#------------------------------------------------------------------------------ #$Date: 2021-11-26 01:55:05 +0200 (Fri, 26 Nov 2021) $ #$Revision: 270882 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/89/7708934.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708934 loop_ _publ_author_name 'Cong, Zhenzhong' 'Zhu, Mingchang' 'Zhang, Ying' 'Yao, Wei' 'Kosinova, Marina' 'Fedin, Vladimir P.' 'Wu, Shuangyan' 'Gao, Enjun' _publ_section_title ; Three novel metal-organic frameworks with different coordination modes for trace detection of anthrax biomarkers ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03760A _journal_year 2021 _chemical_formula_moiety 'C24 H9 O16.5 Zn3' _chemical_formula_sum 'C24 H13 O17 Zn3' _chemical_formula_weight 769.45 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2021-08-06 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2021-08-06 deposited with the CCDC. 2021-11-25 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 93.623(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.2364(5) _cell_length_b 13.3601(8) _cell_length_c 29.3596(18) _cell_measurement_reflns_used 9924 _cell_measurement_temperature 150.02 _cell_measurement_theta_max 26.41 _cell_measurement_theta_min 2.58 _cell_volume 4007.2(4) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 150.02 _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0551 _diffrn_reflns_av_unetI/netI 0.0298 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 36 _diffrn_reflns_limit_l_min -36 _diffrn_reflns_number 63223 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.021 _diffrn_reflns_theta_min 2.152 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.838 _exptl_absorpt_correction_T_max 0.028 _exptl_absorpt_correction_T_min 0.011 _exptl_absorpt_correction_type none _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0763 before and 0.0617 after correction. The Ratio of minimum to maximum transmission is 0.3986. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.275 _exptl_crystal_description block _exptl_crystal_F_000 1532 _exptl_crystal_size_max 0.01 _exptl_crystal_size_mid 0.01 _exptl_crystal_size_min 0.01 _refine_diff_density_max 2.178 _refine_diff_density_min -1.144 _refine_diff_density_rms 0.117 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.082 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 385 _refine_ls_number_reflns 7900 _refine_ls_number_restraints 19 _refine_ls_restrained_S_all 2.487 _refine_ls_R_factor_all 0.0706 _refine_ls_R_factor_gt 0.0578 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1140P)^2^+5.8080P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1744 _refine_ls_wR_factor_ref 0.1878 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6141 _reflns_number_total 7900 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03760a2.cif _cod_data_source_block mo_0910_7_0m _cod_database_code 7708934 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.982 _shelx_estimated_absorpt_t_min 0.982 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All O(H) groups 2. Restrained distances O1-O2 5 with sigma of 0.03 3. Uiso/Uaniso restraints and constraints Uanis(O019) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O00O) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O00F) \\sim Ueq: with sigma of 0.001 and sigma for terminal atoms of 0.002 Uanis(O019) = Uanis(O00O) = Uanis(O00F) 4. Others Fixed Sof: O1(0.75) O2(0.75) 5.a Ternary CH refined with riding coordinates: O004(H004) 5.b Aromatic/amide H refined with riding coordinates: C00P(H00P), C00Q(H00Q), C00S(H00S), C00T(H00T), C00V(H00V), C011(H011), C012(H012), C017(H017) ; _smtbx_masks_void_probe_radius 1.2 _smtbx_masks_void_truncation_radius 1.2 _shelx_res_file ; TITL mo_0910_7_0m_a.res in P2(1)/n mo_0910_7_0m.res created by SHELXL-2017/1 at 16:37:34 on 06-Aug-2021 REM Old TITL mo_0910_7_0m in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.136, Rweak 0.007, Alpha 0.030 REM 0.551 for 359 systematic absences, Orientation as input REM Formula found by SHELXT: C33 O15 Zn3 CELL 0.71073 10.2364 13.3601 29.3596 90 93.623 90 ZERR 4 0.0005 0.0008 0.0018 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H O Zn UNIT 96 52 68 12 DFIX 5 0.03 O1 O2 ISOR 0.001 0.002 O019 ISOR 0.001 0.002 O00O ISOR 0.001 0.002 O00F EADP O019 O00O O00F L.S. 20 0 0 PLAN 18 SIZE 0.01 0.01 0.01 TEMP -123.13 CONF BOND list 4 MORE -1 ABIN BOND $H fmap 2 53 acta OMIT -1 3 1 REM REM REM WGHT 0.114000 5.808000 FVAR 0.31134 ZN01 4 1.081904 0.737180 0.619693 11.00000 0.03519 0.03631 = 0.03613 0.00137 0.00588 0.00764 ZN02 4 0.881261 0.024314 0.418079 11.00000 0.03443 0.03822 = 0.03426 0.00090 0.00277 0.00310 ZN03 4 0.625121 0.406944 0.851714 11.00000 0.03963 0.04150 = 0.04570 0.00096 0.00973 -0.00645 O004 3 0.935108 0.115021 0.370969 11.00000 0.03622 0.03600 = 0.03552 -0.00140 0.00550 0.00416 AFIX 13 H004 2 0.877018 0.099234 0.343233 11.00000 -1.50000 AFIX 0 O005 3 0.258769 0.061455 0.610105 11.00000 0.04437 0.04897 = 0.03263 -0.00333 0.00020 -0.00439 O006 3 0.551615 0.413614 0.542476 11.00000 0.04685 0.04118 = 0.04250 -0.00816 -0.00654 0.01329 O007 3 0.920099 0.657065 0.602403 11.00000 0.03429 0.05322 = 0.05077 0.00120 0.01034 0.00207 O008 3 0.815142 0.078376 0.473706 11.00000 0.05183 0.04546 = 0.03539 -0.00203 0.00509 0.00827 O009 3 0.589976 0.339495 0.629378 11.00000 0.06992 0.03947 = 0.03764 -0.00553 0.01907 -0.00053 O00A 3 0.228081 0.645711 0.607370 11.00000 0.04179 0.06182 = 0.04823 0.00504 0.00859 0.01820 O00B 3 0.988540 0.077169 0.562041 11.00000 0.04574 0.05251 = 0.04391 0.00745 0.00524 0.02018 O00C 3 0.419271 0.211994 0.810992 11.00000 0.06342 0.05985 = 0.03366 -0.00950 0.01062 -0.01324 O00D 3 0.914993 0.222033 0.458984 11.00000 0.06128 0.06086 = 0.04989 -0.01096 0.02430 -0.00521 O00F 3 0.587229 0.312297 0.798042 11.00000 0.08636 0.09204 = 0.08912 0.00080 0.00896 -0.00453 O00G 3 0.233314 0.004685 0.680676 11.00000 0.07437 0.07296 = 0.04609 -0.00036 -0.00019 -0.02292 O00H 3 0.331100 0.788662 0.614810 11.00000 0.05059 0.06932 = 0.11919 -0.04328 -0.00425 0.02451 C00J 1 0.785431 0.213622 0.522805 11.00000 0.03764 0.03548 = 0.04012 -0.00398 0.00172 0.00398 C00K 1 0.642330 0.337844 0.551843 11.00000 0.03625 0.03286 = 0.03496 -0.00186 0.00091 0.00977 C00L 1 0.688713 0.647211 0.591555 11.00000 0.03804 0.04147 = 0.03340 0.00341 0.00009 0.00304 C00M 1 0.792028 0.167761 0.565981 11.00000 0.03739 0.03294 = 0.04473 0.00423 0.00527 0.00471 C00N 1 0.566643 0.505005 0.564958 11.00000 0.04061 0.03649 = 0.03218 -0.00294 0.00236 0.00936 O00O 3 0.815046 0.426930 0.832566 11.00000 0.08636 0.09204 = 0.08912 0.00080 0.00896 -0.00453 C00P 1 0.709588 0.300097 0.516406 11.00000 0.04691 0.03914 = 0.03274 0.00291 0.00112 0.00699 AFIX 43 H00P 2 0.704385 0.332867 0.487632 11.00000 -1.20000 AFIX 0 C00Q 1 0.685625 0.550811 0.573253 11.00000 0.03404 0.04181 = 0.03615 0.00462 0.00390 0.00968 AFIX 43 H00Q 2 0.764311 0.517605 0.566677 11.00000 -1.20000 AFIX 0 C00R 1 0.653048 0.293789 0.594767 11.00000 0.03971 0.03733 = 0.03409 -0.00423 0.01180 0.00009 C00S 1 0.727395 0.207985 0.601425 11.00000 0.04594 0.04019 = 0.03415 0.00603 0.00370 0.00172 AFIX 43 H00S 2 0.733896 0.176699 0.630538 11.00000 -1.20000 AFIX 0 C00T 1 0.571877 0.694147 0.601752 11.00000 0.04035 0.04084 = 0.04507 -0.00341 -0.00238 0.01040 AFIX 43 H00T 2 0.574146 0.760374 0.613556 11.00000 -1.20000 AFIX 0 C00U 1 0.843474 0.169339 0.482279 11.00000 0.03798 0.04259 = 0.03768 0.00218 0.00239 0.00978 C00V 1 0.449921 0.550300 0.576118 11.00000 0.03563 0.04490 = 0.03417 -0.00020 0.00377 0.00580 AFIX 43 H00V 2 0.368904 0.516219 0.570899 11.00000 -1.20000 AFIX 0 C00W 1 0.453593 0.645485 0.594882 11.00000 0.03748 0.04408 = 0.03925 -0.00191 -0.00266 0.01002 C00X 1 0.329945 0.697135 0.606472 11.00000 0.03726 0.06616 = 0.03935 -0.01093 -0.00133 0.01428 C00Y 1 0.814485 0.704830 0.600148 11.00000 0.04168 0.05433 = 0.03915 0.00677 -0.00023 -0.00059 C00Z 1 0.524625 0.276980 0.658352 11.00000 0.04755 0.04974 = 0.03839 -0.00638 0.01455 -0.00128 C010 1 0.280529 0.062734 0.653243 11.00000 0.04734 0.05457 = 0.04684 -0.00173 0.00903 -0.00493 C011 1 0.438607 0.204219 0.641119 11.00000 0.04172 0.06319 = 0.03105 -0.00978 0.00602 -0.00237 AFIX 43 H011 2 0.424453 0.195040 0.609101 11.00000 -1.20000 AFIX 0 C012 1 0.545718 0.292776 0.704630 11.00000 0.04861 0.05425 = 0.03705 -0.01032 0.00872 -0.00919 AFIX 43 H012 2 0.606993 0.341637 0.715883 11.00000 -1.20000 AFIX 0 C013 1 0.876205 0.076236 0.575166 11.00000 0.04645 0.04470 = 0.04952 0.00275 -0.00098 0.00969 C014 1 0.372953 0.144529 0.671338 11.00000 0.04563 0.05705 = 0.04211 -0.00671 0.00843 -0.00695 C015 1 0.475480 0.235725 0.734881 11.00000 0.04710 0.06621 = 0.03841 -0.01281 0.01122 -0.01040 C016 1 0.493779 0.254386 0.785430 11.00000 0.03788 0.07419 = 0.03592 -0.01424 0.00657 -0.01191 C017 1 0.390013 0.161824 0.718161 11.00000 0.04769 0.06826 = 0.04165 -0.00540 0.01122 -0.01408 AFIX 43 H017 2 0.342982 0.122899 0.738699 11.00000 -1.20000 AFIX 0 O019 3 0.565454 0.532582 0.813638 11.00000 0.08636 0.09204 = 0.08912 0.00080 0.00896 -0.00453 O1 3 0.805372 0.794455 0.602777 10.75000 0.03575 0.02411 = 0.07121 0.00599 -0.02561 -0.00072 O2 3 0.824914 0.007114 0.594561 10.75000 0.03455 0.04296 = 0.12100 0.05992 0.01071 0.00849 HKLF 4 REM mo_0910_7_0m_a.res in P2(1)/n REM R1 = 0.0578 for 6141 Fo > 4sig(Fo) and 0.0706 for all 7900 data REM 385 parameters refined using 19 restraints END WGHT 0.1143 5.9396 REM Highest difference peak 2.178, deepest hole -1.144, 1-sigma level 0.117 Q1 1 0.6202 0.5567 0.7794 11.00000 0.05 2.18 Q2 1 0.5996 0.2833 0.8015 11.00000 0.05 1.53 Q3 1 0.8164 0.8195 0.6029 11.00000 0.05 1.30 Q4 1 0.5435 0.5033 0.7833 11.00000 0.05 1.20 Q5 1 0.5370 0.5302 0.7764 11.00000 0.05 1.17 Q6 1 0.8354 -0.0103 0.5860 11.00000 0.05 0.98 Q7 1 0.8552 0.0354 0.6204 11.00000 0.05 0.93 Q8 1 0.7657 0.7980 0.6149 11.00000 0.05 0.76 Q9 1 0.7916 0.4652 0.8158 11.00000 0.05 0.69 Q10 1 0.4706 0.9350 0.6193 11.00000 0.05 0.67 Q11 1 0.2265 0.1259 0.6406 11.00000 0.05 0.67 Q12 1 0.1287 0.1195 0.6588 11.00000 0.05 0.62 Q13 1 0.8277 0.3939 0.8364 11.00000 0.05 0.62 Q14 1 0.2062 -0.0627 0.7147 11.00000 0.05 0.57 Q15 1 0.3411 0.2012 0.6606 11.00000 0.05 0.54 Q16 1 0.2065 0.6044 0.6016 11.00000 0.05 0.46 Q17 1 0.6889 0.4963 0.7964 11.00000 0.05 0.40 Q18 1 0.5691 0.3930 0.8405 11.00000 0.05 0.38 ; _shelx_res_checksum 96213 _shelx_hkl_file ; 2 0 0 2218.08 67.99 -2 0 0 2274.07 68.09 3 0 0 2.50 3.30 3 0 0 -0.10 1.30 -3 0 0 2.00 3.50 4 0 0 3467.85 102.89 -4 0 0 3473.75 105.49 4 0 0 3453.45 105.29 4 0 0 3460.55 102.89 5 0 0 -0.30 4.10 5 0 0 0.20 2.40 5 0 0 3.00 2.50 6 0 0 1078.39 34.70 6 0 0 1100.69 37.20 6 0 0 1097.39 34.70 7 0 0 0.80 3.10 7 0 0 2.60 4.60 7 0 0 1.00 3.10 8 0 0 8.50 5.20 8 0 0 2.10 3.70 8 0 0 9.30 3.80 9 0 0 7.60 5.30 9 0 0 4.70 4.10 9 0 0 1.60 4.20 10 0 0 56.59 7.40 10 0 0 54.39 6.20 10 0 0 60.99 6.50 11 0 0 -6.50 5.20 11 0 0 -5.50 4.90 11 0 0 -2.30 4.60 12 0 0 22.40 6.00 12 0 0 19.80 6.40 1 -1 0 4463.95 124.29 -1 -1 0 3882.71 124.59 1 -1 0 4501.05 124.39 1 -1 0 4555.74 125.09 1 1 0 4424.56 124.09 1 1 0 4498.65 123.99 -1 1 0 3816.12 124.49 -1 1 0 3874.41 125.69 -1 1 0 3644.74 125.19 2 -1 0 251.17 9.90 2 -1 0 257.67 10.00 2 -1 0 259.37 11.90 2 1 0 249.78 9.00 2 1 0 257.47 9.10 -2 1 0 252.57 12.10 -2 1 0 251.67 8.90 3 -1 0 2276.97 68.19 3 -1 0 2228.28 68.29 3 -1 0 2325.67 70.39 3 1 0 2313.27 68.99 3 1 0 2257.37 67.49 -3 1 0 2222.38 70.29 3 1 0 2201.68 67.39 4 -1 0 884.91 28.40 4 -1 0 884.31 28.40 4 -1 0 915.91 31.00 -4 1 0 861.61 31.00 4 1 0 872.31 29.40 4 1 0 883.11 27.50 4 1 0 883.61 27.50 5 -1 0 931.81 30.30 5 -1 0 936.81 30.20 5 -1 0 955.30 33.00 5 1 0 936.91 29.50 5 1 0 922.01 29.40 -5 1 0 893.51 32.90 5 1 0 942.51 31.50 6 -1 0 38.30 6.30 6 -1 0 37.60 4.60 6 -1 0 39.60 4.60 6 1 0 42.10 5.40 6 1 0 41.40 4.10 6 1 0 45.10 5.70 -6 1 0 37.80 6.40 7 -1 0 184.48 10.30 7 -1 0 194.88 10.50 7 -1 0 202.88 13.20 -7 1 0 193.88 13.40 7 1 0 183.88 9.70 7 1 0 206.78 9.80 7 1 0 212.08 11.90 8 -1 0 410.06 19.40 8 -1 0 430.46 17.40 8 -1 0 430.56 17.20 8 1 0 444.76 18.40 8 1 0 406.16 16.40 8 1 0 411.06 16.40 9 -1 0 71.39 8.70 9 -1 0 62.89 6.60 9 -1 0 76.59 8.50 9 1 0 73.69 7.40 9 1 0 64.99 7.90 9 1 0 67.39 8.00 10 -1 0 103.99 10.30 10 -1 0 122.99 10.30 10 -1 0 140.69 12.80 10 1 0 124.29 9.70 10 1 0 116.89 10.60 10 1 0 132.69 9.80 11 -1 0 57.39 6.80 11 -1 0 65.39 7.00 11 1 0 51.29 6.40 11 1 0 49.30 6.40 11 1 0 60.79 6.60 12 -1 0 -4.30 5.60 12 1 0 1.90 5.50 12 1 0 1.10 5.60 12 1 0 -1.10 5.10 0 -2 0 309.77 12.60 0 -2 0 295.07 12.10 0 -2 0 311.67 12.20 0 2 0 298.57 12.40 0 2 0 300.97 12.40 0 2 0 306.37 12.20 1 -2 0 630.34 22.40 -1 -2 0 645.64 21.30 1 -2 0 642.04 21.80 -1 -2 0 600.34 21.30 -1 2 0 618.64 21.70 1 2 0 622.84 21.40 -1 2 0 614.24 21.50 1 2 0 620.44 21.50 1 2 0 617.54 21.00 -1 2 0 615.24 22.40 2 -2 0 150.98 10.80 -2 -2 0 142.49 7.50 2 -2 0 147.99 9.10 2 -2 0 153.68 9.00 -2 -2 0 143.69 7.40 -2 2 0 152.28 10.20 2 2 0 144.29 8.30 2 2 0 146.89 8.50 -2 2 0 141.19 8.50 -2 2 0 148.39 8.50 3 -2 0 376.26 16.70 3 -2 0 375.66 15.00 3 -2 0 357.36 14.70 -3 2 0 400.96 13.60 3 2 0 366.06 14.00 -3 2 0 371.26 16.80 3 2 0 359.66 13.90 -3 2 0 373.66 13.50 4 -2 0 74.99 7.90 4 -2 0 86.49 7.60 4 -2 0 74.39 7.40 -4 2 0 82.89 10.00 4 2 0 77.79 6.50 4 2 0 84.89 6.60 5 -2 0 5.20 3.60 5 -2 0 -8.50 4.60 5 -2 0 2.00 3.50 5 2 0 -0.10 2.90 5 2 0 -5.40 3.30 5 2 0 0.00 2.90 -5 2 0 -5.40 5.00 6 -2 0 296.27 13.30 6 -2 0 301.57 16.10 6 -2 0 280.47 13.30 6 2 0 290.27 13.40 6 2 0 292.27 12.30 -6 2 0 298.77 16.50 6 2 0 273.07 12.20 7 -2 0 189.98 11.20 7 -2 0 171.28 10.70 7 -2 0 191.68 13.60 7 2 0 187.78 11.00 7 2 0 176.48 9.90 7 2 0 183.58 9.80 -7 2 0 182.38 14.00 8 -2 0 855.61 30.30 8 -2 0 856.71 32.70 8 -2 0 857.01 30.20 8 2 0 832.82 29.20 8 2 0 881.81 29.80 -8 2 0 863.71 33.00 8 2 0 870.71 29.30 9 -2 0 111.89 10.20 9 -2 0 125.09 13.60 9 -2 0 111.79 10.70 9 2 0 109.69 9.30 9 2 0 109.39 9.70 9 2 0 112.09 9.10 10 -2 0 12.20 5.30 10 -2 0 8.70 5.20 10 2 0 -1.00 4.30 10 2 0 2.60 4.60 10 2 0 0.70 4.60 11 -2 0 5.50 5.40 11 2 0 4.60 5.10 11 2 0 -5.70 4.90 11 2 0 -4.50 4.40 12 -2 0 226.68 17.00 12 -2 0 212.08 14.40 12 2 0 212.58 13.20 12 2 0 223.58 11.20 12 2 0 229.78 13.30 0 -3 0 4.20 4.70 0 -3 0 2.90 4.60 0 -3 0 8.40 5.00 0 3 0 2.90 4.40 0 3 0 10.10 5.00 0 3 0 8.10 4.90 1 -3 0 160.38 11.20 -1 -3 0 168.48 10.00 1 -3 0 151.78 10.60 -1 -3 0 143.09 10.50 -1 -3 0 149.69 10.30 1 -3 0 169.28 11.80 1 3 0 163.48 10.50 -1 3 0 160.78 12.00 1 3 0 145.09 10.60 -1 3 0 163.08 10.90 1 3 0 165.18 10.20 -1 3 0 169.78 11.00 2 -3 0 39.10 5.70 2 -3 0 40.80 5.90 -2 -3 0 57.79 7.20 -2 -3 0 39.50 4.90 2 -3 0 46.80 7.10 -2 3 0 40.20 5.40 -2 3 0 40.20 6.60 2 3 0 35.70 5.20 2 3 0 44.90 5.60 -2 3 0 49.50 5.90 2 3 0 42.60 5.00 -3 -3 0 36.60 4.20 3 -3 0 35.30 5.30 -3 -3 0 44.50 5.50 3 -3 0 40.30 5.70 3 -3 0 47.40 7.30 3 3 0 36.80 5.00 -3 3 0 38.10 4.90 -3 3 0 41.90 7.00 -3 3 0 40.10 4.90 3 3 0 36.80 4.90 4 -3 0 4479.75 135.39 4 -3 0 4352.86 133.49 4 -3 0 4387.96 133.39 -4 3 0 4391.56 135.39 -4 3 0 4426.26 131.59 -4 3 0 4328.97 131.49 4 3 0 4447.46 132.59 4 3 0 4337.87 132.39 5 -3 0 836.82 28.80 5 -3 0 763.12 30.60 5 -3 0 792.42 28.60 5 3 0 841.02 27.80 5 3 0 772.42 27.40 -5 3 0 768.52 30.90 6 -3 0 129.79 10.20 6 -3 0 112.29 9.80 6 -3 0 112.49 12.50 6 3 0 127.29 8.90 -6 3 0 121.49 13.00 6 3 0 108.59 9.00 6 3 0 123.89 8.90 7 -3 0 3.60 4.60 7 -3 0 1.50 4.50 7 -3 0 4.10 5.90 -7 3 0 8.30 6.50 7 3 0 -0.10 4.00 7 3 0 2.80 3.80 7 3 0 -2.80 3.80 8 -3 0 82.29 9.70 8 -3 0 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131.19 10.80 2 4 0 150.38 11.00 -2 4 0 151.88 11.10 -3 -4 0 1067.69 34.60 3 -4 0 998.60 36.50 -3 -4 0 1040.60 34.60 3 -4 0 1062.59 36.60 3 -4 0 1017.40 37.50 3 4 0 1090.89 36.20 -3 4 0 1060.39 35.90 3 4 0 1010.30 35.70 -3 4 0 1006.40 35.50 3 4 0 1056.69 35.00 -3 4 0 1010.60 37.90 -4 -4 0 19.40 3.60 4 -4 0 21.60 7.10 4 -4 0 21.10 5.70 -4 -4 0 19.60 3.50 4 -4 0 22.30 5.70 -4 4 0 24.00 4.80 -4 4 0 27.50 5.00 4 4 0 21.50 5.20 -4 4 0 23.20 7.50 4 4 0 26.10 5.40 4 4 0 23.10 4.80 5 -4 0 26.20 5.90 5 -4 0 19.40 6.80 5 -4 0 12.60 5.40 -5 4 0 12.50 6.40 5 4 0 20.40 5.00 -5 4 0 15.30 3.70 5 4 0 19.60 5.00 -5 4 0 16.10 3.80 6 -4 0 265.67 17.00 6 -4 0 272.97 14.90 6 -4 0 265.77 14.70 6 4 0 264.97 13.60 -6 4 0 290.87 17.80 6 4 0 270.37 13.80 7 -4 0 12.50 5.40 7 -4 0 -4.10 4.90 7 4 0 8.20 4.70 7 4 0 2.70 4.00 -7 4 0 -7.20 6.50 7 4 0 7.60 4.70 8 -4 0 26.10 6.30 8 -4 0 35.30 6.50 -8 4 0 17.30 7.70 8 4 0 27.40 5.70 8 4 0 28.70 5.10 8 4 0 29.60 5.60 9 -4 0 17.40 7.40 9 -4 0 21.60 6.10 9 -4 0 13.10 6.00 9 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176.98 11.90 3 -5 0 172.68 13.50 3 -5 0 165.38 14.70 -3 5 0 172.68 12.60 -3 5 0 160.38 12.50 3 5 0 177.48 13.00 -3 5 0 175.38 15.30 3 5 0 183.48 13.20 3 5 0 171.68 11.70 -4 -5 0 1016.60 34.20 -4 -5 0 1053.39 34.30 4 -5 0 1019.30 38.40 4 -5 0 1016.40 37.30 4 -5 0 1034.80 37.30 -4 5 0 1040.90 35.80 4 5 0 986.30 34.80 4 5 0 1019.40 36.50 4 5 0 1020.70 36.40 -4 5 0 1031.10 39.20 -4 5 0 1031.10 35.70 5 -5 0 261.87 15.60 -5 -5 0 260.97 10.40 -5 -5 0 270.67 10.40 5 -5 0 281.27 17.40 5 -5 0 286.57 16.10 -5 5 0 264.37 13.30 5 5 0 275.77 15.10 5 5 0 273.07 13.60 -5 5 0 292.87 13.70 5 5 0 292.47 15.40 -5 5 0 248.98 17.90 6 -5 0 70.09 8.70 6 -5 0 76.89 8.80 6 5 0 80.59 10.00 -6 5 0 65.69 10.10 -6 5 0 82.99 6.70 6 5 0 82.59 10.00 -6 5 0 89.09 6.80 6 5 0 62.39 6.40 7 -5 0 5.90 5.70 7 -5 0 -2.10 5.70 7 5 0 8.00 4.30 -7 5 0 8.50 7.60 7 5 0 -2.00 4.90 7 5 0 7.10 5.10 8 -5 0 234.48 15.40 8 -5 0 274.17 18.60 8 5 0 232.78 14.20 -8 5 0 235.88 18.10 8 5 0 248.58 12.00 8 5 0 236.38 12.20 8 5 0 251.47 14.10 9 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850.01 32.40 3 -6 0 -7.40 5.40 3 -6 0 0.80 5.70 -3 -6 0 1.80 4.70 -3 -6 0 -4.20 4.70 3 -6 0 -2.60 5.90 -3 6 0 0.70 6.40 3 6 0 -1.80 5.20 3 6 0 6.50 5.70 -3 6 0 1.80 5.40 -3 6 0 -2.90 5.30 3 6 0 7.10 5.20 4 -6 0 1.60 5.70 4 -6 0 -1.60 5.70 -4 -6 0 0.40 4.40 -4 -6 0 -0.30 4.10 -4 6 0 1.70 7.40 4 6 0 0.60 4.80 -4 6 0 3.40 5.30 4 6 0 -3.40 5.40 -4 6 0 -9.40 4.60 4 6 0 3.70 5.40 5 -6 0 820.42 31.80 -5 -6 0 800.82 27.20 -5 -6 0 794.22 27.00 -5 6 0 788.62 33.50 5 6 0 796.12 30.70 5 6 0 757.62 30.40 -5 6 0 795.12 29.20 5 6 0 764.92 28.60 -5 6 0 804.22 29.40 6 -6 0 8.20 6.20 6 -6 0 4.90 7.10 -6 6 0 7.30 7.60 -6 6 0 6.80 4.20 6 6 0 -3.90 5.20 6 6 0 7.40 5.70 6 6 0 14.40 4.90 -6 6 0 -0.90 4.10 7 -6 0 159.08 16.50 7 -6 0 158.28 14.40 -7 6 0 179.08 8.00 -7 6 0 168.28 8.00 7 6 0 171.88 13.40 7 6 0 162.68 11.00 -7 6 0 169.18 16.50 7 6 0 179.78 13.50 8 -6 0 4.10 8.30 8 -6 0 1.90 6.20 8 -6 0 0.50 6.10 8 6 0 -2.80 4.20 -8 6 0 -2.40 8.00 8 6 0 2.10 5.80 8 6 0 1.30 4.20 9 -6 0 131.49 14.30 9 -6 0 139.89 14.00 9 -6 0 115.89 14.60 9 6 0 139.39 9.40 9 6 0 139.99 13.10 9 6 0 139.19 9.20 10 -6 0 10.00 7.00 10 -6 0 12.00 9.50 10 -6 0 15.90 8.50 10 6 0 14.50 3.70 10 6 0 9.90 3.60 10 6 0 14.20 6.80 -10 6 0 2.10 9.20 11 -6 0 93.29 10.50 11 -6 0 89.19 11.60 11 -6 0 87.29 12.60 11 6 0 111.79 10.80 11 6 0 82.89 9.40 -11 6 0 79.29 12.70 0 -7 0 8.40 6.30 0 -7 0 -3.30 6.20 0 -7 0 -6.00 5.30 0 7 0 -1.80 6.00 0 7 0 8.40 7.10 0 7 0 2.40 5.80 -1 -7 0 37.10 8.00 1 -7 0 56.69 8.60 -1 -7 0 45.60 8.20 1 -7 0 26.60 7.60 -1 -7 0 45.60 8.20 1 -7 0 40.20 8.00 1 7 0 37.60 7.60 -1 7 0 45.10 8.80 1 7 0 45.90 8.60 1 7 0 51.49 8.90 -1 7 0 37.20 8.30 2 -7 0 121.19 13.40 -2 -7 0 114.59 12.70 -2 -7 0 94.79 11.60 2 -7 0 85.79 10.60 -2 -7 0 111.49 12.10 2 -7 0 93.29 10.60 2 7 0 77.29 9.70 -2 7 0 110.69 13.30 2 7 0 121.29 13.30 2 7 0 101.49 12.20 -2 7 0 123.19 13.20 -2 7 0 104.09 10.90 3 -7 0 1.70 6.60 -3 -7 0 2.10 5.20 -3 -7 0 1.10 5.50 3 7 0 0.10 6.10 3 7 0 -2.30 5.50 3 7 0 0.00 5.70 -3 7 0 0.70 5.40 -3 7 0 4.30 7.40 -3 7 0 10.40 6.10 4 -7 0 193.58 15.80 -4 -7 0 193.78 12.80 -4 -7 0 189.98 13.10 -4 7 0 182.18 16.40 4 7 0 205.48 15.40 4 7 0 184.08 13.50 -4 7 0 205.48 14.30 -4 7 0 191.68 14.30 4 7 0 182.58 14.70 -5 -7 0 2.30 4.40 5 -7 0 -3.50 6.40 5 -7 0 8.60 7.90 -5 -7 0 2.20 4.20 -5 7 0 0.00 7.90 -5 7 0 -2.20 5.20 5 7 0 5.00 6.20 -5 7 0 -0.90 5.20 5 7 0 -0.70 5.10 6 -7 0 447.56 23.90 6 -7 0 474.55 23.60 -6 -7 0 463.25 16.60 -6 -7 0 485.05 16.60 6 -7 0 425.96 22.90 6 7 0 446.96 22.00 -6 7 0 499.75 25.90 -6 7 0 478.75 20.00 -6 7 0 479.35 20.20 6 7 0 487.45 20.20 7 -7 0 52.49 9.50 7 -7 0 71.69 11.80 7 7 0 62.99 7.10 -7 7 0 75.69 8.20 -7 7 0 50.39 10.70 7 7 0 60.79 8.80 -7 7 0 81.49 8.20 8 -7 0 34.70 10.30 8 -7 0 42.70 8.80 8 7 0 28.40 7.60 8 7 0 34.80 5.60 -8 7 0 25.70 12.40 9 -7 0 43.80 11.10 9 7 0 32.10 5.30 9 7 0 33.50 5.30 -9 7 0 40.30 10.40 9 7 0 47.70 8.30 9 7 0 35.00 7.70 10 -7 0 357.46 23.60 10 -7 0 328.77 21.80 10 7 0 340.57 13.30 10 7 0 311.47 18.70 10 7 0 322.77 13.00 10 7 0 357.46 20.00 -10 7 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141.09 14.60 -5 8 0 119.49 12.80 -5 8 0 141.59 13.40 -5 8 0 116.59 14.00 5 8 0 162.08 14.60 5 8 0 128.09 12.60 6 -8 0 207.38 17.40 -6 -8 0 200.88 11.20 -6 -8 0 197.78 11.00 6 -8 0 163.78 19.50 6 -8 0 224.48 17.70 -6 8 0 217.68 19.40 6 8 0 222.98 14.10 6 8 0 209.08 16.20 6 8 0 196.78 16.20 -6 8 0 197.78 13.90 -6 8 0 201.88 13.80 7 -8 0 115.89 13.50 7 -8 0 126.49 15.90 7 -8 0 127.29 15.70 7 8 0 135.39 14.60 -7 8 0 103.29 13.20 7 8 0 128.59 15.00 7 8 0 125.79 11.70 -7 8 0 135.89 10.80 -7 8 0 138.59 10.90 8 -8 0 10.90 9.00 8 -8 0 7.90 7.90 8 -8 0 5.00 7.50 -8 8 0 1.20 3.20 8 8 0 -8.30 6.90 -8 8 0 -1.20 3.20 -8 8 0 5.90 9.30 8 8 0 1.40 5.20 8 8 0 3.40 7.30 9 -8 0 4.30 9.80 9 -8 0 1.70 8.10 9 -8 0 5.70 8.10 9 8 0 9.40 4.90 9 8 0 9.50 8.50 9 8 0 1.50 7.20 10 -8 0 18.70 10.50 10 -8 0 6.50 9.10 10 -8 0 9.70 8.90 10 8 0 5.40 8.00 10 8 0 0.60 3.90 -10 8 0 -4.60 9.60 10 8 0 7.20 7.70 10 8 0 4.20 4.10 11 -8 0 30.20 9.90 11 -8 0 24.30 11.70 11 -8 0 5.70 9.30 -11 8 0 27.00 12.10 11 8 0 4.80 8.90 11 8 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345.37 16.90 0 -4 -4 325.17 16.60 0 -4 -4 327.77 16.50 0 -4 4 322.77 16.70 0 4 4 323.77 17.10 0 4 -4 358.26 17.20 0 4 4 329.17 16.70 0 4 -4 338.17 16.60 0 4 -4 357.56 17.10 0 4 4 318.37 16.40 -1 -4 -4 3.70 4.50 1 -4 4 0.80 4.90 -1 -4 -4 2.60 4.60 1 -4 4 -1.70 4.70 1 -4 4 2.70 5.90 -1 4 -4 3.40 4.60 -1 4 -4 4.80 5.80 1 4 4 0.30 4.70 1 4 4 2.50 5.00 -1 4 -4 0.10 4.60 1 4 4 -4.10 4.70 2 -4 4 156.78 11.90 2 -4 4 176.48 11.80 2 -4 4 151.18 12.80 -2 -4 -4 155.98 10.30 -2 -4 -4 144.69 10.00 -2 4 -4 134.39 10.50 2 4 4 153.08 11.10 2 4 4 155.08 11.20 -2 4 -4 151.18 12.90 -2 4 -4 156.28 11.20 3 -4 4 1930.21 63.39 -3 -4 -4 1942.71 60.79 -3 -4 -4 1999.50 60.79 3 -4 4 1974.50 65.99 3 -4 4 1983.60 63.49 -3 4 -4 2021.40 66.39 -3 4 -4 2005.40 62.49 3 4 4 1951.90 62.59 -3 4 -4 1972.90 62.29 3 4 4 1950.01 62.59 4 -4 4 45.40 8.50 4 -4 4 49.50 6.50 4 -4 4 36.50 6.20 4 4 4 32.00 5.10 -4 4 -4 39.40 4.60 -4 4 -4 46.30 9.00 4 4 4 48.00 5.70 -4 4 -4 40.80 4.60 5 -4 4 21.70 7.70 5 -4 4 22.10 5.20 5 -4 4 23.00 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12.00 9 -11 4 57.59 14.40 9 11 4 34.90 10.50 9 11 4 33.10 9.30 -9 11 -4 47.70 14.60 9 11 4 79.79 11.90 8 -12 -4 -16.30 10.80 -8 -12 4 -2.20 5.10 8 -12 -4 13.80 11.30 -8 -12 4 4.10 5.20 8 -12 -4 -12.90 11.90 8 12 -4 -11.30 10.10 -8 12 4 -8.00 8.50 8 12 -4 -1.30 6.60 -8 12 4 -3.30 7.80 8 12 -4 15.00 11.10 -8 12 4 -13.80 11.80 -7 -12 4 -3.80 6.90 7 -12 -4 1.50 10.50 7 -12 -4 10.90 11.10 7 -12 -4 5.90 10.30 7 12 -4 3.50 9.60 7 12 -4 1.40 7.40 -7 12 4 -6.70 8.40 -7 12 4 13.90 8.50 7 12 -4 11.50 10.50 -7 12 4 18.10 12.30 6 -12 -4 42.80 11.70 6 -12 -4 51.29 12.00 -6 -12 4 73.59 9.90 -6 -12 4 62.49 9.40 6 -12 -4 74.29 13.10 -6 12 4 52.79 10.20 6 12 -4 55.99 12.00 -6 12 4 64.19 10.60 6 12 -4 76.79 12.30 -6 12 4 60.99 13.60 6 12 -4 56.49 9.40 -5 -12 4 27.00 10.60 5 -12 -4 42.20 10.90 -5 -12 4 13.50 12.80 5 -12 -4 19.20 10.00 5 -12 -4 20.60 10.90 -5 12 4 7.40 8.90 5 12 -4 25.90 10.20 -5 12 4 15.80 9.80 5 12 -4 26.30 8.90 5 12 -4 34.70 10.80 -5 12 4 30.20 10.70 -4 -12 4 133.39 16.00 -4 -12 4 111.39 12.60 4 -12 -4 74.69 12.90 4 -12 -4 149.49 18.60 4 -12 -4 118.09 14.70 -4 12 4 107.79 13.90 4 12 -4 121.79 14.20 -4 12 4 115.49 13.80 4 12 -4 98.59 11.70 4 12 -4 85.19 12.70 3 -12 -4 37.80 10.10 -3 -12 4 27.00 9.30 3 -12 -4 32.60 10.40 -3 -12 4 25.10 9.10 3 12 -4 12.40 9.00 -3 12 4 31.90 10.00 3 12 -4 26.60 10.40 -3 12 4 22.00 9.90 3 12 -4 9.40 9.40 -2 -12 4 5.70 8.40 2 -12 -4 8.70 9.40 2 -12 -4 0.70 8.40 -2 -12 4 14.70 9.20 -2 -12 4 -5.50 7.30 2 12 -4 3.70 9.10 -2 12 4 -1.80 8.70 -2 12 4 -5.90 8.10 2 12 -4 1.20 8.80 2 12 -4 -4.70 9.60 1 -12 -4 189.98 18.80 -1 -12 4 167.08 18.60 -1 -12 4 191.08 18.10 1 -12 -4 179.58 18.90 -1 -12 4 161.28 18.10 1 12 -4 169.18 18.30 1 12 -4 186.28 18.70 -1 12 4 190.98 18.80 -1 12 4 160.58 18.80 0 -12 4 -18.60 10.80 0 -12 4 22.80 9.40 0 -12 4 23.10 9.20 0 -12 -4 20.50 9.70 0 -12 -4 17.20 9.30 0 12 4 15.10 10.20 0 12 -4 -4.00 8.20 0 12 -4 31.60 10.50 0 12 4 17.90 9.40 -1 -12 -4 1.30 8.40 1 -12 4 11.50 8.70 -1 -12 -4 -0.50 8.10 1 -12 4 3.80 8.50 -1 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158.08 14.90 -3 4 -9 161.28 10.50 4 -4 9 19.70 5.50 4 -4 9 31.90 6.20 -4 4 -9 33.50 9.40 4 4 9 28.20 5.50 -4 4 -9 24.60 3.80 -4 4 -9 26.90 3.80 5 -4 9 314.77 16.20 5 -4 9 346.47 16.40 5 4 9 330.47 15.20 -5 4 -9 333.67 20.70 5 4 9 338.47 15.20 6 -4 9 5.10 4.60 6 -4 9 -2.50 4.60 6 -4 9 2.10 7.60 6 4 9 5.20 4.20 -6 4 -9 2.40 8.00 6 4 9 4.60 4.20 7 -4 9 64.59 7.20 7 -4 9 77.19 11.70 7 -4 9 69.09 7.30 -7 4 -9 74.59 11.80 7 4 9 71.99 8.10 7 4 9 59.49 5.90 8 -4 9 75.09 7.60 8 -4 9 65.39 7.00 8 -4 9 74.89 12.20 8 4 9 69.29 7.50 -8 4 -9 50.79 11.30 8 4 9 71.69 8.00 9 -4 9 25.80 10.30 9 -4 9 17.20 5.70 9 -4 9 12.90 5.20 9 4 9 16.20 4.50 9 4 9 26.00 4.60 9 4 9 29.20 8.40 10 -4 9 3.50 5.30 10 -4 9 1.80 5.60 10 -4 9 6.90 10.50 10 4 9 5.50 4.40 10 4 9 16.60 8.20 10 4 9 18.50 4.20 11 -4 9 125.09 15.10 11 -4 9 93.49 8.70 11 4 9 93.29 9.00 11 4 9 91.89 8.00 11 4 9 95.59 11.80 11 -5 -9 16.40 9.50 11 -5 -9 26.80 10.70 11 5 -9 23.10 10.30 -11 5 9 13.30 8.40 11 5 -9 20.00 9.10 10 -5 -9 7.00 8.40 10 -5 -9 6.20 8.60 -10 5 9 1.90 7.60 10 5 -9 4.60 9.20 10 5 -9 -2.20 8.00 9 -5 -9 73.29 9.70 9 -5 -9 94.79 11.40 9 -5 -9 77.59 10.90 9 5 -9 90.09 11.90 -9 5 9 65.49 9.70 -9 5 9 72.79 6.80 9 5 -9 74.19 10.50 -9 5 9 77.19 6.90 8 -5 -9 257.87 18.90 -8 -5 9 274.67 11.10 8 -5 -9 271.27 19.00 -8 -5 9 266.87 11.20 8 5 -9 286.37 19.40 -8 5 9 264.07 14.00 -8 5 9 268.57 17.70 8 5 -9 242.88 18.10 -8 5 9 261.97 14.10 7 -5 -9 49.70 9.70 7 -5 -9 42.70 8.80 -7 -5 9 53.69 6.50 -7 -5 9 51.19 6.10 -7 5 9 50.49 8.80 7 5 -9 55.69 9.00 7 5 -9 40.30 8.80 -7 5 9 40.00 6.90 -7 5 9 53.09 7.30 6 -5 -9 53.59 9.60 -6 -5 9 86.69 10.10 6 -5 -9 63.29 10.30 -6 -5 9 57.99 7.70 -6 5 9 62.69 8.30 -6 5 9 92.29 11.10 -6 5 9 64.09 9.60 6 5 -9 49.50 8.50 5 -5 -9 33.60 8.50 -5 -5 9 34.10 7.00 -5 -5 9 35.70 7.30 -5 5 9 47.80 8.10 -5 5 9 45.20 8.60 5 5 -9 36.40 7.90 -5 5 9 33.60 7.60 -4 -5 9 9.20 5.80 4 -5 -9 5.20 6.80 -4 -5 9 9.50 6.10 -4 -5 9 2.90 3.30 -4 5 9 -1.50 5.70 -4 5 9 7.50 6.70 4 5 -9 27.50 7.30 -4 5 9 1.00 6.50 4 5 -9 0.80 3.70 4 5 -9 -0.80 6.30 -3 -5 9 4.30 4.10 -3 -5 9 3.90 6.00 3 -5 -9 6.60 6.30 3 -5 -9 0.10 6.50 -3 -5 9 7.50 6.30 3 5 -9 10.80 6.50 3 5 -9 1.00 4.40 3 5 -9 -0.20 5.90 -3 5 9 -6.00 5.80 -3 5 9 8.60 6.50 -3 5 9 0.00 6.00 2 -5 -9 -1.10 5.80 -2 -5 9 -2.40 4.50 -2 -5 9 -0.10 6.20 2 -5 -9 -3.30 6.20 -2 -5 9 3.60 5.60 2 5 -9 -4.80 5.90 -2 5 9 -5.20 6.40 -2 5 9 9.60 6.30 2 5 -9 4.60 5.20 -2 5 9 0.30 6.30 2 5 -9 -2.40 6.20 1 -5 -9 17.20 7.10 -1 -5 9 13.50 7.30 -1 -5 9 2.30 5.30 1 -5 -9 12.30 6.60 -1 -5 9 14.30 6.70 -1 5 9 5.00 6.20 1 5 -9 6.80 6.90 -1 5 9 12.60 7.10 1 5 -9 9.90 6.30 1 5 -9 7.30 6.50 -1 5 9 20.90 7.40 0 -5 9 43.10 8.00 0 -5 -9 47.20 7.60 0 -5 9 42.80 8.20 0 -5 9 43.00 8.20 0 5 -9 42.20 7.80 0 5 9 43.80 8.20 0 5 9 49.60 8.50 0 5 -9 45.80 8.60 0 5 -9 38.70 7.30 -1 -5 -9 434.86 20.10 1 -5 9 422.36 21.90 -1 -5 -9 411.26 19.80 1 -5 9 433.36 21.40 1 -5 9 446.96 21.40 -1 5 -9 389.86 22.10 1 5 9 392.76 20.80 -1 5 -9 434.06 20.60 1 5 9 419.26 20.90 -1 5 -9 433.06 20.60 -2 -5 -9 34.20 6.10 2 -5 9 37.10 8.60 2 -5 9 28.30 7.30 -2 -5 -9 28.00 5.90 2 -5 9 17.80 6.50 -2 5 -9 32.20 6.30 2 5 9 28.00 6.80 -2 5 -9 35.10 6.70 2 5 9 32.20 6.90 -2 5 -9 30.70 8.80 -3 -5 -9 630.04 23.10 3 -5 9 597.54 26.10 -3 -5 -9 607.04 22.80 3 -5 9 651.03 26.20 -3 5 -9 605.34 29.20 3 5 9 614.64 25.50 3 5 9 628.34 25.50 -3 5 -9 663.73 24.70 -3 5 -9 616.24 24.50 -4 -5 -9 109.69 5.30 4 -5 9 119.89 12.20 -4 -5 -9 119.39 5.30 4 -5 9 125.69 12.00 -4 5 -9 114.79 9.20 -4 5 -9 116.29 9.00 4 5 9 102.19 11.20 -4 5 -9 113.89 13.20 5 -5 9 0.50 5.00 5 -5 9 1.90 7.40 5 -5 9 -2.20 5.30 -5 5 -9 0.60 2.40 5 5 9 -3.10 4.40 -5 5 -9 -8.50 7.50 5 5 9 5.00 4.90 -5 5 -9 3.60 2.50 6 -5 9 239.38 14.60 6 -5 9 258.07 19.60 6 -5 9 227.08 14.60 -6 5 -9 245.58 19.10 6 5 9 233.28 13.30 6 5 9 240.58 13.50 7 -5 9 176.58 12.60 7 -5 9 115.89 12.10 -7 5 -9 115.59 13.40 7 5 9 144.99 10.80 7 5 9 137.59 10.40 8 -5 9 14.00 5.80 8 -5 9 25.60 6.50 8 -5 9 13.90 9.00 -8 5 -9 15.40 10.00 8 5 9 17.90 5.30 8 5 9 20.90 5.20 9 -5 9 299.77 14.80 9 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9 530.25 22.70 7 6 -9 492.15 25.00 -7 6 9 499.65 22.50 7 6 -9 529.35 25.30 6 -6 -9 23.30 8.60 -6 -6 9 7.30 5.90 -6 -6 9 18.60 5.80 6 -6 -9 22.50 7.50 6 -6 -9 6.60 7.60 -6 6 9 12.60 6.60 -6 6 9 25.00 8.30 6 6 -9 24.10 7.90 6 6 -9 8.00 7.50 5 -6 -9 5.40 7.10 5 -6 -9 12.30 8.00 -5 -6 9 23.60 6.50 -5 -6 9 4.40 6.00 5 6 -9 13.10 7.60 5 6 -9 20.00 7.60 -5 6 9 21.60 7.70 5 6 -9 15.20 4.00 -5 6 9 7.50 6.70 -4 -6 9 1282.07 42.80 4 -6 -9 1357.16 48.50 -4 -6 9 1318.97 47.40 -4 -6 9 1344.67 46.90 4 -6 -9 1269.67 48.40 4 6 -9 1281.07 47.90 -4 6 9 1448.96 47.40 -4 6 9 1333.07 48.30 4 6 -9 1287.57 43.20 -4 6 9 1288.87 47.60 4 6 -9 1311.57 48.00 -3 -6 9 31.40 7.40 -3 -6 9 33.40 8.40 3 -6 -9 45.00 8.70 -3 -6 9 51.79 6.60 -3 6 9 35.50 8.20 3 6 -9 38.70 8.30 -3 6 9 47.10 8.70 3 6 -9 39.10 6.70 -2 -6 9 80.69 9.60 2 -6 -9 87.99 10.50 -2 -6 9 90.19 10.40 -2 -6 9 85.69 10.40 -2 6 9 108.59 13.00 -2 6 9 113.29 13.10 2 6 -9 94.09 11.60 2 6 -9 87.99 10.50 -2 6 9 82.09 10.20 1 -6 -9 46.80 8.00 -1 -6 9 60.49 9.60 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-14 9 5.80 9.70 -1 -14 -9 27.00 11.40 1 -14 9 34.10 11.50 -1 -14 -9 29.10 10.90 1 14 9 44.70 13.10 1 14 9 40.20 12.00 -1 14 -9 35.10 13.40 -1 14 -9 21.90 11.40 -1 14 -9 37.10 11.70 1 14 9 41.80 12.20 2 -14 9 -4.00 11.00 2 -14 9 12.60 10.00 -2 -14 -9 3.00 10.00 -2 -14 -9 27.00 9.90 2 -14 9 20.50 12.10 2 14 9 17.70 12.00 2 14 9 17.30 11.90 2 14 9 10.60 11.30 -2 14 -9 18.40 13.10 -2 14 -9 11.40 10.60 -3 -14 -9 21.30 11.50 3 -14 9 -1.10 10.50 3 -14 9 3.80 11.80 3 -14 9 11.60 11.20 3 14 9 3.80 11.40 -3 14 -9 6.60 12.50 3 14 9 49.30 12.40 -3 14 -9 -8.10 10.70 3 14 9 5.60 11.40 -3 14 -9 4.70 10.10 -4 -14 -9 10.10 8.80 4 -14 9 11.20 12.30 4 -14 9 -5.10 11.30 -4 -14 -9 15.90 9.40 4 -14 9 -5.20 10.30 4 14 9 12.80 11.60 4 14 9 22.30 12.60 -4 14 -9 -8.50 12.60 4 14 9 9.70 11.00 -4 14 -9 3.30 9.80 -4 14 -9 8.40 10.60 5 -14 9 47.00 13.20 5 -14 9 42.80 14.60 5 -14 9 53.69 12.60 5 14 9 59.09 14.40 -5 14 -9 54.69 11.20 -5 14 -9 34.80 14.40 5 14 9 45.30 13.50 -5 14 -9 38.90 11.80 5 14 9 56.49 13.30 -4 -15 9 12.50 11.40 -4 -15 9 -6.30 10.50 4 15 -9 -3.50 14.40 -4 15 9 -7.00 11.60 4 15 -9 7.00 11.10 -4 15 9 -2.60 11.50 3 -15 -9 12.90 13.00 -3 -15 9 22.90 12.20 3 -15 -9 9.90 12.70 -3 -15 9 22.50 11.50 -3 -15 9 30.20 12.20 -3 15 9 5.40 12.10 3 15 -9 8.00 12.20 3 15 -9 21.90 11.40 3 15 -9 9.30 12.20 -3 15 9 7.30 11.70 -3 15 9 14.60 13.70 -2 -15 9 171.48 17.60 -2 -15 9 148.79 15.40 -2 -15 9 192.48 23.10 2 -15 -9 155.58 16.80 2 -15 -9 155.18 17.90 -2 15 9 188.78 18.70 2 15 -9 182.88 22.00 -2 15 9 155.48 18.80 -2 15 9 140.69 16.80 2 15 -9 148.99 17.80 2 15 -9 155.58 17.60 -1 -15 9 25.10 12.10 -1 -15 9 6.00 10.80 1 -15 -9 17.60 11.60 -1 -15 9 -1.20 11.10 1 -15 -9 15.20 12.20 -1 15 9 14.80 11.70 -1 15 9 5.10 11.00 1 15 -9 5.60 11.40 -1 15 9 -3.80 12.70 1 15 -9 -1.80 11.30 1 15 -9 -0.20 13.70 0 -15 9 46.80 12.70 0 -15 -9 12.50 11.10 0 -15 9 23.40 12.70 0 -15 -9 54.39 13.00 0 -15 9 10.90 11.30 0 15 -9 34.10 12.60 0 15 9 36.40 13.50 0 15 9 28.80 12.10 0 15 9 33.10 12.80 0 15 -9 20.20 12.30 0 15 -9 39.40 12.80 -1 -15 -9 -8.30 11.60 1 -15 9 -5.10 10.90 1 -15 9 2.00 10.20 1 -15 9 -2.10 11.10 -1 -15 -9 14.50 10.70 1 15 9 -3.50 10.90 -1 15 -9 19.40 13.50 -1 15 -9 9.30 12.60 -1 15 -9 -0.10 11.10 1 15 9 -5.30 11.60 1 15 9 -7.50 11.00 2 -15 9 93.19 14.40 -2 -15 -9 113.49 15.10 2 -15 9 74.59 15.00 -2 -15 -9 96.79 13.50 2 -15 9 84.39 15.00 2 15 9 91.89 14.90 -2 15 -9 110.29 16.10 2 15 9 87.89 15.40 -2 15 -9 76.59 15.60 2 15 9 103.99 15.10 -2 15 -9 87.09 14.10 3 -15 9 21.50 12.70 3 -15 9 24.50 13.50 -3 -15 -9 0.90 11.80 3 -15 9 3.90 12.10 -3 -15 -9 5.90 9.80 3 15 9 -1.90 11.80 -3 15 -9 12.20 12.40 -3 15 -9 -1.60 10.00 3 15 9 11.60 13.10 -3 15 -9 11.90 14.00 3 15 9 -2.80 12.00 -4 -15 -9 30.60 11.10 -4 15 -9 18.00 12.30 4 15 9 10.70 11.90 -4 15 -9 21.60 11.20 4 15 9 42.50 13.30 4 15 9 27.50 14.70 12 0 -10 9.70 8.80 12 0 -10 25.20 9.00 11 0 -10 2.60 8.60 11 0 -10 -8.50 7.50 10 0 -10 154.88 15.70 10 0 -10 145.99 15.50 9 0 -10 6.00 7.00 9 0 -10 2.80 7.10 -8 0 10 544.55 19.00 -8 0 10 545.25 18.40 -8 0 10 550.14 19.20 8 0 -10 532.55 25.10 8 0 -10 598.44 24.70 7 0 -10 -7.30 5.80 -7 0 10 0.70 3.80 -7 0 10 -0.50 4.00 -7 0 10 -1.20 2.90 6 0 -10 92.29 10.30 6 0 -10 103.69 12.30 -6 0 10 104.89 9.80 -6 0 10 103.89 10.10 -6 0 10 98.79 7.00 5 0 -10 -7.50 5.20 -5 0 10 2.00 5.00 -5 0 10 -1.50 4.50 -5 0 10 -1.50 3.10 5 0 -10 -0.90 5.90 -4 0 10 2378.16 74.79 -4 0 10 2307.07 71.49 4 0 -10 2331.97 75.79 4 0 -10 2272.17 75.49 -4 0 10 2324.97 74.79 3 0 -10 -1.20 5.60 -3 0 10 6.60 5.80 3 0 -10 5.00 5.80 -3 0 10 -0.40 5.50 -2 0 10 37.60 7.10 2 0 -10 32.60 6.80 2 0 -10 22.70 6.30 -2 0 10 20.10 6.10 -1 0 10 0.50 5.10 -1 0 10 0.60 5.40 1 0 -10 -0.30 5.30 1 0 -10 2.10 5.10 0 0 10 3927.01 118.49 0 0 10 3844.52 118.39 0 0 -10 3794.12 117.99 0 0 -10 3769.32 117.99 1 0 10 -1.50 4.60 -1 0 -10 0.40 4.10 1 0 10 2.00 4.60 -1 0 -10 -2.40 4.00 -2 0 -10 823.92 27.80 2 0 10 837.42 29.40 -2 0 -10 851.31 27.90 2 0 10 819.32 29.30 3 0 10 0.90 3.60 3 0 10 -0.20 3.50 3 0 10 6.50 7.20 4 0 10 208.98 10.30 4 0 10 228.58 10.50 4 0 10 206.48 16.60 5 0 10 2.90 2.70 5 0 10 -1.00 2.70 5 0 10 5.40 7.20 6 0 10 572.04 19.00 6 0 10 590.24 19.10 7 0 10 -2.10 2.20 7 0 10 -5.60 2.10 8 0 10 24.40 8.80 8 0 10 39.30 3.80 8 0 10 30.70 3.80 9 0 10 4.20 2.30 9 0 10 4.60 8.40 9 0 10 -0.80 2.00 10 0 10 255.27 9.30 10 0 10 262.77 9.20 10 0 10 263.37 20.20 11 0 10 -3.00 2.40 11 0 10 1.00 2.50 11 0 10 0.80 9.90 12 -1 -10 61.09 10.80 12 -1 -10 92.49 11.40 12 1 -10 101.19 11.50 12 1 -10 78.09 11.20 11 -1 -10 16.70 8.60 11 1 -10 18.30 8.80 11 1 -10 6.00 8.30 10 -1 -10 26.80 9.80 10 -1 -10 4.60 7.60 10 1 -10 20.50 8.30 10 1 -10 12.30 7.80 9 -1 -10 110.89 11.50 9 -1 -10 90.99 10.70 -9 1 10 98.99 8.40 9 1 -10 111.59 13.80 9 1 -10 100.99 11.00 8 -1 -10 13.50 7.10 -8 -1 10 2.50 3.00 8 -1 -10 10.10 7.00 -8 -1 10 7.00 3.10 -8 1 10 12.10 3.70 -8 1 10 14.70 3.70 8 1 -10 15.90 7.20 -8 1 10 8.90 4.30 -7 -1 10 193.18 11.30 7 -1 -10 186.08 15.30 -7 -1 10 208.58 11.70 -7 1 10 198.88 12.00 -7 1 10 204.28 11.10 -7 1 10 203.28 11.60 7 1 -10 224.58 14.50 7 1 -10 199.08 15.30 -6 -1 10 169.08 11.50 6 -1 -10 163.38 13.90 6 -1 -10 175.58 14.60 -6 -1 10 152.88 11.60 6 1 -10 145.99 13.80 -6 1 10 163.28 10.20 6 1 -10 161.08 14.00 -6 1 10 159.68 12.10 -6 1 10 181.68 12.00 -5 -1 10 482.25 21.30 5 -1 -10 483.65 23.10 5 -1 -10 510.45 23.20 -5 -1 10 491.25 21.00 -5 -1 10 509.35 16.60 -5 1 10 497.05 19.40 5 1 -10 524.75 23.20 5 1 -10 473.85 22.60 -5 1 10 513.95 21.70 -5 1 10 485.95 21.50 -4 -1 10 520.25 22.50 -4 -1 10 512.55 22.10 4 -1 -10 503.95 23.30 4 -1 -10 512.75 23.50 -4 1 10 533.65 22.60 4 1 -10 518.15 23.40 4 1 -10 479.75 22.90 -4 1 10 506.05 22.60 -4 1 10 519.25 20.10 -3 -1 10 180.08 14.00 3 -1 -10 185.38 14.40 3 -1 -10 167.58 13.90 -3 -1 10 182.98 13.10 -3 1 10 183.98 13.80 -3 1 10 189.58 13.60 3 1 -10 174.18 13.90 3 1 -10 177.58 14.10 2 -1 -10 227.28 15.00 -2 -1 10 217.48 14.20 -2 -1 10 240.48 14.90 2 -1 -10 212.98 14.50 -2 1 10 209.98 14.30 -2 1 10 210.08 14.60 2 1 -10 229.98 15.00 2 1 -10 218.78 14.30 -1 -1 10 845.12 31.00 1 -1 -10 800.62 30.90 -1 -1 10 815.22 31.10 1 -1 -10 831.42 31.00 1 1 -10 810.32 30.70 -1 1 10 798.32 31.00 -1 1 10 801.22 30.60 1 1 -10 822.82 30.70 0 -1 -10 1420.16 48.10 0 -1 10 1394.56 48.30 0 -1 10 1463.85 48.60 0 -1 -10 1436.56 48.10 0 1 10 1432.76 48.60 0 1 10 1454.25 48.50 0 1 -10 1445.86 48.00 0 1 -10 1450.45 48.40 1 -1 10 129.59 11.20 1 -1 10 110.79 10.40 -1 -1 -10 120.39 9.90 1 -1 10 118.89 12.10 -1 -1 -10 139.49 10.20 1 1 10 138.89 11.00 -1 1 -10 117.09 10.00 1 1 10 114.19 10.60 -1 1 -10 132.99 10.20 -2 -1 -10 336.37 13.40 2 -1 10 325.27 15.30 2 -1 10 319.37 15.30 2 -1 10 342.57 19.30 -2 -1 -10 315.17 13.30 -2 1 -10 311.37 13.70 2 1 10 322.17 15.20 -2 1 -10 314.97 13.70 2 1 10 337.17 15.10 3 -1 10 7.80 4.10 3 -1 10 -1.50 3.80 3 -1 10 -3.00 6.40 3 1 10 3.30 3.80 3 1 10 3.10 3.80 4 -1 10 1.30 3.40 4 -1 10 7.70 7.20 4 -1 10 3.10 3.50 4 1 10 6.00 3.10 4 1 10 3.40 3.30 5 -1 10 37.90 4.40 5 -1 10 54.89 9.70 5 -1 10 40.60 4.50 5 1 10 45.50 8.60 5 1 10 43.50 5.30 5 1 10 50.29 5.50 6 -1 10 584.24 20.20 6 -1 10 609.34 20.40 6 1 10 584.84 19.20 6 1 10 591.94 19.20 7 -1 10 389.86 14.30 7 -1 10 399.06 23.20 7 -1 10 384.16 14.20 7 1 10 399.86 12.80 8 -1 10 69.89 6.00 8 -1 10 67.89 6.10 8 -1 10 66.89 11.30 8 1 10 81.19 10.90 9 -1 10 6.30 3.00 9 -1 10 0.90 3.10 9 -1 10 8.50 11.10 9 1 10 0.00 8.30 10 -1 10 27.60 4.00 10 -1 10 45.00 5.60 10 -1 10 35.00 10.40 11 -1 10 68.79 6.80 11 -1 10 82.49 6.70 11 -1 10 84.99 12.40 11 1 10 77.79 12.20 12 -2 -10 7.50 9.10 12 -2 -10 22.50 9.60 12 2 -10 25.00 10.20 12 2 -10 21.20 9.30 11 -2 -10 14.90 8.40 11 -2 -10 12.50 8.10 11 2 -10 27.60 9.40 11 2 -10 10.80 12.40 10 -2 -10 2.90 9.00 10 -2 -10 -2.60 7.40 10 2 -10 -8.20 7.00 10 2 -10 -15.50 7.40 -10 2 10 -2.40 4.90 9 -2 -10 121.69 14.80 9 -2 -10 102.79 11.30 9 2 -10 119.69 13.90 -9 2 10 112.39 10.40 9 2 -10 121.59 14.40 8 -2 -10 651.13 28.70 -8 -2 10 653.83 21.80 -8 -2 10 650.73 21.70 8 -2 -10 672.63 28.80 -8 2 10 639.04 24.60 -8 2 10 667.73 23.10 8 2 -10 656.03 28.20 8 2 -10 658.63 28.20 -8 2 10 655.83 23.30 7 -2 -10 101.49 10.20 -7 -2 10 96.69 9.10 7 -2 -10 95.99 11.10 -7 -2 10 115.59 9.50 -7 2 10 127.39 10.60 -7 2 10 123.79 10.00 7 2 -10 122.49 13.20 -7 2 10 115.89 10.30 6 -2 -10 549.25 22.60 -6 -2 10 448.66 19.60 -6 -2 10 471.35 19.90 6 -2 -10 438.96 22.80 -6 2 10 437.16 19.40 -6 2 10 452.05 20.30 -6 2 10 481.65 20.50 6 2 -10 458.35 22.40 6 2 -10 452.35 22.40 -5 -2 10 1036.30 37.20 -5 -2 10 1071.59 37.70 5 -2 -10 1039.00 39.30 5 -2 -10 1070.49 39.60 -5 2 10 1045.80 36.40 5 2 -10 1062.19 39.00 5 2 -10 1057.39 39.40 -5 2 10 1044.80 37.90 -5 2 10 1049.09 37.90 -4 -2 10 72.69 5.70 4 -2 -10 76.19 9.20 4 -2 -10 58.59 8.90 -4 -2 10 70.09 8.10 -4 -2 10 76.69 8.40 -4 2 10 59.19 7.80 -4 2 10 56.29 7.10 4 2 -10 69.79 8.90 4 2 -10 62.99 9.00 -4 2 10 59.19 8.50 -3 -2 10 624.14 21.90 3 -2 -10 622.94 26.50 -3 -2 10 593.14 25.70 -3 -2 10 635.64 25.60 3 -2 -10 613.24 26.50 -3 2 10 599.34 24.30 -3 2 10 636.34 26.10 3 2 -10 603.74 26.30 3 2 -10 594.84 25.90 -3 2 10 592.94 25.90 -2 -2 10 1493.65 49.99 -2 -2 10 1459.95 50.19 2 -2 -10 1448.96 50.29 2 -2 -10 1433.06 50.29 -2 -2 10 1516.75 47.80 2 2 -10 1478.55 50.59 -2 2 10 1437.76 49.80 2 2 -10 1422.16 49.90 -2 2 10 1436.96 49.99 -1 -2 10 165.58 11.90 -1 -2 10 168.68 12.20 1 -2 -10 157.08 13.20 -1 -2 10 152.18 13.00 1 -2 -10 168.08 13.20 1 2 -10 162.98 13.00 -1 2 10 163.18 13.20 -1 2 10 158.68 13.20 1 2 -10 167.88 12.30 0 -2 10 1151.58 41.40 0 -2 -10 1174.58 40.70 0 -2 10 1196.48 41.20 0 -2 -10 1178.98 40.70 0 -2 10 1102.19 40.80 0 2 -10 1174.18 40.70 0 2 10 1173.78 40.90 0 2 10 1185.38 41.00 0 2 -10 1178.48 40.90 -1 -2 -10 516.25 20.60 1 -2 10 491.65 22.70 -1 -2 -10 516.75 20.50 1 -2 10 510.55 21.40 1 -2 10 488.75 21.50 1 2 10 490.85 21.10 -1 2 -10 523.85 21.20 -1 2 -10 503.55 20.70 1 2 10 501.75 21.40 2 -2 10 1640.24 55.79 2 -2 10 1780.52 56.09 2 -2 10 1712.23 58.99 -2 -2 -10 1751.62 53.99 2 2 10 1712.43 55.59 -2 2 -10 1707.83 54.59 2 2 10 1734.03 55.49 -2 2 -10 1678.73 54.49 3 -2 10 570.34 22.10 3 -2 10 568.84 22.00 3 -2 10 563.24 25.90 -3 2 -10 556.74 19.10 -3 2 -10 546.45 19.00 3 2 10 565.24 21.50 3 2 10 561.34 21.20 4 -2 10 533.15 20.40 4 -2 10 552.44 26.00 4 -2 10 523.85 20.40 4 2 10 523.85 19.50 4 2 10 528.15 19.70 5 -2 10 160.48 9.80 5 -2 10 160.68 9.80 5 -2 10 200.98 14.10 5 2 10 149.69 8.60 5 2 10 152.38 8.80 6 -2 10 110.69 8.30 6 -2 10 113.09 8.20 6 2 10 106.79 6.90 7 -2 10 12.90 8.90 7 -2 10 7.80 4.00 7 -2 10 8.40 3.60 7 2 10 13.40 3.00 7 2 10 14.20 3.00 8 -2 10 49.80 10.30 8 -2 10 41.10 5.00 8 -2 10 49.00 5.00 8 2 10 51.89 4.80 8 2 10 33.20 8.50 8 2 10 43.00 4.60 9 -2 10 11.20 4.20 9 -2 10 30.60 10.10 9 -2 10 18.50 4.20 9 2 10 24.00 3.00 9 2 10 16.20 2.70 9 2 10 13.60 8.20 10 -2 10 -20.00 9.00 10 -2 10 2.00 4.10 10 -2 10 3.00 3.80 10 2 10 0.70 2.20 10 2 10 0.90 2.40 10 2 10 6.30 8.90 11 -2 10 22.00 10.80 11 -2 10 12.50 4.70 11 -2 10 11.10 4.30 11 2 10 14.40 10.00 12 -3 -10 33.60 9.90 12 -3 -10 7.80 9.30 12 3 -10 23.00 9.40 12 3 -10 41.60 11.60 11 -3 -10 47.60 10.20 11 -3 -10 52.09 10.30 -11 3 10 49.50 7.50 11 3 -10 69.59 11.40 11 3 -10 39.50 12.90 10 -3 -10 232.28 18.80 10 -3 -10 213.18 18.30 -10 3 10 241.68 14.80 10 3 -10 263.17 18.00 9 -3 -10 27.90 8.70 9 -3 -10 24.70 8.50 9 3 -10 22.90 8.60 -9 3 10 22.90 6.60 9 3 -10 35.50 8.20 -9 3 10 29.60 3.60 8 -3 -10 -9.60 6.30 8 -3 -10 -10.00 6.40 -8 -3 10 2.10 3.20 -8 -3 10 0.90 3.20 -8 3 10 0.20 3.80 8 3 -10 -8.40 6.20 -8 3 10 13.50 5.90 8 3 -10 -3.90 6.70 -8 3 10 0.10 4.20 -7 -3 10 174.08 10.80 -7 -3 10 162.88 11.00 7 -3 -10 173.28 15.40 7 -3 -10 138.79 14.90 7 3 -10 154.88 14.50 -7 3 10 161.68 11.90 -7 3 10 156.38 12.70 -7 3 10 166.78 12.30 6 -3 -10 1092.59 41.20 -6 -3 10 1070.49 38.10 -6 -3 10 1075.69 37.90 -6 3 10 1062.49 38.80 6 3 -10 1036.80 40.40 6 3 -10 1275.47 41.00 -6 3 10 1069.29 38.50 -6 3 10 1105.59 39.00 -5 -3 10 37.20 6.40 5 -3 -10 30.00 8.00 -5 -3 10 23.50 6.60 5 -3 -10 36.20 7.40 -5 3 10 18.20 6.10 5 3 -10 37.40 7.90 -5 3 10 47.60 7.60 -5 3 10 28.70 6.70 5 3 -10 31.50 7.70 4 -3 -10 870.01 34.80 -4 -3 10 886.61 33.40 -4 -3 10 885.81 28.60 4 -3 -10 875.21 35.00 -4 -3 10 876.01 33.80 4 3 -10 916.31 34.80 -4 3 10 923.01 34.30 -4 3 10 896.91 34.20 -4 3 10 911.91 33.20 4 3 -10 935.21 35.40 3 -3 -10 1692.23 57.19 3 -3 -10 1589.34 56.99 -3 -3 10 1661.93 52.39 -3 -3 10 1684.63 56.09 -3 -3 10 1702.43 56.59 3 3 -10 1683.53 57.19 -3 3 10 1680.93 56.59 3 3 -10 1632.44 56.59 -3 3 10 1632.44 55.39 -3 3 10 1669.83 56.59 2 -3 -10 2015.20 65.99 -2 -3 10 1895.91 65.39 -2 -3 10 2005.20 65.49 2 -3 -10 1954.20 65.89 -2 -3 10 2016.90 63.09 2 3 -10 2006.20 66.09 -2 3 10 1990.60 65.79 2 3 -10 2007.10 65.79 -2 3 10 1925.91 65.49 -1 -3 10 76.59 8.30 -1 -3 10 74.39 8.70 1 -3 -10 71.79 8.70 1 -3 -10 71.89 9.10 -1 -3 10 68.19 8.80 -1 3 10 82.69 9.50 -1 3 10 65.09 8.30 1 3 -10 58.99 8.20 1 3 -10 91.89 10.70 1 3 -10 96.19 11.00 0 -3 -10 620.24 25.10 0 -3 10 633.14 25.70 0 -3 10 576.84 25.40 0 -3 10 616.24 25.40 0 -3 -10 615.24 25.00 0 3 10 591.44 25.40 0 3 -10 608.64 25.50 0 3 10 642.24 25.70 0 3 -10 593.44 24.90 0 3 -10 597.34 25.50 -1 -3 -10 1090.19 39.00 1 -3 10 1171.58 40.70 1 -3 10 1148.89 40.40 -1 -3 -10 1147.79 39.30 1 -3 10 1147.29 41.80 1 3 10 1163.48 40.20 -1 3 -10 1135.89 39.50 1 3 10 1109.89 39.90 -1 3 -10 1113.19 41.30 -1 3 -10 1148.39 39.80 2 -3 10 321.07 18.80 -2 -3 -10 331.67 14.90 2 -3 10 333.67 17.10 -2 -3 -10 312.47 14.60 2 -3 10 340.17 17.20 2 3 10 348.37 16.80 2 3 10 303.97 16.40 -2 3 -10 335.57 15.60 -2 3 -10 346.27 19.30 -2 3 -10 334.57 15.70 3 -3 10 50.59 9.50 -3 -3 -10 45.30 5.00 3 -3 10 30.30 6.20 3 -3 10 36.20 6.40 -3 -3 -10 32.50 3.50 3 3 10 33.50 5.80 -3 3 -10 38.50 5.00 -3 3 -10 38.20 4.80 3 3 10 36.20 5.60 -3 3 -10 31.00 8.30 4 -3 10 -0.30 4.50 4 -3 10 2.40 4.60 4 -3 10 25.90 7.20 4 3 10 6.80 4.20 4 3 10 8.20 4.20 -4 3 -10 -1.80 6.80 5 -3 10 335.37 15.10 5 -3 10 323.47 14.90 5 -3 10 237.08 19.10 5 3 10 309.67 13.70 -5 3 -10 317.97 21.10 6 -3 10 1.50 4.10 6 -3 10 -3.00 7.70 6 -3 10 4.80 4.30 6 3 10 5.70 3.70 6 3 10 3.10 3.50 7 -3 10 64.49 11.30 7 -3 10 55.69 6.10 7 -3 10 66.89 8.40 7 3 10 67.49 7.20 7 3 10 60.49 6.70 8 -3 10 23.40 5.10 8 -3 10 19.60 4.90 8 3 10 33.00 4.10 8 3 10 25.00 4.00 8 3 10 17.50 8.30 9 -3 10 92.59 9.10 9 -3 10 93.69 9.30 9 -3 10 100.69 13.20 9 3 10 98.49 6.80 9 3 10 87.89 7.40 9 3 10 95.09 11.50 10 -3 10 36.10 5.50 10 -3 10 36.30 5.60 10 -3 10 28.10 11.00 10 3 10 29.50 9.20 10 3 10 29.40 3.90 10 3 10 32.80 4.00 11 -3 10 -3.00 4.90 11 -3 10 6.00 5.30 11 -3 10 2.80 10.70 11 3 10 12.80 4.30 11 3 10 12.90 9.70 11 3 10 3.00 3.10 11 -4 -10 39.40 10.00 11 -4 -10 10.80 9.00 -11 4 10 -0.10 7.50 11 4 -10 21.90 9.30 11 4 -10 25.10 11.60 10 -4 -10 88.89 11.70 10 -4 -10 110.89 12.40 10 4 -10 129.69 15.60 10 4 -10 147.19 14.40 -10 4 10 98.09 10.20 9 -4 -10 14.20 8.50 9 -4 -10 3.70 8.20 9 4 -10 20.70 7.90 -9 4 10 18.60 3.70 -9 4 10 23.50 3.80 -9 4 10 15.60 6.90 9 4 -10 11.10 8.90 8 -4 -10 13.30 7.60 -8 -4 10 17.20 4.00 8 -4 -10 19.20 8.30 -8 -4 10 20.10 3.90 8 4 -10 21.30 8.90 -8 4 10 17.00 5.00 8 4 -10 11.40 7.20 -8 4 10 10.90 5.00 -8 4 10 19.50 7.00 7 -4 -10 -5.60 6.30 -7 -4 10 -1.50 4.20 -7 -4 10 3.80 4.70 7 -4 -10 3.20 6.90 -7 4 10 7.70 6.10 -7 4 10 -9.50 4.80 7 4 -10 9.00 6.90 7 4 -10 -6.40 7.30 -7 4 10 2.50 5.20 -6 -4 10 20.80 5.80 -6 -4 10 6.10 5.50 6 -4 -10 14.90 7.70 -6 4 10 11.80 6.10 -6 4 10 10.50 6.40 -6 4 10 5.50 5.50 6 4 -10 5.80 6.70 -5 -4 10 312.57 16.40 -5 -4 10 295.27 16.80 5 -4 -10 294.57 18.90 -5 4 10 281.77 17.10 -5 4 10 289.17 16.80 -5 4 10 297.27 17.20 5 4 -10 284.37 18.30 -4 -4 10 286.47 17.50 4 -4 -10 317.87 19.00 -4 -4 10 309.07 12.30 4 -4 -10 317.57 18.80 -4 -4 10 308.77 17.10 -4 4 10 295.07 17.50 4 4 -10 296.67 18.70 -4 4 10 324.87 18.00 4 4 -10 289.57 18.10 -4 4 10 318.47 18.00 -3 -4 10 401.66 16.10 3 -4 -10 372.36 20.80 3 -4 -10 390.76 20.80 -3 -4 10 350.46 19.90 -3 -4 10 424.66 20.00 3 4 -10 403.16 20.70 3 4 -10 392.76 20.40 -3 4 10 388.46 20.50 -3 4 10 394.36 20.00 -3 4 10 380.06 20.20 2 -4 -10 235.28 16.20 -2 -4 10 236.38 16.10 -2 -4 10 237.68 13.40 -2 -4 10 235.98 15.70 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1 -14 145.49 15.00 -6 1 14 127.69 13.20 -6 1 14 138.29 13.10 -5 -1 14 513.35 25.00 5 -1 -14 538.05 26.20 -5 -1 14 551.94 24.60 -5 1 14 575.34 25.30 -5 1 14 561.44 22.20 5 1 -14 580.44 26.50 -5 1 14 563.74 25.30 -4 -1 14 343.17 19.10 4 -1 -14 319.07 19.40 -4 -1 14 342.77 19.50 4 -1 -14 290.07 18.60 4 1 -14 331.27 19.60 4 1 -14 355.46 19.00 -4 1 14 344.27 19.60 -4 1 14 340.27 19.40 3 -1 -14 237.08 16.80 -3 -1 14 239.18 17.50 -3 -1 14 270.37 17.30 3 -1 -14 249.48 17.60 3 1 -14 272.57 17.30 3 1 -14 259.97 17.40 -3 1 14 253.27 16.60 -3 1 14 232.38 17.20 -2 -1 14 9.80 7.00 2 -1 -14 7.20 6.80 -2 -1 14 7.60 6.70 2 -1 -14 9.20 6.40 2 1 -14 6.70 6.10 -2 1 14 8.20 6.30 2 1 -14 10.10 6.80 -2 1 14 5.20 7.10 1 -1 -14 1967.80 65.49 -1 -1 14 1937.11 65.59 1 -1 -14 1965.80 65.39 -1 -1 14 1912.11 65.49 1 1 -14 2035.70 65.89 1 1 -14 1963.60 65.29 -1 1 14 1902.81 65.59 -1 1 14 1942.41 65.59 0 -1 -14 331.57 18.00 0 -1 -14 316.67 17.90 0 -1 14 332.47 18.60 0 -1 14 332.07 19.00 0 1 14 345.67 19.10 0 1 -14 332.57 18.30 0 1 -14 322.37 17.80 0 1 14 312.17 18.30 -1 -1 -14 819.72 31.00 1 -1 14 835.82 34.00 1 -1 14 820.72 32.10 -1 -1 -14 832.42 31.00 1 -1 14 798.22 31.90 1 1 14 839.22 31.90 1 1 14 845.02 32.30 -1 1 -14 824.52 31.10 -1 1 -14 808.52 31.10 -2 -1 -14 607.84 22.80 2 -1 14 616.14 28.40 2 -1 14 561.94 24.40 2 -1 14 615.04 24.90 -2 -1 -14 595.84 22.70 -2 1 -14 561.14 23.00 2 1 14 600.04 24.70 -2 1 -14 574.84 22.80 2 1 14 601.54 24.50 -3 -1 -14 508.85 17.70 3 -1 14 478.55 21.30 3 -1 14 512.35 21.60 3 1 14 510.55 21.50 -3 1 -14 490.25 18.30 -3 1 -14 484.15 18.20 3 1 14 515.25 21.30 4 -1 14 303.17 15.40 4 -1 14 319.17 15.60 4 1 14 302.27 15.30 4 1 14 293.87 15.10 5 -1 14 84.59 12.00 5 -1 14 58.89 6.70 5 -1 14 57.89 6.60 5 1 14 69.39 8.30 5 1 14 48.60 10.80 5 1 14 68.79 8.30 6 -1 14 571.84 21.70 6 -1 14 584.44 21.70 6 -1 14 563.54 29.10 6 1 14 568.74 21.20 6 1 14 565.74 21.20 6 1 14 567.84 28.70 7 -1 14 250.57 12.30 7 -1 14 242.58 12.30 7 1 14 237.48 11.60 7 1 14 239.58 20.10 7 1 14 258.07 11.90 8 -1 14 136.29 9.20 8 -1 14 139.79 9.20 8 -1 14 141.39 15.40 8 1 14 121.59 8.20 8 1 14 151.08 17.40 8 1 14 116.99 8.40 9 -1 14 111.59 8.60 9 -1 14 110.99 14.50 9 -1 14 115.89 8.70 9 1 14 121.69 14.10 9 1 14 114.69 7.50 9 1 14 108.49 7.60 10 -1 14 12.10 11.10 10 -1 14 8.70 4.10 10 -1 14 14.90 4.20 10 1 14 9.00 10.40 10 1 14 17.10 3.60 10 1 14 11.90 3.40 11 -1 14 103.99 14.80 11 -1 14 78.19 7.50 11 -1 14 71.29 7.30 11 1 14 112.29 15.20 11 1 14 65.69 5.50 11 1 14 68.19 5.50 11 -2 -14 6.70 9.20 11 -2 -14 -3.00 8.90 11 2 -14 -1.60 9.10 -11 2 14 1.90 4.20 11 2 -14 -4.20 9.70 10 -2 -14 7.60 9.10 10 -2 -14 5.60 8.40 -10 2 14 1.40 2.90 -10 2 14 -4.00 2.80 10 2 -14 -4.90 8.70 10 2 -14 14.30 8.60 -10 2 14 1.90 4.70 -9 -2 14 30.80 5.10 -9 -2 14 22.70 5.10 9 -2 -14 28.30 9.40 9 -2 -14 14.40 8.50 9 2 -14 18.30 9.00 -9 2 14 22.80 5.50 -9 2 14 29.70 6.10 -9 2 14 32.60 5.50 -8 -2 14 108.29 10.60 8 -2 -14 87.19 13.10 -8 -2 14 107.69 11.00 8 -2 -14 103.69 12.30 -8 2 14 110.59 11.30 -8 2 14 95.79 11.50 8 2 -14 102.99 11.70 -8 2 14 108.09 10.30 -7 -2 14 1.20 5.80 7 -2 -14 -3.80 7.10 -7 -2 14 4.20 5.30 7 -2 -14 -1.20 7.40 7 2 -14 -0.70 7.60 -7 2 14 -3.20 5.40 -7 2 14 -9.40 5.20 -7 2 14 -0.70 5.10 7 2 -14 4.80 7.40 -6 -2 14 357.26 19.20 -6 -2 14 326.67 11.80 6 -2 -14 331.87 20.80 6 -2 -14 326.37 21.10 -6 -2 14 344.67 11.80 -6 -2 14 370.46 18.70 -6 2 14 426.26 19.00 -6 2 14 347.27 17.00 -6 2 14 348.97 19.20 6 2 -14 348.07 20.90 6 2 -14 350.86 20.60 -5 -2 14 200.58 10.20 5 -2 -14 200.88 17.20 -5 -2 14 195.08 14.90 -5 -2 14 209.68 16.20 5 -2 -14 185.18 16.50 -5 2 14 186.78 13.20 5 2 -14 250.27 17.20 -5 2 14 244.98 15.50 -5 2 14 237.48 16.10 -4 -2 14 70.49 10.00 -4 -2 14 73.89 9.70 -4 -2 14 74.29 8.50 4 -2 -14 69.59 10.20 4 2 -14 53.29 9.00 -4 2 14 60.49 9.40 -4 2 14 53.09 8.80 -4 2 14 61.19 7.70 -3 -2 14 49.80 8.30 3 -2 -14 48.20 8.90 -3 -2 14 36.50 8.60 -3 -2 14 42.80 6.80 -3 2 14 34.90 8.40 3 2 -14 45.20 8.90 -3 2 14 38.80 7.90 3 2 -14 46.90 8.80 -2 -2 14 1254.07 43.00 -2 -2 14 1235.88 45.20 2 -2 -14 1234.88 44.90 -2 -2 14 1229.98 44.70 2 -2 -14 1152.28 44.40 2 2 -14 1254.47 45.20 -2 2 14 1255.57 45.00 2 2 -14 1237.18 44.70 -2 2 14 1173.48 44.70 -1 -2 14 829.92 32.60 1 -2 -14 783.12 31.80 -1 -2 14 792.52 31.90 -1 -2 14 767.22 32.20 1 -2 -14 830.92 32.50 -1 2 14 768.22 31.70 -1 2 14 817.42 32.90 1 2 -14 853.61 32.80 1 2 -14 754.52 31.50 0 -2 14 2077.39 67.59 0 -2 -14 2035.20 66.79 0 -2 14 1937.51 67.19 0 -2 14 2007.10 67.99 0 -2 -14 2028.90 66.79 0 2 14 2053.69 67.69 0 2 14 2005.80 67.09 0 2 -14 1992.60 66.89 0 2 -14 2009.60 66.69 1 -2 14 482.95 22.30 -1 -2 -14 442.36 20.90 1 -2 14 470.75 22.20 -1 -2 -14 472.95 21.10 1 -2 14 467.45 24.30 -1 2 -14 476.55 21.30 1 2 14 478.15 22.30 1 2 14 462.25 22.00 -1 2 -14 500.65 21.80 2 -2 14 594.44 28.20 -2 -2 -14 605.34 23.10 2 -2 14 597.64 25.20 2 -2 14 598.54 25.00 -2 -2 -14 590.24 22.90 2 2 14 577.04 24.50 2 2 14 587.14 25.10 -2 2 -14 591.94 23.50 -2 2 -14 579.34 23.40 3 -2 14 874.71 32.70 -3 -2 -14 886.51 28.90 3 -2 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96.49 10.90 6 -2 23 30.60 8.30 6 -2 23 34.90 8.10 6 -2 23 24.40 11.10 6 2 23 40.20 8.50 6 2 23 44.30 12.30 6 2 23 27.70 8.40 7 -2 23 11.00 7.10 7 -2 23 18.40 10.90 7 -2 23 20.20 7.90 7 2 23 1.50 6.70 7 2 23 12.90 7.10 7 2 23 -1.90 11.50 8 -2 23 13.00 7.30 8 -2 23 15.40 7.70 8 -2 23 10.30 12.40 8 2 23 9.90 7.40 8 2 23 5.20 7.10 8 2 23 9.20 12.90 9 -2 23 151.58 17.60 9 -2 23 137.19 14.20 9 -2 23 94.99 17.70 9 2 23 121.09 13.60 9 2 23 127.19 11.10 9 2 23 123.29 17.10 -9 -3 23 43.80 9.60 9 -3 -23 30.80 12.30 9 -3 -23 21.80 11.30 -9 -3 23 19.10 8.70 9 3 -23 27.30 13.30 -9 3 23 24.30 9.40 9 3 -23 27.10 11.40 -9 3 23 14.90 7.30 -9 3 23 33.70 9.70 8 -3 -23 42.30 11.50 8 -3 -23 26.80 11.40 -8 -3 23 34.00 9.60 -8 -3 23 51.29 10.20 -8 3 23 48.10 11.70 8 3 -23 36.10 11.50 8 3 -23 38.80 12.40 -8 3 23 35.10 10.40 -8 3 23 25.30 7.90 7 -3 -23 8.10 10.20 -7 -3 23 6.20 8.80 -7 -3 23 13.00 4.40 -7 -3 23 16.10 4.60 -7 -3 23 16.90 9.10 7 -3 -23 23.50 11.10 7 3 -23 12.30 10.80 7 3 -23 8.00 10.00 -7 3 23 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29.10 11.70 -5 -2 28 30.10 11.20 -5 -2 28 51.99 10.10 -5 -2 28 33.40 11.40 5 2 -28 26.50 11.70 -5 2 28 32.10 11.00 -5 2 28 27.60 11.60 5 2 -28 11.60 11.60 -4 -2 28 55.99 11.70 4 -2 -28 83.39 12.80 -4 -2 28 71.49 12.70 -4 -2 28 62.89 11.20 -4 2 28 51.49 12.10 4 2 -28 47.90 11.60 -4 2 28 62.39 12.50 -3 -2 28 36.80 11.10 3 -2 -28 30.20 10.90 -3 -2 28 45.50 10.50 -3 2 28 28.00 10.60 3 2 -28 5.30 13.30 3 2 -28 34.40 11.20 -2 -2 28 -0.60 10.20 2 -2 -28 17.10 10.00 -2 -2 28 1.60 8.50 2 2 -28 20.20 9.70 -2 2 28 18.10 9.50 1 -2 -28 37.10 9.90 -1 -2 28 41.50 11.40 -1 -2 28 52.89 11.90 1 -2 -28 30.50 11.00 -1 -2 28 40.70 10.80 -1 2 28 53.79 12.40 1 2 -28 48.30 10.70 -1 2 28 49.10 10.70 1 2 -28 55.39 11.50 0 -2 28 98.09 12.80 0 -2 -28 90.29 11.70 0 -2 -28 125.49 14.00 0 -2 28 100.09 13.80 0 -2 28 75.59 13.40 0 2 28 89.19 13.40 0 2 -28 97.19 11.60 0 2 28 77.29 12.10 0 2 -28 110.49 13.00 -1 -2 -28 -3.20 8.00 1 -2 28 0.90 10.90 1 -2 28 7.40 9.30 -1 -2 -28 7.20 7.60 1 -2 28 14.80 9.20 1 2 28 8.50 8.90 1 2 28 10.90 9.90 -2 -2 -28 40.90 8.10 -2 -2 -28 28.70 7.70 2 -2 28 22.80 9.80 2 -2 28 29.30 12.20 2 -2 28 28.40 10.30 -2 2 -28 20.40 7.70 2 2 28 29.30 10.70 -2 2 -28 23.20 8.60 2 2 28 11.40 9.70 3 -2 28 12.10 9.30 -3 -2 -28 30.80 6.80 -3 -2 -28 41.60 7.10 3 -2 28 41.20 12.30 3 -2 28 35.40 10.90 3 2 28 27.50 10.20 3 2 28 18.60 10.00 -3 2 -28 22.40 7.20 4 -2 28 12.80 9.30 -4 -2 -28 12.50 4.00 4 -2 28 27.30 12.30 4 -2 28 37.40 10.10 -4 -2 -28 12.20 4.10 4 2 28 12.60 10.00 4 2 28 7.20 8.90 -4 2 -28 12.70 4.80 -4 2 -28 15.00 5.00 5 -2 28 -2.70 8.50 5 -2 28 26.60 9.40 5 -2 28 18.90 11.70 5 2 28 -10.30 8.90 5 2 28 4.00 11.20 5 2 28 -2.80 8.50 6 -2 28 3.90 12.50 6 -2 28 10.90 9.40 6 -2 28 17.90 9.80 6 2 28 6.60 9.80 6 2 28 17.70 9.00 6 2 28 -18.00 12.60 7 -2 28 33.30 9.90 7 -2 28 30.80 9.90 7 -2 28 23.40 15.20 7 2 28 39.10 15.00 7 2 28 33.80 10.00 7 2 28 31.00 9.80 -8 -3 28 221.18 11.30 -8 -3 28 260.87 22.20 8 -3 -28 171.18 21.80 8 -3 -28 217.08 25.40 -8 -3 28 227.58 11.60 -8 -3 28 218.48 21.90 -8 3 28 226.18 22.50 -8 3 28 264.27 22.90 8 3 -28 163.68 19.00 8 3 -28 268.87 29.10 -7 -3 28 71.39 7.80 7 -3 -28 48.90 13.00 7 -3 -28 71.09 14.50 -7 -3 28 52.89 12.60 -7 -3 28 85.79 13.20 7 3 -28 58.69 14.30 -7 3 28 72.19 12.90 -7 3 28 92.69 11.30 -7 3 28 54.19 12.40 7 3 -28 58.59 13.90 -6 -3 28 28.10 11.70 6 -3 -28 30.70 11.80 6 -3 -28 20.30 11.10 -6 -3 28 24.20 10.80 -6 3 28 38.20 10.90 6 3 -28 14.10 11.50 6 3 -28 58.19 13.80 -6 3 28 30.70 11.80 -6 3 28 13.90 9.20 -5 -3 28 -5.50 7.40 -5 -3 28 -4.70 9.60 5 -3 -28 4.30 9.60 5 -3 -28 2.10 10.40 -5 -3 28 -20.90 8.70 -5 3 28 5.10 10.60 5 3 -28 -4.20 10.60 -5 3 28 6.30 10.10 5 3 -28 10.60 10.30 -4 -3 28 28.00 10.90 -4 -3 28 29.40 9.70 4 -3 -28 42.40 12.10 -4 -3 28 43.10 10.90 4 -3 -28 34.80 10.60 -4 3 28 43.40 10.90 4 3 -28 14.80 10.70 -4 3 28 75.49 13.30 3 -3 -28 83.69 12.80 -3 -3 28 91.29 12.60 -3 -3 28 81.39 12.70 3 3 -28 94.09 13.50 3 3 -28 76.09 12.70 -3 3 28 74.69 12.20 -2 -3 28 11.40 9.20 -2 -3 28 -22.20 8.80 2 -3 -28 -8.70 8.60 -2 3 28 9.50 8.70 2 3 -28 -16.20 8.80 1 -3 -28 94.09 12.20 -1 -3 28 114.69 14.10 -1 -3 28 109.49 13.70 1 -3 -28 132.89 14.40 -1 -3 28 142.99 15.50 1 3 -28 100.09 13.00 -1 3 28 104.99 13.50 -1 3 28 118.29 14.70 1 3 -28 144.49 18.20 0 -3 28 17.10 10.70 0 -3 28 25.50 10.10 0 -3 -28 39.60 10.70 0 -3 -28 14.60 8.20 0 -3 28 7.20 8.90 0 3 -28 43.20 10.20 0 3 28 30.30 10.30 0 3 28 18.30 11.10 0 3 -28 32.80 10.70 1 -3 28 26.80 10.90 -1 -3 -28 0.50 8.90 1 -3 28 22.00 9.70 1 -3 28 5.30 10.80 -1 -3 -28 18.50 13.70 -1 3 -28 29.80 9.80 -1 3 -28 24.50 8.60 1 3 28 12.70 9.60 1 3 28 18.10 10.40 -2 -3 -28 -0.90 6.80 2 -3 28 12.50 9.00 2 -3 28 6.00 9.70 2 -3 28 2.40 10.00 -2 -3 -28 -3.00 6.80 -2 3 -28 12.20 7.90 2 3 28 4.80 9.00 2 3 28 5.80 10.20 -2 3 -28 12.30 7.60 3 -3 28 80.59 12.50 3 -3 28 89.49 12.80 3 -3 28 77.29 13.40 3 3 28 91.59 12.10 -3 3 -28 79.19 9.20 3 3 28 120.79 13.70 4 -3 28 18.70 9.80 4 -3 28 16.90 9.30 -4 -3 -28 9.40 4.00 4 -3 28 -17.40 10.70 -4 -3 -28 14.40 4.30 -4 3 -28 20.80 5.30 4 3 28 18.40 9.30 4 3 28 16.10 9.30 -4 3 -28 17.80 5.60 5 -3 28 20.40 9.90 5 -3 28 3.00 12.10 5 -3 28 -1.90 9.20 5 3 28 12.90 9.00 5 3 28 32.80 10.30 6 -3 28 82.89 12.60 6 -3 28 50.89 10.70 6 -3 28 67.19 15.10 6 3 28 85.39 11.70 6 3 28 65.49 14.70 6 3 28 67.09 12.00 7 -3 28 12.70 11.20 7 -3 28 13.20 9.40 7 3 28 7.20 9.60 7 3 28 7.90 10.20 7 3 28 11.30 14.60 -8 -4 28 107.99 13.80 -8 -4 28 87.79 13.90 -8 4 28 73.59 13.00 -8 4 28 90.19 12.20 8 4 -28 64.89 19.70 -8 4 28 134.49 15.50 -7 -4 28 10.60 11.50 -7 -4 28 -19.80 10.30 7 -4 -28 -0.30 12.40 -7 -4 28 10.50 5.80 7 -4 -28 -10.40 11.70 -7 4 28 -6.90 9.00 7 4 -28 10.80 11.50 -7 4 28 -16.90 10.70 7 4 -28 8.00 12.00 -7 4 28 18.10 11.30 -6 -4 28 21.10 10.60 6 -4 -28 9.50 11.60 -6 -4 28 28.10 11.50 6 -4 -28 16.00 11.10 -6 4 28 15.90 9.80 6 4 -28 40.70 12.70 -6 4 28 32.60 11.60 -6 4 28 18.80 10.80 6 4 -28 33.80 12.50 -5 -4 28 23.60 11.40 5 -4 -28 16.40 11.40 -5 -4 28 17.50 7.70 -5 -4 28 18.80 10.50 5 -4 -28 40.30 11.40 5 4 -28 13.40 11.10 -5 4 28 26.40 11.50 5 4 -28 34.80 11.90 -5 4 28 11.80 9.30 -5 4 28 26.70 11.00 -4 -4 28 158.48 19.20 4 -4 -28 169.28 20.30 4 -4 -28 157.58 16.70 -4 -4 28 161.48 20.00 -4 -4 28 122.19 13.20 -4 4 28 187.98 19.60 4 4 -28 139.89 16.20 -4 4 28 176.08 20.50 -3 -4 28 8.90 9.30 3 -4 -28 14.10 9.90 -3 -4 28 4.90 10.40 3 -4 -28 10.00 9.80 3 4 -28 -3.70 8.90 3 4 -28 23.80 10.10 -3 4 28 -23.60 9.50 -2 -4 28 318.67 23.00 2 -4 -28 300.17 22.80 -2 -4 28 332.47 22.80 2 4 -28 310.67 22.70 -2 4 28 318.87 23.50 -1 -4 28 245.18 20.70 -1 -4 28 209.28 20.30 1 -4 -28 214.58 23.10 1 -4 -28 241.58 20.80 -1 -4 28 205.48 21.40 1 4 -28 209.78 19.90 -1 4 28 239.88 21.20 -1 4 28 223.58 20.90 0 -4 -28 92.59 12.30 0 -4 28 74.39 12.80 0 -4 -28 73.39 10.90 0 -4 28 114.59 14.90 0 -4 28 93.29 13.60 0 4 -28 74.89 11.30 0 4 -28 86.79 12.30 0 4 28 96.49 12.90 0 4 28 78.99 13.40 1 -4 28 10.50 9.70 -1 -4 -28 0.80 12.20 1 -4 28 19.00 10.80 1 -4 28 5.80 9.80 -1 -4 -28 10.70 11.00 1 4 28 15.70 10.70 1 4 28 27.60 10.00 -1 4 -28 22.30 10.20 -1 4 -28 20.20 9.30 -2 -4 -28 316.17 19.70 2 -4 28 260.97 22.70 -2 -4 -28 316.57 18.80 2 -4 28 374.66 25.80 2 -4 28 365.16 23.50 -2 4 -28 315.07 19.90 2 4 28 307.17 23.00 -2 4 -28 330.07 19.80 2 4 28 292.17 23.50 3 -4 28 79.39 12.30 3 -4 28 85.59 13.20 3 -4 28 65.69 13.60 -3 -4 -28 67.29 8.30 3 4 28 78.59 12.30 3 4 28 71.69 12.70 -3 4 -28 79.29 9.20 -3 4 -28 68.69 9.20 4 -4 28 -1.90 9.10 4 -4 28 6.50 10.10 -4 -4 -28 5.80 4.30 4 -4 28 0.90 11.60 -4 -4 -28 3.80 3.90 -4 4 -28 0.80 5.40 4 4 28 -11.30 9.20 4 4 28 -6.10 9.30 -4 4 -28 7.30 5.70 5 -4 28 77.79 13.40 5 -4 28 54.09 11.20 5 -4 28 46.60 13.60 5 4 28 67.89 11.40 5 4 28 49.90 11.60 6 -4 28 82.29 12.40 6 -4 28 95.39 14.60 6 -4 28 83.59 16.60 6 4 28 117.49 14.10 6 4 28 106.49 12.50 7 -5 -28 151.18 17.60 -7 -5 28 170.28 20.80 -7 -5 28 190.28 22.10 -7 -5 28 144.79 11.30 7 -5 -28 150.48 18.10 7 5 -28 156.68 18.10 -7 5 28 212.98 22.60 -7 5 28 120.79 15.50 7 5 -28 184.38 23.20 6 -5 -28 47.10 12.90 6 -5 -28 95.39 14.90 -6 -5 28 99.59 14.10 -6 -5 28 82.39 13.60 6 5 -28 61.49 13.80 6 5 -28 69.59 14.60 -6 5 28 89.39 14.10 -6 5 28 85.89 13.50 -5 -5 28 67.79 13.70 5 -5 -28 84.29 13.80 5 -5 -28 61.39 13.30 -5 -5 28 72.09 13.10 -5 -5 28 68.59 9.80 -5 5 28 60.69 12.30 5 5 -28 53.59 13.00 -5 5 28 79.19 13.20 5 5 -28 70.29 14.10 -4 -5 28 11.90 8.20 4 -5 -28 6.90 9.80 -4 -5 28 3.30 9.20 -4 -5 28 14.10 11.10 4 -5 -28 39.50 11.60 -4 5 28 16.80 10.10 4 5 -28 19.60 10.60 4 5 -28 6.70 11.20 -4 5 28 11.60 10.40 3 -5 -28 38.80 11.40 3 -5 -28 68.09 12.80 -3 -5 28 45.20 11.30 -3 -5 28 70.19 11.40 3 5 -28 60.79 12.20 -3 5 28 47.70 12.50 3 5 -28 54.09 12.30 2 -5 -28 268.67 22.60 -2 -5 28 237.88 22.00 -2 -5 28 234.18 19.40 -2 5 28 212.78 22.20 -2 5 28 234.58 21.80 2 5 -28 265.37 21.30 2 5 -28 241.58 22.10 -1 -5 28 27.80 11.40 -1 -5 28 11.60 9.80 1 -5 -28 25.10 9.70 -1 -5 28 6.20 9.60 -1 5 28 6.80 9.90 1 5 -28 6.30 10.20 -1 5 28 12.40 10.10 0 -5 -28 244.78 19.50 0 -5 -28 208.48 18.90 0 -5 28 193.38 21.20 0 -5 28 244.58 21.80 0 -5 28 233.48 20.90 0 5 -28 231.18 20.70 0 5 28 235.18 21.50 0 5 28 229.38 21.70 1 -5 28 170.58 20.10 -1 -5 -28 173.18 17.80 1 -5 28 159.38 19.80 -1 -5 -28 102.19 12.10 1 -5 28 113.09 14.90 1 5 28 193.78 19.80 1 5 28 173.38 20.20 -1 5 -28 173.58 17.50 -1 5 -28 122.59 13.70 2 -5 28 11.20 10.60 2 -5 28 9.50 10.10 -2 -5 -28 20.80 8.40 2 -5 28 -5.30 9.70 -2 5 -28 1.20 7.20 2 5 28 6.40 9.60 2 5 28 0.80 8.90 -2 5 -28 11.60 8.00 3 -5 28 5.50 9.60 3 -5 28 10.60 10.40 3 -5 28 17.10 12.50 -3 -5 -28 24.70 7.10 3 5 28 22.10 10.30 3 5 28 21.90 10.90 -3 5 -28 16.90 7.60 -3 5 -28 19.30 7.50 4 -5 28 188.98 19.50 -4 -5 -28 177.98 10.30 -4 -5 -28 191.28 10.70 4 -5 28 158.18 18.60 4 -5 28 201.98 22.70 -4 5 -28 232.68 13.20 4 5 28 200.58 19.90 -4 5 -28 178.18 13.60 4 5 28 220.58 20.80 5 -5 28 100.59 16.40 5 -5 28 74.59 12.30 5 -5 28 79.29 14.30 5 5 28 88.29 12.60 -5 5 -28 70.79 5.90 5 5 28 109.69 13.90 6 -5 28 32.70 20.90 6 -5 28 16.20 10.10 6 -5 28 -1.60 11.30 6 5 28 41.00 10.70 6 5 28 5.20 9.60 -7 -6 28 11.20 11.70 -7 -6 28 13.10 5.50 -7 -6 28 13.40 11.30 -7 6 28 3.90 11.90 -7 6 28 14.10 10.70 -7 6 28 8.00 11.90 7 6 -28 16.10 21.20 -6 -6 28 151.48 16.80 6 -6 -28 230.18 23.20 -6 -6 28 195.68 21.30 6 -6 -28 128.99 16.10 -6 6 28 177.18 21.80 6 6 -28 143.69 17.70 6 6 -28 204.08 23.10 -6 6 28 174.48 19.40 -6 6 28 134.99 16.20 -5 -6 28 -7.60 7.30 5 -6 -28 -10.10 10.00 5 -6 -28 7.40 10.80 -5 -6 28 -9.70 11.30 -5 -6 28 -13.80 9.90 -5 6 28 1.60 11.10 5 6 -28 11.20 11.70 -5 6 28 -11.40 11.10 5 6 -28 3.70 11.60 -5 6 28 15.40 9.80 -4 -6 28 5.90 11.20 4 -6 -28 -9.10 10.20 -4 -6 28 -0.90 10.20 4 -6 -28 1.10 10.80 4 6 -28 6.90 10.90 -4 6 28 0.60 11.10 -4 6 28 20.00 10.20 4 6 -28 -15.60 11.10 -4 6 28 13.60 11.20 -3 -6 28 14.20 10.50 3 -6 -28 14.10 10.80 3 -6 -28 11.90 11.10 -3 -6 28 13.50 9.80 -3 -6 28 21.10 10.80 3 6 -28 16.30 11.00 -3 6 28 22.70 10.50 3 6 -28 13.90 11.10 -3 6 28 28.00 11.10 -2 -6 28 63.99 11.80 2 -6 -28 94.29 13.20 -2 -6 28 50.59 12.20 2 -6 -28 76.09 13.20 -2 -6 28 48.90 12.20 -2 6 28 85.19 12.90 2 6 -28 65.59 12.50 -2 6 28 50.89 12.30 2 6 -28 43.90 12.50 -1 -6 28 8.70 10.10 1 -6 -28 -3.60 10.10 -1 -6 28 18.50 10.10 -1 -6 28 7.30 10.60 1 6 -28 7.30 9.00 -1 6 28 5.40 10.90 1 6 -28 20.20 10.40 -1 6 28 -1.70 10.00 0 -6 -28 4.70 9.50 0 -6 28 -14.10 9.80 0 -6 28 13.00 10.40 0 -6 -28 7.70 11.20 0 -6 28 3.80 9.90 0 6 28 14.90 11.00 0 6 -28 -23.60 8.40 0 6 28 -25.40 9.00 1 -6 28 22.70 10.40 1 -6 28 32.20 11.40 -1 -6 -28 6.80 9.20 -1 -6 -28 39.00 9.30 1 -6 28 1.80 9.80 -1 6 -28 14.40 8.90 1 6 28 -2.70 9.30 1 6 28 10.80 10.90 -1 6 -28 17.00 8.90 2 -6 28 12.60 11.50 2 -6 28 18.50 11.40 -2 -6 -28 6.60 7.80 -2 -6 -28 13.20 8.80 2 -6 28 14.30 9.90 2 6 28 12.40 10.40 -2 6 -28 13.40 8.50 2 6 28 31.00 11.40 -2 6 -28 8.90 8.60 3 -6 28 0.90 10.00 3 -6 28 -15.40 10.50 -3 -6 -28 -2.30 6.40 3 -6 28 1.00 12.00 -3 6 -28 -8.90 7.00 -3 6 -28 -2.20 7.40 3 6 28 7.80 10.40 3 6 28 -5.50 9.80 4 -6 28 109.69 13.90 -4 -6 -28 105.29 9.20 4 -6 28 82.29 15.50 -4 -6 -28 139.89 9.60 4 -6 28 116.99 14.80 4 6 28 123.29 14.40 -4 6 -28 109.59 12.80 4 6 28 139.39 15.10 5 -6 28 -1.10 10.20 5 -6 28 -18.00 9.90 5 -6 28 4.20 13.00 5 6 28 -4.40 9.90 -5 6 -28 -4.20 4.00 5 6 28 -12.60 10.10 6 -7 -28 19.30 15.40 -6 -7 28 -13.40 11.90 -6 -7 28 5.40 12.00 6 -7 -28 9.00 12.30 6 7 -28 21.10 16.10 -6 7 28 10.90 11.90 6 7 -28 30.90 13.30 -6 7 28 23.00 12.30 -6 7 28 -1.10 10.80 -5 -7 28 7.10 11.20 5 -7 -28 7.90 11.90 5 -7 -28 -16.90 10.50 -5 -7 28 2.90 7.60 -5 -7 28 3.50 11.10 5 7 -28 -3.30 12.00 -5 7 28 5.20 11.90 -5 7 28 6.10 11.70 5 7 -28 6.30 11.90 -5 7 28 0.90 10.40 -4 -7 28 -10.00 10.10 4 -7 -28 23.10 12.10 4 -7 -28 14.30 11.40 -4 -7 28 14.70 11.10 -4 -7 28 21.40 8.60 -4 7 28 17.70 12.10 -4 7 28 8.40 11.20 4 7 -28 17.50 11.40 -4 7 28 3.20 10.60 4 7 -28 27.40 12.50 3 -7 -28 181.68 21.70 3 -7 -28 198.08 21.40 -3 -7 28 199.38 20.90 -3 -7 28 217.28 22.90 -3 -7 28 191.38 19.30 3 7 -28 174.98 21.80 -3 7 28 195.48 21.20 -3 7 28 160.78 17.70 -3 7 28 203.78 21.40 3 7 -28 193.28 21.40 -2 -7 28 62.09 12.30 2 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0.2538 8 8 11 -2.7086 0.0336 8 8 12 -2.3756 0.2514 8 8 13 -0.8235 -0.0859 8 8 14 -1.2699 -0.2171 8 8 15 0.5166 0.0342 8 8 16 2.5957 -0.0401 8 8 17 5.2721 -0.1755 8 8 18 -1.0551 -0.1569 8 8 19 1.2426 0.3905 8 8 20 -2.2191 -0.4255 8 9 8 -0.1600 -0.2318 8 9 9 -0.0413 0.0657 8 9 10 1.3112 -0.3338 8 9 11 2.5475 0.1021 8 9 12 -0.0649 -0.0145 8 9 13 -3.1492 0.1349 8 9 14 -0.8752 0.1457 8 9 15 2.1083 0.3155 8 9 16 2.4295 0.1337 8 9 17 3.0929 0.1085 8 9 18 -1.3017 -0.3157 8 10 8 -2.5555 -0.1737 8 10 9 1.1944 -0.1470 8 10 10 1.1769 0.1619 8 10 11 -0.8936 0.1514 8 10 12 -1.5713 0.1095 8 10 13 1.1442 -0.2080 8 10 14 -0.5840 -0.1111 8 10 15 3.5103 0.0943 8 11 8 1.3041 -0.0855 8 11 9 0.3000 -0.3424 8 11 10 2.6262 0.0870 8 11 11 5.2157 0.1854 8 11 12 -2.1888 0.1148 8 12 8 3.8618 -0.0419 9 0 9 0.4836 1.7487 9 0 11 -1.0179 1.8624 9 0 13 -0.0805 1.3934 9 0 15 -1.6443 -0.9062 9 0 17 -2.2222 -1.5934 9 0 19 -5.4729 0.0193 9 0 21 2.1753 0.8255 9 0 23 -1.3212 -0.4021 9 1 9 0.1604 0.4783 9 1 10 0.1018 0.5647 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0.1663 9 4 13 1.9826 0.1163 9 4 14 0.2994 -0.0761 9 4 15 0.1112 0.1979 9 4 16 -0.1204 -0.1446 9 4 17 1.6204 -0.0574 9 4 18 -0.9860 0.3113 9 4 19 -0.3256 0.4405 9 4 20 0.1581 0.5571 9 4 21 1.6834 -0.2430 9 4 22 0.8583 0.2007 9 5 9 1.1650 -0.3665 9 5 10 -1.8559 -0.2785 9 5 11 -0.7094 0.0647 9 5 12 1.4334 -0.0528 9 5 13 3.5952 0.4302 9 5 14 -1.1185 0.0096 9 5 15 -0.1525 -0.0673 9 5 16 0.9236 0.2848 9 5 17 1.8640 -0.4159 9 5 18 0.5896 0.0362 9 5 19 -2.1315 -0.3385 9 5 20 -0.1135 0.2602 9 5 21 1.9839 -0.0347 9 6 9 0.6951 0.0602 9 6 10 -0.3917 -0.0319 9 6 11 -2.2852 -0.2309 9 6 12 -1.7453 0.0234 9 6 13 0.6968 -0.1314 9 6 14 -0.1609 0.3487 9 6 15 -3.9049 0.1736 9 6 16 -0.2673 0.0650 9 6 17 2.3228 -0.0267 9 6 18 -1.0888 -0.0333 9 6 19 -4.3781 -0.1976 9 6 20 -0.3653 0.5371 9 7 9 0.0606 0.1501 9 7 10 -2.1849 -0.2206 9 7 11 -1.6517 0.2048 9 7 12 1.5303 -0.3438 9 7 13 2.3051 -0.0369 9 7 14 -1.5105 0.1620 9 7 15 0.7521 0.3354 9 7 16 0.9160 0.3890 9 7 17 -2.8551 0.1670 9 7 18 -2.3851 -0.3716 9 8 9 1.1538 -0.1774 9 8 10 -1.5064 -0.1517 9 8 11 0.2144 0.0123 9 8 12 -1.2280 0.0313 9 8 13 1.8853 -0.1072 9 8 14 1.5824 -0.4024 9 8 15 -1.4651 -0.1450 9 8 16 -1.0315 0.1715 9 9 9 1.2197 0.4037 9 9 10 -0.5428 0.0813 9 9 11 0.5323 0.0659 9 9 12 3.3356 0.5669 9 9 13 -1.2820 0.4982 9 9 14 -2.4078 -0.1134 9 10 9 -1.1517 -0.1651 9 10 10 -0.4284 0.1612 9 10 11 -0.9964 -0.6223 10 0 10 -1.4621 -2.7246 10 0 12 1.1123 0.7264 10 0 14 -1.8766 0.8425 10 0 16 -2.3886 0.7520 10 0 18 0.2815 0.4712 10 0 20 -3.1906 -0.4402 10 1 10 -1.0813 -0.0006 10 1 11 -2.0091 -0.4869 10 1 12 0.2226 0.9857 10 1 13 3.1143 1.1335 10 1 14 2.0962 0.4772 10 1 15 0.0160 0.3118 10 1 16 -1.9589 0.4302 10 1 17 3.2558 -0.3862 10 1 18 0.7356 -0.4864 10 1 19 0.9672 -0.3221 10 1 20 -5.1409 -0.4787 10 2 10 1.7243 -0.2502 10 2 11 2.3668 -0.9163 10 2 12 3.5858 0.1698 10 2 13 0.5912 -0.4877 10 2 14 -0.4871 0.2833 10 2 15 -1.2011 -0.2001 10 2 16 -2.6570 0.1781 10 2 17 1.5985 0.5667 10 2 18 -2.4247 0.7548 10 2 19 -0.2423 -0.1677 10 3 10 -0.1126 0.1431 10 3 11 0.2564 -0.4537 10 3 12 2.1027 -0.4904 10 3 13 1.2777 -0.0252 10 3 14 -1.1478 0.3657 10 3 15 -0.7578 0.1989 10 3 16 -1.0873 -0.3782 10 3 17 -0.1211 -0.2404 10 3 18 -0.1414 0.0606 10 3 19 -1.1227 -0.2832 10 4 10 0.4652 0.5589 10 4 11 1.1105 -0.3371 10 4 12 -0.8713 -0.1012 10 4 13 -1.7480 -0.3282 10 4 14 -2.5728 0.0582 10 4 15 -1.1483 0.3248 10 4 16 -0.7965 0.0691 10 4 17 -2.4887 0.2871 10 4 18 -1.3195 -0.3528 10 5 10 -3.1438 0.1226 10 5 11 -0.6881 0.2640 10 5 12 2.2380 -0.3026 10 5 13 -1.0770 0.1291 10 5 14 -0.4078 -0.3033 10 5 15 0.0734 -0.1379 10 5 16 0.1843 0.5969 10 5 17 -0.6334 -0.4287 10 6 10 2.1933 0.0283 10 6 11 -2.0145 0.1932 10 6 12 0.2489 -0.3912 10 6 13 2.1543 -0.1167 10 6 14 0.3894 -0.4348 10 6 15 -0.6356 0.2401 10 7 10 -1.1414 0.3038 10 7 11 0.0644 0.7772 10 7 12 -1.5519 0.3244 10 7 13 -0.5748 -0.0418 10 7 14 0.8902 -0.7638 10 8 10 -0.1343 -0.4039 10 8 11 -2.2409 0.1224 11 0 11 -1.4195 0.8103 11 0 13 1.1161 -3.0841 11 0 15 -4.8753 -0.9568 11 1 11 -0.1849 0.0931 11 1 12 -1.2255 0.4784 11 1 13 -2.5096 0.0773 11 1 14 0.0766 -0.3583 11 1 15 0.2227 -0.6554 11 2 11 -2.2600 -0.1502 11 2 12 -0.7808 0.4757 11 2 13 -0.0973 0.0187 11 2 14 -0.4930 0.0021 11 2 15 -0.6245 -0.6074 11 3 11 0.1242 0.2652 11 3 12 -0.1844 -0.2661 11 3 13 2.1043 0.3158 11 3 14 2.4071 0.2032 11 4 11 1.0767 0.0464 11 4 12 0.5740 -0.3270 11 4 13 0.3265 -0.1257 11 5 11 -0.5205 0.9006 11 5 12 0.6968 -0.3930 0 0 0 0.0 0.0 ; _shelx_fab_checksum 31230 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn01 Zn 1.08190(5) 0.73718(4) 0.61969(2) 0.03572(17) Uani 1 1 d . . . . . Zn02 Zn 0.88126(5) 0.02431(4) 0.41808(2) 0.03561(17) Uani 1 1 d . . . . . Zn03 Zn 0.62512(6) 0.40694(4) 0.85171(2) 0.04198(18) Uani 1 1 d . . . . . O004 O 0.9351(3) 0.1150(2) 0.37097(11) 0.0358(7) Uani 1 1 d . . . . . H004 H 0.877018 0.099234 0.343233 0.054 Uiso 1 1 calc R . . . . O005 O 0.2588(3) 0.0615(3) 0.61011(11) 0.0421(8) Uani 1 1 d . . . . . O006 O 0.5516(3) 0.4136(3) 0.54248(12) 0.0439(8) Uani 1 1 d . . . . . O007 O 0.9201(3) 0.6571(3) 0.60240(13) 0.0458(8) Uani 1 1 d . . . . . O008 O 0.8151(4) 0.0784(3) 0.47371(12) 0.0441(8) Uani 1 1 d . . . . . O009 O 0.5900(4) 0.3395(3) 0.62938(12) 0.0483(9) Uani 1 1 d . . . . . O00A O 0.2281(3) 0.6457(3) 0.60737(13) 0.0504(9) Uani 1 1 d . . . . . O00B O 0.9885(4) 0.0772(3) 0.56204(12) 0.0473(9) Uani 1 1 d . . . . . O00C O 0.4193(4) 0.2120(3) 0.81099(12) 0.0520(9) Uani 1 1 d . . . . . O00D O 0.9150(4) 0.2220(3) 0.45898(14) 0.0565(10) Uani 1 1 d . . . . . O00F O 0.5872(6) 0.3123(4) 0.7980(2) 0.0890(9) Uani 1 1 d . U . . . O00G O 0.2333(5) 0.0047(4) 0.68068(14) 0.0646(11) Uani 1 1 d . . . . . O00H O 0.3311(4) 0.7887(4) 0.6148(2) 0.0801(16) Uani 1 1 d . . . . . C00J C 0.7854(5) 0.2136(4) 0.52280(17) 0.0378(10) Uani 1 1 d . . . . . C00K C 0.6423(4) 0.3378(3) 0.55184(16) 0.0347(10) Uani 1 1 d . . . . . C00L C 0.6887(5) 0.6472(4) 0.59155(16) 0.0377(10) Uani 1 1 d . . . . . C00M C 0.7920(5) 0.1678(3) 0.56598(17) 0.0382(10) Uani 1 1 d . . . . . C00N C 0.5666(5) 0.5050(4) 0.56496(16) 0.0364(10) Uani 1 1 d . . . . . O00O O 0.8150(6) 0.4269(4) 0.8326(2) 0.0890(9) Uani 1 1 d . U . . . C00P C 0.7096(5) 0.3001(4) 0.51641(16) 0.0397(10) Uani 1 1 d . . . . . H00P H 0.704385 0.332867 0.487632 0.048 Uiso 1 1 calc R . . . . C00Q C 0.6856(4) 0.5508(4) 0.57325(16) 0.0373(10) Uani 1 1 d . . . . . H00Q H 0.764311 0.517605 0.566677 0.045 Uiso 1 1 calc R . . . . C00R C 0.6530(5) 0.2938(4) 0.59477(16) 0.0366(10) Uani 1 1 d . . . . . C00S C 0.7274(5) 0.2080(4) 0.60143(16) 0.0400(10) Uani 1 1 d . . . . . H00S H 0.733896 0.176699 0.630538 0.048 Uiso 1 1 calc R . . . . C00T C 0.5719(5) 0.6941(4) 0.60175(18) 0.0423(11) Uani 1 1 d . . . . . H00T H 0.574146 0.760374 0.613556 0.051 Uiso 1 1 calc R . . . . C00U C 0.8435(5) 0.1693(4) 0.48228(17) 0.0394(10) Uani 1 1 d . . . . . C00V C 0.4499(5) 0.5503(4) 0.57612(16) 0.0382(10) Uani 1 1 d . . . . . H00V H 0.368904 0.516219 0.570899 0.046 Uiso 1 1 calc R . . . . C00W C 0.4536(5) 0.6455(4) 0.59488(17) 0.0405(11) Uani 1 1 d . . . . . C00X C 0.3299(5) 0.6971(5) 0.60647(18) 0.0477(13) Uani 1 1 d . . . . . C00Y C 0.8145(5) 0.7048(4) 0.60015(18) 0.0452(12) Uani 1 1 d . . . . . C00Z C 0.5246(5) 0.2770(4) 0.65835(18) 0.0447(12) Uani 1 1 d . . . . . C010 C 0.2805(5) 0.0627(4) 0.65324(19) 0.0493(13) Uani 1 1 d . . . . . C011 C 0.4386(5) 0.2042(4) 0.64112(17) 0.0452(12) Uani 1 1 d . . . . . H011 H 0.424453 0.195040 0.609101 0.054 Uiso 1 1 calc R . . . . C012 C 0.5457(5) 0.2928(4) 0.70463(17) 0.0464(12) Uani 1 1 d . . . . . H012 H 0.606993 0.341637 0.715883 0.056 Uiso 1 1 calc R . . . . C013 C 0.8762(5) 0.0762(4) 0.57517(19) 0.0471(12) Uani 1 1 d . . . . . C014 C 0.3730(5) 0.1445(4) 0.67134(18) 0.0480(12) Uani 1 1 d . . . . . C015 C 0.4755(5) 0.2357(5) 0.73488(18) 0.0502(13) Uani 1 1 d . . . . . C016 C 0.4938(5) 0.2544(5) 0.78543(18) 0.0492(13) Uani 1 1 d . . . . . C017 C 0.3900(5) 0.1618(5) 0.71816(19) 0.0522(13) Uani 1 1 d . . . . . H017 H 0.342982 0.122899 0.738699 0.063 Uiso 1 1 calc R . . . . O019 O 0.5655(6) 0.5326(4) 0.8136(2) 0.0890(9) Uani 1 1 d . U . . . O1 O 0.8054(4) 0.7945(3) 0.60278(18) 0.0449(12) Uani 0.75 1 d D . P . . O2 O 0.8249(5) 0.0071(4) 0.5946(2) 0.0659(18) Uani 0.75 1 d D . P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn01 0.0352(3) 0.0363(3) 0.0361(3) 0.0014(2) 0.0059(2) 0.0076(2) Zn02 0.0344(3) 0.0382(3) 0.0343(3) 0.0009(2) 0.0028(2) 0.0031(2) Zn03 0.0396(3) 0.0415(3) 0.0457(3) 0.0010(2) 0.0097(2) -0.0064(2) O004 0.0362(16) 0.0360(17) 0.0355(17) -0.0014(13) 0.0055(13) 0.0042(13) O005 0.0444(18) 0.049(2) 0.0326(18) -0.0033(15) 0.0002(14) -0.0044(15) O006 0.0468(19) 0.0412(19) 0.0425(19) -0.0082(15) -0.0065(15) 0.0133(15) O007 0.0343(17) 0.053(2) 0.051(2) 0.0012(17) 0.0103(15) 0.0021(15) O008 0.052(2) 0.045(2) 0.0354(18) -0.0020(15) 0.0051(15) 0.0083(16) O009 0.070(2) 0.0395(19) 0.0376(19) -0.0055(15) 0.0191(17) -0.0005(17) O00A 0.0418(19) 0.062(2) 0.048(2) 0.0050(18) 0.0086(16) 0.0182(18) O00B 0.046(2) 0.053(2) 0.044(2) 0.0074(16) 0.0052(16) 0.0202(16) O00C 0.063(2) 0.060(2) 0.0337(18) -0.0095(17) 0.0106(17) -0.0132(19) O00D 0.061(2) 0.061(2) 0.050(2) -0.0110(19) 0.0243(19) -0.0052(19) O00F 0.0864(11) 0.0920(11) 0.0891(11) 0.0008(8) 0.0090(8) -0.0045(8) O00G 0.074(3) 0.073(3) 0.046(2) 0.000(2) 0.000(2) -0.023(2) O00H 0.051(2) 0.069(3) 0.119(4) -0.043(3) -0.004(2) 0.025(2) C00J 0.038(2) 0.035(2) 0.040(3) -0.004(2) 0.0017(19) 0.0040(19) C00K 0.036(2) 0.033(2) 0.035(2) -0.0019(18) 0.0009(18) 0.0098(18) C00L 0.038(2) 0.041(3) 0.033(2) 0.003(2) 0.0001(19) 0.0030(19) C00M 0.037(2) 0.033(2) 0.045(3) 0.004(2) 0.005(2) 0.0047(19) C00N 0.041(2) 0.036(2) 0.032(2) -0.0029(19) 0.0024(19) 0.0094(19) O00O 0.0864(11) 0.0920(11) 0.0891(11) 0.0008(8) 0.0090(8) -0.0045(8) C00P 0.047(3) 0.039(3) 0.033(2) 0.003(2) 0.001(2) 0.007(2) C00Q 0.034(2) 0.042(3) 0.036(2) 0.005(2) 0.0039(19) 0.0097(19) C00R 0.040(2) 0.037(2) 0.034(2) -0.0042(19) 0.0118(19) 0.0001(19) C00S 0.046(3) 0.040(3) 0.034(2) 0.006(2) 0.004(2) 0.002(2) C00T 0.040(2) 0.041(3) 0.045(3) -0.003(2) -0.002(2) 0.010(2) C00U 0.038(2) 0.043(3) 0.038(3) 0.002(2) 0.0024(19) 0.010(2) C00V 0.036(2) 0.045(3) 0.034(2) 0.000(2) 0.0038(19) 0.006(2) C00W 0.037(2) 0.044(3) 0.039(3) -0.002(2) -0.003(2) 0.010(2) C00X 0.037(3) 0.066(4) 0.039(3) -0.011(3) -0.001(2) 0.014(2) C00Y 0.042(3) 0.054(3) 0.039(3) 0.007(2) 0.000(2) -0.001(2) C00Z 0.048(3) 0.050(3) 0.038(3) -0.006(2) 0.015(2) -0.001(2) C010 0.047(3) 0.055(3) 0.047(3) -0.002(3) 0.009(2) -0.005(2) C011 0.042(3) 0.063(3) 0.031(2) -0.010(2) 0.006(2) -0.002(2) C012 0.049(3) 0.054(3) 0.037(3) -0.010(2) 0.009(2) -0.009(2) C013 0.046(3) 0.045(3) 0.050(3) 0.003(2) -0.001(2) 0.010(2) C014 0.046(3) 0.057(3) 0.042(3) -0.007(2) 0.008(2) -0.007(2) C015 0.047(3) 0.066(4) 0.038(3) -0.013(2) 0.011(2) -0.010(2) C016 0.038(3) 0.074(4) 0.036(3) -0.014(3) 0.007(2) -0.012(2) C017 0.048(3) 0.068(4) 0.042(3) -0.005(3) 0.011(2) -0.014(3) O019 0.0864(11) 0.0920(11) 0.0891(11) 0.0008(8) 0.0090(8) -0.0045(8) O1 0.036(2) 0.024(2) 0.071(3) 0.006(2) -0.026(2) -0.0007(17) O2 0.035(2) 0.043(3) 0.121(5) 0.060(3) 0.011(3) 0.008(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O004 Zn01 O007 118.83(14) 3_766 . ? O004 Zn01 O00C 91.14(15) 3_766 2_656 ? O004 Zn01 O00D 85.04(14) 3_766 3_766 ? O007 Zn01 O00C 96.09(16) . 2_656 ? O007 Zn01 O00D 86.45(15) . 3_766 ? O00A Zn01 O004 134.89(15) 1_655 3_766 ? O00A Zn01 O007 104.18(16) 1_655 . ? O00A Zn01 O00C 97.52(15) 1_655 2_656 ? O00A Zn01 O00D 84.68(15) 1_655 3_766 ? O00C Zn01 O00D 176.10(15) 2_656 3_766 ? O004 Zn02 O005 107.12(14) . 3_656 ? O004 Zn02 O008 119.66(14) . . ? O004 Zn02 O00B 115.09(14) . 3_756 ? O008 Zn02 O005 106.57(15) . 3_656 ? O008 Zn02 O00B 105.80(15) . 3_756 ? O00B Zn02 O005 100.65(16) 3_756 3_656 ? O004 Zn03 O019 90.69(18) 4_566 . ? O004 Zn03 O1 90.64(16) 4_566 2_646 ? O004 Zn03 O2 94.19(16) 4_566 2_656 ? O00F Zn03 O004 89.26(18) . 4_566 ? O00F Zn03 O00O 90.4(2) . . ? O00F Zn03 O019 92.9(2) . . ? O00F Zn03 O1 95.0(2) . 2_646 ? O00F Zn03 O2 176.5(2) . 2_656 ? O00O Zn03 O004 179.28(19) . 4_566 ? O00O Zn03 O019 89.9(2) . . ? O00O Zn03 O1 88.8(2) . 2_646 ? O00O Zn03 O2 86.2(2) . 2_656 ? O019 Zn03 O1 172.0(2) . 2_646 ? O019 Zn03 O2 86.5(3) . 2_656 ? O1 Zn03 O2 85.5(2) 2_646 2_656 ? Zn01 O004 Zn03 105.50(14) 3_766 4_665 ? Zn01 O004 H004 105.5 3_766 . ? Zn02 O004 Zn01 119.08(16) . 3_766 ? Zn02 O004 Zn03 114.66(15) . 4_665 ? Zn02 O004 H004 105.5 . . ? Zn03 O004 H004 105.5 4_665 . ? C010 O005 Zn02 120.1(3) . 3_656 ? C00K O006 C00N 119.5(4) . . ? C00Y O007 Zn01 115.9(4) . . ? C00U O008 Zn02 115.7(3) . . ? C00R O009 C00Z 116.7(4) . . ? C00X O00A Zn01 107.8(4) . 1_455 ? C013 O00B Zn02 121.9(3) . 3_756 ? C016 O00C Zn01 124.4(3) . 2_646 ? C00U O00D Zn01 134.9(4) . 3_766 ? C016 O00F Zn03 135.1(5) . . ? C00M C00J C00U 123.3(4) . . ? C00P C00J C00M 118.4(4) . . ? C00P C00J C00U 117.9(4) . . ? C00P C00K O006 118.5(4) . . ? C00P C00K C00R 121.0(4) . . ? C00R C00K O006 120.1(4) . . ? C00Q C00L C00T 119.8(5) . . ? C00Q C00L C00Y 122.3(4) . . ? C00T C00L C00Y 117.9(5) . . ? C00J C00M C013 120.5(4) . . ? C00S C00M C00J 120.9(4) . . ? C00S C00M C013 118.5(5) . . ? O006 C00N C00V 114.9(4) . . ? C00Q C00N O006 123.1(4) . . ? C00Q C00N C00V 121.9(5) . . ? C00J C00P H00P 120.0 . . ? C00K C00P C00J 120.0(4) . . ? C00K C00P H00P 120.0 . . ? C00L C00Q H00Q 120.7 . . ? C00N C00Q C00L 118.6(4) . . ? C00N C00Q H00Q 120.7 . . ? O009 C00R C00K 117.8(4) . . ? O009 C00R C00S 122.8(4) . . ? C00S C00R C00K 119.4(4) . . ? C00M C00S C00R 120.2(4) . . ? C00M C00S H00S 119.9 . . ? C00R C00S H00S 119.9 . . ? C00L C00T H00T 119.6 . . ? C00W C00T C00L 120.8(5) . . ? C00W C00T H00T 119.6 . . ? O008 C00U C00J 116.2(4) . . ? O00D C00U O008 124.4(5) . . ? O00D C00U C00J 119.4(5) . . ? C00N C00V H00V 120.4 . . ? C00W C00V C00N 119.3(5) . . ? C00W C00V H00V 120.4 . . ? C00T C00W C00V 119.5(4) . . ? C00T C00W C00X 119.7(5) . . ? C00V C00W C00X 120.7(5) . . ? O00A C00X C00W 118.0(5) . . ? O00H C00X O00A 122.2(5) . . ? O00H C00X C00W 119.9(5) . . ? O007 C00Y C00L 118.3(5) . . ? O1 C00Y O007 125.0(5) . . ? O1 C00Y C00L 116.7(5) . . ? C011 C00Z O009 121.1(5) . . ? C012 C00Z O009 117.3(5) . . ? C012 C00Z C011 121.6(5) . . ? O005 C010 C014 115.1(5) . . ? O00G C010 O005 126.0(5) . . ? O00G C010 C014 118.9(5) . . ? C00Z C011 H011 120.4 . . ? C00Z C011 C014 119.3(5) . . ? C014 C011 H011 120.4 . . ? C00Z C012 H012 120.5 . . ? C00Z C012 C015 119.1(5) . . ? C015 C012 H012 120.5 . . ? O00B C013 C00M 117.9(5) . . ? O2 C013 O00B 126.1(5) . . ? O2 C013 C00M 116.0(5) . . ? C011 C014 C010 120.2(5) . . ? C017 C014 C010 120.0(5) . . ? C017 C014 C011 119.8(5) . . ? C012 C015 C016 119.8(5) . . ? C017 C015 C012 120.0(5) . . ? C017 C015 C016 120.2(5) . . ? O00C C016 O00F 125.7(5) . . ? O00C C016 C015 118.6(5) . . ? O00F C016 C015 115.7(5) . . ? C014 C017 H017 119.9 . . ? C015 C017 C014 120.2(5) . . ? C015 C017 H017 119.9 . . ? C00Y O1 Zn03 136.6(4) . 2_656 ? C013 O2 Zn03 137.6(5) . 2_646 ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Zn01 O004 2.003(3) 3_766 ? Zn01 O007 2.010(4) . ? Zn01 O00A 1.983(3) 1_655 ? Zn01 O00C 2.063(4) 2_656 ? Zn01 O00D 2.376(4) 3_766 ? Zn02 O004 1.945(3) . ? Zn02 O005 1.975(3) 3_656 ? Zn02 O008 1.946(3) . ? Zn02 O00B 1.964(3) 3_756 ? Zn03 O004 2.080(3) 4_566 ? Zn03 O00F 2.038(6) . ? Zn03 O00O 2.075(6) . ? Zn03 O019 2.087(6) . ? Zn03 O1 2.105(5) 2_646 ? Zn03 O2 2.107(5) 2_656 ? O004 H004 1.0000 . ? O005 C010 1.272(6) . ? O006 C00K 1.389(5) . ? O006 C00N 1.392(6) . ? O007 C00Y 1.254(6) . ? O008 C00U 1.271(6) . ? O009 C00R 1.380(5) . ? O009 C00Z 1.393(6) . ? O00A C00X 1.250(7) . ? O00B C013 1.236(7) . ? O00C C016 1.240(6) . ? O00D C00U 1.250(6) . ? O00F C016 1.267(7) . ? O00G C010 1.238(7) . ? O00H C00X 1.247(7) . ? C00J C00M 1.406(7) . ? C00J C00P 1.398(7) . ? C00J C00U 1.486(7) . ? C00K C00P 1.379(6) . ? C00K C00R 1.389(7) . ? C00L C00Q 1.395(7) . ? C00L C00T 1.399(7) . ? C00L C00Y 1.508(7) . ? C00M C00S 1.377(7) . ? C00M C013 1.510(7) . ? C00N C00Q 1.371(7) . ? C00N C00V 1.397(6) . ? C00P H00P 0.9500 . ? C00Q H00Q 0.9500 . ? C00R C00S 1.383(7) . ? C00S H00S 0.9500 . ? C00T H00T 0.9500 . ? C00T C00W 1.378(7) . ? C00V H00V 0.9500 . ? C00V C00W 1.385(7) . ? C00W C00X 1.499(7) . ? C00Y O1 1.204(7) . ? C00Z C011 1.386(8) . ? C00Z C012 1.378(7) . ? C010 C014 1.519(8) . ? C011 H011 0.9500 . ? C011 C014 1.396(7) . ? C012 H012 0.9500 . ? C012 C015 1.403(8) . ? C013 O2 1.221(7) . ? C014 C017 1.394(7) . ? C015 C016 1.505(7) . ? C015 C017 1.388(8) . ? C017 H017 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag Zn01 O007 C00Y C00L -174.5(3) . . . . ? Zn01 O007 C00Y O1 8.2(7) . . . . ? Zn01 O00A C00X O00H 3.5(7) 1_455 . . . ? Zn01 O00A C00X C00W -176.4(4) 1_455 . . . ? Zn01 O00C C016 O00F 6.5(9) 2_646 . . . ? Zn01 O00C C016 C015 -174.5(4) 2_646 . . . ? Zn01 O00D C00U O008 52.7(7) 3_766 . . . ? Zn01 O00D C00U C00J -127.0(4) 3_766 . . . ? Zn02 O005 C010 O00G 10.2(8) 3_656 . . . ? Zn02 O005 C010 C014 -169.5(3) 3_656 . . . ? Zn02 O008 C00U O00D -4.0(6) . . . . ? Zn02 O008 C00U C00J 175.7(3) . . . . ? Zn02 O00B C013 C00M 167.9(4) 3_756 . . . ? Zn02 O00B C013 O2 -13.3(9) 3_756 . . . ? Zn03 O00F C016 O00C -28.6(11) . . . . ? Zn03 O00F C016 C015 152.3(5) . . . . ? O005 C010 C014 C011 -7.2(8) . . . . ? O005 C010 C014 C017 171.3(5) . . . . ? O006 C00K C00P C00J -169.7(4) . . . . ? O006 C00K C00R O009 -11.9(7) . . . . ? O006 C00K C00R C00S 169.3(4) . . . . ? O006 C00N C00Q C00L 173.1(4) . . . . ? O006 C00N C00V C00W -174.3(4) . . . . ? O007 C00Y O1 Zn03 -52.6(9) . . . 2_656 ? O009 C00R C00S C00M -177.6(5) . . . . ? O009 C00Z C011 C014 -178.6(5) . . . . ? O009 C00Z C012 C015 176.0(5) . . . . ? O00B C013 O2 Zn03 45.5(12) . . . 2_646 ? O00G C010 C014 C011 173.1(6) . . . . ? O00G C010 C014 C017 -8.4(9) . . . . ? C00J C00M C00S C00R 1.0(8) . . . . ? C00J C00M C013 O00B 45.8(7) . . . . ? C00J C00M C013 O2 -133.2(6) . . . . ? C00K O006 C00N C00Q 40.5(7) . . . . ? C00K O006 C00N C00V -143.3(4) . . . . ? C00K C00R C00S C00M 1.2(7) . . . . ? C00L C00T C00W C00V -2.3(8) . . . . ? C00L C00T C00W C00X 179.5(5) . . . . ? C00L C00Y O1 Zn03 130.1(5) . . . 2_656 ? C00M C00J C00P C00K -0.7(7) . . . . ? C00M C00J C00U O008 49.8(7) . . . . ? C00M C00J C00U O00D -130.5(5) . . . . ? C00M C013 O2 Zn03 -135.6(6) . . . 2_646 ? C00N O006 C00K C00P -121.4(5) . . . . ? C00N O006 C00K C00R 66.0(6) . . . . ? C00N C00V C00W C00T 0.7(7) . . . . ? C00N C00V C00W C00X 178.9(5) . . . . ? C00P C00J C00M C00S -1.2(7) . . . . ? C00P C00J C00M C013 -177.9(5) . . . . ? C00P C00J C00U O008 -123.6(5) . . . . ? C00P C00J C00U O00D 56.1(7) . . . . ? C00P C00K C00R O009 175.7(4) . . . . ? C00P C00K C00R C00S -3.1(7) . . . . ? C00Q C00L C00T C00W 1.4(7) . . . . ? C00Q C00L C00Y O007 -19.0(7) . . . . ? C00Q C00L C00Y O1 158.5(5) . . . . ? C00Q C00N C00V C00W 1.9(7) . . . . ? C00R O009 C00Z C011 -49.7(7) . . . . ? C00R O009 C00Z C012 132.5(5) . . . . ? C00R C00K C00P C00J 2.9(7) . . . . ? C00S C00M C013 O00B -131.0(5) . . . . ? C00S C00M C013 O2 50.0(8) . . . . ? C00T C00L C00Q C00N 1.1(7) . . . . ? C00T C00L C00Y O007 162.2(5) . . . . ? C00T C00L C00Y O1 -20.3(7) . . . . ? C00T C00W C00X O00A -167.9(5) . . . . ? C00T C00W C00X O00H 12.2(8) . . . . ? C00U C00J C00M C00S -174.6(5) . . . . ? C00U C00J C00M C013 8.7(7) . . . . ? C00U C00J C00P C00K 173.1(5) . . . . ? C00V C00N C00Q C00L -2.8(7) . . . . ? C00V C00W C00X O00A 13.9(8) . . . . ? C00V C00W C00X O00H -166.0(5) . . . . ? C00Y C00L C00Q C00N -177.7(4) . . . . ? C00Y C00L C00T C00W -179.7(5) . . . . ? C00Z O009 C00R C00K 137.8(5) . . . . ? C00Z O009 C00R C00S -43.4(7) . . . . ? C00Z C011 C014 C010 -178.6(5) . . . . ? C00Z C011 C014 C017 2.9(8) . . . . ? C00Z C012 C015 C016 -177.9(5) . . . . ? C00Z C012 C015 C017 2.5(9) . . . . ? C010 C014 C017 C015 179.3(6) . . . . ? C011 C00Z C012 C015 -1.9(9) . . . . ? C011 C014 C017 C015 -2.3(9) . . . . ? C012 C00Z C011 C014 -0.9(8) . . . . ? C012 C015 C016 O00C 171.2(6) . . . . ? C012 C015 C016 O00F -9.7(9) . . . . ? C012 C015 C017 C014 -0.5(9) . . . . ? C013 C00M C00S C00R 177.7(5) . . . . ? C016 C015 C017 C014 180.0(6) . . . . ? C017 C015 C016 O00C -9.2(9) . . . . ? C017 C015 C016 O00F 169.9(6) . . . . ? loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons _smtbx_masks_void_content 1 -0.619 -0.941 -0.458 1826.3 470.7 ?