#------------------------------------------------------------------------------ #$Date: 2022-02-04 21:33:56 +0200 (Fri, 04 Feb 2022) $ #$Revision: 272658 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/89/7708930.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708930 loop_ _publ_author_name 'Kajiwara, Yuu' 'Miyata, Seiya' 'Nakai, Hidetaka' _publ_section_title ; Unusual motion of the n-methoxypropyl moiety observed in the photochromic crystals of an organorhodium dithionite complex with n-methoxypropyltetramethylcyclopentadienyl ligands. ; _journal_issue 1 _journal_name_full 'Dalton transactions (Cambridge, England : 2003)' _journal_page_first 48 _journal_page_last 52 _journal_paper_doi 10.1039/d1dt03347f _journal_volume 51 _journal_year 2021 _chemical_absolute_configuration 'CHOOSE rm ad rmad syn or unk' _chemical_formula_moiety 'C28 H46 O6 Rh2 S2' _chemical_formula_sum 'C28 H46 O6 Rh2 S2' _chemical_formula_weight 748.60 _space_group_crystal_system monoclinic _space_group_IT_number 9 _space_group_name_Hall 'C -2yc' _space_group_name_H-M_alt 'C 1 c 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_update_record ; 2021-10-02 deposited with the CCDC. 2021-11-25 downloaded from the CCDC. ; _cell_angle_alpha 90.0000 _cell_angle_beta 92.884(4) _cell_angle_gamma 90.0000 _cell_formula_units_Z 4 _cell_length_a 15.1520(6) _cell_length_b 19.2929(11) _cell_length_c 10.7055(5) _cell_measurement_reflns_used 8320 _cell_measurement_temperature 296 _cell_measurement_theta_max 31.29 _cell_measurement_theta_min 3.44 _cell_volume 3125.5(3) _computing_cell_refinement 'CrysAlisPro 1.171.39.20a (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.39.20a (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.39.20a (Rigaku OD, 2015)' _computing_molecular_graphics 'CrystalStructure 4.2.2' _computing_publication_material 'CrystalStructure 4.2.2 (Rigaku, 2016)' _computing_structure_refinement 'SHELXL Version 2014/7 (Sheldrick, 2008)' _computing_structure_solution 'SHELXT Version 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 296 _diffrn_detector_area_resol_mean 5.811 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.909 _diffrn_measurement_device_type 'Rigaku XtaLAB P200' _diffrn_measurement_method \w _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0363 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.909 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 18758 _diffrn_reflns_point_group_measured_fraction_full 0.926 _diffrn_reflns_point_group_measured_fraction_max 0.795 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.266 _diffrn_reflns_theta_min 2.610 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.225 _exptl_absorpt_correction_T_max 0.885 _exptl_absorpt_correction_T_min 0.816 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.20a (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow-orange _exptl_crystal_density_diffrn 1.591 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 1536.00 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.100 _refine_diff_density_max 1.21 _refine_diff_density_min -0.55 _refine_ls_abs_structure_details ; Flack x determined using 2656 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack -0.06(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_hydrogen_treatment constr _refine_ls_number_parameters 370 _refine_ls_number_reflns 8106 _refine_ls_number_restraints 2 _refine_ls_R_factor_all 0.0523 _refine_ls_R_factor_gt 0.0422 _refine_ls_shift/su_max 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w = 1/[\s^2^(Fo^2^)+(0.0523P)^2^+4.2557P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1033 _refine_ls_wR_factor_ref 0.1088 _reflns_Friedel_coverage 0.748 _reflns_Friedel_fraction_full 0.854 _reflns_Friedel_fraction_max 0.681 _reflns_number_gt 6973 _reflns_number_total 8106 _reflns_threshold_expression F^2^>2.0\s(F^2^) _cod_data_source_file d1dt03347f2.cif _cod_data_source_block sample4 _cod_depositor_comments 'Adding full bibliography for 7708925--7708931.cif.' _cod_database_code 7708930 _shelx_res_file ; shelxl.res created by SHELXL-2014/7 TITL sample4 CELL 0.71075 15.15200 19.29290 10.70550 90.00000 92.88400 90.00000 ZERR 4 0.00060 0.00110 0.00050 0.00000 0.00400 0.00000 LATT -7 SYMM +X, -Y, .50+Z SFAC C H RH S O UNIT 112 184 8 8 24 L.S. 30 FMAP 2 PLAN 5 WPDB -2 HTAB BOND $H CONF LIST 4 TEMP 23.0 ACTA SIZE 0.200 0.150 0.100 WGHT 0.052300 4.255700 FVAR 0.22123 RH1 3 0.561828 0.141783 0.447820 11.00000 0.03783 0.04647 = 0.04144 0.00084 0.00557 -0.00311 RH2 3 0.487892 0.228085 0.601080 11.00000 0.03161 0.05492 = 0.04308 -0.00720 -0.00478 0.00186 S1 4 0.695606 0.144286 0.556125 11.00000 0.03685 0.10683 = 0.06864 -0.00105 -0.00205 0.01510 S2 4 0.612252 0.236309 0.730869 11.00000 0.04588 0.11996 = 0.07005 -0.03132 -0.02465 0.01123 O1 5 0.715767 0.091396 0.634936 10.74000 0.06524 0.13046 = 0.12419 0.04356 0.00841 0.03007 O2 5 0.764790 0.173905 0.487456 10.86000 0.05526 0.13107 = 0.11176 0.01838 0.00488 -0.01979 O3 5 0.606256 0.199652 0.844361 10.95000 0.10041 0.14553 = 0.08174 0.00655 -0.04509 0.02085 O4 5 0.659232 0.294961 0.723493 10.51000 0.05903 0.14923 = 0.09982 -0.02857 -0.01540 -0.01715 O5 5 0.677604 0.162622 0.698212 10.31000 0.04371 0.08236 = 0.05788 -0.00439 -0.01693 0.02644 O6 5 0.698196 0.220857 0.646277 10.63000 0.03757 0.12266 = 0.09624 -0.02215 -0.01480 -0.00353 O7 5 0.237073 -0.026302 0.387783 11.00000 0.10400 0.22368 = 0.16662 -0.03638 0.03382 -0.07670 O8 5 0.499965 0.545032 0.670218 11.00000 0.10759 0.07789 = 0.19488 0.02204 -0.01230 -0.00713 C1 1 0.463937 0.083535 0.318364 11.00000 0.05267 0.05443 = 0.05934 -0.01116 0.00883 -0.01061 C2 1 0.525924 0.035550 0.370756 11.00000 0.07209 0.04925 = 0.06308 -0.00747 0.01808 -0.00685 C3 1 0.610727 0.053757 0.332329 11.00000 0.06973 0.07148 = 0.07242 -0.02306 0.00767 0.00662 C4 1 0.601125 0.113626 0.257682 11.00000 0.06996 0.08781 = 0.05493 -0.01921 0.02674 -0.02340 C5 1 0.511385 0.131926 0.245836 11.00000 0.10010 0.05530 = 0.04321 -0.00521 -0.00425 -0.00832 C6 1 0.366298 0.078229 0.331053 11.00000 0.05056 0.08823 = 0.10252 -0.03755 0.00733 -0.00581 AFIX 23 H6A 2 0.339690 0.123531 0.317759 11.00000 -1.20000 H6B 2 0.354706 0.063421 0.415252 11.00000 -1.20000 AFIX 0 C7 1 0.506747 -0.027139 0.446458 11.00000 0.15024 0.05204 = 0.09961 0.01300 0.01298 -0.01409 AFIX 137 H7A 2 0.539414 -0.024707 0.525529 11.00000 -1.20000 H7B 2 0.523831 -0.067954 0.402420 11.00000 -1.20000 H7C 2 0.444660 -0.029079 0.460117 11.00000 -1.20000 AFIX 0 C8 1 0.692407 0.013406 0.355371 11.00000 0.07905 0.12257 = 0.15656 -0.06528 0.00566 0.02754 AFIX 137 H8A 2 0.693429 -0.024362 0.297079 11.00000 -1.20000 H8B 2 0.694395 -0.004497 0.439133 11.00000 -1.20000 H8C 2 0.742653 0.042769 0.344923 11.00000 -1.20000 AFIX 0 C9 1 0.676739 0.145017 0.189784 11.00000 0.12016 0.14959 = 0.08648 -0.02362 0.05818 -0.06104 AFIX 137 H9A 2 0.660723 0.190764 0.161590 11.00000 -1.20000 H9B 2 0.689177 0.116631 0.119147 11.00000 -1.20000 H9C 2 0.728268 0.147562 0.245556 11.00000 -1.20000 AFIX 0 C10 1 0.473329 0.186486 0.163672 11.00000 0.16171 0.08867 = 0.06095 0.01060 -0.01506 0.00325 AFIX 137 H10A 2 0.476232 0.172390 0.077977 11.00000 -1.20000 H10B 2 0.506124 0.228645 0.176957 11.00000 -1.20000 H10C 2 0.412790 0.194036 0.182452 11.00000 -1.20000 AFIX 0 C11 1 0.324077 0.026846 0.237154 11.00000 0.05977 0.12457 = 0.11632 -0.04779 0.00474 -0.02445 AFIX 23 H11A 2 0.323112 0.046613 0.153785 11.00000 -1.20000 H11B 2 0.358819 -0.015381 0.237008 11.00000 -1.20000 AFIX 0 C12 1 0.230575 0.010216 0.271682 11.00000 0.06783 0.21274 = 0.14457 -0.07788 0.00932 -0.04675 AFIX 23 H12A 2 0.196885 0.052558 0.280201 11.00000 -1.20000 H12B 2 0.201235 -0.018218 0.207432 11.00000 -1.20000 AFIX 0 C13 1 0.160802 -0.044275 0.437570 11.00000 0.12135 0.45060 = 0.15135 -0.04531 0.05970 -0.10654 AFIX 33 H13A 2 0.173154 -0.068376 0.514936 11.00000 -1.20000 H13B 2 0.126967 -0.003354 0.452910 11.00000 -1.20000 H13C 2 0.127740 -0.073951 0.380470 11.00000 -1.20000 AFIX 0 C14 1 0.419936 0.330797 0.610814 11.00000 0.03821 0.05674 = 0.07676 0.00518 -0.00160 0.00715 C15 1 0.419441 0.299496 0.730585 11.00000 0.03892 0.07077 = 0.05780 0.00111 -0.00542 0.01139 C16 1 0.369105 0.237083 0.719978 11.00000 0.04991 0.05837 = 0.06472 -0.00284 0.02113 0.01356 C17 1 0.335204 0.231897 0.595206 11.00000 0.03648 0.06721 = 0.07455 -0.01873 0.00848 -0.00170 C18 1 0.365376 0.288597 0.526106 11.00000 0.03412 0.07577 = 0.06170 0.00147 -0.00838 0.01011 C19 1 0.459431 0.399460 0.582776 11.00000 0.04108 0.06594 = 0.12441 0.01615 0.00114 0.00701 AFIX 23 H19A 2 0.473584 0.400961 0.495454 11.00000 -1.20000 H19B 2 0.513951 0.405324 0.633123 11.00000 -1.20000 AFIX 0 C20 1 0.458499 0.327881 0.850365 11.00000 0.07228 0.09230 = 0.08441 -0.03747 -0.00745 0.02097 AFIX 137 H20A 2 0.412088 0.338902 0.904877 11.00000 -1.20000 H20B 2 0.491503 0.369059 0.833797 11.00000 -1.20000 H20C 2 0.497084 0.293977 0.889629 11.00000 -1.20000 AFIX 0 C21 1 0.344379 0.190644 0.826509 11.00000 0.10293 0.07783 = 0.11029 0.02044 0.04891 0.01274 AFIX 137 H21A 2 0.305859 0.215280 0.879492 11.00000 -1.20000 H21B 2 0.396871 0.177019 0.874210 11.00000 -1.20000 H21C 2 0.314709 0.150152 0.793455 11.00000 -1.20000 AFIX 0 C22 1 0.267038 0.180471 0.549300 11.00000 0.04680 0.11756 = 0.13658 -0.04573 0.01437 -0.01245 AFIX 137 H22A 2 0.258888 0.183895 0.460004 11.00000 -1.20000 H22B 2 0.212132 0.190021 0.586880 11.00000 -1.20000 H22C 2 0.286387 0.134525 0.571582 11.00000 -1.20000 AFIX 0 C23 1 0.340036 0.306325 0.393767 11.00000 0.05569 0.18430 = 0.07171 0.02331 -0.01490 0.02201 AFIX 137 H23A 2 0.278626 0.318726 0.386837 11.00000 -1.20000 H23B 2 0.350081 0.267005 0.341394 11.00000 -1.20000 H23C 2 0.375063 0.344675 0.367743 11.00000 -1.20000 AFIX 0 C24 1 0.395571 0.459438 0.610137 11.00000 0.05527 0.08581 = 0.23626 0.05506 0.00847 0.00913 AFIX 23 H24A 2 0.341365 0.453271 0.559213 11.00000 -1.20000 H24B 2 0.380776 0.456956 0.697131 11.00000 -1.20000 AFIX 0 C25 1 0.431807 0.529084 0.585429 11.00000 0.08429 0.07370 = 0.19490 0.04121 0.00351 0.03382 AFIX 23 H25A 2 0.453022 0.530418 0.501473 11.00000 -1.20000 H25B 2 0.385354 0.563409 0.590565 11.00000 -1.20000 AFIX 0 C26 1 0.531802 0.609821 0.655220 11.00000 0.21606 0.09964 = 0.11626 -0.00628 -0.01422 0.01909 AFIX 137 H26A 2 0.483763 0.642319 0.652168 11.00000 -1.20000 H26B 2 0.562009 0.612172 0.578629 11.00000 -1.20000 H26C 2 0.572236 0.620966 0.724214 11.00000 -1.20000 AFIX 0 C27 1 0.502362 0.123281 0.612722 11.00000 0.05256 0.05941 = 0.04561 0.00581 0.00761 0.01134 AFIX 23 H27A 2 0.447853 0.096910 0.605040 11.00000 -1.20000 H27B 2 0.541459 0.107024 0.681058 11.00000 -1.20000 AFIX 0 C28 1 0.563944 0.247376 0.451878 11.00000 0.04922 0.03870 = 0.06645 -0.01088 0.00685 -0.00475 AFIX 23 H28A 2 0.533565 0.269996 0.381131 11.00000 -1.20000 H28B 2 0.621224 0.267943 0.472696 11.00000 -1.20000 AFIX 0 HKLF 4 REM sample4 REM R1 = 0.0422 for 6973 Fo > 4sig(Fo) and 0.0523 for all 8106 data REM 370 parameters refined using 2 restraints END WGHT 0.0515 4.3982 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 1.210, deepest hole -0.553, 1-sigma level 0.093 Q1 1 0.5101 0.2611 0.5815 11.00000 0.05 1.14 Q2 1 0.5400 0.1633 0.3947 11.00000 0.05 1.04 Q3 1 0.5828 0.1604 0.5048 11.00000 0.05 0.89 Q4 1 0.4751 0.2590 0.6420 11.00000 0.05 0.82 Q5 1 0.6366 0.2223 0.2983 11.00000 0.05 0.76 ; _shelx_res_checksum 55474 _shelx_hkl_file ; 0 0 2 973.37 38.36 0 0 3 1.39 0.68 0 0 4 645.00 26.06 0 0 4 703.90 26.32 0 0 -4 674.90 26.92 0 0 5 -0.03 1.32 0 0 5 0.86 0.44 0 0 -5 0.64 1.18 0 0 6 1118.59 45.07 0 0 6 1231.38 45.53 0 0 -6 1295.04 51.48 0 0 7 -2.86 2.79 0 0 7 -0.33 0.59 0 0 -7 -1.74 1.89 0 0 8 678.81 27.74 0 0 8 831.81 28.61 0 0 -8 840.89 33.99 0 0 9 -2.64 3.54 0 0 -9 -2.58 3.18 0 0 -9 -3.20 2.66 0 0 10 47.66 4.95 0 0 -10 43.86 4.07 0 0 -10 40.21 4.57 0 0 11 -4.99 4.81 0 0 -11 -4.44 4.59 0 0 -11 -4.97 3.71 0 0 12 79.22 6.89 0 0 -12 91.58 6.99 0 0 -12 87.73 6.24 0 0 13 0.07 6.20 0 0 -13 1.57 5.55 0 0 -13 -0.31 4.61 0 0 14 77.09 7.95 0 0 -14 81.25 8.21 0 0 -14 88.04 7.12 0 -2 1 3853.83 151.36 0 2 1 3861.29 151.38 0 2 2 2500.07 92.11 0 -2 2 2360.12 92.08 0 2 -2 2319.45 92.20 0 -2 -2 2381.26 92.23 0 -2 3 187.16 7.64 0 2 3 180.64 7.83 0 2 3 203.82 7.84 0 2 -3 157.82 6.52 0 -2 -3 166.97 6.66 0 2 4 78.47 3.59 0 -2 4 76.16 3.27 0 2 4 76.96 3.60 0 -2 -4 75.49 3.48 0 2 -4 76.46 3.25 0 -2 5 563.75 22.32 0 2 5 552.95 22.46 0 -2 5 544.89 22.12 0 2 5 586.42 22.51 0 -2 -5 559.83 21.52 0 -2 -5 529.92 21.56 0 2 -5 524.08 21.19 0 2 6 412.39 16.73 0 -2 6 451.38 16.58 0 -2 6 458.95 16.22 0 -2 -6 406.01 17.05 0 -2 -6 432.18 17.20 0 -2 7 343.98 13.84 0 -2 7 332.90 13.31 0 2 7 317.81 13.23 0 -2 -7 388.26 16.03 0 -2 -7 415.00 15.96 0 2 8 326.60 11.95 0 -2 8 353.74 11.68 0 -2 -8 343.71 14.63 0 -2 -8 359.48 14.52 0 2 -8 324.85 14.60 0 2 9 132.98 6.32 0 -2 9 152.06 6.01 0 -2 -9 150.19 7.45 0 -2 -9 142.61 7.03 0 2 -9 145.30 7.35 0 -2 10 42.83 4.58 0 2 10 46.51 5.09 0 -2 -10 37.13 3.62 0 2 -10 36.96 4.06 0 -2 -10 46.08 4.50 0 -2 11 65.73 5.68 0 2 11 72.57 6.35 0 -2 -11 60.46 4.86 0 -2 -11 80.03 5.98 0 2 -11 70.69 5.47 0 2 12 27.40 6.25 0 -2 12 23.77 5.35 0 -2 -12 23.57 5.21 0 -2 -12 21.34 4.01 0 2 -12 32.02 4.94 0 2 -12 28.55 5.81 0 -2 13 23.33 5.98 0 2 13 29.07 6.77 0 2 -13 30.61 6.44 0 -2 -13 32.15 6.08 0 -2 -13 33.03 4.74 0 2 -13 26.05 5.43 0 -2 14 27.14 6.54 0 2 14 16.57 7.18 0 2 -14 34.13 6.91 0 -2 -14 30.18 6.61 0 2 -14 26.11 6.00 0 -2 -14 25.88 5.32 0 2 15 -1.15 7.66 0 -4 0 255.40 10.22 0 4 -1 944.12 37.18 0 -4 -1 945.53 37.31 0 4 2 1012.15 40.25 0 4 2 1022.57 40.13 0 4 -2 984.33 38.89 0 4 3 1319.72 51.52 0 4 3 1288.37 51.62 0 -4 -3 1234.84 50.30 0 -4 -3 1316.90 50.43 0 4 -3 1286.88 50.31 0 -4 4 779.66 32.49 0 4 4 846.09 32.75 0 4 4 867.83 32.73 0 -4 -4 833.14 32.64 0 -4 -4 848.14 32.78 0 4 -4 796.95 32.56 0 4 5 477.96 19.09 0 4 5 464.95 19.12 0 -4 5 467.84 18.77 0 4 -5 454.56 16.11 0 -4 -5 448.14 16.26 0 -4 -5 464.00 16.47 0 4 6 181.66 7.68 0 4 6 165.20 7.84 0 -4 -6 177.04 6.57 0 -4 -6 171.34 6.31 0 4 -6 163.79 5.99 0 -4 7 271.01 11.46 0 4 7 285.56 11.70 0 4 7 261.90 11.93 0 -4 -7 289.78 9.98 0 -4 -7 280.67 9.67 0 -4 8 362.67 14.06 0 4 8 386.43 14.65 0 -4 -8 408.19 12.77 0 -4 -8 393.21 12.33 0 4 9 10.04 4.33 0 -4 9 12.15 3.25 0 4 9 8.62 0.87 0 -4 -9 16.68 3.24 0 -4 -9 19.94 2.39 0 4 -9 10.05 3.51 0 4 10 281.58 12.64 0 -4 10 261.91 11.91 0 -4 -10 292.62 12.42 0 4 -10 268.03 12.83 0 -4 -10 284.16 12.86 0 -4 11 11.15 4.14 0 4 11 10.84 5.56 0 -4 -11 2.00 2.97 0 4 -11 7.52 4.52 0 -4 -11 7.49 4.20 0 -4 12 14.83 4.84 0 4 12 24.18 6.14 0 -4 -12 21.35 3.69 0 -4 -12 21.74 4.94 0 4 -12 23.57 5.23 0 4 13 18.31 6.98 0 -4 13 19.06 5.59 0 -4 -13 18.52 3.98 0 4 -13 13.74 5.59 0 -4 -13 22.01 5.67 0 4 14 -1.53 7.52 0 -4 14 0.06 5.76 0 -4 -14 0.75 5.75 0 4 -14 -0.09 5.86 0 -4 -14 -0.24 4.27 0 4 15 -0.50 8.26 0 -6 0 42.18 2.04 0 6 1 1119.22 44.45 0 -6 1 1126.83 44.30 0 6 -1 1086.24 42.59 0 -6 -1 1071.39 42.74 0 6 2 1580.73 62.38 0 6 -2 1538.21 60.60 0 6 -2 1553.43 60.43 0 -6 -2 1497.71 60.64 0 6 3 1254.01 49.73 0 -6 3 1230.54 49.68 0 6 3 1337.60 49.94 0 6 -3 1205.81 47.73 0 6 4 529.31 21.49 0 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84.15 4.76 0 14 -7 73.89 3.93 0 14 -7 79.70 4.61 0 14 8 42.90 3.41 0 14 8 40.72 4.55 0 14 -8 36.56 3.28 0 14 -8 38.65 2.72 0 14 9 45.66 3.46 0 14 9 38.89 4.47 0 14 -9 26.97 2.53 0 14 -9 29.44 3.03 0 14 10 18.77 4.40 0 14 10 17.13 6.67 0 -14 10 11.96 1.30 0 14 10 20.84 3.21 0 14 -10 16.99 2.69 0 14 11 8.21 4.09 0 14 11 5.30 2.91 0 14 -11 8.83 2.53 0 14 -11 7.83 6.73 0 14 -11 6.79 6.58 0 14 -12 16.89 7.36 0 -16 0 73.53 4.63 0 -16 0 76.83 3.90 0 -16 1 126.24 5.92 0 -16 1 121.88 6.39 0 -16 -1 152.69 7.61 0 -16 -1 159.48 7.21 0 16 2 54.09 4.79 0 -16 2 47.36 2.92 0 -16 -2 57.58 3.57 0 16 -2 49.88 4.49 0 16 3 252.76 10.19 0 16 3 256.08 10.99 0 -16 -3 242.09 10.25 0 16 -3 210.73 10.60 0 16 4 34.18 2.84 0 16 4 32.86 2.03 0 16 4 35.47 4.61 0 -16 4 31.80 2.11 0 -16 -4 30.76 3.07 0 16 -4 30.35 3.62 0 16 5 116.02 5.90 0 -16 5 118.90 5.12 0 16 5 114.32 5.19 0 -16 5 113.27 6.35 0 16 5 117.23 6.97 0 -16 -5 125.22 6.43 0 16 -5 118.20 6.49 0 16 6 28.12 2.85 0 -16 6 27.61 1.62 0 16 6 27.86 4.80 0 -16 6 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20 -5 12.04 4.59 0 -20 -5 13.82 3.09 0 -20 6 7.92 1.14 0 20 6 13.16 2.66 0 20 6 8.08 6.14 0 -20 6 8.61 4.52 0 20 -6 5.75 4.19 0 -20 7 24.13 4.70 0 20 7 33.88 6.42 0 20 7 39.90 3.56 0 20 -7 33.02 4.75 0 20 8 23.13 6.41 0 20 8 20.30 3.31 0 20 -8 24.81 4.35 0 20 9 3.10 6.33 0 20 9 8.85 3.08 0 20 -9 7.26 3.86 0 20 10 21.76 3.67 0 20 -10 16.26 3.92 0 -22 0 94.35 5.14 0 22 0 95.11 7.80 0 -22 0 74.90 6.16 0 22 1 12.41 6.23 0 -22 1 14.61 2.52 0 -22 -1 12.15 5.16 0 -22 -1 9.60 2.69 0 22 2 16.32 6.20 0 -22 2 17.20 2.35 0 -22 -2 13.91 5.47 0 22 -2 19.74 5.81 0 -22 -2 17.48 2.89 0 22 3 19.53 6.33 0 -22 3 18.07 2.21 0 22 3 20.32 2.84 0 -22 -3 10.82 5.84 0 -22 -3 21.73 3.09 0 22 -3 19.69 5.78 0 -22 4 5.73 1.76 0 22 4 6.95 1.19 0 22 4 8.37 2.60 0 22 -4 6.25 5.26 0 -22 -4 4.66 5.80 0 -22 -4 11.81 3.03 0 22 5 6.49 6.65 0 -22 5 1.73 5.54 0 22 5 10.31 2.68 0 22 5 5.92 1.06 0 -22 5 2.50 1.48 0 22 -5 7.53 5.41 0 22 6 36.17 7.30 0 -22 6 30.07 5.78 0 22 6 41.09 3.81 0 22 -6 40.93 5.86 0 22 7 14.25 3.18 0 22 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66.92 6.71 -1 1 13 58.50 7.09 1 -1 -12 35.16 5.44 1 1 -12 23.33 4.56 1 -1 -12 24.65 4.25 1 1 -12 18.10 5.34 -1 -1 12 19.19 5.32 -1 1 12 20.28 5.78 1 -1 -11 160.07 8.35 1 1 -11 171.99 8.59 1 1 -11 170.21 9.12 1 -1 -11 168.53 8.94 -1 1 11 158.93 8.92 -1 -1 11 167.40 8.73 1 -1 -10 65.82 5.18 1 1 -10 60.02 5.27 1 -1 -10 74.47 4.62 1 1 -10 69.39 4.84 -1 -1 10 61.21 5.30 -1 1 10 73.86 5.64 1 1 -9 29.71 3.75 1 -1 -9 35.57 3.56 1 -1 -9 31.18 3.02 1 1 -9 28.04 3.28 -1 -1 9 26.24 3.78 -1 1 9 33.45 3.97 1 1 -8 63.73 4.18 1 -1 -8 76.00 4.10 1 1 -8 67.13 4.39 1 -1 -8 79.71 4.36 -1 -1 8 63.55 4.29 -1 1 8 73.20 4.65 1 1 -7 1112.22 46.35 1 -1 -7 1200.27 46.31 1 -1 -7 1160.30 46.21 -1 -1 7 1128.12 44.11 -1 1 7 1084.59 44.22 1 -1 -6 227.94 9.68 1 -1 -6 223.95 9.60 -1 1 6 225.58 9.34 -1 -1 6 209.87 9.17 1 -1 -5 1563.19 61.88 -1 -1 5 1551.55 62.39 -1 1 5 1617.29 62.49 1 -1 -4 45.84 1.98 1 -1 -4 45.11 2.07 -1 -1 4 47.72 2.37 -1 1 4 51.12 2.49 1 -1 -3 37.72 2.20 1 -1 -3 53.95 2.21 -1 -1 3 41.48 1.87 -1 1 3 38.70 2.01 1 1 -2 2477.06 97.25 -1 -1 2 2285.41 90.29 -1 1 2 2325.31 90.40 1 -1 1 7124.74 279.46 -1 1 -1 7671.25 300.88 1 1 2 224.81 9.65 1 -1 2 253.01 9.62 -1 1 -2 293.26 9.92 -1 1 -2 193.02 9.95 1 -1 3 910.22 35.16 1 1 3 860.10 35.30 -1 1 -3 925.97 36.53 1 1 4 145.26 6.19 1 -1 4 144.65 5.95 -1 -1 -4 141.00 6.04 1 -1 5 346.16 13.77 1 1 5 335.38 13.77 1 1 5 358.19 14.14 -1 -1 -5 351.18 14.39 1 1 6 220.96 8.06 1 -1 6 172.37 8.44 1 -1 6 176.90 8.00 1 1 6 220.70 8.66 -1 -1 -6 225.36 8.42 -1 1 -6 162.72 8.25 1 -1 7 1472.12 56.85 1 1 7 1370.12 56.40 1 1 7 1442.44 56.91 1 -1 7 1473.34 56.44 -1 1 -7 1566.99 59.76 -1 -1 -7 1443.05 59.65 1 1 8 130.42 6.62 1 -1 8 113.91 6.39 1 1 8 131.00 5.31 1 -1 8 120.64 5.31 -1 -1 -8 139.34 6.30 -1 1 -8 112.70 6.27 1 -1 9 180.02 7.04 1 1 9 185.51 8.57 1 -1 9 184.01 8.36 -1 -1 -9 184.81 8.51 -1 1 -9 180.74 8.66 1 1 10 29.91 1.51 1 1 10 32.43 4.95 1 -1 10 30.14 4.67 1 -1 10 26.64 1.54 -1 -1 -10 32.29 4.43 -1 -1 -10 28.71 3.55 -1 1 -10 30.36 4.00 1 -1 11 11.28 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3.39 5 15 -10 4.93 2.34 -5 15 10 8.15 4.02 5 15 -9 19.48 2.72 5 -15 -9 24.60 3.74 -5 15 9 22.00 4.42 5 15 -8 63.95 4.21 -5 15 8 63.21 5.38 -5 15 8 68.25 4.04 5 15 -7 11.07 2.61 -5 -15 7 5.92 1.66 -5 15 7 9.20 1.97 -5 15 7 7.73 4.60 5 15 -6 111.89 5.96 5 -15 -6 121.51 6.32 -5 15 6 122.57 7.25 -5 15 6 128.66 5.92 5 -15 -5 68.92 4.44 -5 15 5 70.14 5.49 -5 15 5 62.30 3.38 5 -15 -4 11.04 4.92 5 -15 -4 12.35 2.49 -5 15 4 12.06 1.61 -5 15 4 13.17 4.36 5 -15 -3 129.63 7.95 5 -15 -3 139.12 6.84 -5 15 3 130.36 6.92 -5 15 3 109.74 5.13 5 -15 -2 169.76 7.98 5 -15 -2 170.05 8.93 -5 15 2 143.70 6.35 -5 15 2 159.07 7.99 5 -15 -1 1.64 4.32 5 -15 -1 -1.44 2.25 -5 15 1 4.39 3.85 5 -15 0 163.26 8.00 5 15 0 143.19 6.78 5 -15 0 166.20 8.26 -5 15 0 110.05 4.92 -5 15 0 156.62 7.04 5 15 1 147.71 7.08 5 -15 1 162.66 8.26 5 -15 1 164.33 8.26 -5 15 -1 131.01 5.91 5 -15 2 24.91 4.44 5 15 2 19.91 2.50 -5 15 -2 19.06 2.79 5 15 3 131.92 6.58 5 -15 3 135.31 7.51 -5 15 -3 135.10 6.19 -5 15 -3 130.74 7.14 -5 15 -3 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5.17 -7 5 -9 39.59 5.28 -7 5 -9 30.47 2.71 -7 5 -9 38.42 5.35 7 -5 10 6.19 2.22 7 5 10 11.47 5.94 7 5 10 11.30 2.37 7 5 10 10.82 2.83 -7 5 -10 8.49 2.13 -7 -5 -10 3.07 5.24 -7 5 -10 7.59 5.21 -7 5 -10 12.08 5.86 7 5 11 20.05 6.79 7 5 11 27.34 2.93 7 -5 11 23.40 2.83 -7 5 -11 27.59 6.43 -7 -5 -11 26.53 6.38 -7 5 -11 24.07 2.51 -7 5 -11 22.93 6.23 7 5 12 8.65 2.47 7 5 12 2.41 7.06 7 -5 12 8.93 2.55 -7 5 -12 7.04 6.90 -7 -5 -12 5.35 6.43 -7 5 -12 8.49 2.20 7 5 13 37.25 8.16 7 -5 13 36.84 7.97 -7 5 -13 28.66 7.46 7 -5 14 8.29 7.71 7 -7 -14 30.02 4.77 7 -7 -13 0.07 3.49 7 -7 -13 -1.80 2.62 7 7 -13 3.73 5.97 7 -7 -12 42.20 3.45 7 -7 -12 49.91 4.26 7 7 -12 44.66 6.16 7 -7 -12 44.30 3.32 7 -7 -11 2.61 2.05 7 -7 -11 4.64 2.47 7 -7 -11 3.96 2.78 7 -7 -11 5.33 2.06 7 -7 -10 23.34 2.50 7 -7 -10 23.69 3.00 7 -7 -10 17.91 2.65 7 -7 -10 21.99 2.24 7 -7 -9 32.31 3.12 7 -7 -9 28.48 2.69 7 -7 -9 32.30 2.72 7 7 -9 26.52 1.87 7 -7 -9 30.78 2.35 7 -7 -8 237.11 10.27 7 -7 -8 250.05 10.53 7 -7 -8 250.57 10.64 7 7 -8 233.03 10.08 7 -7 -8 265.31 10.98 7 -7 -7 58.87 3.53 7 -7 -7 62.49 3.83 7 -7 -7 71.19 4.13 -7 7 7 45.35 3.08 7 -7 -6 548.97 22.16 7 -7 -6 551.81 22.00 7 -7 -6 520.31 21.62 -7 -7 6 436.91 18.05 -7 7 6 498.50 18.54 7 7 -5 102.19 3.78 7 -7 -5 94.09 3.98 7 -7 -5 95.17 4.61 7 -7 -5 95.13 4.49 7 -7 -5 88.83 3.82 -7 7 5 86.42 4.64 7 -7 -4 96.20 4.77 7 7 -4 90.47 4.05 7 -7 -4 96.65 4.07 7 -7 -4 97.85 4.45 -7 7 4 91.40 4.80 7 -7 -3 205.80 8.95 7 -7 -3 215.62 9.17 -7 7 3 221.55 9.65 7 -7 -2 218.59 9.74 7 -7 -2 230.89 9.62 -7 7 2 226.20 9.89 7 -7 -1 489.84 20.13 7 -7 -1 494.33 19.63 -7 7 1 505.35 19.96 -7 -7 1 478.32 19.38 7 -7 0 1932.90 75.28 7 -7 0 1874.14 74.70 7 -7 0 1911.63 75.12 -7 7 0 1933.95 76.65 7 -7 1 359.52 14.60 -7 7 -1 306.92 13.15 -7 7 -1 296.58 12.40 -7 7 -1 351.27 13.20 -7 7 -1 333.29 13.07 7 -7 2 438.34 17.79 -7 7 -2 436.31 17.87 -7 7 -2 429.16 17.45 -7 7 -2 447.07 18.02 7 -7 3 358.91 15.62 7 7 3 393.37 15.74 -7 7 -3 368.52 15.01 -7 7 -3 352.62 14.53 -7 7 -3 364.56 14.80 -7 7 -3 339.27 14.96 7 -7 4 14.27 1.78 -7 7 -4 12.62 1.61 -7 7 -4 8.78 2.41 -7 7 -4 12.49 2.10 -7 7 -4 8.73 1.84 7 -7 5 27.45 2.48 7 7 5 39.02 2.70 -7 7 -5 32.43 3.36 -7 7 -5 35.66 2.50 -7 7 -5 34.11 3.61 -7 7 -5 31.87 2.93 7 -7 6 315.57 13.45 7 7 6 313.19 13.47 -7 7 -6 329.63 14.06 -7 7 -6 326.71 13.77 -7 7 -6 326.78 14.32 -7 7 -6 329.32 14.15 7 7 7 63.28 4.24 7 -7 7 81.70 4.36 -7 7 -7 87.87 4.98 -7 7 -7 88.30 6.05 -7 7 -7 81.21 5.80 -7 7 -7 88.36 4.58 7 -7 8 285.98 12.60 7 7 8 297.25 12.86 -7 7 -8 286.87 12.22 -7 7 -8 290.30 13.30 -7 7 -8 284.97 13.21 7 7 9 50.42 3.69 7 -7 9 40.01 3.33 7 7 9 37.62 5.87 -7 7 -9 36.03 5.66 -7 7 -9 39.18 2.86 -7 7 -9 38.91 5.84 7 7 10 4.24 2.31 7 7 10 3.78 2.50 7 7 10 -0.92 6.03 7 -7 10 3.02 2.26 -7 7 -10 11.15 5.81 -7 7 -10 6.47 1.96 -7 7 -10 6.05 5.60 7 7 11 25.20 7.07 7 7 11 19.47 2.77 7 -7 11 15.10 2.73 -7 7 -11 21.19 6.38 -7 7 -11 14.04 2.25 -7 7 -11 15.61 6.61 7 7 12 36.77 3.40 7 -7 12 32.42 3.29 7 7 12 35.69 7.70 -7 7 -12 27.13 2.60 -7 7 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181.83 8.65 -7 9 2 185.05 8.51 7 -9 -1 420.05 17.62 7 -9 -1 416.91 17.27 -7 9 1 402.94 15.31 -7 -9 1 350.37 14.38 7 -9 0 499.83 20.94 7 -9 0 504.84 20.87 7 -9 0 525.21 21.14 -7 9 0 492.51 20.35 7 -9 1 390.71 16.38 -7 9 -1 369.20 15.29 -7 9 -1 349.81 14.41 -7 9 -2 285.47 11.86 -7 9 -2 303.16 12.49 7 -9 3 623.47 25.48 -7 9 -3 643.76 24.69 -7 9 -3 585.68 24.66 -7 9 -3 587.16 24.13 7 -9 4 94.47 5.13 7 9 4 110.96 5.50 -7 9 -4 87.55 4.91 -7 9 -4 90.55 5.28 -7 9 -4 94.28 4.97 -7 9 -4 100.88 5.20 7 -9 5 92.34 4.89 7 9 5 92.38 5.42 -7 9 -5 93.11 5.23 -7 9 -5 94.18 5.01 -7 9 -5 88.39 5.49 -7 9 -5 88.30 5.25 -7 9 -5 92.44 4.66 7 9 6 154.17 8.21 7 -9 6 165.47 7.57 7 9 6 155.95 7.49 -7 9 -6 164.18 8.49 -7 9 -6 168.72 8.24 -7 9 -6 174.65 8.11 -7 9 -6 168.22 7.98 -7 9 -6 166.12 7.65 7 9 7 20.52 2.58 7 -9 7 22.00 2.65 -7 9 -7 18.38 2.98 -7 9 -7 22.57 4.61 -7 9 -7 21.71 4.41 -7 9 -7 13.74 2.24 7 -9 8 124.67 6.47 7 9 8 130.22 6.56 -7 9 -8 117.45 7.59 -7 9 -8 121.94 5.89 -7 9 -8 121.69 7.57 -7 9 -8 122.17 6.46 7 -9 9 112.61 6.24 7 9 9 128.79 6.46 -7 9 -9 104.49 7.54 -7 9 -9 107.56 7.53 7 -9 10 35.47 3.46 7 9 10 36.42 6.84 7 9 10 45.20 3.78 -7 9 -10 22.72 6.39 -7 9 -10 25.42 6.29 7 9 11 45.64 7.68 7 -9 11 41.30 3.49 7 9 11 45.94 3.68 7 9 11 40.71 4.43 -7 9 -11 51.98 7.15 -7 9 -11 41.25 7.06 7 9 12 22.01 7.68 7 -9 12 15.29 2.69 7 9 12 15.58 2.95 7 9 12 15.39 3.62 -7 9 -12 17.55 7.06 -7 9 -12 11.99 7.19 7 -11 -13 2.81 3.22 7 -11 -12 12.58 2.97 7 -11 -12 8.78 3.26 7 -11 -12 17.08 3.61 7 -11 -11 4.94 2.85 7 -11 -11 9.77 3.63 7 11 -11 4.24 1.64 7 -11 -11 8.21 2.79 7 -11 -10 120.23 6.18 7 -11 -10 130.35 6.72 7 -11 -10 126.70 5.93 7 -11 -9 2.43 2.95 7 11 -9 3.51 2.02 7 -11 -9 5.13 2.25 -7 11 9 4.47 2.93 7 -11 -8 224.90 7.96 7 11 -8 182.80 6.91 -7 11 8 160.30 7.64 7 -11 -7 11.85 2.50 7 11 -7 3.88 0.57 -7 11 7 8.76 3.32 7 -11 -6 27.09 2.91 -7 11 6 29.41 3.69 7 -11 -5 57.87 4.15 -7 11 5 50.41 4.35 7 -11 -4 464.86 19.16 7 -11 -4 446.05 19.47 -7 11 4 461.19 19.28 7 -11 -3 27.54 3.37 7 -11 -3 29.73 2.32 7 -11 -3 33.23 4.20 -7 11 3 34.52 3.93 7 11 -2 467.12 19.57 7 -11 -2 533.06 20.71 7 -11 -2 514.78 20.16 -7 11 2 530.07 21.91 7 -11 -1 85.57 5.27 7 -11 -1 83.53 4.10 -7 -11 1 41.23 1.91 -7 11 1 83.68 4.25 7 11 0 7.00 1.41 7 -11 0 6.51 3.07 7 -11 0 8.76 3.70 7 -11 0 7.03 1.65 -7 11 0 4.35 0.65 -7 11 0 9.62 3.11 7 -11 1 38.21 3.69 7 -11 1 39.63 4.05 -7 11 -1 29.76 1.86 -7 11 -1 28.47 3.50 -7 11 -1 30.31 2.66 7 11 2 512.88 20.67 7 -11 2 491.51 20.94 -7 11 -2 483.55 19.80 -7 11 -2 514.61 20.45 7 -11 3 45.84 3.23 7 11 3 37.74 3.28 -7 11 -3 30.83 3.92 -7 11 -3 40.02 3.07 -7 11 -3 34.79 3.45 -7 11 -3 41.30 3.26 7 -11 4 402.26 17.44 7 11 4 426.19 17.50 -7 11 -4 366.63 16.37 -7 11 -4 403.89 16.56 -7 11 -4 400.05 16.79 -7 11 -4 407.79 16.65 7 -11 5 37.34 3.06 7 11 5 27.75 3.71 -7 11 -5 41.30 4.43 -7 11 -5 43.95 4.12 -7 11 -5 36.48 3.75 -7 11 -5 41.29 3.22 7 11 6 64.71 3.96 7 -11 6 67.40 4.13 7 11 6 55.59 5.00 -7 11 -6 57.91 4.41 -7 11 -6 64.02 4.07 -7 11 -6 57.97 5.03 -7 11 -6 61.43 5.21 7 11 7 -0.64 2.40 7 -11 7 -0.49 2.19 7 11 7 1.92 4.32 7 11 7 -2.16 2.16 -7 11 -7 -1.25 2.41 -7 11 -7 -1.70 3.01 -7 11 -7 0.59 4.57 -7 11 -7 1.81 4.55 7 11 8 129.72 6.61 7 11 8 113.66 8.11 7 11 8 130.38 6.86 7 -11 8 128.23 6.55 -7 11 -8 121.61 6.45 -7 11 -8 114.32 7.61 -7 11 -8 118.01 7.81 -7 11 -8 120.37 6.59 7 -11 9 5.88 2.80 7 11 9 11.91 2.90 7 11 9 8.01 3.07 -7 11 -9 12.97 6.00 -7 11 -9 5.18 5.68 -7 11 -9 9.98 3.34 7 11 10 155.93 8.10 7 11 10 148.80 7.62 7 -11 10 137.63 7.23 -7 11 -10 115.31 8.56 -7 11 -10 130.04 6.87 -7 11 -10 119.59 8.75 7 -11 11 11.48 2.58 7 11 11 4.38 3.09 7 11 11 5.70 7.17 -7 11 -11 3.69 6.79 -7 11 -11 6.09 6.64 -7 11 -12 15.45 7.66 7 -13 -12 6.58 3.23 7 -13 -11 19.74 3.97 7 -13 -11 19.29 3.84 7 13 -10 35.29 2.10 7 13 -10 51.55 3.31 -7 13 10 44.72 3.90 7 13 -9 39.09 2.81 7 -13 -9 48.48 3.91 -7 13 9 37.87 4.27 7 -13 -8 70.21 4.60 7 13 -8 52.21 3.67 -7 13 8 54.42 4.70 7 -13 -7 63.83 4.35 -7 13 7 47.45 4.67 -7 13 6 18.27 4.16 7 -13 -5 37.10 5.24 -7 13 5 42.39 4.82 7 -13 -4 199.36 9.49 7 -13 -4 191.57 10.14 -7 13 4 186.06 9.10 7 -13 -3 94.48 5.21 7 -13 -3 90.57 6.46 -7 13 3 75.43 3.31 -7 13 3 95.08 5.48 7 -13 -2 245.55 10.80 7 -13 -2 238.24 9.76 -7 13 2 237.92 8.62 -7 13 2 156.44 6.52 7 -13 -1 43.14 4.43 7 -13 -1 46.00 3.11 7 -13 -1 46.11 5.25 7 13 -1 42.38 2.61 -7 13 1 29.64 1.43 -7 13 1 49.95 4.50 7 -13 0 10.55 1.89 7 -13 0 9.63 3.62 7 13 0 7.80 1.65 7 -13 0 11.45 4.31 -7 13 0 10.11 3.92 7 13 1 83.64 4.31 7 -13 1 81.50 5.92 7 -13 1 78.98 5.71 -7 13 -1 79.78 5.43 7 13 2 152.28 7.13 7 -13 2 154.86 8.06 -7 13 -2 149.38 7.16 7 -13 3 172.31 8.95 7 13 3 192.63 8.41 7 -13 3 170.92 8.43 -7 13 -3 149.39 8.07 -7 13 -3 171.94 7.48 -7 13 -3 146.33 7.35 -7 13 -3 151.79 7.16 7 13 4 152.25 7.72 7 -13 4 160.08 7.63 7 13 4 159.35 7.68 -7 13 -4 147.12 7.34 -7 13 -4 149.42 8.00 -7 13 -4 147.64 7.59 -7 13 -4 162.52 7.43 7 13 5 35.23 4.04 7 -13 5 29.51 3.23 7 13 5 42.53 3.37 -7 13 -5 27.24 4.13 -7 13 -5 23.36 4.13 -7 13 -5 31.57 3.05 -7 13 -5 23.17 4.04 7 13 6 27.45 4.34 7 13 6 31.72 3.01 7 -13 6 29.19 2.95 7 13 6 26.85 2.81 -7 13 -6 29.32 4.64 -7 13 -6 27.68 3.01 -7 13 -6 25.82 4.77 -7 13 -6 31.58 4.05 7 13 7 27.37 5.06 7 13 7 34.93 3.32 7 13 7 25.58 2.93 7 -13 7 28.78 2.96 -7 13 -7 31.27 3.45 -7 13 -7 33.40 4.12 -7 13 -7 31.55 5.14 -7 13 -7 33.70 5.42 7 13 8 58.13 6.36 7 13 8 56.50 4.24 7 13 8 46.61 3.95 7 -13 8 57.58 3.99 -7 13 -8 52.40 4.58 -7 13 -8 43.44 6.06 -7 13 -8 53.73 6.33 -7 13 -8 53.60 4.21 7 -13 9 37.06 3.54 7 13 9 33.96 3.65 7 13 9 34.28 4.06 7 13 9 38.80 6.73 -7 13 -9 34.64 6.64 -7 13 -9 29.12 3.89 -7 13 -9 34.05 4.24 -7 13 -9 37.84 6.31 7 13 10 63.80 5.03 7 13 10 63.84 4.72 7 -13 10 67.33 4.50 -7 13 -10 57.44 4.85 -7 13 -10 60.83 7.38 -7 13 -10 59.32 4.89 -7 13 -10 58.60 7.41 7 13 11 16.05 3.58 -7 13 -11 4.88 7.08 -7 13 -11 7.17 3.41 -7 13 -11 16.99 7.63 -7 13 -12 8.07 3.60 7 -15 -12 16.10 4.07 7 -15 -10 2.07 3.20 7 15 -10 3.06 2.38 7 -15 -9 36.46 4.02 7 15 -9 29.47 3.14 -7 15 9 27.59 4.64 7 15 -8 25.45 3.05 7 -15 -8 35.33 3.82 -7 15 8 25.25 4.75 7 15 -7 19.79 2.90 -7 15 7 23.43 5.00 7 -15 -6 128.64 8.77 -7 15 6 120.94 7.38 7 -15 -5 12.38 2.79 7 -15 -5 17.10 5.64 -7 15 5 14.09 4.61 7 -15 -4 12.50 5.49 7 -15 -4 16.31 2.72 -7 15 4 13.87 1.25 -7 15 4 14.16 4.53 7 -15 -3 105.69 7.71 7 -15 -3 119.62 6.16 -7 15 3 112.77 6.68 -7 15 3 92.31 4.06 7 -15 -2 51.82 5.96 7 -15 -2 39.31 5.04 -7 15 2 44.83 5.31 -7 15 2 35.55 1.83 7 -15 -1 42.29 5.58 7 15 -1 37.09 2.60 7 -15 -1 43.25 5.00 -7 15 1 30.79 1.69 -7 15 1 42.79 5.07 7 15 0 284.33 12.37 7 -15 0 304.10 13.48 7 -15 0 309.55 13.75 -7 15 0 299.41 13.68 7 15 1 29.92 2.76 7 -15 1 32.34 4.85 -7 15 -1 29.18 4.73 7 -15 2 164.44 8.94 7 15 2 171.72 7.84 7 15 3 105.13 5.86 7 -15 3 111.24 5.87 7 -15 3 118.51 6.99 -7 15 -3 115.21 5.67 -7 15 -3 96.25 5.76 7 15 4 19.78 2.64 7 15 4 13.42 3.15 7 -15 4 11.08 2.59 -7 15 -4 17.36 2.57 -7 15 -4 9.46 4.20 -7 15 -4 9.07 3.58 -7 15 -4 8.99 3.82 7 -15 5 24.43 3.04 7 15 5 20.74 3.98 -7 15 -5 16.34 4.44 -7 15 -5 25.91 4.15 -7 15 -5 21.63 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232.11 10.16 -8 6 -8 225.75 11.24 8 6 9 59.74 4.09 8 -6 9 46.73 3.77 8 6 9 60.58 4.23 8 6 9 51.38 3.96 8 6 9 57.95 6.56 -8 6 -9 50.12 6.06 -8 6 -9 50.42 3.45 8 6 10 5.22 6.26 8 6 10 7.04 2.48 8 6 10 10.02 2.62 8 6 10 5.73 2.93 8 -6 10 -0.12 2.52 -8 6 -10 3.50 2.03 -8 6 -10 6.41 5.86 8 6 11 -0.30 2.43 8 6 11 0.36 2.66 8 6 11 0.83 7.00 8 -6 11 -2.20 2.43 -8 6 -11 -0.30 1.97 -8 6 -11 -1.33 6.08 8 6 12 8.22 7.38 8 6 12 8.27 2.66 8 6 12 11.03 3.25 8 -6 12 8.11 2.67 -8 6 -12 7.06 2.23 -8 6 -12 5.49 7.12 8 -6 13 28.67 7.98 8 -8 -13 28.88 3.80 8 -8 -12 3.36 3.27 8 -8 -12 3.12 2.95 8 -8 -12 1.74 2.26 8 -8 -12 2.78 2.48 8 -8 -11 30.63 3.04 8 -8 -11 31.27 2.78 8 -8 -11 34.03 3.30 8 -8 -10 70.78 4.14 8 -8 -10 74.73 3.74 8 -8 -10 66.29 4.07 8 8 -9 0.92 1.42 8 -8 -9 0.69 1.63 8 -8 -9 1.51 1.97 8 -8 -9 4.06 2.25 8 -8 -9 4.04 2.65 8 -8 -8 128.29 6.24 8 -8 -8 136.09 6.54 8 -8 -8 126.36 5.91 8 -8 -8 115.86 5.58 8 -8 -7 218.26 9.32 8 -8 -7 256.76 10.09 8 8 -7 198.20 9.28 8 -8 -7 255.60 10.28 8 -8 -7 232.64 9.56 -8 8 7 219.02 9.53 8 -8 -6 11.38 1.51 8 -8 -6 9.24 2.42 8 8 -6 10.97 1.28 8 -8 -6 9.14 2.31 -8 8 6 10.28 3.02 -8 -8 6 9.98 1.20 8 8 -5 175.29 7.94 8 -8 -5 254.06 9.20 8 -8 -5 240.58 8.33 8 8 -5 200.71 8.21 8 -8 -5 247.91 8.74 8 -8 -5 260.40 9.35 -8 8 5 228.03 10.07 8 -8 -4 147.48 6.58 8 -8 -4 142.28 6.88 -8 8 4 137.47 6.77 8 -8 -3 36.60 2.57 8 -8 -3 41.70 2.95 -8 8 3 37.52 3.64 8 -8 -2 729.14 29.41 8 -8 -2 741.21 30.14 8 -8 -2 793.89 30.05 -8 8 2 844.99 34.11 8 -8 -1 397.44 17.29 8 -8 -1 407.30 16.40 8 -8 -1 425.66 16.99 -8 -8 1 380.71 15.77 -8 8 1 426.37 16.57 8 -8 0 104.39 4.57 8 -8 0 109.84 5.85 8 -8 0 109.63 5.19 -8 -8 0 117.46 5.08 -8 8 0 106.84 5.99 8 -8 1 946.26 37.61 -8 8 -1 935.53 32.36 -8 8 -1 972.08 32.32 8 -8 2 202.81 8.63 -8 8 -2 182.58 8.00 -8 8 -2 202.13 8.58 -8 8 -2 209.29 8.78 8 8 3 68.95 3.88 8 -8 3 64.53 3.80 -8 8 -3 66.53 3.62 -8 8 -3 61.11 3.77 -8 8 -3 59.70 3.54 8 -8 4 48.81 3.26 8 8 4 58.11 3.47 -8 8 -4 48.11 2.96 -8 8 -4 44.61 3.18 -8 8 -4 41.63 3.29 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2.73 8 -10 -11 17.24 3.00 8 10 -11 8.91 1.47 8 -10 -10 45.07 3.73 8 10 -10 38.78 2.69 8 -10 -10 38.09 2.71 8 -10 -10 44.62 4.06 8 -10 -10 41.64 3.27 8 10 -9 113.17 5.65 8 -10 -9 134.72 6.49 8 -10 -9 129.39 5.96 8 -10 -9 147.62 6.84 8 -10 -9 105.49 5.38 8 -10 -8 69.39 3.59 8 -10 -8 91.18 4.93 8 -10 -8 87.89 4.16 8 10 -8 69.67 3.59 8 -10 -8 95.56 5.06 -8 10 8 63.93 4.37 8 -10 -7 72.88 3.42 8 10 -7 52.21 2.78 8 -10 -7 83.67 4.42 8 -10 -7 81.22 4.40 8 -10 -7 58.84 2.79 -8 -10 7 44.50 2.13 -8 10 7 74.11 4.27 8 -10 -6 58.50 3.52 8 -10 -6 57.44 3.72 -8 10 6 56.11 4.40 8 -10 -5 41.73 3.34 8 -10 -5 40.47 3.56 -8 10 5 35.93 3.92 8 -10 -4 178.57 6.86 8 -10 -4 177.96 6.22 -8 10 4 181.72 8.67 8 -10 -3 385.91 16.59 8 -10 -3 393.25 15.94 8 -10 -3 399.12 16.27 8 10 -3 373.00 15.32 -8 10 3 387.02 16.39 8 -10 -2 450.94 18.48 8 -10 -2 438.75 18.94 -8 10 2 457.13 19.14 8 -10 -1 453.62 19.56 8 -10 -1 470.00 19.19 -8 -10 1 396.80 16.43 -8 10 1 474.28 17.46 8 -10 0 102.55 6.24 8 -10 0 109.53 5.87 8 -10 0 107.17 5.35 -8 10 0 117.57 6.37 8 -10 1 61.48 4.65 -8 10 -1 57.38 4.04 -8 10 -1 56.72 3.25 -8 10 -2 200.61 8.60 -8 10 -2 182.03 7.83 8 -10 3 170.01 7.96 -8 10 -3 157.51 7.24 -8 10 -3 179.06 7.84 8 -10 4 36.54 3.10 8 10 4 37.16 3.42 -8 10 -4 40.77 3.16 -8 10 -4 29.18 3.32 -8 10 -4 38.01 3.84 8 -10 5 184.86 8.78 8 10 5 192.96 9.15 -8 10 -5 178.84 8.57 -8 10 -5 186.83 8.63 -8 10 -5 185.75 8.92 -8 10 -5 178.01 8.78 8 10 6 97.50 5.68 8 10 6 110.90 6.68 8 -10 6 120.42 5.91 -8 10 -6 111.15 6.55 -8 10 -6 113.86 7.06 -8 10 -6 117.24 6.53 -8 10 -6 122.16 6.32 8 -10 7 34.46 3.05 8 10 7 28.84 4.96 8 10 7 22.38 2.85 -8 10 -7 34.86 5.24 -8 10 -7 24.21 3.31 -8 10 -7 34.36 4.79 -8 10 -7 36.14 3.75 8 -10 8 22.37 2.99 8 10 8 18.26 3.04 -8 10 -8 20.64 5.29 -8 10 -8 23.45 3.64 -8 10 -8 19.16 3.08 -8 10 -8 17.46 5.35 8 -10 9 104.11 6.20 8 10 9 129.07 6.47 -8 10 -9 100.37 7.55 -8 10 -9 86.27 7.69 8 10 10 52.32 4.16 8 -10 10 46.58 4.01 -8 10 -10 38.10 6.65 -8 10 -10 37.96 6.94 8 10 11 38.28 3.63 8 10 11 36.76 7.64 8 -10 11 33.46 3.44 -8 10 -11 32.22 7.28 -8 10 -11 24.53 7.02 8 -10 12 16.84 2.93 -8 10 -12 17.94 7.61 8 -12 -12 -0.07 2.86 8 -12 -12 3.83 3.47 8 -12 -11 46.89 4.53 8 -12 -11 39.62 4.07 8 -12 -10 2.75 3.15 8 12 -10 2.37 2.00 8 -12 -10 -1.46 3.30 8 12 -10 1.02 1.21 8 -12 -9 129.14 5.81 8 12 -9 110.25 4.64 -8 12 9 112.67 6.18 8 12 -8 17.62 2.35 8 -12 -8 10.64 3.44 8 -12 -8 15.62 3.15 -8 12 8 8.31 3.93 8 -12 -7 100.99 5.97 8 -12 -7 106.28 5.78 -8 12 7 84.85 5.65 8 -12 -6 6.43 2.33 8 -12 -6 0.85 3.00 8 -12 -6 3.81 4.85 -8 12 6 2.95 3.87 8 -12 -5 93.17 6.84 8 -12 -5 95.86 5.85 -8 12 5 92.26 5.82 8 -12 -4 20.20 3.73 8 -12 -4 18.72 4.81 -8 12 4 18.47 4.17 8 -12 -3 457.50 17.69 8 -12 -3 445.06 17.31 8 -12 -3 452.19 16.89 -8 12 3 479.85 20.19 8 12 -2 19.68 1.77 8 -12 -2 24.04 2.61 8 -12 -2 25.77 4.61 -8 12 2 23.90 4.02 8 -12 -1 484.63 18.67 8 -12 -1 486.41 19.25 8 12 -1 420.94 18.05 8 -12 -1 426.88 18.77 -8 12 1 486.70 13.80 -8 -12 1 282.34 11.81 8 -12 0 3.49 1.81 8 -12 0 1.13 3.62 8 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5.69 -8 14 -7 64.29 6.57 -8 14 -7 62.99 6.15 -8 14 -7 79.83 4.86 8 14 8 36.28 3.87 8 14 8 33.56 6.17 8 14 8 30.84 3.51 8 -14 8 38.74 3.55 -8 14 -8 32.45 4.68 -8 14 -8 33.82 6.32 -8 14 -8 36.60 3.84 -8 14 -8 28.00 5.81 8 14 9 20.28 6.49 8 -14 9 20.94 3.05 8 14 9 12.03 3.21 8 14 9 10.61 3.07 -8 14 -9 15.70 4.27 -8 14 -9 10.40 3.44 -8 14 -9 17.54 6.31 -8 14 -9 11.90 6.53 8 14 10 37.94 7.51 8 -14 10 37.29 3.70 8 14 10 29.43 3.94 8 14 10 28.53 3.64 -8 14 -10 32.75 7.17 -8 14 -10 24.55 7.17 -8 14 -10 25.54 4.36 -8 14 -10 28.96 4.14 8 14 11 2.55 3.12 -8 14 -11 9.80 3.78 -8 14 -11 3.70 7.41 8 -16 -11 22.47 4.94 8 -16 -10 5.23 4.50 8 -16 -10 6.50 3.45 8 16 -9 4.14 2.48 8 -16 -9 2.98 3.21 8 -16 -9 -1.76 4.47 -8 16 9 1.23 4.74 8 16 -8 7.19 2.65 8 -16 -8 3.82 4.70 8 -16 -8 6.58 3.32 -8 16 8 3.58 4.93 8 16 -7 64.15 4.56 8 -16 -7 61.57 7.92 8 -16 -7 73.37 6.21 -8 16 7 63.99 6.05 8 -16 -6 10.36 6.64 8 -16 -6 20.38 4.73 -8 16 6 11.06 5.28 8 -16 -5 103.39 5.92 8 -16 -5 87.59 7.77 8 -16 -5 95.72 6.99 -8 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24.95 2.17 10 -10 -9 42.68 2.59 10 -10 -9 52.58 4.16 10 -10 -9 51.60 3.04 10 10 -9 34.36 2.53 10 -10 -9 59.29 4.37 10 -10 -8 29.46 1.96 10 10 -8 27.29 1.99 10 -10 -8 34.74 6.11 10 -10 -8 37.19 3.69 10 -10 -8 39.36 2.45 10 -10 -8 39.06 3.78 10 -10 -7 100.19 6.88 10 -10 -7 104.31 5.32 10 -10 -7 103.54 5.32 -10 10 7 93.12 5.87 -10 -10 7 91.68 4.17 10 -10 -6 66.66 3.98 10 -10 -6 57.72 3.15 10 -10 -6 65.96 4.22 -10 10 6 58.14 4.94 10 10 -5 2.43 0.49 10 -10 -5 2.71 2.97 10 -10 -5 3.25 1.77 -10 10 5 0.37 4.02 10 -10 -4 225.10 7.67 10 -10 -4 221.88 6.98 -10 10 4 210.37 10.08 10 -10 -3 209.29 7.34 10 -10 -3 203.41 8.02 -10 10 3 192.90 9.47 10 -10 -2 211.07 10.25 10 -10 -2 200.55 8.42 10 -10 -2 229.72 9.43 -10 10 2 225.08 10.70 10 -10 -1 198.81 8.80 10 -10 -1 199.18 9.79 10 -10 -1 186.24 7.89 -10 10 1 209.13 10.06 -10 -10 1 203.24 8.53 10 -10 0 74.47 4.35 10 -10 0 71.16 5.96 10 -10 0 76.67 3.60 -10 10 0 72.16 5.46 -10 -10 0 70.43 3.53 10 -10 1 94.58 5.09 -10 10 -1 90.39 6.06 -10 10 -1 93.93 5.16 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15.61 3.78 10 -22 -3 13.03 9.03 -10 22 3 8.10 7.63 10 -22 -2 37.88 9.20 10 -22 -2 37.31 4.37 10 -22 -2 40.31 7.92 -10 22 2 34.84 7.99 10 -22 -1 4.02 7.92 10 -22 -1 2.83 3.39 10 -22 -1 5.26 7.48 -10 22 1 -1.41 7.18 10 -22 0 16.84 7.21 10 -22 0 18.05 3.74 -10 22 0 15.79 7.32 10 -22 1 5.57 7.26 -10 22 -1 3.65 7.25 10 22 2 -0.96 3.03 10 -22 2 -3.28 7.29 10 22 3 2.81 3.43 10 22 4 21.13 4.35 10 22 5 5.98 4.95 10 22 6 16.12 3.57 10 -24 1 -1.03 3.21 10 -24 2 -1.52 3.37 10 -24 3 2.29 3.35 11 -1 -13 21.48 4.05 11 1 -13 27.02 4.58 11 1 -12 6.78 3.52 11 -1 -12 3.94 3.05 11 1 -11 -0.58 2.10 11 -1 -11 -1.21 2.14 11 1 -11 1.26 2.80 11 -1 -11 1.98 2.63 11 1 -10 7.38 2.14 11 -1 -10 4.82 2.16 11 -1 -10 7.06 2.60 11 1 -10 12.29 2.89 11 1 -9 115.47 5.97 11 -1 -9 129.85 5.83 11 -1 -9 124.30 6.31 11 -1 -9 131.36 5.74 11 1 -9 128.07 5.55 11 1 -8 49.40 2.79 11 1 -8 48.86 3.81 11 -1 -8 57.65 4.21 11 -1 -8 55.42 2.77 11 -1 -8 57.01 3.62 11 1 -8 50.26 3.46 11 1 -7 277.00 11.64 11 1 -7 277.19 12.22 11 -1 -7 290.13 12.45 11 -1 -7 285.12 11.63 11 -1 -7 290.04 12.10 11 1 -7 264.80 11.92 11 -1 -6 38.91 3.27 11 1 -6 42.60 2.64 11 -1 -6 35.61 2.53 11 1 -6 43.54 3.07 11 1 -5 20.67 1.98 11 -1 -5 21.31 2.56 11 1 -5 21.76 2.28 11 -1 -5 22.80 2.00 -11 -1 5 20.21 2.07 11 1 -4 137.98 6.11 11 1 -4 152.29 6.32 11 -1 -4 108.54 5.92 11 -1 -4 125.93 6.30 -11 1 4 113.88 5.95 -11 -1 4 139.33 5.98 11 1 -3 433.31 18.91 11 1 -3 472.27 19.01 11 -1 -3 470.28 19.14 11 -1 -3 462.41 18.94 -11 -1 3 428.02 18.05 -11 1 3 447.72 18.15 11 -1 -2 130.75 6.23 11 -1 -2 130.75 6.46 11 1 -2 132.10 6.29 -11 1 2 129.34 6.18 -11 -1 2 128.35 6.13 11 1 -1 754.34 30.91 11 -1 -1 770.98 30.92 -11 1 1 727.17 29.22 -11 -1 1 707.79 29.10 -11 1 1 722.60 29.18 11 -1 0 14.53 1.46 11 -1 0 14.34 1.97 -11 1 0 9.19 1.75 -11 -1 0 15.55 1.92 -11 1 0 10.87 1.85 11 -1 1 31.95 2.66 11 1 1 31.77 2.61 11 1 1 35.21 2.33 11 -1 1 39.61 2.22 -11 -1 -1 39.61 2.75 -11 1 -1 39.89 2.93 11 1 2 40.78 2.46 11 -1 2 29.86 2.18 -11 1 -2 28.23 2.67 -11 -1 -2 44.88 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3.18 11 -3 -12 19.22 3.25 11 3 -12 18.62 4.28 11 3 -11 27.45 4.03 11 -3 -11 32.43 3.27 11 -3 -11 28.91 3.31 11 3 -10 17.35 2.16 11 -3 -10 19.34 2.81 11 -3 -10 17.57 2.67 11 3 -10 16.52 2.77 11 -3 -9 23.50 2.82 11 3 -9 28.89 2.28 11 3 -9 27.67 2.82 11 -3 -9 23.27 2.59 11 3 -9 18.93 1.51 11 3 -8 101.44 5.53 11 3 -8 96.12 4.88 11 -3 -8 115.59 4.81 11 -3 -8 111.35 6.26 11 3 -8 100.33 5.14 11 -3 -8 119.67 5.48 11 -3 -8 113.73 5.72 11 -3 -7 40.20 3.84 11 3 -7 35.43 2.56 11 3 -7 46.30 3.07 11 3 -7 39.60 2.66 11 -3 -7 34.73 3.14 11 -3 -7 33.26 2.41 11 -3 -7 41.37 2.71 11 -3 -6 172.89 7.93 11 3 -6 150.74 7.09 11 -3 -6 159.68 7.03 11 3 -6 158.85 7.30 -11 -3 6 150.91 6.78 11 -3 -5 206.39 9.45 11 3 -5 207.45 8.99 11 -3 -5 199.72 8.84 -11 -3 5 206.30 8.94 11 -3 -4 132.02 6.34 11 3 -4 127.54 5.79 -11 -3 4 121.28 5.68 11 -3 -3 480.47 20.53 11 -3 -3 499.13 20.85 11 3 -3 521.14 20.49 -11 3 3 490.39 20.24 11 -3 -2 508.65 21.40 11 -3 -2 519.05 21.15 -11 3 2 476.23 19.69 11 -3 -1 127.60 6.19 11 -3 -1 127.78 5.42 -11 -3 1 109.66 5.60 -11 3 1 127.41 5.86 -11 3 1 123.59 5.88 11 -3 0 240.25 9.80 11 -3 0 235.83 10.49 -11 3 0 244.64 10.52 -11 -3 0 244.66 10.35 -11 3 0 226.11 10.37 11 -3 1 146.13 7.55 11 -3 1 163.45 6.99 -11 -3 -1 183.91 7.78 -11 3 -1 154.61 7.79 11 -3 2 44.27 2.46 11 -3 2 50.42 3.01 -11 3 -2 50.16 3.29 -11 -3 -2 42.50 3.02 11 -3 3 219.52 9.69 11 -3 3 215.44 9.33 11 3 3 228.93 9.71 11 -3 3 216.16 9.87 -11 3 -3 220.85 10.01 11 -3 4 370.20 14.72 11 3 4 332.45 14.89 11 -3 4 364.79 15.15 11 -3 4 343.16 14.91 11 3 4 344.89 15.16 -11 3 -4 330.42 14.35 11 -3 5 99.23 4.99 11 -3 5 90.11 4.56 11 3 5 70.61 4.64 11 3 5 67.26 4.92 11 -3 5 92.11 5.01 11 -3 6 161.16 7.68 11 -3 6 162.39 8.02 11 3 6 160.21 8.11 11 3 6 167.15 7.90 11 -3 6 170.67 8.11 -11 3 -6 171.24 8.76 11 3 7 174.10 7.85 11 -3 7 145.79 7.78 11 -3 7 144.53 7.74 11 3 7 164.42 7.98 -11 3 -7 135.25 7.92 11 3 8 4.95 2.43 11 3 8 5.87 2.52 11 -3 8 5.41 2.56 11 -3 8 4.54 2.48 -11 3 -8 9.37 5.45 11 -3 9 37.98 3.56 11 3 9 49.02 4.02 11 3 9 46.63 3.80 11 3 9 43.47 3.78 -11 3 -9 34.19 6.19 11 3 10 8.59 2.89 11 -3 10 8.95 2.62 11 3 10 11.73 2.80 11 3 10 9.14 2.83 -11 3 -10 11.95 6.24 11 -3 11 37.84 3.83 11 3 11 28.03 3.70 -11 3 -11 38.60 7.44 -11 3 -11 36.87 3.69 11 3 12 28.70 3.78 11 -3 12 28.57 3.69 -11 3 -12 29.96 3.64 -11 3 -12 30.04 7.82 11 -5 -12 7.21 2.72 11 -5 -12 11.52 3.28 11 -5 -12 10.47 2.95 11 5 -12 7.10 4.78 11 5 -12 7.71 2.77 11 -5 -11 53.74 4.07 11 -5 -11 62.69 4.50 11 5 -11 55.45 3.97 11 5 -10 23.91 2.71 11 5 -10 14.35 1.09 11 -5 -10 22.35 3.17 11 -5 -10 24.76 2.64 11 5 -9 29.14 2.05 11 5 -9 25.79 1.93 11 5 -9 28.30 2.61 11 -5 -9 23.73 2.52 11 -5 -9 26.31 3.07 11 -5 -8 2.79 1.64 11 5 -8 3.93 1.79 11 5 -8 4.14 1.35 11 -5 -8 4.74 2.29 11 -5 -8 0.78 3.52 11 -5 -8 1.36 1.21 11 5 -8 1.22 1.50 11 -5 -7 65.68 3.61 11 5 -7 67.41 3.86 11 5 -7 67.15 3.53 11 -5 -7 73.83 4.35 11 -5 -7 79.66 5.27 11 -5 -7 72.31 3.59 11 5 -6 48.98 3.20 11 -5 -6 56.54 3.14 11 -5 -6 53.60 2.92 11 -5 -6 55.24 4.64 -11 -5 6 46.87 2.89 11 -5 -5 401.98 17.05 11 5 -5 433.08 17.44 11 -5 -5 442.11 17.48 11 -5 -5 448.92 18.23 -11 -5 5 461.62 18.88 11 -5 -4 109.85 5.89 11 -5 -4 91.12 4.14 11 -5 -4 101.85 4.89 11 5 -4 98.35 4.69 11 -5 -3 450.15 15.76 11 -5 -3 443.11 15.20 11 -5 -2 68.96 4.85 11 -5 -2 72.25 3.98 -11 5 2 69.90 4.06 11 -5 -1 -1.23 1.68 11 -5 -1 -0.03 0.28 11 -5 -1 -1.98 2.93 -11 -5 1 0.54 1.36 -11 5 1 -0.21 1.57 -11 5 1 -0.27 1.70 11 -5 0 100.62 4.92 11 -5 0 90.46 3.87 -11 5 0 91.94 4.92 -11 -5 0 95.03 4.72 -11 5 0 99.92 5.06 11 -5 1 218.86 9.84 11 -5 1 221.09 9.02 11 -5 1 220.99 9.55 -11 -5 -1 219.90 9.80 -11 5 -1 232.30 10.16 11 -5 2 133.11 5.83 11 -5 2 127.40 6.26 -11 5 -2 137.39 6.64 11 -5 3 501.87 22.23 11 5 3 543.21 22.19 11 -5 3 558.75 22.06 -11 5 -3 577.97 23.83 11 -5 4 66.37 4.21 11 -5 4 72.37 4.01 -11 5 -4 69.16 4.25 11 5 5 10.50 2.37 11 -5 5 8.46 2.23 11 -5 5 8.07 2.29 -11 5 -5 7.32 2.21 -11 5 -5 8.87 3.65 11 5 6 2.01 2.35 11 5 6 2.01 2.37 11 -5 6 4.31 2.46 11 -5 6 9.06 2.35 -11 5 -6 8.69 2.44 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131.70 6.78 -11 7 -4 138.03 7.10 11 -7 5 79.35 4.93 11 -7 5 83.29 5.08 -11 7 -5 86.07 5.17 -11 7 -5 81.63 4.72 -11 7 -5 75.83 5.27 11 7 6 29.55 3.31 11 7 6 35.69 3.45 11 -7 6 28.26 3.11 -11 7 -6 25.92 4.53 -11 7 -6 24.37 2.95 -11 7 -6 24.04 3.32 11 -7 7 18.34 3.00 11 7 7 22.46 3.00 11 7 7 22.40 3.11 -11 7 -7 15.48 3.17 -11 7 -7 17.21 4.86 -11 7 -7 12.06 2.64 11 7 8 84.88 5.53 11 7 8 104.02 5.66 11 -7 8 90.57 5.35 11 7 8 90.06 5.55 -11 7 -8 89.03 5.05 -11 7 -8 76.75 6.75 11 7 9 3.50 2.59 11 -7 9 5.43 2.64 11 7 9 2.21 2.61 11 7 9 3.15 2.64 -11 7 -9 3.22 6.00 -11 7 -9 3.87 2.38 11 7 10 41.63 4.03 11 7 10 47.49 4.21 11 -7 10 41.59 4.01 11 7 10 41.92 7.81 11 7 10 53.58 4.38 -11 7 -10 48.59 3.80 -11 7 -10 41.05 7.07 11 7 11 6.18 3.12 11 7 11 4.42 3.00 11 -7 11 7.81 3.00 11 7 11 10.14 3.39 -11 7 -11 6.30 2.72 -11 7 -11 5.78 7.31 11 -7 12 4.06 3.09 11 -9 -12 11.51 3.51 11 -9 -11 12.48 3.46 11 -9 -11 13.69 2.90 11 -9 -11 10.55 2.63 11 -9 -10 21.14 3.50 11 -9 -10 15.21 2.05 11 -9 -10 15.23 3.01 11 -9 -10 18.52 2.43 11 9 -10 13.19 2.14 11 9 -10 13.14 1.89 11 -9 -9 28.90 2.28 11 9 -9 25.67 2.37 11 -9 -9 32.61 2.57 11 -9 -9 28.16 3.38 11 -9 -9 36.75 3.67 11 -9 -9 22.95 5.95 11 -9 -8 25.18 3.36 11 -9 -8 31.27 3.53 11 -9 -8 29.82 2.21 11 9 -8 21.20 2.06 11 -9 -8 25.70 5.68 11 -9 -7 91.93 3.97 11 -9 -7 97.29 5.38 11 -9 -7 99.31 6.97 11 -9 -7 93.07 5.32 -11 -9 7 93.72 4.37 11 -9 -6 76.17 4.55 11 -9 -6 77.41 6.33 11 -9 -6 73.43 4.55 11 -9 -6 74.43 3.75 -11 -9 6 66.44 3.50 11 -9 -5 109.32 7.36 11 -9 -5 109.80 5.51 11 -9 -5 112.66 6.12 -11 9 5 111.35 6.64 11 -9 -4 202.60 9.20 11 -9 -4 209.05 9.69 -11 9 4 196.04 9.73 11 -9 -3 331.03 14.25 11 -9 -3 338.66 14.61 -11 9 3 331.46 14.73 11 -9 -2 144.26 6.24 11 -9 -2 151.74 7.09 -11 9 2 151.60 8.24 11 -9 -1 149.03 6.49 11 -9 -1 154.28 7.17 -11 9 1 152.99 8.66 -11 -9 1 171.24 7.23 11 -9 0 169.15 7.99 11 -9 0 172.21 7.39 -11 9 0 159.42 8.38 -11 -9 0 158.02 7.00 11 -9 1 76.84 4.53 11 -9 1 78.42 3.93 -11 -9 -1 71.11 3.86 -11 9 -1 79.99 5.64 11 -9 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1.45 -13 -5 6 9.17 1.91 13 -5 -5 105.84 5.12 13 -5 -5 91.03 4.26 13 -5 -5 108.86 6.34 -13 -5 5 95.70 4.98 13 -5 -4 86.54 5.64 13 -5 -4 89.20 4.42 -13 -5 4 81.05 4.46 13 -5 -3 150.66 6.33 13 -5 -3 233.43 8.79 13 -5 -3 229.91 7.81 13 -5 -2 49.30 4.64 13 -5 -2 51.75 3.54 -13 5 2 46.38 3.45 13 -5 -1 22.16 1.14 13 -5 -1 33.92 2.73 -13 -5 1 31.61 2.58 -13 5 1 32.60 2.89 13 -5 0 25.48 1.42 13 -5 0 25.79 2.70 -13 5 0 29.12 2.75 -13 5 0 29.61 2.91 13 -5 1 109.03 5.96 13 5 1 107.17 5.72 13 -5 1 112.35 4.88 13 -5 1 118.37 5.67 -13 5 -1 121.59 6.49 -13 -5 -1 123.00 6.08 13 -5 2 113.75 5.11 13 -5 2 105.96 5.71 13 5 2 117.91 5.93 -13 5 -2 121.75 6.53 -13 -5 -2 123.03 6.35 13 -5 3 608.46 25.30 13 5 3 622.49 25.42 -13 5 -3 638.12 26.40 -13 -5 -3 625.25 26.27 -13 5 -3 650.54 26.61 13 5 4 96.20 5.28 13 -5 4 89.37 5.15 13 -5 4 82.29 5.36 -13 5 -4 88.54 5.21 13 -5 5 91.99 5.55 13 5 5 88.42 5.42 13 5 5 94.76 5.69 13 -5 5 93.32 5.27 -13 5 -5 82.65 5.06 13 5 6 3.01 2.50 13 5 6 2.45 2.47 13 -5 6 6.57 2.30 13 -5 6 1.00 2.58 -13 5 -6 2.09 2.45 13 5 7 7.40 2.50 13 -5 7 2.24 2.45 13 -5 7 6.10 2.47 13 5 7 5.00 2.53 -13 5 -7 4.72 2.49 13 5 8 17.70 3.07 13 5 8 16.27 3.10 13 5 8 19.04 3.04 13 -5 8 17.77 3.18 -13 5 -8 18.92 3.06 -13 5 -8 18.81 3.35 13 5 9 76.36 5.55 13 5 9 90.38 5.73 13 -5 9 88.67 5.63 13 5 9 88.90 5.67 -13 5 -9 76.35 7.59 -13 5 -9 89.88 5.51 13 5 10 39.80 4.27 13 5 10 24.96 4.11 13 5 10 36.14 4.34 -13 5 -10 26.25 7.36 -13 5 -10 29.65 3.82 13 5 11 47.36 4.72 13 -5 11 48.73 4.70 -13 5 -11 51.96 4.64 -13 5 -11 43.14 8.09 13 -7 -12 14.06 3.52 13 -7 -11 2.55 6.10 13 -7 -11 4.95 3.44 13 7 -10 51.34 3.83 13 -7 -10 62.60 3.78 13 -7 -10 68.99 4.96 13 -7 -10 69.94 7.13 13 -7 -9 -0.95 2.95 13 -7 -9 1.56 1.79 13 7 -9 -0.67 2.12 13 7 -9 0.71 1.86 13 -7 -9 1.16 5.28 13 -7 -8 53.67 3.00 13 -7 -8 63.69 6.02 13 7 -8 44.47 3.15 13 -7 -8 56.62 4.22 13 7 -8 42.98 2.59 13 -7 -8 46.90 2.86 13 -7 -7 16.93 1.57 13 -7 -7 17.27 3.08 13 7 -7 16.71 2.04 13 -7 -7 19.87 2.20 13 7 -7 21.74 1.79 13 -7 -7 21.48 4.84 -13 -7 7 19.19 2.14 13 -7 -6 18.48 1.31 13 -7 -6 22.18 2.42 -13 -7 6 28.56 2.49 13 -7 -5 46.66 3.28 13 -7 -5 45.54 5.21 -13 -7 5 47.28 3.22 13 -7 -4 295.40 13.37 13 -7 -4 276.15 12.23 13 -7 -3 21.05 2.63 13 -7 -3 17.49 4.64 13 -7 -2 131.28 6.51 13 -7 -2 125.08 7.61 13 -7 -1 18.97 2.50 -13 -7 1 28.96 2.35 13 -7 0 7.31 1.76 13 -7 0 7.63 2.20 -13 -7 0 10.63 1.89 -13 7 0 0.13 2.55 13 -7 1 56.48 4.08 13 -7 1 56.88 3.45 -13 7 -1 55.66 4.35 -13 -7 -1 71.13 3.96 13 7 2 483.43 20.10 13 -7 2 471.79 19.78 -13 -7 -2 491.23 20.54 -13 7 -2 495.71 20.78 13 7 3 55.23 4.10 13 -7 3 61.78 3.98 -13 7 -3 59.99 4.30 13 -7 4 268.36 12.30 13 7 4 290.26 12.60 13 -7 4 286.23 12.72 -13 7 -4 281.73 12.57 13 7 5 38.49 3.54 13 -7 5 26.90 3.43 13 -7 5 32.41 3.20 13 7 5 44.31 3.54 -13 7 -5 26.07 3.07 13 -7 6 1.47 2.43 13 7 6 5.57 2.49 13 7 6 3.11 2.62 -13 7 -6 2.66 2.34 -13 7 -6 3.31 2.77 13 -7 7 3.31 2.52 13 7 7 7.84 2.53 13 7 7 5.91 2.72 13 7 7 12.77 2.70 -13 7 -7 3.16 4.81 -13 7 -7 2.07 2.45 -13 7 -7 2.77 2.78 13 7 8 41.92 3.97 13 7 8 38.84 3.89 13 -7 8 41.73 4.02 13 7 8 48.87 4.15 -13 7 -8 46.88 6.16 -13 7 -8 43.38 4.33 -13 7 -8 47.84 3.97 13 7 9 10.91 3.56 13 -7 9 14.82 3.38 13 7 9 14.82 3.49 13 7 9 15.12 3.54 -13 7 -9 22.89 4.07 -13 7 -9 26.38 6.76 -13 7 -9 19.58 3.44 13 7 10 105.99 6.67 13 -7 10 85.83 6.20 13 7 10 98.82 6.31 -13 7 -10 87.42 8.61 -13 7 -10 103.76 6.21 13 -7 11 12.68 3.66 13 7 11 10.20 3.74 -13 7 -11 7.18 7.69 -13 7 -11 7.28 3.34 13 -9 -11 3.55 3.44 13 -9 -10 25.20 7.03 13 -9 -10 30.63 3.99 13 -9 -9 43.70 4.11 13 -9 -9 44.41 6.82 13 -9 -9 37.01 2.64 13 9 -9 32.08 2.62 13 -9 -8 14.52 6.10 13 -9 -8 13.15 1.55 13 -9 -8 14.99 3.35 13 -9 -7 119.94 7.94 13 -9 -7 116.02 5.03 13 -9 -7 123.68 6.09 -13 -9 7 107.58 5.21 13 -9 -6 33.23 5.92 13 -9 -6 37.53 3.06 -13 -9 6 32.25 2.60 13 -9 -5 94.09 7.46 13 -9 -5 98.95 5.26 13 -9 -4 153.59 7.34 13 -9 -4 152.27 8.96 13 -9 -3 46.71 6.03 13 -9 -3 46.02 3.49 13 -9 -2 98.28 5.28 13 -9 -2 90.82 4.40 13 -9 -1 77.55 4.03 13 -9 -1 87.08 4.85 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11.25 3.34 13 -9 10 44.34 4.30 13 9 10 33.00 4.47 -13 9 -10 34.52 4.07 -13 9 -10 38.33 7.28 13 9 11 9.74 3.86 13 -11 -10 -1.07 3.27 13 -11 -9 15.98 3.54 13 -11 -9 14.53 7.11 13 -11 -8 85.18 5.88 13 -11 -8 79.60 8.28 13 -11 -7 9.44 6.47 13 -11 -7 8.75 3.46 13 -11 -7 4.50 0.73 -13 -11 7 7.37 1.99 13 -11 -6 206.01 9.97 13 -11 -6 200.95 9.22 13 -11 -6 204.24 11.52 13 -11 -5 4.23 2.33 13 -11 -5 0.97 6.21 13 -11 -4 30.95 2.89 13 -11 -4 18.38 1.21 -13 11 4 21.05 5.65 13 -11 -3 20.74 1.45 13 -11 -3 26.82 2.95 -13 11 3 30.33 5.88 13 -11 -2 119.53 6.07 13 -11 -2 110.03 4.95 -13 11 2 128.07 8.25 13 -11 -1 9.47 2.63 13 -11 -1 10.66 1.51 -13 -11 1 10.23 1.73 -13 11 1 6.77 5.26 13 -11 0 205.60 9.15 13 -11 0 236.76 10.19 -13 -11 0 216.71 9.47 -13 11 0 224.93 11.36 13 -11 1 39.80 3.69 -13 11 -1 33.38 3.58 -13 11 -1 36.77 5.98 -13 -11 -1 28.31 2.69 13 11 2 88.26 5.37 -13 11 -2 91.40 7.10 -13 11 -2 90.86 5.59 -13 -11 -2 85.27 4.77 13 11 3 -3.82 2.80 -13 11 -3 -2.81 2.93 13 -11 4 40.99 3.78 13 11 4 40.60 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32.47 2.72 14 2 -8 33.56 3.45 14 -2 -8 32.16 2.55 14 -2 -8 38.17 3.35 14 2 -8 35.39 3.04 14 -2 -8 37.86 2.89 14 -2 -8 35.03 4.18 14 2 -7 106.04 5.41 14 2 -7 109.85 5.97 14 -2 -7 107.34 6.50 14 -2 -7 112.59 5.43 14 -2 -6 129.65 6.90 14 -2 -6 123.47 6.04 14 2 -6 116.07 6.35 14 2 -6 120.80 6.03 -14 -2 6 118.57 5.92 14 -2 -5 106.32 6.10 14 2 -5 99.63 5.54 14 -2 -5 106.03 5.33 14 2 -5 94.91 5.30 -14 -2 5 85.96 4.75 14 -2 -4 70.21 4.30 14 2 -4 77.70 4.40 14 -2 -4 65.92 4.90 -14 -2 4 79.95 4.48 -14 2 4 74.57 4.51 14 -2 -3 21.05 3.24 14 2 -3 28.50 2.79 14 -2 -3 26.52 2.66 -14 2 3 27.19 2.79 -14 -2 3 33.34 2.84 14 -2 -2 75.42 4.56 14 2 -2 80.75 4.73 -14 2 2 84.72 4.78 -14 -2 2 82.34 4.69 14 -2 -1 209.26 9.17 14 -2 -1 226.08 10.05 14 2 -1 230.01 10.12 -14 -2 1 214.68 10.00 -14 2 1 215.61 10.16 -14 2 1 238.20 10.21 14 2 0 313.43 14.11 14 2 0 299.67 13.58 14 -2 0 330.80 13.31 14 -2 0 345.77 14.23 -14 2 0 347.22 14.91 -14 -2 0 315.82 14.63 -14 2 0 368.58 14.87 14 2 1 253.37 11.15 14 2 1 260.07 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19.03 3.52 19 3 -2 16.83 3.52 19 3 -2 14.45 2.74 19 -3 -2 21.74 3.52 -19 -3 2 14.36 3.39 -19 3 2 26.82 3.50 19 3 -1 57.58 3.89 19 3 -1 65.60 4.90 -19 3 1 55.90 4.56 -19 -3 1 59.74 4.60 19 -3 0 6.06 3.15 19 3 0 6.07 2.47 19 3 0 7.09 3.18 -19 3 0 6.97 3.00 -19 -3 0 8.52 2.89 -19 -3 0 9.64 2.96 -19 3 0 9.87 3.16 19 3 1 30.44 3.14 19 -3 1 33.89 3.65 19 3 1 30.43 4.07 19 -3 1 30.57 3.92 -19 3 -1 23.16 3.86 -19 -3 -1 36.45 3.88 -19 -3 -1 35.30 3.70 -19 3 -1 32.13 3.93 19 -3 2 51.12 4.36 19 3 2 48.50 3.90 19 -3 2 57.71 4.87 19 3 2 42.17 4.71 -19 3 -2 52.87 4.64 -19 -3 -2 51.30 4.53 -19 3 -2 55.21 4.68 19 -3 3 28.61 4.04 19 3 3 19.55 3.81 19 3 3 18.64 3.10 19 -3 3 22.03 3.65 -19 -3 -3 18.68 3.82 -19 3 -3 21.59 3.72 19 -3 4 42.02 4.44 19 3 4 40.88 3.96 19 3 4 38.25 4.53 -19 -3 -4 38.24 4.61 -19 3 -4 53.71 4.91 19 3 5 69.56 4.93 19 -3 5 64.86 5.33 -19 -3 -5 74.11 5.88 19 3 6 4.59 3.29 19 3 7 33.93 4.21 19 5 -6 10.63 3.34 19 -5 -6 14.77 3.12 19 -5 -6 8.78 5.89 -19 -5 6 11.68 3.07 19 5 -5 24.56 3.58 19 -5 -5 22.99 3.53 -19 -5 5 22.52 3.35 19 5 -4 0.08 3.14 19 -5 -4 -2.23 3.16 -19 -5 4 -2.10 3.13 19 -5 -3 7.65 3.16 19 5 -3 8.65 3.34 19 5 -2 11.50 3.50 19 -5 -2 12.10 3.41 -19 -5 2 9.64 3.20 19 5 -1 75.13 5.48 19 -5 -1 69.04 5.26 19 5 -1 70.08 4.63 -19 5 1 67.90 5.05 -19 -5 1 63.50 4.89 19 -5 0 34.99 4.09 19 5 0 41.43 4.34 19 -5 0 35.72 3.50 19 5 0 35.56 3.58 -19 5 0 34.32 4.05 -19 -5 0 36.78 3.61 19 5 1 10.51 2.82 19 -5 1 15.46 3.59 19 -5 1 13.42 2.93 19 5 1 7.87 3.32 -19 -5 -1 12.78 3.01 -19 5 -1 13.34 3.34 -19 5 -1 9.28 3.29 19 -5 2 8.15 2.84 19 -5 2 6.44 3.41 19 5 2 4.13 3.43 19 5 2 4.80 2.69 -19 5 -2 4.59 3.24 -19 -5 -2 5.31 2.96 19 5 3 5.60 2.83 19 -5 3 0.81 3.48 19 -5 3 1.17 3.16 -19 5 -3 3.93 3.21 -19 5 -3 2.96 3.41 -19 -5 -3 5.14 3.22 19 5 4 27.11 3.55 19 -5 4 17.82 3.80 -19 -5 -4 23.52 4.12 19 -5 5 87.90 6.02 19 5 5 82.29 5.70 -19 -5 -5 91.97 6.37 19 5 6 25.40 4.04 19 7 -6 42.75 4.40 19 -7 -6 54.68 4.26 19 7 -5 3.67 3.22 19 -7 -5 2.24 3.08 -19 -7 5 3.38 2.92 19 7 -4 7.22 3.29 19 -7 -4 3.21 3.16 -19 -7 4 8.74 3.09 19 7 -3 13.40 3.49 19 -7 -3 8.24 3.30 -19 -7 3 10.30 3.10 19 -7 -2 52.00 3.90 19 -7 -2 46.93 4.55 19 7 -2 53.54 4.78 19 -7 -1 4.22 2.56 19 7 -1 6.45 2.90 19 -7 -1 10.32 3.39 19 7 -1 5.19 3.31 19 7 0 57.76 5.08 19 7 0 55.41 4.44 19 -7 0 52.80 4.03 19 -7 0 65.17 4.99 -19 7 0 53.93 4.69 -19 -7 0 53.03 4.09 19 7 1 1.02 3.24 19 7 1 4.64 3.03 19 -7 1 2.43 2.47 19 -7 1 1.15 3.21 -19 -7 -1 4.31 2.77 -19 7 -1 -1.88 3.47 -19 7 -1 1.07 3.07 19 -7 2 0.57 2.66 19 -7 2 0.99 3.36 19 7 2 0.69 2.98 19 7 2 -0.42 3.51 -19 -7 -2 1.62 2.89 -19 7 -2 -0.21 3.35 19 7 3 9.61 3.23 19 -7 3 6.21 3.03 -19 -7 -3 8.78 3.29 19 7 4 33.98 4.15 19 -7 4 30.36 3.92 -19 -7 -4 34.49 4.26 19 -7 5 19.61 3.86 19 7 5 9.95 3.93 -19 -7 -5 13.22 3.92 19 9 -6 5.93 3.42 19 9 -5 23.91 4.02 19 -9 -5 32.63 3.92 -19 -9 5 25.90 3.73 19 9 -4 15.36 3.71 19 -9 -4 10.10 3.49 -19 -9 4 15.40 3.44 19 9 -3 44.74 4.52 19 -9 -3 37.89 4.12 19 -9 -2 31.94 4.13 19 9 -2 29.40 4.16 19 -9 -1 7.45 3.32 19 9 -1 4.03 3.45 19 9 0 21.07 3.53 19 -9 0 27.92 3.88 19 -9 0 25.61 2.97 19 9 0 22.12 3.94 -19 -9 0 20.76 3.07 19 -9 1 17.62 2.87 19 9 1 14.04 3.48 -19 -9 -1 16.72 3.13 19 -9 2 9.49 2.85 19 9 2 9.99 3.40 -19 -9 -2 14.48 3.21 19 9 3 33.84 4.35 19 -9 3 42.28 3.88 -19 -9 -3 39.07 4.20 19 -9 4 23.06 3.62 19 9 4 26.24 4.15 -19 -9 -4 19.55 3.81 -19 -9 -5 20.85 4.07 19 -11 -5 6.63 3.64 19 -11 -4 60.70 5.10 -19 -11 4 47.62 4.47 19 -11 -3 4.10 3.49 19 -11 -2 28.97 4.06 19 11 0 0.79 3.40 19 11 1 -0.36 3.44 19 11 2 51.90 5.03 20 0 -5 1.25 3.11 20 0 -4 91.04 6.00 -20 0 4 99.32 6.17 20 0 -3 -0.08 3.40 -20 0 3 3.16 3.08 20 0 -2 43.31 4.36 -20 0 2 51.73 4.45 20 0 -1 -0.56 3.16 -20 0 1 -3.58 3.03 20 0 0 2.21 3.21 -20 0 0 -0.09 3.00 -20 0 0 -2.74 3.34 20 0 1 0.70 3.35 -20 0 -1 0.47 3.29 -20 0 -1 -2.44 3.37 20 0 2 80.67 5.71 -20 0 -2 86.51 5.96 20 0 3 -1.28 3.65 -20 0 -3 0.20 3.36 20 2 -5 27.38 3.77 20 -2 -5 19.75 3.63 -20 -2 5 28.48 3.79 20 -2 -4 41.80 4.44 20 2 -4 43.02 4.34 -20 -2 4 45.36 4.38 20 -2 -3 29.76 4.12 20 2 -3 28.37 4.05 -20 -2 3 27.16 3.78 -20 2 3 30.89 3.90 20 2 -2 20.06 3.78 20 -2 -2 19.50 3.66 -20 -2 2 22.18 3.65 -20 2 2 26.61 3.65 20 -2 -1 7.89 3.28 20 2 -1 7.68 3.28 -20 2 1 7.73 3.03 -20 -2 1 5.95 3.06 20 -2 0 3.43 3.26 20 2 0 4.29 3.41 20 2 0 7.16 2.39 -20 -2 0 7.92 3.16 -20 -2 0 7.43 3.11 -20 2 0 3.53 3.17 20 -2 1 25.62 3.89 20 2 1 33.52 4.38 20 -2 1 32.64 4.13 20 2 1 28.79 3.16 -20 2 -1 26.45 4.01 -20 -2 -1 32.93 4.03 -20 2 -1 26.27 3.95 -20 -2 -1 32.63 3.93 20 2 2 29.69 3.24 20 -2 2 31.67 4.02 -20 -2 -2 29.80 4.05 -20 2 -2 34.66 4.21 20 -2 3 38.25 4.50 -20 -2 -3 42.34 4.64 20 -4 -5 7.78 3.35 20 4 -5 5.99 3.41 -20 -4 5 8.95 3.37 20 -4 -4 6.48 3.33 20 4 -4 17.84 3.83 -20 -4 4 11.54 3.34 20 -4 -3 26.56 3.86 20 4 -3 22.73 3.92 -20 -4 3 16.50 3.55 20 4 -2 24.34 3.14 20 4 -2 24.48 3.87 20 -4 -2 17.05 3.83 -20 4 2 24.25 3.56 -20 -4 2 19.57 3.52 20 4 -1 2.22 3.16 20 4 -1 1.23 2.56 20 -4 -1 3.77 3.35 -20 -4 1 -0.18 3.04 -20 4 1 3.64 2.99 20 -4 0 62.96 4.63 20 -4 0 60.09 5.10 20 4 0 68.98 5.33 20 4 0 58.01 4.44 -20 4 0 69.71 5.29 -20 -4 0 67.90 5.12 -20 -4 0 69.05 4.96 20 -4 1 11.09 3.31 20 4 1 11.56 2.91 -20 4 -1 7.35 3.43 -20 -4 -1 8.06 3.23 -20 -4 -1 8.78 3.25 20 -4 2 12.53 3.49 20 4 2 19.46 3.22 -20 -4 -2 23.15 3.81 20 -4 3 28.34 4.06 20 4 3 24.88 3.46 -20 -4 -3 23.23 4.01 20 4 4 14.68 3.42 20 -4 4 8.94 3.79 -20 -4 -4 16.04 3.92 20 6 -5 35.86 4.29 20 -6 -5 37.18 4.15 -20 -6 5 29.96 4.06 20 -6 -4 4.00 3.24 20 6 -4 3.30 3.50 -20 -6 4 5.89 3.25 20 -6 -3 -0.87 3.27 20 6 -3 -1.03 3.37 -20 -6 3 -4.20 3.29 20 -6 -2 24.22 3.24 20 6 -2 27.58 4.23 20 -6 -2 28.90 3.94 20 6 -2 28.36 3.50 -20 -6 2 24.28 3.72 20 6 -1 45.94 4.60 20 6 -1 40.46 3.92 20 -6 -1 38.16 3.78 20 -6 -1 46.31 4.52 -20 -6 1 36.49 4.08 20 -6 0 14.09 3.08 20 6 0 12.26 3.18 -20 -6 0 14.20 3.12 20 -6 1 18.36 3.27 20 6 1 26.24 3.57 -20 -6 -1 21.41 3.47 20 6 2 7.82 3.07 20 -6 2 11.75 3.23 -20 -6 -2 13.05 3.54 20 6 3 2.30 3.16 20 -6 3 0.81 3.23 -20 -6 -3 1.76 3.39 20 -6 4 9.28 3.64 20 6 4 10.11 3.50 -20 -6 -4 11.55 3.80 20 6 5 17.67 3.76 20 8 -5 29.59 4.26 20 -8 -5 34.16 4.18 20 8 -4 24.35 4.11 20 -8 -4 27.09 3.97 -20 -8 4 26.83 3.83 20 -8 -3 3.68 3.43 -20 -8 3 4.64 3.22 20 -8 -2 5.32 3.40 -20 -8 2 8.20 3.21 20 8 -1 36.08 3.96 20 8 0 -0.16 3.07 20 8 1 32.41 3.95 20 8 2 25.77 3.83 -20 -8 -2 14.09 3.63 20 8 3 5.27 3.41 -20 -8 -3 5.30 3.62 -20 -8 -4 36.17 4.53 -20 -10 3 43.25 4.45 20 10 -1 10.20 3.44 20 10 0 0.35 3.51 20 10 1 7.75 3.57 21 -1 -5 1.66 3.38 21 1 -5 5.20 3.36 21 1 -4 2.37 3.35 21 -1 -4 1.05 3.27 -21 -1 4 4.66 3.22 21 1 -3 38.04 4.42 21 -1 -3 39.76 4.44 21 -1 1 -1.07 3.51 -21 -1 -1 -1.74 3.40 21 3 -5 24.28 3.95 -21 -3 5 30.05 4.08 21 -3 -4 15.34 3.78 21 3 -4 11.58 3.74 -21 -3 4 15.05 3.49 21 -3 -3 15.44 3.91 -21 -3 3 15.04 3.41 21 -3 0 -1.54 3.16 21 -3 1 32.15 4.20 -21 -3 -1 39.03 4.45 21 -3 2 17.08 3.75 -21 -3 -2 17.90 3.86 -21 -5 4 2.85 3.31 21 -5 0 11.04 3.26 21 -5 1 48.27 4.39 -21 -5 -1 51.16 4.74 21 -5 2 8.06 3.46 -21 -5 -2 6.43 3.59 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 2510 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 +X,+Y,+Z 2 +X,-Y,1/2+Z 3 1/2+X,1/2+Y,+Z 4 1/2+X,1/2-Y,1/2+Z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rh1 Rh 0.56183(3) 0.14178(3) 0.44782(4) 0.04179(12) Uani 1 1 d . . . . . Rh2 Rh 0.48789(3) 0.22808(3) 0.60108(4) 0.04343(13) Uani 1 1 d . . . . . S1 S 0.69561(13) 0.14429(15) 0.5561(2) 0.0709(6) Uani 1 1 d . . . . . S2 S 0.61225(14) 0.23631(17) 0.7309(2) 0.0796(8) Uani 1 1 d . . . . . O1 O 0.7158(7) 0.0914(7) 0.6349(13) 0.107(4) Uani 0.74 1 d . . P . . O2 O 0.7648(6) 0.1739(6) 0.4875(10) 0.099(3) Uani 0.86 1 d . . P . . O3 O 0.6063(7) 0.1997(6) 0.8444(9) 0.111(3) Uani 0.95 1 d . . P . . O4 O 0.6592(10) 0.2950(12) 0.7235(17) 0.103(6) Uani 0.51 1 d . . P . . O5 O 0.6776(12) 0.1626(12) 0.6982(18) 0.062(5) Uani 0.31 1 d . . P . . O6 O 0.6982(6) 0.2209(8) 0.6463(13) 0.086(4) Uani 0.63 1 d . . P . . O7 O 0.2371(9) -0.0263(10) 0.3878(16) 0.164(6) Uani 1 1 d . . . . . O8 O 0.5000(8) 0.5450(5) 0.6702(13) 0.127(4) Uani 1 1 d . . . . . C1 C 0.4639(5) 0.0835(4) 0.3184(8) 0.0553(17) Uani 1 1 d . . . . . C2 C 0.5259(6) 0.0356(4) 0.3708(8) 0.0610(19) Uani 1 1 d . . . . . C3 C 0.6107(7) 0.0538(5) 0.3323(10) 0.071(2) Uani 1 1 d . . . . . C4 C 0.6011(7) 0.1136(6) 0.2577(8) 0.070(2) Uani 1 1 d . . . . . C5 C 0.5114(7) 0.1319(4) 0.2458(7) 0.066(2) Uani 1 1 d . . . . . C6 C 0.3663(6) 0.0782(6) 0.3311(12) 0.080(3) Uani 1 1 d . . . . . H6A H 0.3397 0.1235 0.3178 0.096 Uiso 1 1 calc R U . . . H6B H 0.3547 0.0634 0.4153 0.096 Uiso 1 1 calc R U . . . C7 C 0.5067(11) -0.0271(5) 0.4465(13) 0.100(4) Uani 1 1 d . . . . . H7A H 0.5394 -0.0247 0.5255 0.120 Uiso 1 1 calc R U . . . H7B H 0.5238 -0.0680 0.4024 0.120 Uiso 1 1 calc R U . . . H7C H 0.4447 -0.0291 0.4601 0.120 Uiso 1 1 calc R U . . . C8 C 0.6924(9) 0.0134(8) 0.3554(17) 0.119(6) Uani 1 1 d . . . . . H8A H 0.6934 -0.0244 0.2971 0.143 Uiso 1 1 calc R U . . . H8B H 0.6944 -0.0045 0.4391 0.143 Uiso 1 1 calc R U . . . H8C H 0.7427 0.0428 0.3449 0.143 Uiso 1 1 calc R U . . . C9 C 0.6767(11) 0.1450(9) 0.1898(14) 0.117(6) Uani 1 1 d . . . . . H9A H 0.6607 0.1908 0.1616 0.140 Uiso 1 1 calc R U . . . H9B H 0.6892 0.1166 0.1191 0.140 Uiso 1 1 calc R U . . . H9C H 0.7283 0.1476 0.2456 0.140 Uiso 1 1 calc R U . . . C10 C 0.4733(12) 0.1865(7) 0.1637(11) 0.104(4) Uani 1 1 d . . . . . H10A H 0.4762 0.1724 0.0780 0.125 Uiso 1 1 calc R U . . . H10B H 0.5061 0.2286 0.1770 0.125 Uiso 1 1 calc R U . . . H10C H 0.4128 0.1940 0.1825 0.125 Uiso 1 1 calc R U . . . C11 C 0.3241(7) 0.0268(8) 0.2372(14) 0.100(4) Uani 1 1 d . . . . . H11A H 0.3231 0.0466 0.1538 0.120 Uiso 1 1 calc R U . . . H11B H 0.3588 -0.0154 0.2370 0.120 Uiso 1 1 calc R U . . . C12 C 0.2306(9) 0.0102(12) 0.2717(19) 0.142(8) Uani 1 1 d . . . . . H12A H 0.1969 0.0526 0.2802 0.170 Uiso 1 1 calc R U . . . H12B H 0.2012 -0.0182 0.2074 0.170 Uiso 1 1 calc R U . . . C13 C 0.1608(15) -0.044(2) 0.438(2) 0.239(19) Uani 1 1 d . . . . . H13A H 0.1732 -0.0684 0.5149 0.287 Uiso 1 1 calc R U . . . H13B H 0.1270 -0.0034 0.4529 0.287 Uiso 1 1 calc R U . . . H13C H 0.1277 -0.0740 0.3805 0.287 Uiso 1 1 calc R U . . . C14 C 0.4199(5) 0.3308(4) 0.6108(8) 0.0574(17) Uani 1 1 d . . . . . C15 C 0.4194(5) 0.2995(5) 0.7306(8) 0.0561(18) Uani 1 1 d . . . . . C16 C 0.3691(5) 0.2371(4) 0.7200(8) 0.0571(18) Uani 1 1 d . . . . . C17 C 0.3352(5) 0.2319(5) 0.5952(9) 0.0592(19) Uani 1 1 d . . . . . C18 C 0.3654(5) 0.2886(5) 0.5261(8) 0.0576(18) Uani 1 1 d . . . . . C19 C 0.4594(6) 0.3995(5) 0.5828(13) 0.077(3) Uani 1 1 d . . . . . H19A H 0.4736 0.4010 0.4955 0.093 Uiso 1 1 calc R U . . . H19B H 0.5140 0.4053 0.6331 0.093 Uiso 1 1 calc R U . . . C20 C 0.4585(7) 0.3279(6) 0.8504(10) 0.083(3) Uani 1 1 d . . . . . H20A H 0.4121 0.3389 0.9049 0.100 Uiso 1 1 calc R U . . . H20B H 0.4915 0.3691 0.8338 0.100 Uiso 1 1 calc R U . . . H20C H 0.4971 0.2940 0.8896 0.100 Uiso 1 1 calc R U . . . C21 C 0.3444(10) 0.1906(6) 0.8265(13) 0.096(4) Uani 1 1 d . . . . . H21A H 0.3059 0.2153 0.8795 0.115 Uiso 1 1 calc R U . . . H21B H 0.3969 0.1770 0.8742 0.115 Uiso 1 1 calc R U . . . H21C H 0.3147 0.1502 0.7935 0.115 Uiso 1 1 calc R U . . . C22 C 0.2670(7) 0.1805(8) 0.5493(15) 0.100(5) Uani 1 1 d . . . . . H22A H 0.2589 0.1839 0.4600 0.120 Uiso 1 1 calc R U . . . H22B H 0.2121 0.1900 0.5869 0.120 Uiso 1 1 calc R U . . . H22C H 0.2864 0.1345 0.5716 0.120 Uiso 1 1 calc R U . . . C23 C 0.3400(7) 0.3063(9) 0.3938(11) 0.105(5) Uani 1 1 d . . . . . H23A H 0.2786 0.3187 0.3868 0.125 Uiso 1 1 calc R U . . . H23B H 0.3501 0.2670 0.3414 0.125 Uiso 1 1 calc R U . . . H23C H 0.3751 0.3447 0.3677 0.125 Uiso 1 1 calc R U . . . C24 C 0.3956(8) 0.4594(7) 0.610(2) 0.126(6) Uani 1 1 d . . . . . H24A H 0.3414 0.4533 0.5592 0.151 Uiso 1 1 calc R U . . . H24B H 0.3808 0.4570 0.6971 0.151 Uiso 1 1 calc R U . . . C25 C 0.4318(9) 0.5291(7) 0.5854(19) 0.118(5) Uani 1 1 d . . . . . H25A H 0.4530 0.5304 0.5015 0.141 Uiso 1 1 calc R U . . . H25B H 0.3854 0.5634 0.5906 0.141 Uiso 1 1 calc R U . . . C26 C 0.5318(16) 0.6098(9) 0.6552(17) 0.145(7) Uani 1 1 d . . . . . H26A H 0.4838 0.6423 0.6522 0.174 Uiso 1 1 calc R U . . . H26B H 0.5620 0.6122 0.5786 0.174 Uiso 1 1 calc R U . . . H26C H 0.5722 0.6210 0.7242 0.174 Uiso 1 1 calc R U . . . C27 C 0.5024(5) 0.1233(5) 0.6127(8) 0.0524(17) Uani 1 1 d . . . . . H27A H 0.4479 0.0969 0.6050 0.063 Uiso 1 1 calc R U . . . H27B H 0.5415 0.1070 0.6811 0.063 Uiso 1 1 calc R U . . . C28 C 0.5639(6) 0.2474(4) 0.4519(10) 0.0513(15) Uani 1 1 d . . . . . H28A H 0.5336 0.2700 0.3811 0.062 Uiso 1 1 calc R U . . . H28B H 0.6212 0.2679 0.4727 0.062 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh1 0.0378(2) 0.0465(2) 0.0414(2) 0.0008(2) 0.00557(16) -0.0031(2) Rh2 0.03161(19) 0.0549(3) 0.0431(2) -0.0072(2) -0.00478(16) 0.0019(2) S1 0.0368(8) 0.1068(18) 0.0686(13) -0.0010(11) -0.0020(8) 0.0151(10) S2 0.0459(10) 0.120(2) 0.0701(14) -0.0313(13) -0.0247(9) 0.0112(12) O1 0.065(6) 0.130(10) 0.124(9) 0.044(8) 0.008(6) 0.030(6) O2 0.055(4) 0.131(8) 0.112(8) 0.018(6) 0.005(5) -0.020(5) O3 0.100(6) 0.146(8) 0.082(5) 0.007(5) -0.045(5) 0.021(6) O4 0.059(8) 0.149(16) 0.100(11) -0.029(11) -0.015(8) -0.017(9) O5 0.044(8) 0.082(13) 0.058(10) -0.004(9) -0.017(7) 0.026(9) O6 0.038(4) 0.123(10) 0.096(8) -0.022(7) -0.015(5) -0.004(5) O7 0.104(8) 0.224(16) 0.167(12) -0.036(11) 0.034(8) -0.077(9) O8 0.108(7) 0.078(6) 0.195(12) 0.022(6) -0.012(8) -0.007(5) C1 0.053(4) 0.054(4) 0.059(4) -0.011(3) 0.009(3) -0.011(3) C2 0.072(5) 0.049(4) 0.063(5) -0.007(3) 0.018(4) -0.007(4) C3 0.070(5) 0.071(6) 0.072(6) -0.023(4) 0.008(4) 0.007(5) C4 0.070(5) 0.088(6) 0.055(5) -0.019(4) 0.027(4) -0.023(5) C5 0.100(7) 0.055(4) 0.043(4) -0.005(3) -0.004(4) -0.008(4) C6 0.051(4) 0.088(7) 0.103(8) -0.038(6) 0.007(5) -0.006(5) C7 0.150(12) 0.052(5) 0.100(8) 0.013(5) 0.013(8) -0.014(6) C8 0.079(8) 0.123(11) 0.157(13) -0.065(10) 0.006(8) 0.028(8) C9 0.120(11) 0.150(13) 0.086(8) -0.024(8) 0.058(8) -0.061(10) C10 0.162(13) 0.089(8) 0.061(6) 0.011(6) -0.015(7) 0.003(8) C11 0.060(5) 0.125(10) 0.116(9) -0.048(8) 0.005(6) -0.024(6) C12 0.068(7) 0.21(2) 0.145(14) -0.078(15) 0.009(9) -0.047(10) C13 0.121(16) 0.45(6) 0.151(19) -0.05(2) 0.060(15) -0.11(2) C14 0.038(3) 0.057(4) 0.077(5) 0.005(4) -0.002(3) 0.007(3) C15 0.039(3) 0.071(5) 0.058(4) 0.001(4) -0.005(3) 0.011(3) C16 0.050(4) 0.058(4) 0.065(5) -0.003(3) 0.021(3) 0.014(3) C17 0.036(3) 0.067(5) 0.075(5) -0.019(4) 0.008(3) -0.002(3) C18 0.034(3) 0.076(5) 0.062(4) 0.001(4) -0.008(3) 0.010(3) C19 0.041(3) 0.066(5) 0.124(8) 0.016(5) 0.001(4) 0.007(4) C20 0.072(6) 0.092(7) 0.084(6) -0.037(6) -0.007(5) 0.021(5) C21 0.103(9) 0.078(7) 0.110(9) 0.020(6) 0.049(7) 0.013(6) C22 0.047(5) 0.118(10) 0.137(11) -0.046(9) 0.014(6) -0.012(6) C23 0.056(5) 0.184(15) 0.072(7) 0.023(8) -0.015(5) 0.022(7) C24 0.055(6) 0.086(8) 0.24(2) 0.055(10) 0.008(8) 0.009(5) C25 0.084(8) 0.074(7) 0.195(16) 0.041(9) 0.004(9) 0.034(6) C26 0.22(2) 0.100(11) 0.116(12) -0.006(9) -0.014(14) 0.019(13) C27 0.053(4) 0.059(4) 0.046(4) 0.006(3) 0.008(3) 0.011(3) C28 0.049(3) 0.039(3) 0.066(4) -0.011(3) 0.007(3) -0.005(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; H H 0.0000 0.0000 ; International Tables for Crystallography (Vol. C, Table 6.1.1.4) ; Rh Rh -1.1178 0.9187 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; S S 0.1246 0.1234 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; O O 0.0106 0.0060 ; International Tables for Crystallography (Vol. C, Tables 4.2.6.8 and 6.1.1.4) ; loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C28 Rh1 C27 99.4(4) . . ? C28 Rh1 C4 105.1(4) . . ? C27 Rh1 C4 153.7(3) . . ? C28 Rh1 C3 139.6(4) . . ? C27 Rh1 C3 120.8(4) . . ? C4 Rh1 C3 36.8(4) . . ? C28 Rh1 C5 96.2(4) . . ? C27 Rh1 C5 131.7(4) . . ? C4 Rh1 C5 36.5(4) . . ? C3 Rh1 C5 61.1(4) . . ? C28 Rh1 C2 156.3(4) . . ? C27 Rh1 C2 92.8(3) . . ? C4 Rh1 C2 61.0(3) . . ? C3 Rh1 C2 36.5(4) . . ? C5 Rh1 C2 60.9(3) . . ? C28 Rh1 C1 121.1(4) . . ? C27 Rh1 C1 97.9(3) . . ? C4 Rh1 C1 61.1(3) . . ? C3 Rh1 C1 61.0(3) . . ? C5 Rh1 C1 36.7(3) . . ? C2 Rh1 C1 36.3(3) . . ? C28 Rh1 S1 87.4(3) . . ? C27 Rh1 S1 89.1(2) . . ? C4 Rh1 S1 101.5(3) . . ? C3 Rh1 S1 89.2(3) . . ? C5 Rh1 S1 137.3(3) . . ? C2 Rh1 S1 113.2(3) . . ? C1 Rh1 S1 148.7(2) . . ? C28 Rh1 Rh2 50.2(3) . . ? C27 Rh1 Rh2 49.8(2) . . ? C4 Rh1 Rh2 150.6(3) . . ? C3 Rh1 Rh2 170.0(3) . . ? C5 Rh1 Rh2 121.0(3) . . ? C2 Rh1 Rh2 134.3(2) . . ? C1 Rh1 Rh2 114.1(2) . . ? S1 Rh1 Rh2 93.73(7) . . ? C27 Rh2 C28 99.5(3) . . ? C27 Rh2 C14 157.6(3) . . ? C28 Rh2 C14 98.8(3) . . ? C27 Rh2 C15 128.5(3) . . ? C28 Rh2 C15 131.7(3) . . ? C14 Rh2 C15 36.9(3) . . ? C27 Rh2 C16 97.4(3) . . ? C28 Rh2 C16 156.7(3) . . ? C14 Rh2 C16 61.6(3) . . ? C15 Rh2 C16 36.9(3) . . ? C27 Rh2 S2 87.1(2) . . ? C28 Rh2 S2 89.0(3) . . ? C14 Rh2 S2 106.1(2) . . ? C15 Rh2 S2 88.5(2) . . ? C16 Rh2 S2 107.9(2) . . ? C27 Rh2 C18 127.4(3) . . ? C28 Rh2 C18 96.4(3) . . ? C14 Rh2 C18 37.1(3) . . ? C15 Rh2 C18 61.0(3) . . ? C16 Rh2 C18 60.5(3) . . ? S2 Rh2 C18 143.2(2) . . ? C27 Rh2 C17 97.9(3) . . ? C28 Rh2 C17 125.0(4) . . ? C14 Rh2 C17 60.7(3) . . ? C15 Rh2 C17 60.3(3) . . ? C16 Rh2 C17 35.9(3) . . ? S2 Rh2 C17 143.7(2) . . ? C18 Rh2 C17 35.6(3) . . ? C27 Rh2 Rh1 50.3(2) . . ? C28 Rh2 Rh1 49.80(19) . . ? C14 Rh2 Rh1 143.3(2) . . ? C15 Rh2 Rh1 177.6(2) . . ? C16 Rh2 Rh1 140.9(2) . . ? S2 Rh2 Rh1 93.39(6) . . ? C18 Rh2 Rh1 117.7(2) . . ? C17 Rh2 Rh1 117.4(2) . . ? O1 S1 O2 118.4(7) . . ? O1 S1 O5 67.4(10) . . ? O2 S1 O5 124.4(10) . . ? O1 S1 O6 107.0(9) . . ? O2 S1 O6 87.1(7) . . ? O5 S1 O6 45.1(9) . . ? O1 S1 Rh1 117.9(6) . . ? O2 S1 Rh1 113.7(4) . . ? O5 S1 Rh1 107.3(6) . . ? O6 S1 Rh1 106.9(3) . . ? O4 S2 O3 122.0(9) . . ? O4 S2 O6 71.6(10) . . ? O3 S2 O6 117.9(7) . . ? O4 S2 O5 111.1(11) . . ? O3 S2 O5 80.2(8) . . ? O6 S2 O5 44.3(8) . . ? O4 S2 Rh2 116.5(8) . . ? O3 S2 Rh2 113.6(4) . . ? O6 S2 Rh2 107.6(4) . . ? O5 S2 Rh2 106.0(6) . . ? S1 O1 O5 63.5(9) . . ? S2 O4 O6 62.4(9) . . ? O6 O5 S1 74.2(12) . . ? O6 O5 O1 116.6(16) . . ? S1 O5 O1 49.1(7) . . ? O6 O5 S2 62.6(10) . . ? S1 O5 S2 119.2(11) . . ? O1 O5 S2 163.2(11) . . ? O5 O6 S2 73.0(11) . . ? O5 O6 S1 60.7(10) . . ? S2 O6 S1 117.1(7) . . ? O5 O6 O4 114.0(15) . . ? S2 O6 O4 46.1(7) . . ? S1 O6 O4 159.1(7) . . ? C13 O7 C12 117(2) . . ? C26 O8 C25 112.9(12) . . ? C2 C1 C5 107.5(7) . . ? C2 C1 C6 124.0(9) . . ? C5 C1 C6 128.3(9) . . ? C2 C1 Rh1 71.5(5) . . ? C5 C1 Rh1 71.2(4) . . ? C6 C1 Rh1 126.6(6) . . ? C3 C2 C1 108.5(8) . . ? C3 C2 C7 124.3(10) . . ? C1 C2 C7 127.0(10) . . ? C3 C2 Rh1 71.1(5) . . ? C1 C2 Rh1 72.2(4) . . ? C7 C2 Rh1 125.8(7) . . ? C4 C3 C2 107.4(9) . . ? C4 C3 C8 126.2(12) . . ? C2 C3 C8 126.1(12) . . ? C4 C3 Rh1 70.4(5) . . ? C2 C3 Rh1 72.4(5) . . ? C8 C3 Rh1 127.2(8) . . ? C5 C4 C3 109.2(8) . . ? C5 C4 C9 127.5(12) . . ? C3 C4 C9 122.8(12) . . ? C5 C4 Rh1 73.6(5) . . ? C3 C4 Rh1 72.8(5) . . ? C9 C4 Rh1 126.0(7) . . ? C4 C5 C1 107.3(8) . . ? C4 C5 C10 125.6(11) . . ? C1 C5 C10 126.8(11) . . ? C4 C5 Rh1 69.9(5) . . ? C1 C5 Rh1 72.0(4) . . ? C10 C5 Rh1 127.9(7) . . ? C1 C6 C11 111.6(8) . . ? C1 C6 H6A 109.3 . . ? C11 C6 H6A 109.3 . . ? C1 C6 H6B 109.3 . . ? C11 C6 H6B 109.3 . . ? H6A C6 H6B 108.0 . . ? C2 C7 H7A 109.5 . . ? C2 C7 H7B 109.5 . . ? H7A C7 H7B 109.5 . . ? C2 C7 H7C 109.5 . . ? H7A C7 H7C 109.5 . . ? H7B C7 H7C 109.5 . . ? C3 C8 H8A 109.5 . . ? C3 C8 H8B 109.5 . . ? H8A C8 H8B 109.5 . . ? C3 C8 H8C 109.5 . . ? H8A C8 H8C 109.5 . . ? H8B C8 H8C 109.5 . . ? C4 C9 H9A 109.5 . . ? C4 C9 H9B 109.5 . . ? H9A C9 H9B 109.5 . . ? C4 C9 H9C 109.5 . . ? H9A C9 H9C 109.5 . . ? H9B C9 H9C 109.5 . . ? C5 C10 H10A 109.5 . . ? C5 C10 H10B 109.5 . . ? H10A C10 H10B 109.5 . . ? C5 C10 H10C 109.5 . . ? H10A C10 H10C 109.5 . . ? H10B C10 H10C 109.5 . . ? C12 C11 C6 110.0(11) . . ? C12 C11 H11A 109.7 . . ? C6 C11 H11A 109.7 . . ? C12 C11 H11B 109.7 . . ? C6 C11 H11B 109.7 . . ? H11A C11 H11B 108.2 . . ? O7 C12 C11 107.0(15) . . ? O7 C12 H12A 110.3 . . ? C11 C12 H12A 110.3 . . ? O7 C12 H12B 110.3 . . ? C11 C12 H12B 110.3 . . ? H12A C12 H12B 108.6 . . ? O7 C13 H13A 109.5 . . ? O7 C13 H13B 109.5 . . ? H13A C13 H13B 109.5 . . ? O7 C13 H13C 109.5 . . ? H13A C13 H13C 109.5 . . ? H13B C13 H13C 109.5 . . ? C15 C14 C18 107.4(7) . . ? C15 C14 C19 125.5(9) . . ? C18 C14 C19 126.6(9) . . ? C15 C14 Rh2 71.8(5) . . ? C18 C14 Rh2 73.9(5) . . ? C19 C14 Rh2 126.0(6) . . ? C14 C15 C16 108.3(7) . . ? C14 C15 C20 127.0(9) . . ? C16 C15 C20 124.5(9) . . ? C14 C15 Rh2 71.3(5) . . ? C16 C15 Rh2 72.2(5) . . ? C20 C15 Rh2 125.5(6) . . ? C17 C16 C15 107.6(7) . . ? C17 C16 C21 125.5(10) . . ? C15 C16 C21 126.3(9) . . ? C17 C16 Rh2 74.0(4) . . ? C15 C16 Rh2 70.9(5) . . ? C21 C16 Rh2 127.8(7) . . ? C18 C17 C16 109.3(7) . . ? C18 C17 C22 125.4(10) . . ? C16 C17 C22 124.8(10) . . ? C18 C17 Rh2 71.8(4) . . ? C16 C17 Rh2 70.1(4) . . ? C22 C17 Rh2 131.3(7) . . ? C17 C18 C14 107.3(7) . . ? C17 C18 C23 127.1(9) . . ? C14 C18 C23 125.4(10) . . ? C17 C18 Rh2 72.6(4) . . ? C14 C18 Rh2 69.0(4) . . ? C23 C18 Rh2 127.8(7) . . ? C14 C19 C24 111.5(8) . . ? C14 C19 H19A 109.3 . . ? C24 C19 H19A 109.3 . . ? C14 C19 H19B 109.3 . . ? C24 C19 H19B 109.3 . . ? H19A C19 H19B 108.0 . . ? C15 C20 H20A 109.5 . . ? C15 C20 H20B 109.5 . . ? H20A C20 H20B 109.5 . . ? C15 C20 H20C 109.5 . . ? H20A C20 H20C 109.5 . . ? H20B C20 H20C 109.5 . . ? C16 C21 H21A 109.5 . . ? C16 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C16 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C17 C22 H22A 109.5 . . ? C17 C22 H22B 109.5 . . ? H22A C22 H22B 109.5 . . ? C17 C22 H22C 109.5 . . ? H22A C22 H22C 109.5 . . ? H22B C22 H22C 109.5 . . ? C18 C23 H23A 109.5 . . ? C18 C23 H23B 109.5 . . ? H23A C23 H23B 109.5 . . ? C18 C23 H23C 109.5 . . ? H23A C23 H23C 109.5 . . ? H23B C23 H23C 109.5 . . ? C25 C24 C19 113.8(11) . . ? C25 C24 H24A 108.8 . . ? C19 C24 H24A 108.8 . . ? C25 C24 H24B 108.8 . . ? C19 C24 H24B 108.8 . . ? H24A C24 H24B 107.7 . . ? O8 C25 C24 111.0(12) . . ? O8 C25 H25A 109.4 . . ? C24 C25 H25A 109.4 . . ? O8 C25 H25B 109.4 . . ? C24 C25 H25B 109.4 . . ? H25A C25 H25B 108.0 . . ? O8 C26 H26A 109.5 . . ? O8 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? O8 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? Rh2 C27 Rh1 79.9(3) . . ? Rh2 C27 H27A 115.3 . . ? Rh1 C27 H27A 115.3 . . ? Rh2 C27 H27B 115.3 . . ? Rh1 C27 H27B 115.3 . . ? H27A C27 H27B 112.3 . . ? Rh1 C28 Rh2 80.0(3) . . ? Rh1 C28 H28A 115.3 . . ? Rh2 C28 H28A 115.3 . . ? Rh1 C28 H28B 115.3 . . ? Rh2 C28 H28B 115.3 . . ? H28A C28 H28B 112.3 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh1 C28 2.038(7) . ? Rh1 C27 2.053(8) . ? Rh1 C4 2.217(8) . ? Rh1 C3 2.248(9) . ? Rh1 C5 2.265(8) . ? Rh1 C2 2.265(8) . ? Rh1 C1 2.275(7) . ? Rh1 S1 2.284(2) . ? Rh1 Rh2 2.6276(7) . ? Rh2 C27 2.037(9) . ? Rh2 C28 2.050(10) . ? Rh2 C14 2.238(8) . ? Rh2 C15 2.245(8) . ? Rh2 C16 2.263(7) . ? Rh2 S2 2.2897(18) . ? Rh2 C18 2.303(7) . ? Rh2 C17 2.312(7) . ? S1 O1 1.349(12) . ? S1 O2 1.429(10) . ? S1 O5 1.60(2) . ? S1 O6 1.764(13) . ? S2 O4 1.34(2) . ? S2 O3 1.413(11) . ? S2 O6 1.650(12) . ? S2 O5 1.777(18) . ? O1 O5 1.65(2) . ? O4 O6 1.77(2) . ? O5 O6 1.30(3) . ? O7 C13 1.34(2) . ? O7 C12 1.43(3) . ? O8 C26 1.35(2) . ? O8 C25 1.375(19) . ? C1 C2 1.414(13) . ? C1 C5 1.431(13) . ? C1 C6 1.496(12) . ? C2 C3 1.413(14) . ? C2 C7 1.493(14) . ? C3 C4 1.408(16) . ? C3 C8 1.472(17) . ? C4 C5 1.404(15) . ? C4 C9 1.514(14) . ? C5 C10 1.471(14) . ? C6 C11 1.529(14) . ? C6 H6A 0.9700 . ? C6 H6B 0.9700 . ? C7 H7A 0.9600 . ? C7 H7B 0.9600 . ? C7 H7C 0.9600 . ? C8 H8A 0.9600 . ? C8 H8B 0.9600 . ? C8 H8C 0.9600 . ? C9 H9A 0.9600 . ? C9 H9B 0.9600 . ? C9 H9C 0.9600 . ? C10 H10A 0.9600 . ? C10 H10B 0.9600 . ? C10 H10C 0.9600 . ? C11 C12 1.516(18) . ? C11 H11A 0.9700 . ? C11 H11B 0.9700 . ? C12 H12A 0.9700 . ? C12 H12B 0.9700 . ? C13 H13A 0.9600 . ? C13 H13B 0.9600 . ? C13 H13C 0.9600 . ? C14 C15 1.418(12) . ? C14 C18 1.447(12) . ? C14 C19 1.490(13) . ? C15 C16 1.427(13) . ? C15 C20 1.489(12) . ? C16 C17 1.410(13) . ? C16 C21 1.512(14) . ? C17 C18 1.410(13) . ? C17 C22 1.497(13) . ? C18 C23 1.489(13) . ? C19 C24 1.546(17) . ? C19 H19A 0.9700 . ? C19 H19B 0.9700 . ? C20 H20A 0.9600 . ? C20 H20B 0.9600 . ? C20 H20C 0.9600 . ? C21 H21A 0.9600 . ? C21 H21B 0.9600 . ? C21 H21C 0.9600 . ? C22 H22A 0.9600 . ? C22 H22B 0.9600 . ? C22 H22C 0.9600 . ? C23 H23A 0.9600 . ? C23 H23B 0.9600 . ? C23 H23C 0.9600 . ? C24 C25 1.480(18) . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C25 H25A 0.9700 . ? C25 H25B 0.9700 . ? C26 H26A 0.9600 . ? C26 H26B 0.9600 . ? C26 H26C 0.9600 . ? C27 H27A 0.9700 . ? C27 H27B 0.9700 . ? C28 H28A 0.9700 . ? C28 H28B 0.9700 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O2 S1 O1 O5 118.1(11) . . . . ? O6 S1 O1 O5 22.1(9) . . . . ? Rh1 S1 O1 O5 -98.3(9) . . . . ? O3 S2 O4 O6 112.0(9) . . . . ? O5 S2 O4 O6 20.5(10) . . . . ? Rh2 S2 O4 O6 -101.0(6) . . . . ? O1 S1 O5 O6 149.5(11) . . . . ? O2 S1 O5 O6 39.7(11) . . . . ? Rh1 S1 O5 O6 -96.8(8) . . . . ? O2 S1 O5 O1 -109.8(10) . . . . ? O6 S1 O5 O1 -149.5(11) . . . . ? Rh1 S1 O5 O1 113.7(6) . . . . ? O1 S1 O5 S2 -165.3(17) . . . . ? O2 S1 O5 S2 84.9(14) . . . . ? O6 S1 O5 S2 45.2(11) . . . . ? Rh1 S1 O5 S2 -51.6(15) . . . . ? S1 O1 O5 O6 -33.1(11) . . . . ? S1 O1 O5 S2 50(6) . . . . ? O4 S2 O5 O6 -28.3(13) . . . . ? O3 S2 O5 O6 -149.0(9) . . . . ? Rh2 S2 O5 O6 99.1(8) . . . . ? O4 S2 O5 S1 -78.5(16) . . . . ? O3 S2 O5 S1 160.8(15) . . . . ? O6 S2 O5 S1 -50.2(12) . . . . ? Rh2 S2 O5 S1 48.9(15) . . . . ? O4 S2 O5 O1 -120(6) . . . . ? O3 S2 O5 O1 119(6) . . . . ? O6 S2 O5 O1 -92(6) . . . . ? Rh2 S2 O5 O1 7(6) . . . . ? S1 O5 O6 S2 135.8(6) . . . . ? O1 O5 O6 S2 161.2(12) . . . . ? O1 O5 O6 S1 25.4(9) . . . . ? S2 O5 O6 S1 -135.8(6) . . . . ? S1 O5 O6 O4 157.4(8) . . . . ? O1 O5 O6 O4 -177.3(10) . . . . ? S2 O5 O6 O4 21.6(8) . . . . ? O4 S2 O6 O5 152.2(13) . . . . ? O3 S2 O6 O5 35.0(11) . . . . ? Rh2 S2 O6 O5 -95.0(9) . . . . ? O4 S2 O6 S1 -164.8(12) . . . . ? O3 S2 O6 S1 78.1(9) . . . . ? O5 S2 O6 S1 43.0(9) . . . . ? Rh2 S2 O6 S1 -52.0(9) . . . . ? O3 S2 O6 O4 -117.1(10) . . . . ? O5 S2 O6 O4 -152.2(13) . . . . ? Rh2 S2 O6 O4 112.8(8) . . . . ? O1 S1 O6 O5 -29.3(10) . . . . ? O2 S1 O6 O5 -148.1(10) . . . . ? Rh1 S1 O6 O5 97.9(9) . . . . ? O1 S1 O6 S2 -77.8(9) . . . . ? O2 S1 O6 S2 163.4(9) . . . . ? O5 S1 O6 S2 -48.5(10) . . . . ? Rh1 S1 O6 S2 49.4(9) . . . . ? O1 S1 O6 O4 -110(3) . . . . ? O2 S1 O6 O4 131(3) . . . . ? O5 S1 O6 O4 -81(3) . . . . ? Rh1 S1 O6 O4 17(3) . . . . ? S2 O4 O6 O5 -29.2(12) . . . . ? S2 O4 O6 S1 41(3) . . . . ? C5 C1 C2 C3 0.3(9) . . . . ? C6 C1 C2 C3 175.6(8) . . . . ? Rh1 C1 C2 C3 -62.2(6) . . . . ? C5 C1 C2 C7 -175.6(10) . . . . ? C6 C1 C2 C7 -0.3(14) . . . . ? Rh1 C1 C2 C7 121.9(10) . . . . ? C5 C1 C2 Rh1 62.5(5) . . . . ? C6 C1 C2 Rh1 -122.1(8) . . . . ? C1 C2 C3 C4 0.8(10) . . . . ? C7 C2 C3 C4 176.9(9) . . . . ? Rh1 C2 C3 C4 -62.1(6) . . . . ? C1 C2 C3 C8 -173.4(10) . . . . ? C7 C2 C3 C8 2.7(16) . . . . ? Rh1 C2 C3 C8 123.7(11) . . . . ? C1 C2 C3 Rh1 62.9(6) . . . . ? C7 C2 C3 Rh1 -121.0(10) . . . . ? C2 C3 C4 C5 -1.7(10) . . . . ? C8 C3 C4 C5 172.5(10) . . . . ? Rh1 C3 C4 C5 -65.1(6) . . . . ? C2 C3 C4 C9 -174.4(9) . . . . ? C8 C3 C4 C9 -0.2(16) . . . . ? Rh1 C3 C4 C9 122.2(10) . . . . ? C2 C3 C4 Rh1 63.4(6) . . . . ? C8 C3 C4 Rh1 -122.4(11) . . . . ? C3 C4 C5 C1 1.9(10) . . . . ? C9 C4 C5 C1 174.2(10) . . . . ? Rh1 C4 C5 C1 -62.7(6) . . . . ? C3 C4 C5 C10 -172.5(9) . . . . ? C9 C4 C5 C10 -0.3(16) . . . . ? Rh1 C4 C5 C10 122.8(9) . . . . ? C3 C4 C5 Rh1 64.6(6) . . . . ? C9 C4 C5 Rh1 -123.1(11) . . . . ? C2 C1 C5 C4 -1.4(9) . . . . ? C6 C1 C5 C4 -176.4(8) . . . . ? Rh1 C1 C5 C4 61.3(6) . . . . ? C2 C1 C5 C10 173.0(9) . . . . ? C6 C1 C5 C10 -2.1(15) . . . . ? Rh1 C1 C5 C10 -124.3(10) . . . . ? C2 C1 C5 Rh1 -62.7(6) . . . . ? C6 C1 C5 Rh1 122.3(9) . . . . ? C2 C1 C6 C11 -80.9(14) . . . . ? C5 C1 C6 C11 93.4(13) . . . . ? Rh1 C1 C6 C11 -172.2(9) . . . . ? C1 C6 C11 C12 166.9(15) . . . . ? C13 O7 C12 C11 178(2) . . . . ? C6 C11 C12 O7 -66(2) . . . . ? C18 C14 C15 C16 2.7(9) . . . . ? C19 C14 C15 C16 175.2(7) . . . . ? Rh2 C14 C15 C16 -63.1(5) . . . . ? C18 C14 C15 C20 -173.2(8) . . . . ? C19 C14 C15 C20 -0.8(13) . . . . ? Rh2 C14 C15 C20 120.9(8) . . . . ? C18 C14 C15 Rh2 65.9(5) . . . . ? C19 C14 C15 Rh2 -121.7(8) . . . . ? C14 C15 C16 C17 -2.8(9) . . . . ? C20 C15 C16 C17 173.3(8) . . . . ? Rh2 C15 C16 C17 -65.4(5) . . . . ? C14 C15 C16 C21 -174.1(8) . . . . ? C20 C15 C16 C21 2.0(14) . . . . ? Rh2 C15 C16 C21 123.4(9) . . . . ? C14 C15 C16 Rh2 62.5(6) . . . . ? C20 C15 C16 Rh2 -121.4(8) . . . . ? C15 C16 C17 C18 1.8(9) . . . . ? C21 C16 C17 C18 173.1(8) . . . . ? Rh2 C16 C17 C18 -61.5(5) . . . . ? C15 C16 C17 C22 -169.5(9) . . . . ? C21 C16 C17 C22 1.8(14) . . . . ? Rh2 C16 C17 C22 127.2(9) . . . . ? C15 C16 C17 Rh2 63.3(5) . . . . ? C21 C16 C17 Rh2 -125.3(9) . . . . ? C16 C17 C18 C14 -0.1(9) . . . . ? C22 C17 C18 C14 171.1(8) . . . . ? Rh2 C17 C18 C14 -60.6(5) . . . . ? C16 C17 C18 C23 -174.9(9) . . . . ? C22 C17 C18 C23 -3.7(15) . . . . ? Rh2 C17 C18 C23 124.6(10) . . . . ? C16 C17 C18 Rh2 60.5(5) . . . . ? C22 C17 C18 Rh2 -128.3(9) . . . . ? C15 C14 C18 C17 -1.6(9) . . . . ? C19 C14 C18 C17 -174.0(8) . . . . ? Rh2 C14 C18 C17 62.9(5) . . . . ? C15 C14 C18 C23 173.3(9) . . . . ? C19 C14 C18 C23 1.0(14) . . . . ? Rh2 C14 C18 C23 -122.2(9) . . . . ? C15 C14 C18 Rh2 -64.5(5) . . . . ? C19 C14 C18 Rh2 123.2(9) . . . . ? C15 C14 C19 C24 -82.6(13) . . . . ? C18 C14 C19 C24 88.4(15) . . . . ? Rh2 C14 C19 C24 -175.2(10) . . . . ? C14 C19 C24 C25 179.3(14) . . . . ? C26 O8 C25 C24 -176.6(16) . . . . ? C19 C24 C25 O8 -69(2) . . . . ?