 0.524969 11.00000 0.04284 0.04316 = 0.03246 0.00142 -0.01633 -0.00254 AFIX 43 H11 2 0.277577 0.404488 0.498328 11.00000 -1.20000 AFIX 0 C33 1 0.687817 -0.015628 0.721677 11.00000 0.03243 0.02443 = 0.05449 0.00584 -0.01346 -0.00019 AFIX 43 H33 2 0.696521 -0.077639 0.744009 11.00000 -1.20000 AFIX 0 C8 1 0.336754 0.578122 0.603277 11.00000 0.03704 0.03891 = 0.01983 -0.00331 0.00193 0.00374 AFIX 43 H8 2 0.351431 0.622624 0.630227 11.00000 -1.20000 AFIX 0 C21 1 0.615804 0.242031 0.521056 11.00000 0.03286 0.04944 = 0.03084 0.00261 0.01206 0.00669 AFIX 43 H21 2 0.655957 0.263120 0.501309 11.00000 -1.20000 AFIX 0 C16 1 0.620735 0.790591 0.575951 11.00000 0.05144 0.02380 = 0.04595 0.00421 0.00032 -0.00660 AFIX 43 H16 2 0.647775 0.859127 0.565900 11.00000 -1.20000 AFIX 0 C28 1 0.601008 0.415673 0.863445 11.00000 0.05226 0.03857 = 0.02376 -0.00383 -0.00103 -0.00450 AFIX 43 H28 2 0.608357 0.440732 0.895046 11.00000 -1.20000 AFIX 0 C9 1 0.273520 0.610477 0.579421 11.00000 0.03454 0.04486 = 0.04121 0.00283 0.00229 0.01130 AFIX 43 H9 2 0.244938 0.676510 0.590254 11.00000 -1.20000 AFIX 0 C15 1 0.637854 0.733060 0.617855 11.00000 0.04487 0.03500 = 0.05594 0.00645 -0.01796 -0.01172 AFIX 43 H15 2 0.675941 0.764284 0.637222 11.00000 -1.20000 AFIX 0 HKLF 4 REM test_j_0ma_a.res in Pbca REM wR2 = 0.132172, GooF = S = 1.08214, Restrained GooF = 1.08214 for all data REM R1 = 0.053286 for 4254 Fo > 4sig(Fo) and 0.074291 for all 5648 data REM 361 parameters refined using 0 restraints END WGHT 0.0331 40.2813 REM Highest difference peak 1.560, deepest hole -1.206, 1-sigma level 0.141 Q1 1 0.5625 0.4348 0.6260 11.00000 0.05 1.56 Q2 1 0.4764 0.0633 0.6180 11.00000 0.05 1.50 Q3 1 0.4774 0.6934 0.6252 11.00000 0.05 1.15 Q4 1 0.4730 0.4348 0.6638 11.00000 0.05 0.89 Q5 1 0.4095 0.4782 0.6233 11.00000 0.05 0.86 Q6 1 0.4765 0.4371 0.5926 11.00000 0.05 0.85 Q7 1 0.4124 0.3978 0.6274 11.00000 0.05 0.78 Q8 1 0.4345 0.0874 0.7890 11.00000 0.05 0.69 Q9 1 0.4276 0.4503 0.6049 11.00000 0.05 0.66 Q10 1 0.5579 0.3029 0.7407 11.00000 0.05 0.65 Q11 1 0.4157 0.4207 0.6412 11.00000 0.05 0.64 Q12 1 0.5705 0.1969 0.5333 11.00000 0.05 0.63 Q13 1 0.4445 0.5654 0.7101 11.00000 0.05 0.61 Q14 1 0.6284 0.3294 0.5488 11.00000 0.05 0.58 Q15 1 0.6371 0.3978 0.8879 11.00000 0.05 0.57 Q16 1 0.4338 0.3430 0.7890 11.00000 0.05 0.55 Q17 1 0.5279 0.4552 0.8696 11.00000 0.05 0.54 Q18 1 0.3267 0.1598 0.7504 11.00000 0.05 0.53 Q19 1 0.6274 0.2445 0.7180 11.00000 0.05 0.51 Q20 1 0.5812 0.1138 0.5571 11.00000 0.05 0.50 ; _shelx_res_checksum 20446 _shelx_hkl_file ; 0 1 0 0.60 1.00 0 2 0 302.87 16.40 0 3 0 0.00 2.60 0 4 0 785.62 42.00 0 5 0 -1.60 2.90 0 6 0 1860.01 91.69 0 -7 0 -1.10 2.80 0 -8 0 1391.96 68.29 0 -9 0 -0.30 3.20 0 9 0 4.70 4.30 0 9 0 -17.90 21.90 0 -10 0 128.89 19.50 0 10 0 162.98 14.80 0 -11 0 1.30 3.50 0 11 0 -5.60 3.00 0 -12 0 11.70 4.80 0 12 0 15.20 4.20 0 13 0 0.80 2.40 -1 13 0 -0.40 2.30 -1 12 0 0.30 3.00 -1 11 0 -1.90 3.50 1 -11 0 -3.50 3.50 1 -11 0 -15.20 8.20 -1 10 0 6.10 4.10 1 -10 0 3.30 8.90 -1 9 0 -0.60 4.90 1 -9 0 -0.50 3.50 1 -8 0 -3.30 2.80 1 -7 0 -0.50 3.20 -1 6 0 -1.60 3.20 -1 5 0 -0.20 3.40 -1 4 0 -0.20 3.00 -1 3 0 0.40 2.50 -1 2 0 1.00 2.10 -1 1 0 0.40 0.90 1 0 0 0.30 0.70 1 1 0 -1.30 1.50 1 1 0 -0.20 1.00 1 2 0 0.50 2.00 1 3 0 -1.70 2.30 1 5 0 3.30 3.40 -1 -7 0 1.10 2.70 -1 -8 0 3.90 3.10 1 8 0 -4.90 14.70 1 8 0 -3.30 5.20 -1 -9 0 -3.00 3.30 1 9 0 5.30 4.50 1 9 0 -25.00 22.10 1 10 0 7.00 3.90 -1 -11 0 -2.20 3.10 1 11 0 -2.20 3.00 1 12 0 -3.40 2.30 1 13 0 -1.10 2.00 -2 13 0 10.50 2.90 -2 12 0 2.10 3.00 2 -12 0 -3.10 5.20 -2 11 0 12.80 4.60 2 -11 0 -1.00 5.80 2 -11 0 -2.30 4.20 -2 10 0 124.69 13.40 2 -10 0 129.19 15.00 -2 9 0 33.70 7.00 2 -9 0 8.30 7.10 2 -9 0 22.70 5.40 -2 8 0 899.11 52.89 2 -7 0 2.70 3.60 -2 6 0 984.80 52.69 -2 5 0 455.15 27.20 -2 4 0 171.28 13.00 -2 3 0 280.97 16.60 -2 2 0 35.20 5.20 -2 1 0 117.39 6.70 2 0 0 9999.00 440.96 2 1 0 118.39 8.20 2 2 0 34.60 5.10 2 2 0 42.90 6.90 2 3 0 289.77 17.40 2 4 0 189.68 14.10 -2 -7 0 6.70 3.00 2 7 0 -13.80 9.90 -2 -8 0 963.90 48.30 2 8 0 918.01 49.30 -2 -9 0 30.70 5.70 2 9 0 -19.00 33.80 -2 -10 0 119.89 14.40 2 10 0 115.19 12.20 -2 -11 0 10.50 4.20 2 11 0 14.10 4.60 -2 -12 0 4.00 3.40 2 12 0 0.80 2.90 2 13 0 9.70 2.70 -3 13 0 -4.30 2.20 3 -13 0 -6.50 6.40 -3 12 0 -1.10 2.70 3 -12 0 -5.20 4.20 -3 11 0 -3.20 3.50 3 -11 0 -6.00 4.70 -3 10 0 -4.30 3.60 3 -10 0 -7.70 4.30 3 -10 0 5.20 5.20 -3 9 0 -2.80 4.30 3 -9 0 -11.30 5.60 3 -9 0 -7.30 4.00 -3 8 0 0.60 5.20 3 -8 0 -3.80 3.80 3 -7 0 -3.00 4.50 -3 6 0 -1.10 3.40 -3 5 0 0.80 3.40 -3 4 0 -1.50 2.80 -3 3 0 -0.40 2.30 -3 2 0 -0.50 1.80 -3 1 0 0.40 1.30 3 -1 0 3.30 3.20 3 0 0 0.30 2.00 3 1 0 0.00 2.60 3 2 0 -1.10 3.80 3 3 0 2.20 4.20 3 4 0 -0.60 5.20 3 5 0 -1.70 6.10 3 6 0 -1.80 7.90 -3 -7 0 -0.20 2.70 3 7 0 -9.20 10.20 -3 -8 0 -3.90 2.50 3 8 0 0.00 4.00 3 8 0 7.80 15.80 -3 -9 0 0.40 3.20 3 9 0 -2.30 3.60 -3 -10 0 -3.40 3.20 3 10 0 0.10 3.70 -3 -11 0 -0.90 3.10 3 11 0 0.00 3.60 -3 -12 0 -1.50 3.20 3 12 0 -1.80 2.50 -3 -13 0 -5.40 3.80 -4 13 0 14.60 3.60 4 -13 0 17.10 5.60 -4 12 0 1.10 2.70 4 -12 0 -5.70 3.70 -4 11 0 509.65 36.40 4 -11 0 508.45 31.30 -4 10 0 145.99 14.70 4 -10 0 158.68 15.70 -4 9 0 1.40 4.90 4 -9 0 8.00 5.10 4 -9 0 -3.00 5.10 -4 8 0 936.71 50.49 4 -8 0 939.11 50.09 4 -8 0 895.71 47.80 -4 7 0 5.40 5.50 4 -7 0 8.10 5.20 -4 6 0 582.04 34.80 -4 5 0 92.69 10.50 -4 4 0 7.10 4.90 -4 3 0 284.67 16.80 -4 2 0 2997.20 134.49 -4 1 0 12.60 2.60 4 -1 0 11.60 4.80 -4 0 0 200.88 12.10 4 0 0 212.98 13.60 4 1 0 11.60 4.60 4 2 0 3077.19 140.99 4 3 0 292.47 20.00 4 4 0 9.40 6.50 4 5 0 90.09 14.50 4 6 0 647.84 43.00 -4 -7 0 14.80 3.80 4 7 0 -4.30 11.10 -4 -9 0 3.40 3.40 4 9 0 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6.90 4.40 20 2 0 18.50 4.70 20 3 0 14.10 6.00 20 4 0 -3.60 3.70 21 -4 0 -0.10 2.80 -21 3 0 -1.30 2.30 21 -3 0 1.00 2.70 21 -2 0 -2.20 2.60 21 -1 0 -3.10 2.60 21 0 0 6.30 3.50 21 1 0 4.20 3.30 21 2 0 -1.20 3.00 22 -2 0 16.00 3.60 22 -1 0 -1.70 3.50 22 0 0 258.77 18.30 22 1 0 -2.70 4.50 22 2 1 -5.00 2.50 22 1 1 0.90 3.00 22 0 1 4.10 3.70 22 -1 1 -8.80 4.60 22 -2 1 198.68 13.40 21 2 1 2.20 3.10 21 1 1 95.79 10.50 21 0 1 2.00 3.20 21 -1 1 114.69 11.40 21 -2 1 2.00 2.90 -21 2 -1 7.50 2.90 21 -3 1 5.80 3.30 -21 3 -1 5.00 2.60 21 -4 1 0.80 3.90 -21 4 -1 -0.60 2.10 20 4 1 4.80 4.90 20 3 1 5.30 5.90 20 2 1 80.89 12.00 20 1 1 9.10 4.20 20 0 1 -2.10 3.20 20 -1 1 8.30 4.10 -20 1 -1 7.30 3.50 20 -2 1 175.98 14.20 -20 2 -1 133.09 11.00 20 -3 1 6.80 3.60 -20 3 -1 -0.90 2.70 20 -4 1 182.88 13.40 -20 4 -1 159.28 11.60 20 -5 1 16.50 3.60 -20 5 -1 15.80 3.20 20 -6 1 99.39 8.60 -20 6 -1 76.69 7.90 19 4 1 -4.50 3.30 19 3 1 -3.80 3.70 19 2 1 1.60 4.70 19 1 1 162.98 16.30 19 0 1 -0.70 3.50 19 -1 1 151.38 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26.50 6.30 17 0 3 -3.30 3.70 17 -1 3 39.40 7.70 -17 1 -3 58.19 8.70 17 -2 3 21.40 5.50 -17 2 -3 26.40 4.80 17 -3 3 20.40 5.80 -17 3 -3 24.00 4.60 17 -4 3 131.49 22.00 -17 4 -3 155.98 12.70 17 -5 3 23.70 5.20 17 -6 3 111.49 11.60 -17 6 -3 114.49 10.40 17 -7 3 18.60 4.00 -17 7 -3 13.50 3.30 17 -8 3 3.70 2.80 -17 8 -3 2.60 2.10 16 5 3 4.60 4.70 16 4 3 21.10 6.90 16 3 3 9.60 5.20 16 2 3 11.30 4.90 16 1 3 206.98 19.30 16 0 3 0.20 5.50 -16 0 -3 3.80 6.10 16 -1 3 243.68 19.70 -16 1 -3 218.58 16.20 16 -2 3 8.20 4.40 16 -3 3 13.90 5.20 -16 3 -3 18.70 4.50 16 -4 3 61.99 11.50 -16 4 -3 31.30 5.40 16 -5 3 71.19 11.70 -16 5 -3 73.99 8.80 16 -6 3 194.28 16.00 16 -6 3 215.08 17.10 -16 6 -3 217.28 15.60 16 -7 3 71.19 9.50 16 -7 3 100.89 10.50 -16 7 -3 84.19 8.50 16 -8 3 13.80 4.10 16 -8 3 22.60 4.10 -16 8 -3 16.30 4.40 16 -9 3 58.69 6.50 -15 -9 -3 79.09 9.60 -15 -7 -3 -0.50 3.90 15 5 3 25.80 6.30 15 4 3 86.09 14.60 15 3 3 40.90 11.60 15 2 3 220.18 19.30 15 1 3 31.50 6.50 15 0 3 -3.00 3.90 15 -1 3 38.10 7.30 -15 1 -3 56.99 8.40 15 -2 3 252.77 20.00 -15 2 -3 249.58 17.10 15 -3 3 98.89 16.90 -15 3 -3 87.29 10.00 15 -4 3 121.89 13.50 15 -4 3 106.69 13.30 -15 4 -3 105.29 14.30 15 -5 3 113.69 14.30 15 -5 3 97.89 13.10 -15 5 -3 117.89 11.40 15 -6 3 164.48 15.50 15 -6 3 147.39 15.50 -15 6 -3 163.68 13.00 15 -7 3 8.40 4.40 15 -7 3 4.50 3.80 15 -8 3 2.30 3.50 15 -8 3 1.10 2.90 -15 8 -3 0.20 2.10 15 -9 3 109.09 9.10 15 -9 3 111.09 10.10 -15 9 -3 96.99 8.10 15 -10 3 68.89 8.30 -14 -10 -3 5.00 3.30 -14 -9 -3 120.79 10.00 -14 -8 -3 15.20 4.00 -14 -7 -3 145.89 16.70 14 6 3 46.80 10.80 14 5 3 111.99 15.70 14 4 3 14.60 6.00 14 3 3 49.00 8.20 14 2 3 12.10 5.40 14 1 3 350.76 24.20 14 0 3 -6.80 3.70 14 -1 3 413.96 26.70 -14 1 -3 404.46 23.50 14 -2 3 16.40 5.90 -14 2 -3 24.20 4.70 14 -3 3 71.99 12.20 14 -3 3 56.29 8.70 -14 3 -3 72.79 9.00 14 -4 3 20.80 5.90 14 -4 3 9.50 5.10 -14 4 -3 19.30 4.60 14 -5 3 246.98 19.40 14 -5 3 232.48 19.10 -14 5 -3 281.77 24.00 14 -6 3 125.69 14.60 14 -6 3 125.29 13.80 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452.55 32.30 -6 6 3 193.28 13.40 -6 6 3 167.88 17.30 -6 5 3 182.08 15.80 -6 4 3 321.17 20.90 -6 3 3 6.20 3.10 -6 2 3 347.17 20.40 6 -2 -3 377.26 24.60 -6 1 3 367.66 21.20 6 -1 -3 401.46 26.70 -6 0 3 -2.90 3.00 6 0 -3 -2.50 3.80 6 1 -3 383.36 25.00 6 2 -3 382.46 35.20 6 3 -3 2.30 5.20 6 4 -3 353.36 27.70 6 5 -3 183.68 19.70 6 6 -3 156.88 22.30 -6 -7 3 438.66 25.60 6 7 -3 521.55 41.30 -6 -8 3 69.29 8.50 6 8 -3 13.80 22.60 6 8 -3 59.49 10.00 -6 -9 3 137.89 13.00 -6 -10 3 14.80 4.50 6 10 -3 23.20 4.50 -6 -11 3 7.20 6.00 6 11 -3 2.50 3.10 -6 -12 3 75.79 8.80 -7 12 3 127.39 11.70 7 -12 -3 107.39 11.20 -7 11 3 7.90 4.50 7 -11 -3 7.20 4.10 -7 10 3 99.59 13.70 7 -10 -3 88.69 12.60 -7 9 3 178.08 17.00 7 -9 -3 160.98 15.40 -7 8 3 10.20 14.60 -7 8 3 17.30 4.30 -7 8 3 6.90 7.00 7 -8 -3 27.30 6.10 -7 7 3 84.09 14.70 -7 7 3 87.59 9.30 7 -7 -3 88.79 11.60 -7 6 3 -1.20 5.60 -7 6 3 8.00 3.40 -7 5 3 4.90 2.90 -7 5 3 10.50 5.40 -7 4 3 446.06 26.80 -7 2 3 253.87 16.40 7 -2 -3 275.37 20.80 -7 1 3 42.50 6.20 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10 -7 -3 156.98 15.30 -10 6 3 65.89 8.80 10 -6 -3 81.29 11.20 -10 5 3 233.18 16.30 -10 5 3 286.47 25.70 -10 4 3 3.60 2.90 -10 4 3 5.80 6.80 -10 3 3 401.26 24.90 -10 2 3 9.40 5.30 -10 1 3 528.55 29.40 10 -1 -3 553.24 39.30 -10 0 3 1.00 4.60 10 0 -3 5.30 6.00 10 1 -3 517.75 35.40 -10 -2 3 4.20 7.60 10 2 -3 8.10 7.10 10 3 -3 408.46 31.60 10 4 -3 5.30 8.70 10 5 -3 233.68 27.20 10 6 -3 10.40 7.80 10 6 -3 -18.60 15.50 -10 -7 3 147.99 12.20 -10 -8 3 25.40 5.40 -10 -9 3 75.29 9.20 -10 -10 3 0.90 2.90 -10 -11 3 18.40 5.80 -10 -12 3 5.50 2.70 11 -11 -3 -0.80 2.30 11 -11 -3 -2.10 2.60 11 -10 -3 132.99 13.00 11 -10 -3 137.99 12.60 -11 9 3 0.30 2.50 11 -9 -3 -1.80 5.40 -11 8 3 100.49 10.70 11 -8 -3 98.29 12.90 -11 7 3 22.50 5.20 -11 6 3 178.78 14.20 11 -6 -3 180.48 15.70 -11 5 3 26.40 4.90 11 -5 -3 21.70 8.30 -11 4 3 663.03 34.60 -11 1 3 12.00 7.10 11 -1 -3 8.70 7.10 -11 0 3 -4.30 5.90 11 0 -3 -8.60 7.30 -11 -1 3 1.00 6.70 11 1 -3 6.00 7.50 -11 -2 3 493.75 34.60 11 2 -3 537.95 37.70 -11 -3 3 -3.50 10.40 11 3 -3 2.30 8.00 11 4 -3 620.54 45.20 11 5 -3 -2.30 10.60 11 5 -3 24.40 15.70 11 6 -3 -20.30 19.60 11 6 -3 -10.80 6.50 -11 -7 3 17.30 5.20 -11 -8 3 74.39 9.90 -11 -9 3 -5.80 2.90 -11 -10 3 113.29 10.60 -11 -11 3 -1.70 2.50 12 -11 -3 4.60 3.00 12 -11 -3 5.20 2.50 12 -10 -3 -2.70 2.50 12 -10 -3 -0.40 2.90 -12 9 3 194.78 13.60 12 -9 -3 179.98 16.00 12 -9 -3 174.18 16.00 12 -8 -3 6.60 4.40 12 -8 -3 6.90 4.60 -12 7 3 267.17 18.80 12 -7 -3 268.97 20.60 12 -7 -3 279.87 21.40 -12 6 3 20.80 4.80 12 -6 -3 24.30 6.10 12 -6 -3 26.40 6.60 -12 5 3 166.88 13.30 12 -5 -3 156.18 15.20 12 -5 -3 174.58 17.00 -12 4 3 2.90 3.00 12 -4 -3 0.10 5.00 -12 3 3 309.67 18.90 12 -3 -3 268.07 28.30 -12 2 3 86.29 10.20 12 0 -3 7.00 7.20 12 1 -3 162.78 21.20 12 2 -3 100.99 17.40 12 3 -3 301.57 30.10 12 4 -3 0.80 12.80 12 5 -3 -11.90 15.60 -12 -8 3 -0.20 3.60 -12 -9 3 165.48 12.90 13 -11 -3 -1.80 1.90 13 -11 -3 2.40 2.50 13 -10 -3 61.19 7.70 13 -10 -3 63.99 8.40 -13 9 3 65.89 7.60 13 -9 -3 62.59 9.60 13 -9 -3 75.09 10.30 -13 8 3 0.10 2.40 13 -8 -3 -1.20 4.50 13 -8 -3 1.90 4.40 -13 7 3 0.10 2.80 13 -7 -3 5.60 4.20 13 -7 -3 3.40 4.20 -13 6 3 201.18 20.40 13 -6 -3 192.08 16.40 13 -6 -3 198.48 17.80 -13 5 3 13.80 4.00 13 -5 -3 5.40 4.70 13 -5 -3 12.80 5.20 -13 4 3 579.54 31.40 13 -4 -3 575.04 32.30 13 -4 -3 542.45 34.30 -13 3 3 12.20 4.10 13 -3 -3 12.20 7.60 13 -3 -3 9.30 5.60 -13 2 3 376.26 22.90 13 -2 -3 409.46 26.20 13 -1 -3 29.20 7.20 13 0 -3 10.40 10.20 13 0 -3 5.20 6.20 13 1 -3 23.00 12.00 13 1 -3 19.20 6.10 13 2 -3 405.66 35.50 13 2 -3 337.87 25.70 13 3 -3 10.80 5.70 13 4 -3 491.25 35.10 13 4 -3 533.05 45.50 13 5 -3 25.10 24.50 13 6 -3 -13.30 7.90 -13 -9 3 48.40 8.10 -13 -10 3 37.00 6.50 14 -10 -3 -0.30 2.30 14 -10 -3 1.60 2.70 -14 9 3 130.69 11.80 14 -9 -3 142.09 12.10 14 -9 -3 157.78 16.80 -14 8 3 7.60 2.90 14 -8 -3 4.50 4.20 14 -8 -3 14.90 4.60 -14 7 3 171.38 13.70 14 -7 -3 171.38 21.40 14 -7 -3 154.68 15.90 -14 6 3 133.59 12.20 14 -6 -3 125.59 15.10 14 -6 -3 122.99 13.40 -14 5 3 279.27 21.80 14 -5 -3 248.58 20.80 14 -5 -3 264.47 19.30 -14 4 3 9.90 3.90 14 -4 -3 17.80 6.20 14 -4 -3 5.80 5.60 -14 3 3 74.89 9.20 14 -3 -3 52.09 8.20 -14 2 3 30.60 6.90 14 -2 -3 11.60 6.40 14 -1 -3 354.66 24.90 14 0 -3 -4.80 4.30 14 1 -3 364.06 25.10 14 1 -3 307.97 34.30 14 2 -3 21.00 5.90 14 2 -3 28.80 15.50 14 3 -3 47.70 8.70 14 3 -3 61.19 27.30 14 4 -3 22.90 22.80 14 4 -3 11.10 7.10 14 5 -3 48.00 9.40 14 6 -3 -8.20 8.70 -14 -8 3 -4.50 4.60 -14 -9 3 133.59 15.20 15 -10 -3 79.99 7.30 -15 9 3 117.09 12.90 15 -9 -3 111.59 9.80 15 -9 -3 111.49 9.70 -15 8 3 1.60 2.30 15 -8 -3 4.40 3.10 15 -8 -3 0.00 3.00 -15 7 3 -2.50 3.90 15 -7 -3 3.10 3.90 15 -7 -3 1.90 3.90 -15 6 3 166.98 13.60 15 -6 -3 155.68 16.10 -15 5 3 112.79 11.40 15 -5 -3 106.09 13.90 15 -4 -3 108.89 14.70 -15 3 3 67.39 9.40 15 -3 -3 62.79 14.50 -15 2 3 240.18 16.70 15 -2 -3 231.48 19.80 15 -1 -3 35.20 7.20 15 0 -3 1.20 4.60 15 1 -3 32.60 6.70 15 2 -3 196.18 19.10 15 2 -3 173.58 29.70 15 3 -3 51.19 12.70 15 3 -3 31.80 32.20 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56.29 9.40 -14 -6 -4 32.90 6.10 14 5 4 123.39 15.70 14 4 4 34.70 7.20 14 3 4 669.53 39.70 14 2 4 38.50 7.10 14 1 4 34.80 7.00 14 0 4 304.77 22.40 14 -1 4 38.50 7.10 -14 1 -4 61.19 8.40 14 -2 4 46.50 7.70 -14 2 -4 57.69 7.90 14 -3 4 694.93 39.50 14 -3 4 669.93 38.80 -14 3 -4 731.13 37.60 14 -4 4 33.00 6.80 14 -4 4 24.30 6.40 -14 4 -4 35.40 5.90 14 -5 4 294.97 21.30 14 -5 4 292.67 21.00 14 -6 4 33.90 6.80 14 -6 4 26.70 5.70 -14 6 -4 28.60 5.20 14 -7 4 62.19 12.60 -14 7 -4 87.49 9.10 14 -8 4 132.09 12.20 14 -8 4 138.79 13.70 -14 8 -4 132.39 10.70 14 -9 4 9.20 3.10 14 -9 4 6.60 4.10 -14 9 -4 10.00 3.00 14 -10 4 -0.20 2.30 14 -10 4 3.50 3.00 -13 -10 -4 18.90 3.90 -13 -9 -4 5.00 3.20 -13 -8 -4 -3.20 4.80 -13 -7 -4 11.20 4.20 13 6 4 27.40 9.30 13 5 4 24.60 7.20 13 4 4 6.00 5.20 13 3 4 -3.00 4.10 13 2 4 7.90 4.80 13 1 4 7.70 5.30 13 -1 4 13.70 5.90 -13 1 -4 13.10 4.30 13 -2 4 3.40 4.50 -13 2 -4 8.40 3.50 13 -3 4 0.60 5.80 13 -3 4 -10.00 6.60 -13 3 -4 -1.10 2.60 13 -4 4 11.90 5.70 13 -4 4 4.60 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209.58 15.70 5 1 -4 128.19 13.20 5 2 -4 132.19 13.90 5 3 -4 7.10 6.30 5 4 -4 12.30 8.20 5 5 -4 6.10 8.40 5 6 -4 7.80 14.00 -5 -7 4 0.90 3.10 5 7 -4 -11.40 12.40 -5 -8 4 12.20 3.80 5 8 -4 3.90 4.90 5 9 -4 -31.40 30.00 -5 -10 4 26.10 5.60 -5 -11 4 62.19 8.70 5 11 -4 65.39 8.70 -5 -12 4 65.89 8.60 -5 -13 4 -5.00 2.70 -6 13 4 163.48 12.20 6 -13 -4 132.29 12.30 -6 12 4 0.60 3.20 6 -12 -4 3.60 3.50 -6 11 4 110.39 13.40 6 -11 -4 120.79 13.50 -6 10 4 78.79 13.20 6 -10 -4 110.29 13.10 -6 8 4 593.74 36.60 -6 8 4 515.15 38.10 -6 8 4 513.65 29.80 6 -8 -4 529.75 32.10 -6 7 4 32.80 10.00 -6 7 4 34.30 5.40 -6 6 4 206.98 14.30 -6 6 4 207.38 18.40 -6 5 4 218.28 14.90 -6 5 4 210.78 17.20 -6 4 4 4.00 4.40 -6 3 4 877.61 44.80 -6 2 4 27.20 5.20 6 -2 -4 38.30 8.50 -6 1 4 10.90 3.90 6 -1 -4 9.80 4.70 -6 0 4 1587.54 85.89 6 0 -4 2054.69 92.99 6 2 -4 35.60 9.70 6 3 -4 936.71 53.49 6 4 -4 1.80 7.20 6 5 -4 227.28 23.50 6 6 -4 229.08 25.80 -6 -7 4 41.80 6.00 6 7 -4 52.49 17.90 -6 -8 4 535.75 30.20 6 8 -4 535.05 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16.00 -8 9 4 218.58 21.00 8 -9 -4 220.28 18.50 -8 8 4 131.29 19.70 -8 8 4 143.39 12.90 -8 8 4 107.59 20.30 8 -8 -4 162.58 14.80 -8 7 4 29.90 5.20 8 -7 -4 26.50 6.20 -8 6 4 5.70 7.00 -8 6 4 9.70 3.00 -8 5 4 1280.57 60.09 -8 5 4 1205.78 64.89 -8 4 4 63.09 9.10 -8 3 4 1287.37 63.69 8 -2 -4 17.70 7.80 -8 1 4 58.39 7.40 8 -1 -4 46.50 9.80 -8 0 4 831.62 43.70 8 0 -4 799.92 46.90 -8 -1 4 46.80 9.10 8 1 -4 43.80 8.90 8 2 -4 11.10 6.80 8 3 -4 1366.76 74.69 8 4 -4 56.29 13.30 8 5 -4 1447.76 82.49 8 6 -4 -7.60 12.60 -8 -7 4 36.80 5.70 8 7 -4 32.20 31.60 -8 -9 4 206.08 16.20 -8 -10 4 6.90 3.30 -8 -11 4 358.66 22.20 -8 -12 4 -3.20 2.40 -9 12 4 15.80 4.50 9 -12 -4 17.30 4.20 9 -12 -4 11.40 3.00 -9 11 4 -6.80 4.00 9 -11 -4 5.50 3.60 -9 10 4 10.90 6.60 9 -10 -4 3.40 4.10 -9 9 4 0.10 7.20 -9 9 4 2.80 3.70 9 -9 -4 6.10 4.10 -9 8 4 20.30 4.60 9 -8 -4 31.80 7.80 -9 7 4 -1.50 2.50 -9 7 4 -1.20 11.70 9 -7 -4 5.00 5.20 -9 6 4 59.09 11.80 9 -6 -4 46.60 7.60 -9 5 4 9.90 6.60 -9 5 4 2.30 2.70 -9 4 4 -0.50 4.70 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-4 14.10 10.80 10 5 -4 983.60 64.09 10 6 -4 -12.70 7.70 10 7 -4 -5.30 27.30 -10 -8 4 38.60 6.30 -10 -9 4 55.89 8.30 -10 -10 4 2.70 2.90 -10 -12 4 2.00 2.30 11 -11 -4 1.90 2.70 11 -11 -4 1.80 2.40 11 -10 -4 21.50 4.60 11 -10 -4 27.90 5.40 -11 9 4 -4.60 2.40 11 -9 -4 1.40 6.20 11 -9 -4 -2.00 4.30 -11 8 4 -0.80 2.90 11 -8 -4 -0.60 3.90 -11 7 4 7.90 3.50 11 -7 -4 8.90 5.30 -11 6 4 81.29 9.50 11 -6 -4 78.39 11.30 -11 5 4 16.20 4.10 11 -5 -4 14.40 6.20 -11 4 4 0.50 2.80 -11 3 4 47.20 10.20 -11 2 4 31.10 8.00 -11 1 4 87.29 11.40 11 -1 -4 81.79 13.50 -11 0 4 107.09 13.00 11 0 -4 118.89 16.90 -11 -1 4 95.09 15.00 11 1 -4 92.49 16.00 -11 -2 4 21.10 10.40 11 2 -4 19.50 10.30 -11 -3 4 20.30 11.30 11 3 -4 36.20 10.00 11 4 -4 11.60 11.70 11 5 -4 3.80 15.20 11 6 -4 -2.70 20.40 11 6 -4 -13.70 7.40 -11 -7 4 10.40 4.60 -11 -8 4 -1.10 3.60 -11 -10 4 26.70 5.30 -11 -11 4 -0.70 2.50 12 -11 -4 314.17 18.90 12 -11 -4 312.87 18.10 12 -10 -4 -0.50 2.60 12 -10 -4 -0.10 3.10 -12 9 4 13.70 3.30 12 -9 -4 23.50 5.60 12 -9 -4 8.40 4.10 -12 8 4 5.60 3.10 12 -8 -4 9.40 4.70 12 -8 -4 14.40 5.40 -12 7 4 8.90 3.40 12 -7 -4 19.60 5.00 12 -7 -4 10.10 4.50 -12 6 4 3.90 3.00 12 -6 -4 -0.80 4.30 12 -6 -4 -4.40 4.10 -12 5 4 315.27 20.10 12 -5 -4 315.37 23.40 12 -5 -4 299.37 21.00 12 -4 -4 -4.50 4.60 12 -4 -4 -2.60 8.30 -12 3 4 1250.87 60.59 12 -3 -4 1253.57 64.09 -12 2 4 13.00 4.40 12 -1 -4 103.19 17.10 12 0 -4 16.40 9.80 12 1 -4 103.59 18.00 12 2 -4 9.60 9.90 -12 -3 4 1227.68 69.69 12 3 -4 1206.28 72.79 12 3 -4 1150.78 67.59 -12 -4 4 9.20 17.10 12 4 -4 -12.70 13.60 12 5 -4 149.88 20.40 12 6 -4 -16.70 22.30 -12 -8 4 9.10 4.20 -12 -9 4 21.20 4.40 -12 -10 4 1.50 4.10 -12 -11 4 290.97 17.60 13 -11 -4 12.60 3.10 13 -10 -4 18.20 3.70 13 -10 -4 22.60 4.40 -13 9 4 -3.20 2.50 13 -9 -4 -0.40 3.50 13 -9 -4 -1.30 2.90 -13 8 4 1.90 2.60 13 -8 -4 1.40 3.90 13 -8 -4 12.70 4.50 -13 7 4 5.90 3.40 13 -7 -4 5.40 4.00 13 -7 -4 6.90 4.60 -13 6 4 -0.60 3.00 13 -6 -4 1.20 4.30 13 -6 -4 -3.20 4.00 -13 5 4 33.10 5.70 13 -5 -4 36.10 7.00 13 -5 -4 36.80 6.80 13 -4 -4 2.90 5.30 13 -4 -4 6.50 5.30 -13 3 4 -4.30 3.50 13 -3 -4 -6.60 4.70 -13 2 4 8.30 4.70 13 -2 -4 8.10 6.30 13 -1 -4 7.30 5.20 13 0 -4 154.48 16.20 13 0 -4 167.08 23.10 13 1 -4 6.40 10.90 13 1 -4 4.50 4.90 13 2 -4 0.40 12.40 13 2 -4 -2.70 4.70 13 3 -4 0.90 5.00 13 3 -4 -2.20 14.00 13 4 -4 9.30 7.00 13 4 -4 9.10 17.40 13 5 -4 2.50 6.10 13 5 -4 5.90 22.60 -13 -8 4 4.70 4.30 -13 -10 4 19.60 4.00 14 -10 -4 0.10 2.40 14 -10 -4 -1.00 2.60 -14 9 4 13.90 5.50 14 -9 -4 8.10 3.50 14 -9 -4 12.90 5.60 -14 8 4 143.09 12.00 14 -8 -4 153.08 13.40 14 -8 -4 133.39 13.50 -14 7 4 80.29 9.60 14 -7 -4 79.49 12.90 -14 6 4 29.40 5.40 14 -6 -4 23.10 6.20 14 -6 -4 28.00 5.90 14 -5 -4 290.67 22.30 14 -5 -4 288.67 19.90 -14 4 4 29.30 5.50 14 -4 -4 30.20 7.00 -14 3 4 697.23 36.50 14 -3 -4 673.83 39.80 14 -2 -4 43.90 8.50 14 -1 -4 42.20 7.60 14 0 -4 286.57 22.00 14 1 -4 47.40 8.40 14 1 -4 11.80 13.10 14 2 -4 15.30 16.00 14 2 -4 33.60 6.90 14 3 -4 614.54 37.50 14 4 -4 12.60 21.10 14 4 -4 17.80 6.90 14 5 -4 56.99 9.80 14 6 -4 -5.40 7.80 -14 -8 4 135.99 13.30 15 -10 -4 4.50 2.30 -15 9 4 6.50 2.80 15 -9 -4 6.60 3.40 15 -9 -4 1.60 2.60 -15 8 4 3.50 2.60 15 -8 -4 -4.20 3.90 15 -8 -4 2.00 3.00 15 -7 -4 5.20 4.20 15 -7 -4 1.80 3.80 -15 6 4 19.90 4.40 15 -6 -4 16.60 5.20 -15 5 4 -0.50 2.80 15 -5 -4 -3.50 3.90 15 -5 -4 -3.90 4.30 -15 4 4 -2.60 2.80 15 -4 -4 -4.80 4.00 -15 3 4 6.60 4.10 -15 2 4 20.40 5.10 15 -2 -4 11.90 5.70 15 -1 -4 52.29 8.20 15 0 -4 3.00 4.60 15 1 -4 77.49 13.70 15 2 -4 -19.00 17.00 15 2 -4 12.00 5.50 15 3 -4 -0.20 21.30 15 4 -4 -1.60 5.10 15 5 -4 3.90 5.50 15 6 -4 171.48 24.30 16 -9 -4 61.09 7.10 16 -8 -4 154.58 12.50 -16 7 4 22.90 4.20 -16 6 4 142.39 14.40 16 -6 -4 128.89 14.00 -16 5 4 230.48 16.50 16 -5 -4 212.38 18.70 -16 4 4 -1.70 2.80 16 -4 -4 3.20 4.60 -16 3 4 263.37 18.20 16 -3 -4 242.08 20.20 -16 2 4 82.09 13.90 16 -2 -4 92.39 13.80 16 -1 -4 135.39 15.50 16 0 -4 653.53 39.30 16 1 -4 107.19 14.80 16 2 -4 81.79 13.50 16 3 -4 204.68 20.30 16 4 -4 -4.60 4.80 16 5 -4 14.60 5.30 -17 8 4 0.80 2.20 17 -8 -4 1.60 2.60 -17 7 4 3.20 2.70 17 -7 -4 5.30 4.80 -17 6 4 -2.20 2.30 17 -6 -4 4.50 3.40 -17 5 4 20.00 4.20 17 -5 -4 13.00 4.70 -17 4 4 -1.70 2.50 17 -4 -4 3.00 6.30 -17 3 4 -3.50 2.90 17 -3 -4 -0.80 3.90 -17 2 4 14.00 4.40 17 -2 -4 1.00 4.20 17 -1 -4 35.70 7.20 17 0 -4 11.40 5.20 17 1 -4 35.10 7.30 17 2 -4 -3.20 4.10 17 3 -4 -6.80 4.40 17 5 -4 -7.30 4.10 18 -8 -4 163.18 10.70 -18 7 4 16.80 3.50 18 -7 -4 15.80 3.70 -18 6 4 172.98 12.30 18 -6 -4 125.69 14.40 -18 5 4 213.78 15.10 18 -5 -4 200.38 15.80 -18 4 4 10.20 3.50 18 -4 -4 10.20 4.60 -18 3 4 117.99 10.50 18 -3 -4 104.89 13.30 -18 2 4 28.50 6.50 18 -2 -4 25.70 7.30 18 -1 -4 45.90 8.60 18 0 -4 159.38 16.10 18 1 -4 35.30 7.60 18 2 -4 25.00 9.30 18 3 -4 70.39 13.20 18 4 -4 -0.20 4.20 18 5 -4 8.70 6.60 19 -7 -4 -3.00 1.90 -19 6 4 -0.80 2.50 19 -6 -4 0.30 2.60 -19 5 4 -0.70 2.50 19 -5 -4 -1.80 2.70 -19 4 4 1.40 2.80 19 -4 -4 0.10 3.20 19 -3 -4 -0.20 3.00 -19 2 4 -5.40 3.70 19 -2 -4 6.00 3.70 19 -1 -4 9.20 4.60 19 0 -4 20.70 5.80 19 1 -4 8.20 4.30 19 2 -4 0.00 4.60 19 3 -4 2.30 4.00 20 -6 -4 107.79 8.40 -20 5 4 14.30 3.10 -20 4 4 0.40 2.90 20 -4 -4 0.60 2.60 -20 3 4 -2.90 2.70 20 -3 -4 1.30 3.30 -20 2 4 193.58 18.40 20 -2 -4 251.87 17.10 20 -1 -4 0.70 3.20 20 0 -4 217.48 17.10 20 1 -4 2.40 3.70 20 2 -4 138.79 13.50 20 3 -4 -0.70 3.20 20 4 -4 4.30 4.60 21 -4 -4 1.70 2.80 21 -3 -4 2.50 2.70 21 -2 -4 5.70 3.00 21 -1 -4 15.80 4.10 21 0 -4 2.50 3.20 21 1 -4 12.90 3.70 21 2 -4 -0.50 2.60 22 -2 -4 168.78 11.80 22 -1 -4 0.00 3.20 22 0 -4 67.19 10.50 22 1 -4 -0.40 2.30 22 2 -4 -4.20 2.50 22 1 5 -6.00 3.10 22 0 5 -2.90 2.40 22 -1 5 1.30 2.50 22 -2 5 19.60 4.50 21 1 5 22.60 4.90 21 0 5 -2.10 3.10 21 -1 5 105.49 10.60 -21 1 -5 116.29 8.80 21 -2 5 3.10 3.00 -21 2 -5 2.80 4.40 -21 3 -5 16.80 3.40 21 -4 5 -3.50 2.30 20 1 5 62.89 9.50 20 0 5 -0.60 3.40 -20 0 -5 1.20 3.10 20 -1 5 28.40 7.00 20 -2 5 147.69 13.20 -20 2 -5 123.49 10.30 20 -3 5 0.10 2.60 -20 3 -5 -0.30 2.10 20 -4 5 243.58 15.20 -20 4 -5 221.18 14.40 20 -5 5 0.70 2.50 19 3 5 3.80 3.80 19 2 5 11.40 4.80 19 1 5 188.18 17.00 -19 -1 -5 180.68 13.30 19 0 5 4.50 4.10 19 -1 5 211.78 17.10 -19 1 -5 199.48 13.80 19 -2 5 17.70 4.80 -19 2 -5 17.80 3.60 19 -3 5 5.90 3.40 -19 3 -5 5.50 2.80 19 -4 5 -1.30 4.10 -19 4 -5 3.40 2.40 19 -5 5 -1.00 2.50 -19 5 -5 2.60 2.60 19 -6 5 64.29 7.50 -19 6 -5 70.29 8.80 18 4 5 19.90 5.80 18 3 5 -4.20 4.80 18 2 5 116.49 14.90 18 0 5 -2.80 4.50 -18 0 -5 1.10 3.90 -18 1 -5 73.59 8.60 18 -2 5 155.98 14.70 -18 2 -5 109.69 14.00 18 -3 5 -0.40 3.60 -18 3 -5 -0.80 2.40 18 -4 5 278.97 19.20 -18 4 -5 275.17 17.90 18 -5 5 6.40 3.20 -18 5 -5 3.90 2.50 18 -6 5 47.50 7.40 -18 6 -5 47.50 6.20 18 -7 5 45.40 6.60 -18 7 -5 44.80 5.90 17 5 5 13.60 8.80 17 4 5 9.40 8.40 17 3 5 -0.60 4.60 17 2 5 52.19 8.70 17 1 5 128.79 14.80 -17 -1 -5 108.09 11.00 17 0 5 0.10 4.00 -17 0 -5 -5.70 2.80 17 -1 5 145.09 15.40 -17 1 -5 134.29 11.80 17 -2 5 85.39 12.00 -17 2 -5 53.79 8.00 17 -3 5 6.30 4.30 -17 3 -5 4.20 3.10 17 -4 5 89.39 12.00 -17 4 -5 75.09 8.70 17 -5 5 0.10 3.30 -17 5 -5 1.70 2.30 17 -6 5 28.00 5.00 -17 6 -5 35.10 5.80 17 -7 5 150.68 11.20 -17 7 -5 137.19 11.10 17 -8 5 6.20 3.50 -16 -8 -5 15.00 5.10 -16 -7 -5 77.29 9.30 -16 -6 -5 30.20 5.90 16 5 5 -8.50 5.40 16 4 5 42.40 8.90 16 3 5 0.60 4.90 16 2 5 42.60 7.40 16 1 5 169.58 16.50 -16 -1 -5 149.99 14.80 16 0 5 0.40 3.90 -16 0 -5 2.50 3.30 16 -1 5 195.48 17.20 -16 1 -5 199.68 19.20 16 -2 5 78.79 12.30 -16 2 -5 58.19 8.40 16 -3 5 -1.00 3.80 -16 3 -5 -1.10 2.80 16 -4 5 186.28 16.80 -16 4 -5 197.78 14.80 16 -5 5 11.20 6.80 16 -5 5 1.40 4.80 -16 5 -5 3.60 2.90 16 -6 5 20.60 4.60 16 -6 5 9.80 4.80 -16 6 -5 23.30 7.70 16 -7 5 73.99 11.90 16 -7 5 95.09 10.00 -16 7 -5 93.29 8.70 16 -8 5 15.30 4.10 16 -8 5 19.70 3.70 -16 8 -5 16.60 3.30 -15 -9 -5 -0.90 3.10 -15 -8 -5 11.90 3.70 -15 -7 -5 211.98 14.90 15 5 5 -8.10 4.60 15 4 5 47.20 10.10 15 3 5 30.00 10.40 15 2 5 9.30 4.60 15 1 5 171.08 16.40 15 0 5 -4.40 3.60 -15 0 -5 1.20 3.20 15 -1 5 221.98 18.60 -15 1 -5 224.18 15.70 15 -2 5 11.10 4.70 -15 2 -5 9.60 3.40 -15 3 -5 35.80 6.00 15 -4 5 148.49 15.60 15 -4 5 171.98 16.10 -15 4 -5 186.18 14.10 15 -5 5 -0.50 3.80 15 -5 5 -3.50 4.90 -15 5 -5 4.40 2.80 -15 6 -5 24.60 4.40 15 -7 5 203.78 16.90 15 -7 5 206.98 15.90 -15 7 -5 205.98 14.90 15 -8 5 7.60 4.10 15 -8 5 8.00 3.90 -15 8 -5 8.20 2.60 15 -9 5 1.60 3.20 15 -9 5 -1.80 3.70 -14 -10 -5 34.80 5.60 -14 -9 -5 175.58 12.50 -14 -8 -5 -0.60 3.40 -14 -6 -5 26.50 5.40 14 5 5 -2.10 6.10 14 4 5 77.29 13.10 14 3 5 32.50 7.00 14 2 5 47.00 7.80 14 1 5 192.78 17.60 14 0 5 -1.70 3.80 14 -1 5 224.68 18.20 14 -2 5 41.00 6.80 -14 2 -5 56.19 7.60 14 -3 5 29.90 7.40 14 -3 5 40.40 7.10 -14 3 -5 49.50 7.70 14 -4 5 115.09 14.50 14 -4 5 102.29 13.40 -14 4 -5 113.89 11.20 14 -5 5 4.20 4.70 14 -5 5 -2.00 3.70 -14 5 -5 3.00 2.70 14 -6 5 28.40 6.10 14 -6 5 30.60 6.70 -14 6 -5 28.60 5.30 14 -7 5 157.18 15.50 -14 7 -5 159.08 12.70 14 -8 5 -1.10 2.80 14 -8 5 6.50 3.90 -14 8 -5 2.20 2.10 14 -9 5 186.28 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53.79 4 3 -9 3.80 7.00 4 4 -9 460.05 35.10 4 5 -9 111.59 18.70 -4 -6 9 161.38 13.30 4 6 -9 189.28 25.80 -4 -7 9 162.48 13.10 4 7 -9 151.68 14.20 4 7 -9 96.69 21.80 -4 -8 9 8.10 3.90 4 8 -9 -2.70 3.90 -4 -9 9 10.50 6.70 4 9 -9 13.20 4.50 -4 -10 9 59.99 9.20 4 10 -9 38.00 6.20 -4 -11 9 8.00 3.10 4 11 -9 6.20 3.00 -4 -12 9 153.98 15.90 -5 12 9 44.50 7.90 5 -12 -9 30.10 5.60 -5 11 9 -1.10 4.00 5 -11 -9 -0.60 3.90 -5 10 9 88.79 15.70 5 -10 -9 75.89 11.50 -5 9 9 224.08 20.70 5 -9 -9 226.08 18.70 -5 8 9 33.80 11.70 -5 8 9 11.70 7.90 -5 8 9 7.00 4.70 5 -8 -9 18.00 5.40 -5 7 9 208.68 24.60 -5 7 9 236.08 16.40 5 -7 -9 198.88 17.80 -5 6 9 0.40 3.10 -5 6 9 6.70 6.10 -5 5 9 282.97 23.20 -5 5 9 293.97 22.20 -5 4 9 1219.08 64.79 -5 3 9 4.40 4.50 -5 2 9 475.45 30.70 5 -2 -9 488.95 32.90 -5 1 9 1002.90 56.19 5 -1 -9 1122.59 58.59 -5 0 9 -2.20 4.10 5 0 -9 -2.20 4.70 -5 -1 9 1083.99 58.29 5 1 -9 1112.59 61.09 5 2 -9 506.45 34.90 5 3 -9 2.70 7.00 5 4 -9 1170.68 68.59 5 5 -9 285.77 29.80 5 6 -9 17.80 12.30 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11.70 4.00 15 -8 15 4.10 2.20 -14 -8 -15 1.80 2.60 -14 -7 -15 90.99 9.50 -14 -6 -15 15.30 3.90 -14 -5 -15 26.80 6.80 -14 -4 -15 8.90 3.50 -14 -3 -15 84.09 9.40 14 2 15 -9.60 4.80 -14 -2 -15 3.30 3.10 14 1 15 191.98 16.40 -14 -1 -15 204.08 15.20 14 0 15 -2.90 4.50 -14 0 -15 -0.40 2.50 14 -1 15 208.78 17.50 -14 1 -15 216.38 16.20 14 -2 15 5.10 4.30 -14 2 -15 5.70 3.10 14 -3 15 75.89 11.50 -14 3 -15 82.99 9.50 14 -4 15 14.50 5.40 -14 4 -15 8.90 3.40 14 -5 15 13.50 4.80 -14 5 -15 16.80 4.10 14 -6 15 16.00 4.90 -14 6 -15 18.30 3.50 14 -7 15 94.69 10.80 -14 7 -15 82.49 7.70 14 -8 15 1.70 2.80 -13 -9 -15 -0.70 2.00 -13 -8 -15 28.00 5.10 -13 -7 -15 12.50 4.10 -13 -6 -15 185.68 18.60 -13 -5 -15 3.30 2.90 -13 -4 -15 522.95 29.80 13 3 15 -8.10 4.70 -13 -3 -15 3.80 2.80 13 2 15 223.08 18.70 -13 -2 -15 272.67 22.70 13 1 15 -0.80 5.00 -13 -1 -15 4.20 3.30 13 0 15 0.40 6.40 -13 0 -15 3.80 3.50 13 -1 15 2.60 4.20 -13 1 -15 5.20 3.40 13 -2 15 247.28 19.70 -13 2 -15 231.48 18.70 13 -3 15 1.50 4.40 -13 3 -15 5.30 3.10 13 -4 15 503.75 32.10 -13 4 -15 490.85 28.50 13 -5 15 3.50 4.70 -13 5 -15 3.30 2.70 13 -6 15 152.18 15.90 -13 6 -15 173.58 13.20 13 -7 15 8.20 3.90 -13 7 -15 5.70 2.80 13 -8 15 26.10 6.30 13 -9 15 1.20 2.50 -12 -9 -15 120.69 10.30 -12 -8 -15 2.90 2.90 -12 -7 -15 108.69 11.00 -12 -6 -15 -0.70 2.70 12 4 15 -4.90 4.90 -12 -4 -15 3.70 3.30 -12 -3 -15 30.10 5.40 12 2 15 34.00 7.20 -12 -2 -15 28.00 5.20 12 1 15 134.59 14.80 -12 -1 -15 124.09 11.70 12 0 15 0.90 4.30 -12 0 -15 0.90 3.00 12 -1 15 131.99 14.90 -12 1 -15 131.89 12.40 12 -2 15 30.70 6.80 -12 2 -15 26.30 5.20 12 -3 15 26.00 8.90 12 -4 15 2.90 5.30 12 -5 15 222.28 20.40 -12 5 -15 208.08 15.40 12 -6 15 0.70 4.40 -12 6 -15 -0.10 2.30 12 -7 15 90.39 12.80 -12 7 -15 94.49 8.50 12 -8 15 1.00 3.20 12 -9 15 103.99 10.60 12 -10 15 0.10 2.10 -11 -10 -15 67.29 7.50 -11 -9 -15 1.90 2.90 -11 -8 -15 9.90 4.00 11 7 15 6.10 3.60 -11 -7 -15 1.40 3.30 11 6 15 108.69 12.40 -11 -6 -15 113.79 11.70 11 5 15 5.10 5.00 -11 -5 -15 2.90 3.30 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-15 165.88 13.10 10 -6 15 44.00 8.30 -10 6 -15 32.50 5.40 -10 6 -15 22.10 8.20 10 -8 15 5.10 4.70 10 -9 15 109.69 13.20 -10 9 -15 125.09 12.90 10 -10 15 3.00 3.10 -10 10 -15 -1.40 3.20 -9 -10 -15 118.79 11.10 9 9 15 2.40 3.30 -9 -9 -15 13.90 4.20 9 8 15 17.30 4.90 -9 -8 -15 15.20 4.50 9 7 15 17.40 5.70 -9 -7 -15 28.40 5.90 9 6 15 154.58 16.20 9 5 15 18.10 7.00 -9 -5 -15 26.00 5.00 9 4 15 162.38 18.60 -9 -4 -15 189.98 14.10 9 3 15 18.20 8.70 -9 -3 -15 20.00 4.10 9 2 15 434.76 29.50 -9 -2 -15 412.86 24.80 9 1 15 41.90 7.70 -9 -1 -15 37.40 6.30 9 0 15 -3.00 5.40 -9 0 -15 -1.40 2.40 9 -1 15 23.10 6.70 -9 1 -15 31.30 5.20 9 -2 15 385.16 27.50 9 -3 15 24.60 7.80 9 -4 15 159.48 18.90 9 -5 15 26.40 6.90 -9 5 -15 29.40 5.20 -9 5 -15 27.20 9.50 9 -6 15 152.18 16.70 -9 6 -15 110.09 17.30 9 -7 15 31.30 8.20 -9 7 -15 22.20 7.10 9 -8 15 18.20 6.80 -9 8 -15 15.40 6.10 9 -9 15 6.10 4.00 -9 9 -15 1.10 3.90 9 -10 15 76.09 10.00 -9 10 -15 110.19 11.20 9 -11 15 -2.10 2.40 -9 11 -15 4.90 2.20 -8 -11 -15 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20.30 -8 -5 -21 186.48 15.20 8 4 21 80.99 14.20 -8 -4 -21 71.29 9.40 8 3 21 9.30 5.10 -8 -2 -21 4.40 3.40 8 1 21 615.44 38.20 -8 -1 -21 631.24 34.40 8 0 21 -3.00 3.90 -8 0 -21 1.70 2.90 8 -1 21 551.44 35.70 -8 1 -21 568.84 31.30 -8 2 -21 12.20 6.80 -8 2 -21 0.30 3.00 8 -3 21 12.50 5.80 -8 3 -21 4.70 6.00 8 -4 21 47.30 8.90 -8 4 -21 64.59 10.40 8 -5 21 188.68 19.30 -8 5 -21 202.98 18.80 8 -6 21 113.09 19.30 -8 6 -21 104.29 13.30 8 -7 21 213.58 18.40 -8 7 -21 202.88 16.90 8 -8 21 -5.30 5.10 -8 8 -21 -3.90 2.60 8 -9 21 138.89 12.20 -8 9 -21 133.19 11.00 7 9 21 25.90 4.30 -7 -9 -21 15.60 4.40 -7 -8 -21 3.20 2.90 7 7 21 -0.50 4.70 -7 -7 -21 2.70 3.10 7 6 21 39.00 8.30 -7 -6 -21 29.40 5.30 7 5 21 34.50 8.20 -7 -5 -21 58.69 8.70 7 4 21 176.28 19.10 -7 -4 -21 174.18 15.70 -7 -3 -21 62.99 8.60 7 2 21 84.89 14.10 -7 -2 -21 92.29 9.90 7 1 21 9.70 5.00 -7 -1 -21 9.50 3.60 7 0 21 -0.50 4.00 -7 0 -21 -1.60 2.80 -7 0 -21 -2.60 8.60 7 -1 21 4.50 4.40 -7 1 -21 2.10 6.20 -7 1 -21 8.90 3.30 7 -2 21 95.49 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6.00 4.60 5 -7 21 53.19 9.60 5 -8 21 39.80 7.70 -5 8 -21 42.40 7.30 5 -9 21 70.49 10.70 -5 9 -21 81.19 12.80 5 -10 21 136.19 14.00 -5 10 -21 100.29 9.20 4 10 21 66.59 8.10 4 9 21 97.79 11.40 4 8 21 1.90 4.50 -4 -8 -21 -2.70 3.60 4 7 21 232.88 22.30 -4 -7 -21 214.28 15.40 -4 -7 -21 199.58 31.00 4 6 21 88.39 15.30 -4 -6 -21 70.79 13.00 -4 -6 -21 72.59 9.50 4 5 21 18.30 7.70 -4 -5 -21 9.60 4.30 4 4 21 387.56 29.20 -4 -4 -21 334.07 28.60 -4 -4 -21 383.56 23.20 4 3 21 3.20 16.20 4 3 21 20.90 7.40 -4 -3 -21 20.70 8.70 -4 -3 -21 26.20 4.90 4 2 21 126.19 16.80 -4 -2 -21 107.49 10.70 4 1 21 128.19 21.60 -4 -1 -21 149.69 17.00 -4 0 -21 -8.30 4.70 -4 0 -21 0.80 3.20 -4 1 -21 91.59 10.00 4 -3 21 36.90 8.70 -4 3 -21 22.60 7.40 -4 3 -21 9.10 24.80 4 -4 21 376.46 30.00 -4 4 -21 409.96 45.00 -4 4 -21 355.66 26.20 4 -5 21 20.80 9.20 4 -5 21 -1.60 3.80 -4 5 -21 6.10 25.10 -4 5 -21 19.30 6.60 4 -6 21 74.09 12.60 -4 6 -21 57.59 9.60 4 -7 21 279.67 30.50 -4 7 -21 237.38 19.80 4 -8 21 -4.00 4.60 -4 8 -21 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6.00 3.40 3 -6 21 5.20 6.40 -3 6 -21 10.30 5.50 3 -8 21 19.00 6.80 -3 8 -21 24.20 5.50 3 -9 21 40.60 8.60 -3 9 -21 50.79 7.80 -3 10 -21 11.40 3.00 2 10 21 148.59 12.70 -2 -10 -21 157.08 14.90 2 9 21 3.20 4.30 -2 -9 -21 -4.90 4.90 2 8 21 20.00 6.80 -2 -8 -21 19.40 6.80 2 7 21 95.09 16.00 -2 -7 -21 50.09 10.70 2 6 21 58.89 11.60 -2 -6 -21 61.99 11.60 2 5 21 12.10 8.00 -2 -5 -21 -1.40 3.70 -2 -5 -21 1.10 6.90 2 4 21 488.95 34.40 -2 -4 -21 465.25 33.40 2 3 21 50.89 13.50 2 3 21 70.79 11.70 -2 -3 -21 63.09 10.70 2 1 21 59.49 8.70 2 1 21 59.29 13.60 2 1 21 66.79 11.70 -2 -1 -21 56.19 9.10 2 0 21 -0.50 3.20 2 0 21 -4.70 8.60 -2 0 -21 2.20 4.30 2 -1 21 62.99 8.40 -2 1 -21 71.89 11.50 2 -2 21 333.57 27.50 -2 2 -21 305.57 36.80 2 -3 21 57.29 7.70 -2 3 -21 44.90 9.10 2 -4 21 481.35 26.80 2 -4 21 460.95 35.20 -2 4 -21 496.05 31.20 2 -5 21 4.10 8.30 2 -5 21 13.40 3.70 -2 5 -21 15.50 5.90 2 -6 21 65.19 8.60 -2 6 -21 71.49 11.10 2 -7 21 71.99 8.10 -2 7 -21 79.49 11.30 2 -8 21 14.70 3.40 -2 8 -21 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3.80 1 -7 21 378.76 22.10 -1 7 -21 382.76 25.40 1 -8 21 6.70 2.90 -1 8 -21 11.40 4.20 1 -9 21 52.09 8.50 -1 9 -21 51.39 7.70 -1 10 -21 0.80 2.00 0 11 21 -3.90 2.20 0 10 21 259.67 17.30 0 -10 -21 202.88 21.90 0 9 21 -2.30 3.70 0 -9 -21 -9.30 4.60 0 8 21 6.90 5.30 0 -8 -21 0.60 5.20 0 7 21 -3.20 6.20 0 -7 -21 -6.00 5.70 0 6 21 291.07 25.30 0 -6 -21 231.08 23.10 0 -5 -21 -7.80 5.60 0 4 21 416.26 32.90 0 -4 -21 412.16 29.80 0 3 21 1.30 5.90 0 3 21 0.50 8.50 0 -3 -21 -4.30 4.50 0 2 21 506.45 28.20 0 -2 -21 522.65 32.40 0 1 21 -7.40 7.20 0 1 21 -0.80 2.80 0 -1 -21 9.50 5.00 0 0 21 -3.00 2.50 0 0 21 2.80 7.50 0 0 -21 -1.60 4.10 0 -1 21 2.40 2.60 0 -1 21 2.10 7.20 0 1 -21 -6.30 3.30 0 1 -21 2.50 14.20 0 -2 21 566.54 43.80 0 -2 21 544.65 29.50 0 2 -21 516.85 44.50 0 -3 21 -1.80 2.40 0 -3 21 7.70 10.10 0 3 -21 0.70 4.20 0 3 -21 -15.00 17.30 0 -4 21 378.66 44.10 0 -4 21 402.16 23.80 0 4 -21 396.06 27.00 0 4 -21 441.56 49.90 0 -5 21 -2.70 2.70 0 5 -21 -15.70 26.90 0 5 -21 0.40 4.00 0 -6 21 246.18 16.60 0 6 -21 227.98 18.90 0 -7 21 3.80 2.90 0 7 -21 0.60 3.60 0 -8 21 4.60 3.80 0 8 -21 5.30 3.60 0 -9 21 -1.00 2.30 0 9 -21 -3.20 2.00 0 10 -21 253.07 15.00 -1 10 21 2.40 3.30 1 -10 -21 -5.90 3.80 -1 9 21 45.80 7.80 1 -9 -21 38.70 7.40 1 -8 -21 8.80 5.40 -1 7 21 422.16 31.60 1 -7 -21 395.86 29.70 -1 6 21 3.10 6.60 1 -6 -21 -7.90 5.30 -1 5 21 5.10 17.90 -1 5 21 13.20 8.10 -1 5 21 0.60 5.70 1 -5 -21 -3.70 5.20 -1 4 21 -1.70 15.30 -1 4 21 13.10 8.40 -1 4 21 -3.40 3.40 1 -4 -21 2.60 5.70 -1 3 21 4.40 3.40 -1 3 21 3.50 8.80 1 -3 -21 -3.70 5.20 -1 2 21 7.40 10.30 1 -2 -21 9.50 7.60 -1 1 21 380.96 22.10 -1 1 21 376.16 30.70 1 -1 -21 359.26 24.80 -1 0 21 1.10 7.10 -1 0 21 -1.70 2.40 1 0 -21 0.60 3.90 -1 -1 21 437.06 26.50 -1 -1 21 350.36 30.20 1 1 -21 389.86 34.50 1 1 -21 334.37 23.80 -1 -2 21 3.60 3.10 1 2 -21 7.40 14.60 -1 -3 21 4.00 2.90 -1 -3 21 -15.70 9.10 1 3 -21 -21.10 15.00 1 3 -21 -2.90 3.90 -1 -4 21 -0.10 2.90 1 4 -21 -2.40 4.10 -1 -5 21 3.40 3.30 1 5 -21 3.30 4.30 -1 -6 21 0.20 3.10 1 6 -21 5.80 4.10 -1 -7 21 397.16 23.90 1 7 -21 408.56 25.80 -1 -8 21 16.20 4.20 1 8 -21 14.00 4.50 -1 -9 21 55.19 6.90 1 9 -21 61.79 7.60 -1 -10 21 0.10 2.90 1 10 -21 -0.80 1.80 -2 10 21 135.39 12.30 2 -10 -21 145.29 12.90 -2 9 21 -1.40 4.20 2 -9 -21 -3.10 3.20 2 -8 -21 14.10 6.30 -2 7 21 49.30 10.30 2 -7 -21 54.29 9.50 -2 6 21 57.09 11.50 2 -6 -21 65.19 10.70 -2 5 21 2.30 4.20 -2 5 21 -0.30 12.70 -2 5 21 4.30 8.80 2 -5 -21 7.60 5.10 -2 4 21 451.25 38.30 -2 4 21 521.05 28.80 -2 4 21 495.55 40.10 2 -4 -21 504.55 32.70 -2 3 21 45.60 12.00 -2 3 21 53.29 8.30 -2 3 21 39.80 12.00 2 -3 -21 61.09 9.80 -2 2 21 316.87 28.90 -2 2 21 335.87 20.40 2 -2 -21 349.67 31.60 2 -1 -21 90.09 12.30 -2 0 21 1.60 8.70 2 0 -21 0.10 3.80 2 0 -21 -2.50 13.70 -2 -1 21 72.89 11.30 2 1 -21 75.29 11.40 2 1 -21 78.69 19.00 -2 -2 21 344.57 30.80 -2 -2 21 348.37 20.80 2 2 -21 337.57 25.40 2 2 -21 342.17 34.60 -2 -3 21 69.99 17.40 -2 -3 21 67.29 8.30 2 3 -21 33.30 19.10 2 3 -21 48.40 7.70 -2 -4 21 515.15 28.50 -2 -4 21 463.95 41.90 2 4 -21 456.15 48.00 2 4 -21 499.45 30.10 -2 -5 21 14.50 4.40 -2 -5 21 -2.10 17.40 2 5 -21 6.50 4.70 2 5 -21 46.70 28.70 -2 -6 21 73.19 9.60 2 6 -21 71.29 11.20 -2 -7 21 89.79 9.70 2 7 -21 79.69 10.80 -2 -8 21 22.00 5.10 2 8 -21 17.40 4.40 -2 -9 21 1.00 2.40 2 9 -21 4.80 2.40 -2 -10 21 132.89 9.70 2 10 -21 152.78 9.90 -3 10 21 13.00 3.90 3 -10 -21 10.50 3.90 3 -9 -21 49.00 8.80 -3 8 21 22.70 7.50 3 -8 -21 25.80 6.70 -3 7 21 136.69 19.40 3 -7 -21 117.19 15.30 -3 6 21 -2.20 4.40 -3 6 21 -0.20 7.40 -3 5 21 14.60 11.90 -3 5 21 47.50 10.30 -3 5 21 21.70 5.40 -3 4 21 45.00 13.80 -3 4 21 34.30 11.60 -3 4 21 26.00 5.50 3 -4 -21 30.90 6.70 -3 3 21 5.30 3.40 -3 3 21 5.80 9.60 3 -3 -21 1.30 4.90 -3 2 21 14.70 4.00 -3 2 21 5.70 8.10 3 -2 -21 14.20 5.40 -3 1 21 326.67 28.70 -3 1 21 327.77 19.90 -3 0 21 -0.10 8.70 -3 0 21 2.10 2.60 3 0 -21 -14.60 15.10 3 0 -21 0.80 5.20 -3 -1 21 319.07 19.30 -3 -1 21 312.27 28.10 3 1 -21 334.67 33.70 -3 -2 21 10.10 3.80 -3 -2 21 12.60 9.30 3 2 -21 7.40 4.70 -3 -3 21 12.20 11.30 -3 -3 21 7.90 3.70 3 3 -21 21.90 16.40 3 3 -21 2.60 4.00 -3 -4 21 15.30 15.90 -3 -4 21 27.00 5.30 3 4 -21 31.60 5.90 3 4 -21 17.50 18.50 -3 -5 21 25.90 5.50 -3 -5 21 17.80 15.50 3 5 -21 22.20 20.40 -3 -6 21 17.30 4.70 3 6 -21 8.90 4.20 -3 -7 21 115.19 10.80 3 7 -21 117.89 11.70 3 8 -21 26.60 5.00 3 9 -21 33.60 6.10 -3 -10 21 9.60 2.50 -4 10 21 68.59 10.70 4 -10 -21 64.29 8.40 -4 9 21 87.19 11.60 4 -9 -21 97.39 10.60 -4 8 21 1.60 5.00 4 -8 -21 4.90 4.30 4 -7 -21 236.18 20.20 -4 6 21 74.49 13.30 -4 6 21 74.09 10.50 4 -6 -21 70.69 10.90 -4 5 21 6.00 4.10 -4 5 21 11.00 17.50 -4 4 21 373.86 36.30 -4 4 21 404.06 24.50 4 -4 -21 400.56 27.30 -4 3 21 36.70 18.90 -4 3 21 31.80 5.60 4 -3 -21 36.40 8.00 -4 2 21 124.89 11.30 -4 2 21 118.19 19.20 4 -2 -21 120.99 14.50 -4 1 21 200.58 13.80 -4 1 21 173.68 21.80 4 -1 -21 168.48 16.50 -4 0 21 -1.60 2.40 -4 0 21 1.40 7.60 4 0 -21 -24.10 14.20 4 0 -21 -1.30 3.70 -4 -1 21 174.28 21.80 -4 -1 21 196.78 13.40 4 1 -21 174.98 28.10 4 1 -21 178.58 15.20 -4 -2 21 120.99 10.90 -4 -2 21 98.39 19.70 4 2 -21 133.49 12.90 4 2 -21 101.79 22.40 -4 -3 21 34.90 6.00 4 3 -21 33.70 6.30 4 3 -21 19.30 19.10 -4 -4 21 352.06 37.70 -4 -4 21 407.46 24.10 4 4 -21 391.36 24.20 4 4 -21 356.96 40.90 -4 -5 21 3.80 18.10 -4 -5 21 14.40 4.50 4 5 -21 13.70 22.30 4 5 -21 14.00 4.40 -4 -6 21 79.69 9.60 4 6 -21 75.29 10.30 -4 -7 21 239.08 17.10 4 7 -21 261.27 17.80 -4 -8 21 7.60 3.20 4 8 -21 2.30 2.80 -4 -9 21 92.99 8.90 4 9 -21 108.09 8.50 -4 -10 21 56.99 6.00 -5 10 21 78.39 11.60 5 -10 -21 110.49 9.70 -5 9 21 89.79 12.20 5 -9 -21 114.09 15.00 -5 8 21 34.40 7.60 5 -8 -21 33.50 6.40 5 -7 -21 55.79 11.60 -5 6 21 8.30 9.30 -5 6 21 4.80 4.00 5 -6 -21 6.80 5.40 -5 5 21 32.00 7.50 5 -5 -21 37.70 7.50 -5 4 21 289.17 19.40 -5 4 21 273.17 33.20 5 -4 -21 265.97 21.50 -5 3 21 55.99 8.30 -5 3 21 33.50 12.10 5 -3 -21 30.50 6.90 -5 2 21 4.30 3.40 5 -2 -21 6.00 5.10 -5 1 21 221.48 15.00 -5 1 21 199.48 24.00 5 -1 -21 148.79 26.50 5 -1 -21 233.88 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-8 4 -23 24.30 8.50 8 -5 23 2.10 4.00 -8 5 -23 10.80 4.90 8 -6 23 4.20 4.40 -8 6 -23 2.60 3.60 8 -7 23 78.39 12.70 -8 7 -23 68.09 10.20 8 -8 23 -1.50 2.80 -8 8 -23 3.90 2.70 8 -9 23 50.39 7.30 -8 9 -23 49.50 8.50 7 9 23 67.49 8.30 -7 -8 -23 -4.40 5.20 7 7 23 22.40 5.20 -7 -7 -23 14.10 3.90 7 6 23 86.29 12.70 -7 -6 -23 72.19 8.30 7 5 23 48.40 8.60 -7 -5 -23 57.49 7.80 7 4 23 187.38 19.40 -7 -4 -23 200.28 15.30 7 3 23 152.38 16.80 -7 -3 -23 132.69 12.40 7 2 23 107.59 14.50 -7 -2 -23 97.19 11.00 7 1 23 89.49 13.70 -7 -1 -23 81.19 16.00 -7 -1 -23 115.99 16.20 7 0 23 2.40 4.20 -7 0 -23 0.30 3.20 7 -1 23 74.59 13.40 -7 1 -23 86.59 14.90 -7 1 -23 80.79 13.10 7 -2 23 103.89 14.60 -7 2 -23 102.29 14.10 7 -3 23 161.98 17.50 -7 3 -23 159.38 16.30 7 -4 23 187.28 19.70 -7 4 -23 201.78 18.50 7 -5 23 42.80 11.00 -7 5 -23 32.50 10.00 7 -6 23 75.89 12.40 -7 6 -23 90.79 11.60 7 -7 23 21.80 5.40 -7 7 -23 22.80 4.90 7 -8 23 -0.50 3.40 -7 8 -23 5.10 2.80 7 -9 23 68.19 9.00 -7 9 -23 80.09 9.50 6 9 23 81.69 8.00 -6 -8 -23 1.40 5.20 6 7 23 16.10 5.60 -6 -7 -23 9.10 3.60 6 6 23 3.30 4.90 -6 -6 -23 7.20 5.80 6 5 23 93.19 15.10 -6 -5 -23 94.39 9.90 6 4 23 223.58 20.90 -6 -4 -23 218.88 16.40 6 3 23 29.50 7.40 -6 -3 -23 29.90 5.80 -6 -3 -23 36.00 9.70 6 2 23 160.08 17.60 -6 -2 -23 178.28 14.10 6 1 23 34.80 10.40 -6 -1 -23 40.00 6.50 6 0 23 -4.00 4.80 -6 0 -23 -0.70 3.10 -6 0 -23 5.80 5.30 6 -1 23 53.09 15.10 -6 1 -23 28.60 5.50 -6 1 -23 36.10 7.60 6 -3 23 33.70 8.20 -6 3 -23 27.00 6.30 6 -4 23 229.48 21.60 -6 4 -23 214.28 19.30 6 -5 23 92.49 14.10 -6 5 -23 83.09 12.00 6 -6 23 -1.10 4.30 -6 6 -23 5.90 4.10 6 -7 23 14.40 4.90 -6 7 -23 13.80 4.10 6 -8 23 0.10 3.50 -6 8 -23 0.60 2.70 6 -9 23 69.49 9.00 -6 9 -23 79.69 7.80 5 9 23 150.68 11.80 5 7 23 246.18 20.60 5 6 23 26.50 9.20 -5 -6 -23 13.60 3.90 5 5 23 118.29 16.10 -5 -5 -23 99.19 10.30 5 4 23 112.89 15.00 -5 -4 -23 84.69 12.70 -5 -4 -23 87.49 10.50 5 3 23 116.19 14.70 -5 -3 -23 120.19 19.10 -5 -3 -23 86.19 10.70 5 2 23 7.10 6.10 -5 -2 -23 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23 17.90 4.80 -2 -9 -23 18.70 6.70 2 8 23 6.70 3.70 -2 -8 -23 9.50 5.80 2 7 23 11.30 5.50 -2 -7 -23 -0.90 6.00 2 6 23 163.88 19.20 -2 -6 -23 177.78 19.60 -2 -5 -23 8.10 5.90 2 4 23 234.38 39.00 2 4 23 244.88 23.40 -2 -4 -23 245.88 29.60 2 3 23 -13.10 12.70 2 3 23 -4.70 5.80 -2 -3 -23 -1.70 5.10 2 2 23 227.78 22.30 -2 -2 -23 260.37 20.70 2 1 23 -1.10 4.20 2 1 23 -0.40 5.40 2 1 23 -5.40 11.90 -2 -1 -23 -3.90 4.40 2 0 23 -6.80 11.80 2 0 23 -6.00 3.30 -2 0 -23 -0.90 4.20 2 -1 23 3.20 12.60 2 -1 23 -0.10 3.50 2 -1 23 3.80 6.20 -2 1 -23 -5.30 3.90 2 -2 23 205.38 23.70 2 -2 23 264.27 16.80 -2 2 -23 257.47 19.90 2 -3 23 3.60 6.80 2 -3 23 -4.00 2.90 -2 3 -23 0.40 3.80 2 -4 23 210.78 14.80 -2 4 -23 207.18 48.30 -2 4 -23 227.18 19.20 2 -5 23 -4.80 6.40 2 -5 23 4.60 3.20 -2 5 -23 10.00 4.70 2 -6 23 178.68 29.60 2 -6 23 137.29 11.10 -2 6 -23 158.68 14.80 2 -7 23 7.20 6.40 -2 7 -23 1.00 3.20 -2 8 -23 10.30 3.30 -2 9 -23 17.60 3.60 -2 10 -23 14.00 3.90 1 10 23 3.30 2.80 -1 -10 -23 0.90 5.50 1 9 23 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4.20 8 -1 -27 97.39 10.00 -8 0 27 -0.10 3.70 8 0 -27 0.00 3.10 -8 -1 27 103.59 12.80 8 1 -27 98.09 9.00 -8 -2 27 14.40 3.70 8 2 -27 0.50 2.70 -8 -3 27 3.80 2.70 -8 -4 27 2.60 2.50 -8 -5 27 8.60 2.80 -8 -6 27 59.99 6.20 -8 -7 27 32.50 4.30 -9 5 27 -2.80 2.70 9 -5 -27 2.20 2.20 -9 4 27 168.58 12.00 9 -4 -27 166.88 11.50 -9 3 27 4.80 2.50 9 -3 -27 5.00 3.40 -9 2 27 262.37 16.40 9 -2 -27 246.38 15.20 -9 1 27 58.79 7.40 9 -1 -27 48.90 6.50 -9 0 27 3.00 2.70 -9 -1 27 68.49 7.70 -9 -2 27 297.57 18.20 -9 -3 27 7.20 3.00 -9 -4 27 207.48 13.50 -9 -5 27 1.70 2.20 -9 -6 27 122.19 8.50 -10 5 27 23.60 4.70 -10 4 27 15.20 3.40 10 -4 -27 17.50 3.50 -10 3 27 4.20 2.60 10 -3 -27 3.70 2.40 -10 2 27 9.50 3.30 -10 1 27 94.39 8.80 -10 0 27 -3.50 2.30 -10 -1 27 107.49 9.30 -10 -2 27 9.30 3.20 -10 -3 27 8.60 3.00 -10 -4 27 16.50 3.40 -10 -5 27 26.80 5.50 -10 -6 27 2.50 2.00 -11 4 27 131.99 12.00 -11 3 27 2.50 2.40 -11 2 27 195.18 13.30 -11 1 27 5.10 2.60 -11 0 27 -0.80 2.30 -11 -1 27 1.40 2.60 -11 -2 27 215.38 14.20 -11 -3 27 2.80 2.60 -12 4 27 -3.60 2.10 -12 3 27 62.89 9.10 -12 2 27 2.00 2.50 -12 1 27 74.39 7.60 -12 0 27 -0.40 2.40 -12 -1 27 73.59 7.50 -12 -2 27 0.40 2.50 -12 -3 27 56.89 6.00 -12 -4 27 1.90 2.20 -13 3 27 7.50 2.40 -13 2 27 169.08 11.00 -13 1 27 10.10 2.60 -13 0 27 -2.40 2.40 -13 -1 27 9.20 2.60 -13 -2 27 188.58 14.80 -14 0 27 -0.90 2.70 13 0 28 13.80 3.20 13 -1 28 1.30 2.40 13 -2 28 7.00 2.90 12 2 28 2.10 4.80 12 1 28 0.00 2.40 12 0 28 7.00 3.20 12 -1 28 1.00 2.90 12 -2 28 -0.80 2.50 12 -3 28 401.06 25.50 11 4 28 2.70 2.80 11 3 28 2.90 2.60 11 2 28 15.70 3.70 11 1 28 18.00 4.30 11 0 28 9.40 3.70 11 -1 28 10.10 3.60 11 -2 28 12.60 3.70 11 -3 28 2.20 2.90 11 -4 28 4.40 2.70 10 5 28 154.18 10.10 10 4 28 0.70 2.60 10 3 28 396.86 23.30 10 2 28 2.30 3.90 10 1 28 8.10 4.00 10 0 28 62.09 9.00 10 -1 28 0.00 3.00 10 -2 28 3.40 4.60 10 -3 28 392.26 23.80 10 -4 28 5.90 3.30 -10 4 -28 9.90 4.60 10 -5 28 160.38 13.30 9 5 28 2.20 2.70 9 4 28 -0.30 2.90 9 3 28 9.10 5.40 9 2 28 9.40 4.10 9 1 28 6.20 3.50 9 0 28 19.50 5.50 9 -1 28 10.00 4.30 -9 1 -28 11.00 5.70 9 -2 28 7.20 3.90 -9 2 -28 -2.30 4.40 -9 3 -28 8.60 4.10 9 -4 28 3.30 3.10 -9 4 -28 -6.70 5.80 9 -5 28 1.80 2.90 -9 5 -28 -2.30 2.80 9 -6 28 7.30 2.90 -9 6 -28 11.80 4.20 8 6 28 75.29 7.90 8 5 28 207.48 14.60 8 4 28 -3.50 4.40 8 3 28 211.18 16.30 8 2 28 30.60 5.90 8 1 28 63.79 10.70 -8 -1 -28 70.49 12.30 8 0 28 396.56 26.90 -8 0 -28 413.06 29.20 8 -1 28 39.40 7.20 -8 1 -28 45.90 9.10 8 -2 28 30.70 7.20 -8 2 -28 29.30 5.80 8 -3 28 207.88 17.00 -8 3 -28 203.38 15.70 8 -4 28 -0.10 2.90 -8 4 -28 -1.50 2.90 8 -5 28 191.28 14.50 -8 5 -28 192.68 13.80 8 -6 28 71.79 9.50 -8 6 -28 72.39 7.70 7 6 28 2.40 2.80 7 5 28 22.00 4.70 7 4 28 2.50 3.60 7 3 28 -3.90 3.30 -7 -3 -28 -5.80 4.90 7 2 28 4.10 4.50 7 1 28 22.30 6.40 -7 -1 -28 17.70 6.00 7 0 28 123.19 14.10 -7 0 -28 117.99 13.20 7 -1 28 28.70 6.60 -7 1 -28 27.70 6.10 7 -2 28 0.20 3.90 -7 2 -28 2.00 3.40 7 -3 28 -1.50 3.40 -7 3 -28 1.20 3.20 7 -4 28 -1.40 3.20 -7 4 -28 -2.50 2.80 7 -5 28 21.10 4.80 -7 5 -28 20.30 4.10 7 -6 28 3.20 3.00 -7 6 -28 2.10 2.20 7 -7 28 2.90 2.40 -7 7 -28 3.10 2.40 6 6 28 143.79 12.00 6 5 28 216.58 17.50 -6 -5 -28 254.07 26.60 6 4 28 4.90 3.80 -6 -4 -28 -3.00 4.70 6 3 28 123.59 14.60 6 2 28 124.29 14.20 -6 -2 -28 93.69 13.30 6 1 28 104.39 14.00 -6 -1 -28 95.39 12.40 6 0 28 525.75 33.90 -6 0 -28 534.95 32.50 6 -1 28 129.09 15.60 -6 1 -28 112.29 13.40 6 -2 28 128.09 15.10 -6 2 -28 112.39 13.00 6 -3 28 123.79 14.20 -6 3 -28 102.29 12.20 6 -4 28 -1.10 3.50 -6 4 -28 2.00 3.10 6 -5 28 248.18 18.20 -6 5 -28 240.88 16.70 6 -6 28 137.89 12.60 -6 6 -28 142.49 11.20 6 -7 28 49.90 7.00 -6 7 -28 42.10 6.00 5 7 28 0.70 2.40 5 6 28 4.00 3.10 -5 -6 -28 8.40 6.90 5 5 28 33.80 6.50 -5 -5 -28 34.90 7.00 5 4 28 -1.70 3.10 -5 -4 -28 8.20 6.20 5 3 28 48.90 8.40 -5 -3 -28 37.90 7.00 5 2 28 8.10 4.90 -5 -2 -28 4.70 4.80 5 1 28 11.10 5.70 -5 -1 -28 14.20 5.30 5 0 28 2.70 4.50 -5 0 -28 5.10 4.50 5 -1 28 20.10 7.10 -5 1 -28 13.30 4.90 5 -2 28 0.20 4.80 -5 2 -28 2.40 3.80 5 -3 28 22.40 6.80 -5 3 -28 41.20 7.20 5 -4 28 1.10 3.80 -5 4 -28 4.80 3.00 5 -5 28 22.00 5.30 5 -6 28 0.10 4.10 -5 6 -28 6.30 2.60 5 -7 28 -1.70 3.30 -5 7 -28 -1.30 1.90 4 7 28 6.40 3.10 -4 -7 -28 9.50 5.00 4 6 28 216.58 16.20 -4 -6 -28 190.98 16.50 4 5 28 143.99 13.70 -4 -5 -28 130.49 13.60 4 4 28 3.70 4.50 -4 -4 -28 1.50 3.80 4 3 28 49.80 9.00 -4 -3 -28 35.80 7.10 4 2 28 171.58 17.30 -4 -2 -28 171.38 16.90 4 1 28 40.50 10.90 -4 -1 -28 65.49 11.70 4 0 28 162.48 25.00 -4 0 -28 153.38 17.40 4 -1 28 42.80 9.50 -4 1 -28 42.50 9.10 4 -2 28 178.38 19.50 -4 2 -28 190.38 16.40 4 -3 28 54.59 9.80 -4 3 -28 61.89 10.60 4 -4 28 6.60 4.50 -4 4 -28 3.90 3.20 4 -5 28 172.78 15.40 -4 5 -28 156.58 12.90 4 -6 28 199.08 16.40 -4 6 -28 214.48 14.50 4 -7 28 11.40 5.10 -4 7 -28 8.90 2.70 3 8 28 4.30 2.20 3 7 28 -0.80 2.40 -3 -7 -28 3.40 4.10 3 6 28 3.00 4.10 -3 -6 -28 -1.40 3.70 3 5 28 14.80 4.80 -3 -5 -28 12.80 7.80 3 4 28 4.40 4.80 -3 -4 -28 -6.70 3.60 3 3 28 22.50 6.40 -3 -3 -28 29.70 6.60 3 2 28 0.80 5.10 -3 -2 -28 1.60 4.40 3 1 28 -7.40 6.00 -3 -1 -28 5.50 6.00 3 0 28 11.90 8.20 -3 0 -28 1.60 4.20 3 -1 28 3.50 7.10 -3 1 -28 -2.20 4.20 3 -2 28 4.80 5.90 -3 2 -28 7.50 6.00 3 -3 28 32.80 7.30 -3 3 -28 30.30 6.40 -3 4 -28 2.50 3.00 3 -5 28 20.20 6.30 -3 5 -28 17.40 3.80 3 -6 28 7.00 5.50 3 -7 28 5.70 7.90 -3 7 -28 1.00 1.90 -3 8 -28 2.80 1.90 2 8 28 180.58 11.80 -2 -8 -28 157.98 14.70 2 7 28 0.90 2.60 -2 -7 -28 3.10 5.60 2 6 28 211.28 18.80 -2 -6 -28 189.78 15.00 2 5 28 69.29 11.40 -2 -5 -28 86.69 10.60 2 4 28 14.20 5.30 -2 -4 -28 13.30 5.20 2 3 28 11.30 5.70 -2 -3 -28 19.10 6.00 2 2 28 409.36 35.30 2 1 28 51.19 14.40 -2 -1 -28 31.80 6.90 2 0 28 508.55 38.90 -2 0 -28 385.16 27.30 -2 1 -28 25.10 5.70 2 -2 28 401.16 31.20 -2 2 -28 488.25 34.90 2 -3 28 34.10 8.80 -2 3 -28 37.60 7.40 2 -4 28 6.40 6.10 -2 4 -28 15.00 4.30 2 -5 28 47.60 8.50 -2 6 -28 192.88 14.10 -2 7 -28 2.80 1.90 -2 8 -28 173.38 11.10 1 8 28 3.80 2.60 -1 -8 -28 3.50 2.90 1 7 28 -2.50 2.80 -1 -7 -28 0.50 2.90 1 6 28 1.30 4.80 -1 -6 -28 -2.50 3.10 1 5 28 72.19 11.30 -1 -5 -28 74.09 10.60 1 4 28 -2.00 4.70 -1 -4 -28 3.90 3.80 1 3 28 1.70 5.60 -1 -3 -28 -2.50 4.10 1 2 28 -1.90 7.30 -1 -2 -28 -1.10 4.50 1 1 28 20.50 9.80 -1 -1 -28 20.90 5.90 1 0 28 17.40 9.10 -1 0 -28 16.70 5.20 1 -1 28 24.90 11.60 -1 1 -28 29.90 6.40 1 -2 28 -1.00 6.50 -1 2 -28 3.10 3.90 1 -3 28 -4.80 3.00 -1 3 -28 8.30 4.90 1 -4 28 4.50 3.70 1 -4 28 7.70 6.80 -1 4 -28 4.90 3.50 -1 5 -28 89.59 9.90 -1 6 -28 2.30 2.20 -1 7 -28 1.30 2.00 -1 8 -28 3.80 1.90 0 8 28 112.19 9.10 0 -8 -28 136.19 11.80 0 -7 -28 0.70 2.70 0 6 28 152.38 14.50 0 -6 -28 191.98 18.50 0 5 28 5.70 4.30 0 -5 -28 -4.80 3.00 0 4 28 32.80 7.10 0 3 28 -7.20 5.10 0 -3 -28 1.00 3.90 0 2 28 224.98 24.60 0 -2 -28 255.57 20.30 0 1 28 -7.70 4.50 0 -1 -28 -0.30 3.70 0 -1 28 -0.10 3.00 0 -1 28 -3.00 8.20 0 1 -28 -0.70 3.50 0 -2 28 230.48 15.40 0 -2 28 236.08 24.60 0 2 -28 250.07 19.10 0 3 -28 -1.20 3.80 0 -4 28 46.30 6.80 0 4 -28 65.99 9.20 0 -5 28 -2.20 2.80 0 5 -28 -0.30 2.70 0 -6 28 130.39 14.50 0 6 -28 158.38 11.80 0 7 -28 -2.10 1.80 0 8 -28 127.89 8.10 -1 8 28 0.40 3.00 1 -8 -28 1.40 2.20 1 -7 -28 -0.40 2.50 -1 6 28 -3.10 3.60 -1 5 28 69.59 10.90 1 -5 -28 56.89 9.40 -1 4 28 4.70 5.00 1 -4 -28 6.60 4.10 -1 3 28 -1.90 6.20 1 -3 -28 1.40 4.00 -1 2 28 -8.50 6.70 1 -2 -28 0.10 3.90 -1 1 28 -0.70 3.10 -1 1 28 1.70 8.70 -1 0 28 -10.40 11.30 -1 0 28 9.20 3.70 1 0 -28 7.50 4.40 -1 -1 28 17.60 4.10 1 1 -28 29.10 6.50 -1 -2 28 -1.80 2.50 1 2 -28 -0.40 3.20 -1 -3 28 -1.30 2.50 1 3 -28 6.30 4.70 -1 -4 28 1.90 2.40 1 4 -28 5.30 3.40 -1 -5 28 71.89 8.00 1 5 -28 91.59 9.50 -1 -6 28 -4.50 2.40 1 6 -28 0.30 2.30 1 7 -28 1.10 1.90 -2 8 28 174.78 12.40 2 -8 -28 172.28 11.50 -2 7 28 4.40 5.40 2 -7 -28 -1.80 2.20 -2 6 28 179.28 15.00 -2 5 28 47.90 12.10 2 -5 -28 71.69 9.50 -2 4 28 12.70 6.00 2 -4 -28 9.20 4.70 -2 3 28 6.30 7.10 -2 3 28 2.70 4.50 -2 2 28 265.27 19.90 -2 2 28 353.46 28.10 2 -2 -28 363.46 24.60 -2 1 28 18.00 4.30 2 -1 -28 19.10 5.50 -2 0 28 369.96 22.40 2 0 -28 413.56 25.90 -2 -1 28 26.70 4.80 2 1 -28 33.00 6.60 -2 -2 28 364.46 22.30 2 2 -28 411.16 26.80 -2 -3 28 31.10 4.80 2 3 -28 29.80 6.00 -2 -4 28 5.80 2.80 2 4 -28 9.90 4.00 -2 -5 28 79.99 7.70 2 5 -28 83.09 9.10 -2 -6 28 201.08 13.70 -2 -7 28 2.00 3.00 2 7 -28 1.70 2.10 3 -8 -28 5.70 2.20 -3 7 28 -1.50 3.70 3 -7 -28 3.00 2.60 -3 6 28 -4.30 4.10 3 -6 -28 0.20 2.80 -3 5 28 7.60 5.60 -3 4 28 -5.60 8.30 3 -4 -28 1.80 3.50 -3 3 28 14.60 4.10 -3 3 28 24.60 10.90 -3 2 28 6.50 3.10 3 -2 -28 -4.20 4.50 -3 1 28 -4.90 2.40 3 -1 -28 1.80 3.70 -3 0 28 3.30 2.90 3 0 -28 4.90 4.00 -3 -1 28 -2.20 2.30 3 1 -28 -1.40 3.50 -3 -2 28 -2.40 2.50 -3 -3 28 32.80 5.90 3 3 -28 27.00 5.50 -3 -4 28 0.00 2.30 3 4 -28 -0.30 2.70 -3 -5 28 15.00 3.50 3 5 -28 20.00 3.80 -3 -6 28 1.00 2.40 3 6 -28 3.70 2.40 -3 -7 28 -2.10 2.60 -4 7 28 -2.60 7.10 4 -7 -28 6.60 2.90 4 -6 -28 172.18 13.70 -4 5 28 106.09 16.70 4 -5 -28 141.89 12.10 -4 4 28 -6.70 4.10 4 -4 -28 3.00 3.80 -4 3 28 26.00 4.20 -4 2 28 155.78 13.20 4 -2 -28 144.59 15.20 -4 1 28 41.90 7.10 -4 0 28 138.29 11.40 4 0 -28 147.89 17.30 -4 -1 28 47.60 7.10 -4 -2 28 157.38 12.60 4 2 -28 163.28 14.00 -4 -3 28 37.00 6.90 4 3 -28 42.10 6.60 4 4 -28 1.70 2.70 -4 -5 28 156.68 11.10 4 5 -28 151.08 11.30 -4 -6 28 213.68 14.80 4 6 -28 201.98 12.30 -4 -7 28 7.50 2.20 5 -7 -28 -0.20 2.20 5 -6 -28 4.70 2.70 5 -5 -28 24.90 4.80 -5 4 28 2.90 3.40 5 -4 -28 8.70 3.50 -5 3 28 22.40 4.00 5 -3 -28 36.70 6.40 -5 2 28 4.40 4.30 5 -2 -28 2.10 3.20 -5 1 28 9.00 3.00 5 -1 -28 16.60 5.10 -5 0 28 4.00 2.70 5 0 -28 2.60 3.70 -5 -1 28 17.00 4.30 5 1 -28 16.90 4.90 -5 -2 28 -2.00 2.80 5 2 -28 3.40 3.40 -5 -3 28 49.80 7.20 5 3 -28 52.89 8.10 -5 -4 28 6.90 2.80 5 4 -28 0.90 2.50 -5 -5 28 38.80 6.00 5 5 -28 23.80 3.70 -5 -6 28 0.90 2.20 -5 -7 28 -1.30 2.20 6 -7 -28 38.50 5.80 6 -6 -28 132.99 10.10 6 -5 -28 237.88 17.50 -6 4 28 4.00 3.20 6 -4 -28 0.10 2.70 -6 3 28 95.49 9.00 6 -3 -28 126.99 11.70 -6 2 28 110.69 9.60 6 -2 -28 101.39 11.40 -6 1 28 92.49 12.40 6 -1 -28 106.79 10.90 -6 0 28 530.35 29.70 6 0 -28 500.45 29.10 -6 -1 28 114.49 12.70 6 1 -28 104.79 11.20 -6 -2 28 102.59 10.70 6 2 -28 111.59 10.60 -6 -3 28 110.89 9.90 6 3 -28 116.69 9.90 -6 -4 28 -0.50 2.20 -6 -5 28 229.68 14.40 -6 -6 28 145.29 10.00 -6 -7 28 39.90 4.50 7 -7 -28 4.40 2.00 7 -6 -28 1.50 2.30 -7 5 28 2.50 4.30 7 -5 -28 14.90 3.30 -7 4 28 -3.50 3.20 7 -4 -28 -0.30 2.50 -7 3 28 -1.10 2.40 7 -3 -28 -1.60 2.50 -7 2 28 -0.30 2.40 7 -2 -28 -1.10 2.80 -7 1 28 26.20 4.60 7 -1 -28 22.60 5.00 -7 0 28 118.09 10.10 7 0 -28 118.29 11.00 -7 -1 28 23.50 4.20 7 1 -28 26.60 4.70 -7 -2 28 0.60 2.50 7 2 -28 0.30 2.70 -7 -3 28 1.20 2.00 -7 -4 28 0.60 2.50 -7 -5 28 22.90 5.10 8 -6 -28 66.69 6.90 -8 5 28 193.58 14.10 8 -5 -28 169.48 11.50 -8 4 28 -0.10 2.80 8 -4 -28 -0.40 2.20 -8 3 28 150.78 11.60 8 -3 -28 168.08 12.00 -8 2 28 20.50 3.80 8 -2 -28 16.40 3.70 -8 1 28 49.40 6.80 8 -1 -28 51.19 6.80 -8 0 28 357.76 21.00 8 0 -28 356.66 19.90 -8 -1 28 58.29 7.50 -8 -2 28 24.80 4.40 -8 -3 28 188.48 13.20 -8 -4 28 2.70 2.40 -8 -5 28 184.18 12.00 -8 -6 28 72.39 6.10 9 -5 -28 1.00 2.60 -9 4 28 0.50 2.90 9 -4 -28 -1.70 2.10 -9 3 28 10.90 3.10 9 -3 -28 5.40 2.50 -9 2 28 8.50 3.00 9 -2 -28 2.00 2.50 -9 1 28 5.30 3.00 9 -1 -28 7.80 2.50 -9 0 28 24.10 4.40 -9 -1 28 5.60 3.10 -9 -2 28 5.50 3.10 -9 -3 28 6.50 2.90 -9 -4 28 -2.00 2.20 -9 -5 28 2.60 2.50 -9 -6 28 5.20 2.50 -10 4 28 2.20 2.20 -10 3 28 342.77 19.50 -10 2 28 -0.90 2.20 -10 1 28 5.00 2.80 -10 0 28 55.19 7.00 -10 -1 28 2.00 2.60 -10 -2 28 3.60 2.50 -10 -3 28 385.86 21.20 -10 -4 28 4.40 2.60 -10 -5 28 141.79 10.30 -11 4 28 -0.90 2.50 -11 3 28 -2.10 2.50 -11 2 28 10.40 3.20 -11 1 28 9.40 3.00 -11 0 28 11.50 3.60 -11 -1 28 12.50 3.10 -11 -2 28 9.70 3.00 -11 -3 28 4.00 3.60 -11 -4 28 7.20 3.60 -12 3 28 293.87 16.50 -12 2 28 -1.70 2.00 -12 1 28 2.90 3.30 -12 0 28 -0.40 3.00 -12 -1 28 0.00 2.50 -12 -2 28 -2.10 1.90 -12 -3 28 325.87 17.40 -13 1 28 -1.40 1.80 -13 0 28 7.50 2.40 -13 -1 28 -1.90 1.90 12 1 29 172.48 11.00 12 0 29 -1.00 2.80 12 -1 29 172.78 13.00 12 -2 29 -1.60 2.20 11 3 29 5.20 2.40 11 2 29 6.30 2.90 11 1 29 1.50 3.10 11 0 29 3.50 2.60 11 -1 29 1.80 2.80 11 -2 29 7.00 3.20 11 -3 29 10.00 4.30 10 4 29 2.20 2.80 10 3 29 55.99 7.80 10 2 29 13.30 3.30 10 1 29 170.98 13.50 10 0 29 -3.30 2.40 10 -1 29 163.48 12.90 10 -2 29 10.00 3.60 10 -3 29 56.09 7.90 -10 3 -29 38.30 7.20 10 -4 29 -2.70 3.00 9 5 29 -1.40 2.20 9 4 29 153.98 11.50 9 3 29 -0.90 2.90 9 2 29 46.90 8.30 9 1 29 48.10 11.40 9 0 29 -3.90 4.00 -9 1 -29 64.89 12.50 9 -2 29 69.09 8.80 -9 2 -29 45.20 9.90 9 -3 29 0.70 2.80 -9 3 -29 -5.90 3.20 9 -4 29 169.18 13.60 -9 4 -29 202.98 18.10 9 -5 29 -0.50 2.60 -9 5 -29 -1.70 3.50 8 5 29 18.20 3.80 8 4 29 7.90 3.40 8 3 29 22.50 6.10 8 2 29 22.70 5.70 8 1 29 197.28 16.40 -8 -1 -29 190.58 17.70 8 0 29 -3.30 2.90 -8 0 -29 -7.60 4.40 8 -1 29 199.08 16.50 -8 1 -29 219.28 16.10 8 -2 29 27.80 6.30 -8 2 -29 23.80 5.60 8 -3 29 19.90 4.50 -8 3 -29 22.90 4.90 8 -4 29 7.90 3.70 -8 4 -29 1.30 3.20 8 -5 29 14.30 3.40 -8 5 -29 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8.40 -5 1 -30 51.59 9.20 5 -2 30 31.10 6.10 -5 2 -30 20.60 4.90 5 -3 30 262.87 19.30 -5 3 -30 242.58 20.00 5 -4 30 -2.40 3.40 -5 4 -30 2.70 2.60 5 -5 30 156.78 17.00 -5 5 -30 126.99 10.50 5 -6 30 108.79 14.00 -5 6 -30 97.59 9.00 4 6 30 2.40 2.80 -4 -6 -30 -4.00 4.20 4 5 30 11.10 3.80 -4 -5 -30 17.00 5.00 4 4 30 2.20 3.50 -4 -4 -30 3.20 3.40 4 3 30 25.50 5.40 -4 -3 -30 19.40 4.80 4 2 30 -3.00 4.20 -4 -2 -30 3.10 3.70 4 1 30 34.70 7.60 -4 -1 -30 57.79 9.70 4 0 30 0.20 4.20 -4 0 -30 -0.10 3.60 4 -1 30 38.00 7.40 -4 1 -30 31.80 6.20 4 -2 30 17.70 4.90 -4 2 -30 6.80 3.90 4 -3 30 19.00 5.10 4 -4 30 3.20 4.10 -4 4 -30 6.70 3.10 4 -5 30 7.30 5.50 -4 5 -30 10.70 2.90 4 -6 30 6.40 4.80 -4 6 -30 1.70 2.10 3 6 30 20.90 4.30 -3 -6 -30 27.60 7.10 3 5 30 288.47 19.40 -3 -5 -30 310.27 19.40 3 4 30 -6.60 5.20 -3 -4 -30 -4.20 2.90 3 3 30 500.55 30.40 -3 -3 -30 451.35 28.30 3 2 30 -2.50 4.50 -3 -2 -30 5.00 3.90 3 1 30 8.90 4.70 -3 -1 -30 4.40 3.80 3 0 30 107.89 13.80 -3 0 -30 128.39 12.90 3 -1 30 -6.80 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285.27 20.60 -2 -2 -32 305.37 19.50 2 1 32 -1.20 4.00 -2 -1 -32 -1.40 2.90 2 0 32 230.38 17.50 -2 0 -32 194.98 20.00 2 -1 32 -6.40 4.90 -2 1 -32 8.00 6.30 2 -2 32 280.77 21.90 -2 2 -32 301.07 18.90 2 -3 32 57.39 9.00 -2 3 -32 81.89 8.00 2 -4 32 -7.70 7.30 -2 4 -32 1.80 2.40 -2 5 -32 11.70 3.80 1 5 32 20.70 4.60 -1 -5 -32 10.50 2.90 1 4 32 -0.20 4.10 -1 -4 -32 2.40 3.10 1 3 32 14.80 5.30 -1 -3 -32 6.50 2.90 1 2 32 5.50 4.70 -1 -2 -32 7.50 3.20 1 1 32 46.70 7.80 -1 -1 -32 34.30 7.00 1 0 32 30.70 6.90 -1 0 -32 22.50 4.70 1 -1 32 42.00 7.90 -1 1 -32 40.70 7.50 -1 2 -32 10.60 4.20 -1 3 -32 14.90 3.30 -1 4 -32 -0.20 2.00 -1 5 -32 15.50 3.20 0 5 32 2.30 3.60 0 -5 -32 3.30 2.60 0 4 32 10.20 4.40 0 -4 -32 -0.70 2.70 0 -3 -32 2.30 2.80 0 2 32 356.66 25.00 0 -2 -32 408.46 24.20 0 1 32 4.60 5.50 0 -1 -32 -0.70 3.40 0 0 32 51.79 9.50 0 0 -32 46.00 8.10 0 -1 32 14.30 11.50 0 2 -32 375.46 26.30 0 3 -32 2.30 2.30 0 4 -32 3.30 2.20 0 5 -32 -1.40 1.90 -1 5 32 9.40 4.40 1 -5 -32 21.00 4.50 -1 4 32 -8.40 6.00 1 -4 -32 3.00 2.70 -1 3 32 5.90 5.80 1 -3 -32 13.40 3.70 -1 2 32 4.90 10.90 1 -2 -32 6.10 3.70 -1 1 32 17.80 13.30 1 -1 -32 68.39 9.30 1 0 -32 22.80 4.50 1 1 -32 58.59 8.20 1 2 -32 7.50 3.90 1 3 -32 10.30 3.20 1 4 -32 1.00 2.10 1 5 -32 18.80 3.90 2 -5 -32 14.90 5.10 -2 4 32 -6.60 7.70 2 -4 -32 4.40 2.60 -2 3 32 56.49 9.80 2 -3 -32 78.59 8.30 2 -2 -32 292.27 19.70 2 -1 -32 2.50 3.20 2 0 -32 223.98 16.70 2 1 -32 -2.00 3.10 2 2 -32 290.07 18.50 2 3 -32 81.69 7.90 2 4 -32 4.20 2.20 2 5 -32 14.00 3.30 3 -5 -32 19.40 3.70 3 -4 -32 2.00 2.50 3 -3 -32 63.69 7.40 3 -2 -32 19.40 3.90 3 -1 -32 6.70 4.60 -3 -1 32 -6.60 3.40 3 1 -32 0.90 3.00 -3 -2 32 16.30 4.10 3 2 -32 26.50 4.40 -3 -3 32 71.79 10.40 3 3 -32 87.89 7.60 3 4 -32 0.00 2.70 4 -5 -32 9.00 2.50 4 -4 -32 5.30 2.60 4 -3 -32 113.99 9.60 4 -2 -32 121.19 10.00 4 -1 -32 8.40 3.30 -4 0 32 312.47 18.70 4 0 -32 383.56 20.60 -4 -1 32 11.60 4.60 4 1 -32 11.50 2.80 -4 -2 32 112.19 8.60 4 2 -32 127.29 9.50 -4 -3 32 87.59 8.50 4 3 -32 111.79 8.20 5 -4 -32 -1.20 2.50 5 -3 -32 3.50 2.60 5 -2 -32 5.50 2.60 -5 1 32 14.10 4.20 5 -1 -32 17.80 3.60 -5 0 32 24.10 4.30 5 0 -32 39.90 5.70 -5 -1 32 19.10 4.10 5 1 -32 29.00 5.20 -5 -2 32 0.70 2.40 5 2 -32 -1.90 2.00 -5 -3 32 -2.10 2.90 6 -4 -32 4.50 2.00 6 -3 -32 208.18 15.20 6 -2 -32 65.09 6.40 -6 1 32 14.00 3.90 6 -1 -32 17.00 3.20 -6 0 32 199.48 12.40 6 0 -32 196.68 11.80 -6 -1 32 18.20 3.20 6 1 -32 17.60 4.40 -6 -2 32 71.39 6.90 -6 -3 32 177.78 10.90 -7 1 32 55.49 7.10 -7 0 32 -0.10 3.60 -7 -1 32 50.19 6.50 -7 -2 32 -0.30 2.90 -8 0 32 23.70 3.70 -8 -1 32 13.30 2.80 7 2 33 36.70 6.10 7 1 33 14.80 3.30 7 0 33 2.00 2.80 -7 0 -33 -1.30 3.10 7 -1 33 11.80 3.30 -7 1 -33 6.40 3.60 7 -2 33 26.80 5.70 -7 2 -33 43.20 6.20 6 2 33 85.19 8.80 -6 -2 -33 74.89 8.50 6 1 33 84.09 12.20 -6 -1 -33 95.59 9.00 6 0 33 6.40 5.70 -6 0 -33 3.30 4.70 6 -1 33 112.39 10.70 -6 1 -33 88.69 9.60 6 -2 33 71.79 8.20 -6 2 -33 81.29 9.50 5 3 33 -1.50 2.60 -5 -3 -33 2.10 4.00 5 2 33 -5.90 4.80 -5 -2 -33 -4.60 3.10 5 1 33 5.90 3.50 -5 -1 -33 13.40 3.80 5 0 33 -0.60 3.00 -5 0 -33 6.50 3.60 -5 1 -33 13.10 5.40 5 -2 33 -4.50 3.00 -5 2 -33 1.40 2.90 5 -3 33 5.10 2.80 -5 3 -33 5.20 2.30 4 4 33 191.38 14.30 -4 -4 -33 188.88 13.80 4 3 33 1.40 3.10 4 2 33 128.19 11.60 -4 -2 -33 124.79 11.90 4 1 33 55.49 8.90 -4 -1 -33 62.29 8.20 4 0 33 0.40 3.50 -4 0 -33 2.90 2.80 4 -1 33 57.69 11.70 -4 1 -33 70.59 8.40 4 -2 33 104.19 10.90 -4 2 -33 116.39 9.70 4 -3 33 5.70 3.60 -4 4 -33 178.38 11.30 3 4 33 24.20 4.50 -3 -4 -33 18.30 3.20 3 3 33 -4.40 2.90 -3 -3 -33 -0.60 2.70 3 2 33 10.80 4.90 -3 -2 -33 10.30 3.20 3 1 33 82.79 11.30 -3 -1 -33 84.19 9.40 3 0 33 3.70 4.50 -3 0 -33 2.60 2.60 3 -1 33 73.89 12.70 -3 1 -33 93.49 9.10 3 -2 33 10.20 4.80 -3 2 -33 9.40 3.20 3 -3 33 -1.00 4.60 -3 3 -33 3.90 2.50 -3 4 -33 28.40 4.70 2 4 33 387.46 24.40 -2 -4 -33 298.27 18.90 2 3 33 -1.60 3.30 -2 -3 -33 -2.20 2.40 2 2 33 139.39 18.90 -2 -2 -33 148.19 11.80 2 1 33 9.10 4.90 -2 -1 -33 9.10 3.30 2 0 33 5.80 6.10 -2 0 -33 0.10 2.30 2 -1 33 8.50 4.50 -2 1 -33 7.10 3.00 2 -2 33 138.89 15.60 -2 2 -33 135.89 10.90 2 -3 33 -10.60 7.50 -2 3 -33 -1.50 2.00 1 4 33 2.80 3.70 -1 -4 -33 5.50 2.70 1 3 33 -2.10 3.50 -1 -3 -33 2.10 2.80 1 2 33 -3.70 4.40 -1 -2 -33 2.30 2.60 1 1 33 221.78 20.50 -1 -1 -33 162.98 13.00 -1 0 -33 0.30 2.50 1 -1 33 155.68 17.60 -1 1 -33 160.08 12.00 1 -2 33 -2.80 6.50 -1 2 -33 0.80 2.20 -1 3 -33 2.90 2.30 -1 4 -33 2.40 2.70 0 4 33 266.97 19.10 0 -4 -33 349.77 19.90 0 3 33 -6.50 4.20 0 -3 -33 -2.30 2.30 0 2 33 151.58 15.30 0 -2 -33 165.48 12.30 0 -1 -33 2.80 2.50 0 0 33 9.10 9.50 0 1 -33 -1.40 2.40 0 2 -33 165.38 11.90 0 3 -33 0.10 2.30 0 4 -33 306.77 18.30 1 -3 -33 -0.50 2.50 -1 2 33 -6.70 5.40 1 -2 -33 -0.20 2.50 1 -1 -33 152.88 12.10 1 0 -33 -1.10 2.50 1 1 -33 164.78 12.20 1 2 -33 0.70 2.30 1 3 -33 3.90 2.50 1 4 -33 2.10 2.80 2 -3 -33 -2.20 2.30 2 -2 -33 136.19 10.70 2 -1 -33 4.50 2.60 2 0 -33 1.90 2.30 2 1 -33 6.30 3.10 2 2 -33 140.69 10.40 2 3 -33 -1.10 1.80 2 4 -33 289.57 15.40 3 -4 -33 18.10 3.60 3 -3 -33 3.10 2.40 3 -2 -33 13.00 3.30 3 -1 -33 88.89 8.40 3 0 -33 0.50 2.40 3 1 -33 92.59 8.30 3 2 -33 13.60 3.10 3 3 -33 -0.20 2.40 4 -4 -33 173.88 10.70 4 -3 -33 2.20 2.30 4 -2 -33 112.79 8.90 4 -1 -33 73.79 7.50 4 0 -33 0.40 2.20 4 1 -33 61.19 6.30 4 2 -33 103.99 8.90 5 -3 -33 -1.00 1.80 5 -2 -33 0.50 3.40 5 -1 -33 15.00 3.00 5 0 -33 -0.30 2.20 5 1 -33 17.20 3.40 6 -2 -33 57.19 6.60 5 1 34 7.20 4.00 -5 -1 -34 8.50 3.80 5 0 34 159.38 15.00 -5 0 -34 156.98 11.20 5 -1 34 5.00 3.20 -5 1 -34 6.80 3.00 -4 -2 -34 8.90 2.90 4 1 34 0.20 3.10 -4 -1 -34 -0.20 2.40 4 0 34 5.20 5.80 -4 0 -34 11.60 3.10 4 -1 34 -6.20 3.00 -4 1 -34 7.80 2.50 4 -2 34 6.00 4.20 -4 2 -34 6.80 2.70 -3 -2 -34 65.19 7.10 3 1 34 90.29 13.10 -3 -1 -34 72.79 8.70 3 0 34 29.80 6.20 -3 0 -34 37.00 6.30 3 -1 34 67.09 9.10 3 -2 34 52.69 9.20 -3 2 -34 60.49 7.40 2 3 34 6.90 3.40 -2 -3 -34 10.00 4.10 2 2 34 8.40 4.50 -2 -2 -34 16.60 4.00 2 1 34 5.20 5.80 -2 -1 -34 -0.90 2.80 2 0 34 12.20 4.30 -2 0 -34 -1.20 2.70 -2 1 -34 2.80 2.40 -2 2 -34 12.70 4.30 -2 3 -34 3.60 2.10 1 3 34 169.48 13.90 -1 -3 -34 167.88 11.50 1 2 34 2.50 4.20 -1 -2 -34 10.80 4.70 1 1 34 40.30 7.70 -1 -1 -34 46.90 6.80 1 0 34 -9.10 5.60 -1 0 -34 -0.30 2.40 -1 1 -34 57.59 7.00 -1 2 -34 7.60 2.90 -1 3 -34 154.38 10.20 0 -3 -34 0.30 2.20 0 -2 -34 8.70 3.00 0 -1 -34 0.90 2.30 0 0 -34 -3.50 2.30 0 1 -34 3.70 2.60 0 2 -34 10.90 2.60 0 3 -34 -0.40 1.90 1 -3 -34 177.68 11.90 1 -2 -34 9.30 3.30 1 -1 -34 41.40 6.30 1 0 -34 -4.30 2.10 1 1 -34 39.30 5.60 1 2 -34 8.60 2.70 1 3 -34 169.58 10.40 2 -3 -34 2.90 2.20 2 -2 -34 13.30 3.40 2 -1 -34 -0.50 2.30 2 0 -34 1.20 2.30 2 1 -34 -1.80 2.00 2 2 -34 9.60 3.70 3 -2 -34 67.39 8.80 3 -1 -34 83.59 7.90 3 0 -34 55.29 6.40 3 1 -34 77.19 9.60 3 2 -34 47.50 5.20 4 -2 -34 3.70 2.00 4 -1 -34 4.60 2.10 4 0 -34 9.40 2.40 4 1 -34 3.60 2.80 -2 0 -35 -0.80 2.30 -1 -1 -35 275.37 15.80 -1 0 -35 -0.20 1.90 -1 1 -35 280.77 15.90 0 -1 -35 0.30 2.10 0 0 -35 -0.20 2.10 0 1 -35 -2.80 1.80 1 -1 -35 283.07 15.90 1 0 -35 -1.60 2.00 1 1 -35 261.27 14.50 2 0 -35 -1.50 1.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 75065 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Sb1 Sb 0.47777(2) 0.43520(3) 0.62623(2) 0.01993(12) Uani 1 1 d . . . . . P1 P 0.56534(8) 0.29161(12) 0.71182(4) 0.0217(3) Uani 1 1 d . . . . . F1 F 0.4501(2) 0.5482(3) 0.67939(10) 0.0313(7) Uani 1 1 d . . . . . O1 O 0.5770(2) 0.3911(4) 0.67586(13) 0.0268(8) Uani 1 1 d . . . . . C25 C 0.5790(3) 0.3373(5) 0.77198(18) 0.0248(11) Uani 1 1 d . . . . . C19 C 0.5243(3) 0.3012(5) 0.57833(17) 0.0239(11) Uani 1 1 d . . . . . C1 C 0.4293(3) 0.3013(4) 0.67255(17) 0.0223(10) Uani 1 1 d . . . . . C5 C 0.3240(3) 0.1854(5) 0.69793(19) 0.0275(12) Uani 1 1 d . . . . . H5 H 0.273820 0.163766 0.693926 0.033 Uiso 1 1 calc R . . . . C7 C 0.3790(3) 0.4817(5) 0.58838(19) 0.0260(11) Uani 1 1 d . . . . . C3 C 0.4387(3) 0.1617(5) 0.73827(18) 0.0241(11) Uani 1 1 d . . . . . H3 H 0.467465 0.125076 0.762229 0.029 Uiso 1 1 calc R . . . . C2 C 0.4709(3) 0.2457(5) 0.70717(18) 0.0227(11) Uani 1 1 d . . . . . C26 C 0.6499(3) 0.3400(5) 0.7909(2) 0.0296(12) Uani 1 1 d . . . . . H26 H 0.690669 0.314194 0.772656 0.035 Uiso 1 1 calc R . . . . C13 C 0.5444(3) 0.5847(5) 0.60466(19) 0.0261(11) Uani 1 1 d . . . . . C18 C 0.5263(4) 0.6434(5) 0.5631(2) 0.0327(13) Uani 1 1 d . . . . . H18 H 0.487893 0.612827 0.543847 0.039 Uiso 1 1 calc R . . . . C31 C 0.6269(3) 0.1682(5) 0.69959(19) 0.0246(11) Uani 1 1 d . . . . . C30 C 0.5204(3) 0.3753(5) 0.7989(2) 0.0311(12) Uani 1 1 d . . . . . H30 H 0.472298 0.374499 0.785756 0.037 Uiso 1 1 calc R . . . . C4 C 0.3650(4) 0.1333(5) 0.7335(2) 0.0304(12) Uani 1 1 d . . . . . H4 H 0.342529 0.078100 0.754662 0.036 Uiso 1 1 calc R . . . . C12 C 0.3562(4) 0.4179(6) 0.5489(2) 0.0345(14) Uani 1 1 d . . . . . H12 H 0.384566 0.351589 0.538127 0.041 Uiso 1 1 calc R . . . . C17 C 0.5641(4) 0.7464(6) 0.5495(2) 0.0366(14) Uani 1 1 d . . . . . H17 H 0.550346 0.786751 0.521333 0.044 Uiso 1 1 calc R . . . . C36 C 0.6604(3) 0.1621(6) 0.6554(2) 0.0330(13) Uani 1 1 d . . . . . H36 H 0.649992 0.221608 0.632384 0.040 Uiso 1 1 calc R . . . . C6 C 0.3563(3) 0.2698(5) 0.66780(19) 0.0274(12) Uani 1 1 d . . . . . H6 H 0.327571 0.305894 0.643729 0.033 Uiso 1 1 calc R . . . . C32 C 0.6401(3) 0.0778(5) 0.7327(2) 0.0299(12) Uani 1 1 d . . . . . H32 H 0.616691 0.080286 0.762577 0.036 Uiso 1 1 calc R . . . . C24 C 0.4986(4) 0.1833(5) 0.57962(19) 0.0306(13) Uani 1 1 d . . . . . H24 H 0.458810 0.162455 0.599685 0.037 Uiso 1 1 calc R . . . . C27 C 0.6604(4) 0.3807(6) 0.8366(2) 0.0347(14) Uani 1 1 d . . . . . H27 H 0.708624 0.384343 0.849427 0.042 Uiso 1 1 calc R . . . . C23 C 0.5315(4) 0.0958(6) 0.5513(2) 0.0356(14) Uani 1 1 d . . . . . H23 H 0.513411 0.015500 0.551926 0.043 Uiso 1 1 calc R . . . . C14 C 0.6001(4) 0.6304(6) 0.6319(2) 0.0370(14) Uani 1 1 d . . . . . H14 H 0.612874 0.591559 0.660535 0.044 Uiso 1 1 calc R . . . . C20 C 0.5818(4) 0.3286(6) 0.54905(19) 0.0324(13) Uani 1 1 d . . . . . H20 H 0.599038 0.409253 0.547804 0.039 Uiso 1 1 calc R . . . . C10 C 0.2515(4) 0.5473(6) 0.5398(2) 0.0394(15) Uani 1 1 d . . . . . H10 H 0.208566 0.570644 0.523022 0.047 Uiso 1 1 calc R . . . . C35 C 0.7091(4) 0.0688(6) 0.6452(2) 0.0377(15) Uani 1 1 d . . . . . H35 H 0.733020 0.065476 0.615495 0.045 Uiso 1 1 calc R . . . . C22 C 0.5901(4) 0.1248(6) 0.5225(2) 0.0363(14) Uani 1 1 d . . . . . H22 H 0.612692 0.064502 0.503696 0.044 Uiso 1 1 calc R . . . . C34 C 0.7225(4) -0.0194(6) 0.6789(3) 0.0411(15) Uani 1 1 d . . . . . H34 H 0.755914 -0.082827 0.672183 0.049 Uiso 1 1 calc R . . . . C29 C 0.5302(4) 0.4146(6) 0.8446(2) 0.0338(14) Uani 1 1 d . . . . . H29 H 0.489330 0.440486 0.862824 0.041 Uiso 1 1 calc R . . . . C11 C 0.2928(4) 0.4497(6) 0.5250(2) 0.0395(15) Uani 1 1 d . . . . . H11 H 0.277577 0.404488 0.498328 0.047 Uiso 1 1 calc R . . . . C33 C 0.6878(4) -0.0156(5) 0.7217(2) 0.0371(14) Uani 1 1 d . . . . . H33 H 0.696521 -0.077639 0.744009 0.045 Uiso 1 1 calc R . . . . C8 C 0.3368(4) 0.5781(6) 0.6033(2) 0.0319(13) Uani 1 1 d . . . . . H8 H 0.351431 0.622624 0.630227 0.038 Uiso 1 1 calc R . . . . C21 C 0.6158(4) 0.2420(6) 0.5211(2) 0.0377(14) Uani 1 1 d . . . . . H21 H 0.655957 0.263120 0.501309 0.045 Uiso 1 1 calc R . . . . C16 C 0.6207(4) 0.7906(6) 0.5760(2) 0.0404(15) Uani 1 1 d . . . . . H16 H 0.647775 0.859127 0.565900 0.048 Uiso 1 1 calc R . . . . C28 C 0.6010(4) 0.4157(6) 0.8634(2) 0.0382(15) Uani 1 1 d . . . . . H28 H 0.608357 0.440732 0.895046 0.046 Uiso 1 1 calc R . . . . C9 C 0.2735(4) 0.6105(7) 0.5794(2) 0.0402(15) Uani 1 1 d . . . . . H9 H 0.244938 0.676510 0.590254 0.048 Uiso 1 1 calc R . . . . C15 C 0.6379(4) 0.7331(6) 0.6179(3) 0.0453(17) Uani 1 1 d . . . . . H15 H 0.675941 0.764284 0.637222 0.054 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb1 0.0238(2) 0.02026(17) 0.01574(17) -0.00016(12) -0.00139(12) 0.00074(13) P1 0.0223(6) 0.0237(6) 0.0190(6) 0.0018(5) -0.0018(5) 0.0002(5) F1 0.042(2) 0.0316(17) 0.0202(15) -0.0044(13) 0.0007(14) -0.0013(15) O1 0.025(2) 0.031(2) 0.0248(18) 0.0067(16) -0.0020(15) -0.0027(16) C25 0.029(3) 0.024(3) 0.021(2) 0.003(2) -0.001(2) 0.000(2) C19 0.028(3) 0.027(3) 0.017(2) -0.005(2) -0.002(2) 0.009(2) C1 0.029(3) 0.020(2) 0.018(2) -0.0005(19) 0.004(2) 0.003(2) C5 0.021(3) 0.032(3) 0.029(3) -0.005(2) 0.000(2) -0.004(2) C7 0.023(3) 0.030(3) 0.025(3) 0.002(2) -0.005(2) 0.001(2) C3 0.025(3) 0.025(3) 0.022(2) 0.001(2) 0.000(2) 0.002(2) C2 0.028(3) 0.020(2) 0.020(2) -0.0011(19) 0.002(2) 0.005(2) C26 0.025(3) 0.035(3) 0.028(3) 0.002(2) -0.004(2) 0.002(2) C13 0.031(3) 0.024(3) 0.023(3) 0.000(2) 0.003(2) -0.001(2) C18 0.045(4) 0.032(3) 0.021(3) 0.002(2) 0.002(2) 0.000(3) C31 0.022(3) 0.026(3) 0.025(3) -0.003(2) -0.004(2) 0.002(2) C30 0.032(3) 0.031(3) 0.030(3) -0.004(2) -0.002(2) 0.002(2) C4 0.039(3) 0.028(3) 0.024(3) -0.001(2) -0.001(2) -0.005(2) C12 0.040(4) 0.033(3) 0.031(3) -0.003(2) -0.009(3) 0.003(3) C17 0.047(4) 0.035(3) 0.028(3) 0.004(2) 0.000(3) 0.006(3) C36 0.030(3) 0.040(3) 0.029(3) -0.002(3) -0.001(2) 0.002(3) C6 0.033(3) 0.023(3) 0.026(3) -0.002(2) -0.003(2) 0.005(2) C32 0.027(3) 0.031(3) 0.032(3) -0.001(2) -0.001(2) -0.003(2) C24 0.038(3) 0.032(3) 0.022(3) 0.001(2) 0.002(2) 0.000(3) C27 0.038(3) 0.036(3) 0.031(3) 0.000(2) -0.012(3) 0.003(3) C23 0.053(4) 0.027(3) 0.027(3) -0.006(2) -0.003(3) 0.007(3) C14 0.046(4) 0.032(3) 0.033(3) 0.008(2) -0.009(3) -0.002(3) C20 0.040(4) 0.033(3) 0.024(3) 0.011(2) 0.007(2) 0.010(3) C10 0.027(3) 0.048(4) 0.043(3) 0.013(3) -0.009(3) -0.004(3) C35 0.031(3) 0.047(4) 0.035(3) -0.010(3) 0.000(3) 0.005(3) C22 0.050(4) 0.029(3) 0.030(3) -0.005(2) 0.009(3) 0.013(3) C34 0.036(4) 0.033(3) 0.054(4) -0.012(3) -0.007(3) 0.006(3) C29 0.042(4) 0.034(3) 0.026(3) -0.009(2) 0.009(3) -0.001(3) C11 0.043(4) 0.043(4) 0.032(3) 0.001(3) -0.016(3) -0.003(3) C33 0.032(3) 0.024(3) 0.054(4) 0.006(3) -0.013(3) 0.000(3) C8 0.037(3) 0.039(3) 0.020(3) -0.003(2) 0.002(2) 0.004(3) C21 0.033(3) 0.049(4) 0.031(3) 0.003(3) 0.012(3) 0.007(3) C16 0.051(4) 0.024(3) 0.046(4) 0.004(3) 0.000(3) -0.007(3) C28 0.052(4) 0.039(3) 0.024(3) -0.004(2) -0.001(3) -0.004(3) C9 0.035(3) 0.045(4) 0.041(3) 0.003(3) 0.002(3) 0.011(3) C15 0.045(4) 0.035(3) 0.056(4) 0.006(3) -0.018(3) -0.012(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Sb Sb -0.0562 5.8946 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F1 Sb1 O1 82.64(14) . . ? F1 Sb1 C19 168.81(17) . . ? F1 Sb1 C1 82.62(16) . . ? F1 Sb1 C7 90.98(18) . . ? F1 Sb1 C13 82.75(18) . . ? C19 Sb1 O1 86.25(17) . . ? C1 Sb1 O1 78.67(17) . . ? C1 Sb1 C19 93.9(2) . . ? C7 Sb1 O1 172.87(18) . . ? C7 Sb1 C19 100.0(2) . . ? C7 Sb1 C1 97.4(2) . . ? C13 Sb1 O1 84.25(18) . . ? C13 Sb1 C19 97.5(2) . . ? C13 Sb1 C1 158.8(2) . . ? C13 Sb1 C7 98.2(2) . . ? O1 P1 C25 114.5(2) . . ? O1 P1 C2 106.9(2) . . ? O1 P1 C31 109.6(2) . . ? C25 P1 C31 108.2(3) . . ? C2 P1 C25 106.4(3) . . ? C2 P1 C31 111.3(2) . . ? P1 O1 Sb1 116.7(2) . . ? C26 C25 P1 120.0(4) . . ? C30 C25 P1 120.5(4) . . ? C30 C25 C26 119.5(5) . . ? C24 C19 Sb1 119.6(4) . . ? C20 C19 Sb1 121.5(4) . . ? C20 C19 C24 118.8(5) . . ? C2 C1 Sb1 121.0(4) . . ? C6 C1 Sb1 120.3(4) . . ? C6 C1 C2 118.8(5) . . ? C4 C5 H5 119.9 . . ? C4 C5 C6 120.2(5) . . ? C6 C5 H5 119.9 . . ? C12 C7 Sb1 122.0(4) . . ? C8 C7 Sb1 119.6(4) . . ? C8 C7 C12 118.4(5) . . ? C2 C3 H3 120.3 . . ? C4 C3 H3 120.3 . . ? C4 C3 C2 119.4(5) . . ? C1 C2 P1 116.6(4) . . ? C1 C2 C3 120.9(5) . . ? C3 C2 P1 122.5(4) . . ? C25 C26 H26 120.2 . . ? C27 C26 C25 119.7(6) . . ? C27 C26 H26 120.2 . . ? C18 C13 Sb1 118.3(4) . . ? C14 C13 Sb1 122.8(4) . . ? C14 C13 C18 118.8(6) . . ? C13 C18 H18 119.8 . . ? C13 C18 C17 120.5(6) . . ? C17 C18 H18 119.8 . . ? C36 C31 P1 118.7(4) . . ? C36 C31 C32 119.7(5) . . ? C32 C31 P1 121.5(4) . . ? C25 C30 H30 119.4 . . ? C25 C30 C29 121.3(6) . . ? C29 C30 H30 119.4 . . ? C5 C4 C3 119.8(5) . . ? C5 C4 H4 120.1 . . ? C3 C4 H4 120.1 . . ? C7 C12 H12 119.5 . . ? C11 C12 C7 121.0(6) . . ? C11 C12 H12 119.5 . . ? C18 C17 H17 119.5 . . ? C16 C17 C18 120.9(6) . . ? C16 C17 H17 119.5 . . ? C31 C36 H36 120.0 . . ? C35 C36 C31 120.1(6) . . ? C35 C36 H36 120.0 . . ? C1 C6 C5 120.9(5) . . ? C1 C6 H6 119.5 . . ? C5 C6 H6 119.5 . . ? C31 C32 H32 120.3 . . ? C33 C32 C31 119.5(6) . . ? C33 C32 H32 120.3 . . ? C19 C24 H24 120.1 . . ? C19 C24 C23 119.8(6) . . ? C23 C24 H24 120.1 . . ? C26 C27 H27 119.9 . . ? C28 C27 C26 120.1(6) . . ? C28 C27 H27 119.9 . . ? C24 C23 H23 119.7 . . ? C22 C23 C24 120.6(6) . . ? C22 C23 H23 119.7 . . ? C13 C14 H14 119.8 . . ? C13 C14 C15 120.4(6) . . ? C15 C14 H14 119.8 . . ? C19 C20 H20 118.9 . . ? C19 C20 C21 122.2(6) . . ? C21 C20 H20 118.9 . . ? C11 C10 H10 120.4 . . ? C11 C10 C9 119.1(6) . . ? C9 C10 H10 120.4 . . ? C36 C35 H35 120.3 . . ? C34 C35 C36 119.3(6) . . ? C34 C35 H35 120.3 . . ? C23 C22 H22 120.1 . . ? C23 C22 C21 119.8(5) . . ? C21 C22 H22 120.1 . . ? C35 C34 H34 119.7 . . ? C33 C34 C35 120.7(6) . . ? C33 C34 H34 119.7 . . ? C30 C29 H29 120.6 . . ? C30 C29 C28 118.9(6) . . ? C28 C29 H29 120.6 . . ? C12 C11 C10 120.1(6) . . ? C12 C11 H11 119.9 . . ? C10 C11 H11 119.9 . . ? C32 C33 H33 119.6 . . ? C34 C33 C32 120.7(6) . . ? C34 C33 H33 119.6 . . ? C7 C8 H8 119.6 . . ? C9 C8 C7 120.8(6) . . ? C9 C8 H8 119.6 . . ? C20 C21 H21 120.6 . . ? C22 C21 C20 118.9(6) . . ? C22 C21 H21 120.6 . . ? C17 C16 H16 120.8 . . ? C17 C16 C15 118.5(6) . . ? C15 C16 H16 120.8 . . ? C27 C28 C29 120.5(6) . . ? C27 C28 H28 119.7 . . ? C29 C28 H28 119.7 . . ? C10 C9 H9 119.8 . . ? C8 C9 C10 120.5(6) . . ? C8 C9 H9 119.8 . . ? C14 C15 H15 119.5 . . ? C16 C15 C14 120.9(6) . . ? C16 C15 H15 119.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb1 F1 2.028(3) . ? Sb1 O1 2.342(4) . ? Sb1 C19 2.188(5) . ? Sb1 C1 2.173(5) . ? Sb1 C7 2.156(5) . ? Sb1 C13 2.144(6) . ? P1 O1 1.520(4) . ? P1 C25 1.801(5) . ? P1 C2 1.795(6) . ? P1 C31 1.803(6) . ? C25 C26 1.397(8) . ? C25 C30 1.377(8) . ? C19 C24 1.390(8) . ? C19 C20 1.370(8) . ? C1 C2 1.386(7) . ? C1 C6 1.379(8) . ? C5 H5 0.9500 . ? C5 C4 1.383(8) . ? C5 C6 1.399(8) . ? C7 C12 1.391(8) . ? C7 C8 1.384(8) . ? C3 H3 0.9500 . ? C3 C2 1.412(7) . ? C3 C4 1.384(8) . ? C26 H26 0.9500 . ? C26 C27 1.389(8) . ? C13 C18 1.388(8) . ? C13 C14 1.372(9) . ? C18 H18 0.9500 . ? C18 C17 1.390(9) . ? C31 C36 1.397(8) . ? C31 C32 1.398(8) . ? C30 H30 0.9500 . ? C30 C29 1.382(8) . ? C4 H4 0.9500 . ? C12 H12 0.9500 . ? C12 C11 1.383(9) . ? C17 H17 0.9500 . ? C17 C16 1.366(10) . ? C36 H36 0.9500 . ? C36 C35 1.394(9) . ? C6 H6 0.9500 . ? C32 H32 0.9500 . ? C32 C33 1.388(9) . ? C24 H24 0.9500 . ? C24 C23 1.396(8) . ? C27 H27 0.9500 . ? C27 C28 1.377(10) . ? C23 H23 0.9500 . ? C23 C22 1.383(9) . ? C14 H14 0.9500 . ? C14 C15 1.390(9) . ? C20 H20 0.9500 . ? C20 C21 1.392(9) . ? C10 H10 0.9500 . ? C10 C11 1.384(10) . ? C10 C9 1.387(10) . ? C35 H35 0.9500 . ? C35 C34 1.392(10) . ? C22 H22 0.9500 . ? C22 C21 1.383(10) . ? C34 H34 0.9500 . ? C34 C33 1.370(10) . ? C29 H29 0.9500 . ? C29 C28 1.395(10) . ? C11 H11 0.9500 . ? C33 H33 0.9500 . ? C8 H8 0.9500 . ? C8 C9 1.382(9) . ? C21 H21 0.9500 . ? C16 H16 0.9500 . ? C16 C15 1.387(9) . ? C28 H28 0.9500 . ? C9 H9 0.9500 . ? C15 H15 0.9500 . ?