#------------------------------------------------------------------------------ #$Date: 2021-11-30 02:03:46 +0200 (Tue, 30 Nov 2021) $ #$Revision: 270922 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/70/89/7708955.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7708955 loop_ _publ_author_name 'Jurowska, Anna' 'Hodorowicz, Maciej' 'Krucza\/la, Krzysztof' 'Szklarzewicz, Janusz' _publ_section_title ; Anion--cation interactions in a series of salts with substituted Hphen, Hbpy and H2bpy cations and [W(CN)8]4− anion: polymer with “super-short” N--H⋯N hydrogen bridges containing exclusively anions and H+ ; _journal_name_full 'Dalton Transactions' _journal_paper_doi 10.1039/D1DT03224K _journal_year 2021 _chemical_formula_sum 'C44 H44 N14 O2 W' _chemical_formula_weight 984.78 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2017/1 _audit_update_record ; 2021-04-06 deposited with the CCDC. 2021-11-16 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90.1580(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 17.32210(10) _cell_length_b 10.98930(10) _cell_length_c 22.60420(10) _cell_measurement_temperature 100(2) _cell_volume 4302.87(5) _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.995 _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0851 _diffrn_reflns_av_unetI/netI 0.0262 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 128751 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 77.064 _diffrn_reflns_theta_min 3.210 _exptl_absorpt_coefficient_mu 5.421 _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.520 _exptl_crystal_F_000 1984 _exptl_crystal_size_max 1.000 _exptl_crystal_size_mid 0.100 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.832 _refine_diff_density_min -2.456 _refine_diff_density_rms 0.114 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.083 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 580 _refine_ls_number_reflns 9045 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.083 _refine_ls_R_factor_all 0.0293 _refine_ls_R_factor_gt 0.0289 _refine_ls_shift/su_max 0.012 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0435P)^2^+6.1641P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0757 _refine_ls_wR_factor_ref 0.0760 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8960 _reflns_number_total 9045 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1dt03224k2.cif _cod_data_source_block shelx _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 7708955 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.074 _shelx_estimated_absorpt_t_max 0.613 _shelx_res_file ; TITL exp_15464,4'-dimetylo-2,2'-bpy[w(cn)8]_a.res in P2(1)/n shelx.res created by SHELXL-2017/1 at 11:20:58 on 06-Apr-2021 CELL 1.54184 17.3221 10.9893 22.6042 90.000 90.158 90.000 ZERR 4.00 0.0001 0.0001 0.0001 0.000 0.001 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N W O UNIT 176 176 56 4 8 MERG 2 OMIT 12 11 7 OMIT 10 12 4 OMIT 2 12 14 OMIT 3 2 28 OMIT -10 7 21 OMIT 4 0 4 OMIT 7 5 25 OMIT -1 4 27 OMIT -2 11 17 ABIN HTAB N9 N58 HTAB N25 N48 EQIV $1 -x, -y, -z+1 HTAB C27 N50_$1 HTAB C21 N50_$1 EQIV $2 -x+1, -y+1, -z+1 HTAB C41 N18_$2 HTAB C36 N18_$2 HTAB C8 N60 EQIV $3 x, y-1, z HTAB C13 N60_$3 HTAB C24 N52 EQIV $4 -x, -y+1, -z+1 HTAB O2 N50_$4 HTAB O2 N48 EQIV $5 x, y+1, z HTAB N34 N58_$5 HTAB O1 N54 EQIV $6 -x+1/2, y+1/2, -z+1/2 HTAB O1 N52_$6 EQIV $7 -x+1/2, y-1/2, -z+1/2 HTAB O1 N56_$7 FMAP 2 PLAN 20 SIZE 0.100 0.100 1.000 ACTA BOND $H L.S. 5 0 15 TEMP -173.15 WGHT 0.043500 6.164100 FVAR 0.18785 W1 4 0.243273 0.369148 0.422201 11.00000 0.00801 0.00733 = 0.00667 0.00056 0.00167 0.00072 N9 3 0.262740 0.183197 0.629589 11.00000 0.01702 0.02173 = 0.01320 0.00141 0.00203 0.00093 AFIX 43 H9N 2 0.288479 0.148661 0.600580 11.00000 -1.20000 AFIX 0 N18 3 0.425531 0.400202 0.380587 11.00000 0.01466 0.01621 = 0.01381 -0.00105 -0.00131 0.00007 N25 3 0.081728 0.019579 0.542727 11.00000 0.01153 0.01608 = 0.01252 -0.00063 0.00237 -0.00062 AFIX 43 H25N 2 0.083390 0.095834 0.554548 11.00000 -1.20000 AFIX 0 N31 3 0.015337 0.105914 0.637742 11.00000 0.01619 0.01688 = 0.01452 -0.00109 0.00343 -0.00258 N34 3 0.403748 0.965568 0.521546 11.00000 0.01368 0.01740 = 0.01875 0.00245 0.00299 0.00334 N45 3 0.449112 1.065160 0.622008 11.00000 0.02024 0.01627 = 0.01811 0.00136 0.00477 0.00393 N48 3 0.125102 0.280214 0.529667 11.00000 0.01750 0.02406 = 0.01451 -0.00003 0.00357 -0.00269 N50 3 0.063590 0.401132 0.373467 11.00000 0.01587 0.01812 = 0.02085 0.00245 0.00119 0.00046 N52 3 0.224362 0.080749 0.381721 11.00000 0.02085 0.01465 = 0.01168 -0.00053 0.00287 0.00032 N54 3 0.251757 0.360641 0.275899 11.00000 0.01569 0.01521 = 0.01488 0.00063 0.00110 0.00010 N56 3 0.231590 0.658681 0.382732 11.00000 0.01946 0.01397 = 0.01634 0.00067 0.00234 0.00057 N15 3 0.259104 -0.052038 0.603072 11.00000 0.01727 0.02044 = 0.01836 0.00349 0.00014 0.00091 N58 3 0.338929 0.192465 0.515719 11.00000 0.02026 0.02229 = 0.01518 0.00375 0.00218 0.00646 C57 1 0.234387 0.558308 0.396839 11.00000 0.01191 0.01210 = 0.01080 0.00156 0.00298 0.00057 C61 1 0.281971 0.482223 0.495578 11.00000 0.01375 0.01377 = 0.01202 -0.00044 0.00153 -0.00042 N60 3 0.306284 0.537180 0.534874 11.00000 0.02460 0.02284 = 0.02045 -0.00352 0.00017 -0.00291 C53 1 0.228409 0.182408 0.394919 11.00000 0.01163 0.01379 = 0.00763 0.00064 0.00301 -0.00006 C19 1 0.362266 0.391944 0.396196 11.00000 0.01164 0.01084 = 0.01047 -0.00023 0.00104 0.00124 C51 1 0.125786 0.390181 0.391129 11.00000 0.01059 0.01150 = 0.01367 0.00206 0.00121 0.00002 C28 1 -0.073289 -0.035396 0.716179 11.00000 0.01573 0.01887 = 0.01358 0.00103 0.00205 0.00189 C49 1 0.164589 0.317255 0.492769 11.00000 0.01260 0.01729 = 0.01020 -0.00100 0.00269 -0.00040 C27 1 -0.040663 -0.086546 0.665629 11.00000 0.01349 0.01448 = 0.01459 -0.00183 0.00120 0.00111 AFIX 43 H27 2 -0.048219 -0.170167 0.656664 11.00000 -1.20000 AFIX 0 C55 1 0.249471 0.364715 0.326464 11.00000 0.01163 0.01171 = 0.00582 0.00018 0.00292 0.00073 C35 1 0.455535 0.901308 0.553312 11.00000 0.01201 0.01543 = 0.01719 0.00313 0.00256 -0.00072 C20 1 0.040823 -0.061647 0.575052 11.00000 0.00957 0.01943 = 0.01322 0.00119 -0.00039 0.00108 C59 1 0.308059 0.253809 0.481590 11.00000 0.01286 0.01417 = 0.01188 -0.00108 0.00276 0.00151 C43 1 0.529481 1.074598 0.708699 11.00000 0.02517 0.01641 = 0.01903 -0.00192 0.00316 -0.00240 AFIX 43 H43 2 0.544368 1.118275 0.743159 11.00000 -1.20000 AFIX 0 C40 1 0.482159 0.957222 0.609495 11.00000 0.01439 0.01357 = 0.01664 0.00067 0.00456 -0.00150 C26 1 0.003079 -0.013081 0.628614 11.00000 0.00998 0.01841 = 0.01083 -0.00198 -0.00095 0.00080 C21 1 0.038107 -0.181397 0.555938 11.00000 0.01198 0.01741 = 0.01370 -0.00181 0.00147 0.00139 AFIX 43 H21 2 0.009344 -0.239398 0.577907 11.00000 -1.20000 AFIX 0 C42 1 0.563161 0.962520 0.695929 11.00000 0.01552 0.01501 = 0.01620 0.00044 0.00412 -0.00436 C39 1 0.374878 0.927210 0.469782 11.00000 0.01370 0.02600 = 0.01738 0.00657 0.00094 0.00172 AFIX 43 H39 2 0.337481 0.974993 0.449570 11.00000 -1.20000 AFIX 0 C41 1 0.538647 0.903661 0.644474 11.00000 0.01292 0.01400 = 0.01804 -0.00014 0.00274 -0.00149 AFIX 43 H41 2 0.560443 0.827634 0.633511 11.00000 -1.20000 AFIX 0 C10 1 0.217050 -0.019141 0.650559 11.00000 0.01150 0.02283 = 0.01767 0.00088 -0.00359 0.00130 C5 1 0.179395 0.167009 0.711039 11.00000 0.01153 0.02642 = 0.01644 0.00359 -0.00122 0.00107 AFIX 43 H5 2 0.149600 0.118559 0.737247 11.00000 -1.20000 AFIX 0 C36 1 0.481666 0.792270 0.530302 11.00000 0.01483 0.01449 = 0.01947 0.00194 -0.00209 0.00057 AFIX 43 H36 2 0.517992 0.745185 0.551998 11.00000 -1.20000 AFIX 0 C6 1 0.182829 0.292721 0.719266 11.00000 0.01311 0.02749 = 0.01475 0.00066 -0.00451 0.00301 C11 1 0.174174 -0.100710 0.684006 11.00000 0.01390 0.02422 = 0.02052 0.00377 -0.00214 -0.00156 AFIX 43 H11 2 0.145542 -0.073004 0.717164 11.00000 -1.20000 AFIX 0 C37 1 0.455323 0.750839 0.475741 11.00000 0.01727 0.01655 = 0.02097 0.00079 -0.00086 -0.00305 C23 1 0.118050 -0.130210 0.473489 11.00000 0.01468 0.02600 = 0.01313 -0.00269 0.00310 0.00274 AFIX 43 H23 2 0.144754 -0.152146 0.438420 11.00000 -1.20000 AFIX 0 C29 1 -0.060388 0.087998 0.726400 11.00000 0.02087 0.02021 = 0.01454 -0.00465 0.00526 0.00115 AFIX 43 H29 2 -0.081010 0.126249 0.760573 11.00000 -1.20000 AFIX 0 C4 1 0.219094 0.111964 0.664921 11.00000 0.01355 0.02303 = 0.01289 0.00433 -0.00198 0.00180 C46 1 0.623103 0.907593 0.735688 11.00000 0.01991 0.01946 = 0.01927 -0.00187 -0.00279 -0.00330 AFIX 137 H46A 2 0.668167 0.961387 0.737549 11.00000 -1.50000 H46B 2 0.638649 0.828133 0.720055 11.00000 -1.50000 H46C 2 0.601699 0.897333 0.775464 11.00000 -1.50000 AFIX 0 C8 1 0.268713 0.303991 0.636609 11.00000 0.02124 0.02254 = 0.01707 0.00422 0.00131 0.00037 AFIX 43 H8 2 0.299931 0.350254 0.610443 11.00000 -1.20000 AFIX 0 C44 1 0.474074 1.121930 0.670743 11.00000 0.02738 0.01477 = 0.02122 -0.00142 0.00559 0.00386 AFIX 43 H44 2 0.452609 1.199192 0.679909 11.00000 -1.20000 AFIX 0 C22 1 0.076965 -0.218273 0.504893 11.00000 0.01007 0.02410 = 0.01547 -0.00187 -0.00009 0.00217 C13 1 0.217560 -0.258207 0.620227 11.00000 0.02097 0.01980 = 0.02569 0.00031 -0.00477 -0.00075 AFIX 43 H13 2 0.219681 -0.341184 0.608555 11.00000 -1.20000 AFIX 0 C7 1 0.229798 0.360694 0.681515 11.00000 0.02254 0.01753 = 0.02283 0.00064 -0.00218 0.00378 AFIX 43 H7 2 0.234740 0.446057 0.686973 11.00000 -1.20000 AFIX 0 C38 1 0.399176 0.819064 0.445862 11.00000 0.01606 0.02587 = 0.01662 0.00383 -0.00227 -0.00317 AFIX 43 H38 2 0.378173 0.790849 0.409499 11.00000 -1.20000 AFIX 0 C12 1 0.173468 -0.223695 0.668537 11.00000 0.01510 0.02493 = 0.02089 0.00389 -0.00614 -0.00153 C24 1 0.119984 -0.011827 0.493162 11.00000 0.01357 0.02496 = 0.01234 0.00402 0.00202 -0.00025 AFIX 43 H24 2 0.148258 0.047779 0.471841 11.00000 -1.20000 AFIX 0 C30 1 -0.016864 0.154855 0.685929 11.00000 0.02200 0.01648 = 0.01809 -0.00546 0.00403 -0.00186 AFIX 43 H30 2 -0.009750 0.239350 0.692956 11.00000 -1.20000 AFIX 0 C32 1 -0.121527 -0.110849 0.757870 11.00000 0.03086 0.01950 = 0.01969 -0.00025 0.01141 -0.00055 AFIX 137 H32A 2 -0.175131 -0.082418 0.756645 11.00000 -1.50000 H32B 2 -0.101299 -0.102664 0.798206 11.00000 -1.50000 H32C 2 -0.119472 -0.196454 0.745829 11.00000 -1.50000 AFIX 0 C16 1 0.126328 -0.312900 0.702954 11.00000 0.02168 0.02590 = 0.03064 0.00586 -0.00217 -0.00479 AFIX 137 H16A 2 0.150602 -0.326997 0.741562 11.00000 -1.50000 H16B 2 0.123268 -0.389869 0.681178 11.00000 -1.50000 H16C 2 0.074224 -0.280290 0.708675 11.00000 -1.50000 AFIX 0 C33 1 0.074429 -0.348124 0.485694 11.00000 0.02112 0.02305 = 0.02434 -0.00823 0.00678 0.00196 AFIX 137 H33A 2 0.119632 -0.391138 0.501360 11.00000 -1.50000 H33B 2 0.074696 -0.352133 0.442384 11.00000 -1.50000 H33C 2 0.027295 -0.386384 0.500727 11.00000 -1.50000 AFIX 0 C47 1 0.487266 0.636765 0.449540 11.00000 0.04019 0.02176 = 0.02285 -0.00644 -0.00766 0.00410 AFIX 137 H47A 2 0.539163 0.622135 0.465378 11.00000 -1.50000 H47B 2 0.489914 0.645199 0.406433 11.00000 -1.50000 H47C 2 0.453681 0.568101 0.459615 11.00000 -1.50000 AFIX 0 C17 1 0.134740 0.350882 0.766075 11.00000 0.01880 0.03076 = 0.02022 -0.00244 0.00008 0.00398 AFIX 137 H17A 2 0.084649 0.374218 0.749313 11.00000 -1.50000 H17B 2 0.161168 0.423465 0.781108 11.00000 -1.50000 H17C 2 0.126823 0.293160 0.798544 11.00000 -1.50000 AFIX 0 C14 1 0.258697 -0.170530 0.588939 11.00000 0.02112 0.02364 = 0.01945 -0.00114 -0.00042 0.00121 AFIX 43 H14 2 0.288083 -0.196072 0.555759 11.00000 -1.20000 AFIX 0 O1 5 0.239612 0.365321 0.162811 11.00000 0.02467 0.01201 = 0.01323 0.00153 0.00060 0.00022 O2 5 0.062246 0.421666 0.637622 11.00000 0.03127 0.03314 = 0.02303 -0.00828 -0.00985 0.01637 H2B 2 0.026785 0.475556 0.630815 11.00000 0.03171 H2A 2 0.074715 0.386162 0.609259 11.00000 0.06121 H34N 2 0.391660 1.032210 0.534594 11.00000 0.01402 H1A 2 0.252934 0.363725 0.202265 11.00000 0.06372 H1B 2 0.256743 0.431746 0.148137 11.00000 0.08519 H1C 2 0.254474 0.289623 0.144561 11.00000 0.02543 HKLF 4 REM exp_15464,4'-dimetylo-2,2'-bpy[w(cn)8]_a.res in P2(1)/n REM R1 = 0.0289 for 8960 Fo > 4sig(Fo) and 0.0293 for all 9045 data REM 580 parameters refined using 0 restraints END WGHT 0.0435 6.1626 REM Highest difference peak 0.832, deepest hole -2.456, 1-sigma level 0.114 Q1 1 0.1987 0.3669 0.4764 11.00000 0.05 0.83 Q2 1 0.2870 0.3703 0.3657 11.00000 0.05 0.80 Q3 1 0.3257 0.3811 0.4130 11.00000 0.05 0.69 Q4 1 0.2436 0.4179 0.3685 11.00000 0.05 0.63 Q5 1 0.2348 0.3219 0.4774 11.00000 0.05 0.59 Q6 1 0.2465 0.3192 0.3685 11.00000 0.05 0.58 Q7 1 0.2423 0.4185 0.4790 11.00000 0.05 0.56 Q8 1 0.2399 0.4941 0.4093 11.00000 0.05 0.49 Q9 1 0.2031 0.3694 0.5111 11.00000 0.05 0.48 Q10 1 0.2406 0.2497 0.4117 11.00000 0.05 0.47 Q11 1 -0.0940 -0.1796 0.7811 11.00000 0.05 0.43 Q12 1 -0.0980 -0.0798 0.7368 11.00000 0.05 0.39 Q13 1 -0.1429 -0.0583 0.7996 11.00000 0.05 0.39 Q14 1 0.1569 0.4484 0.4589 11.00000 0.05 0.37 Q15 1 0.0237 -0.3812 0.5423 11.00000 0.05 0.37 Q16 1 0.1778 0.4241 0.4199 11.00000 0.05 0.36 Q17 1 0.2557 0.4815 0.2960 11.00000 0.05 0.36 Q18 1 0.6759 0.9005 0.7174 11.00000 0.05 0.35 Q19 1 0.6268 0.9637 0.7612 11.00000 0.05 0.35 Q20 1 0.1179 0.2816 0.4206 11.00000 0.05 0.35 ; _shelx_res_checksum 75919 _shelx_hkl_file ; 0 0 -2 1216.06 55.06 0 0 2 1427.05 54.82 0 0 -2 1301.73 54.95 0 0 2 1450.21 54.86 0 0 3 0.91 0.20 0 0 -3 0.89 0.38 0 0 3 1.21 0.30 0 0 -3 1.30 0.39 0 0 3 0.50 0.22 0 0 3 0.71 0.23 0 0 4 629.21 28.03 0 0 -4 691.82 29.09 0 0 4 670.25 28.35 0 0 -4 771.01 29.20 0 0 4 730.76 28.48 0 0 4 755.27 28.64 0 0 -4 727.52 28.86 0 0 5 1.02 0.26 0 0 -5 0.73 0.43 0 0 5 1.03 0.41 0 0 -5 0.53 0.36 0 0 -6 231.80 10.57 0 0 6 215.19 9.24 0 0 -6 211.83 9.94 0 0 6 204.78 9.29 0 0 -6 229.10 10.49 0 0 7 0.67 0.26 0 0 7 1.83 0.51 0 0 -7 1.43 0.65 0 0 -7 2.61 0.89 0 0 7 1.34 0.48 0 0 8 61.00 3.23 0 0 8 76.92 4.10 0 0 -8 71.38 5.41 0 0 -8 81.00 5.55 0 0 8 65.00 4.06 0 0 -8 78.91 5.08 0 0 9 0.75 0.48 0 0 -9 0.90 0.88 0 0 9 0.83 0.48 0 0 10 170.08 8.52 0 0 -10 166.59 10.73 0 0 -10 171.04 10.09 0 0 11 2.77 0.80 0 0 -11 0.70 0.95 0 0 -11 1.52 1.14 0 0 -11 2.44 1.14 0 0 -12 203.40 12.75 0 0 12 175.48 9.42 0 0 -12 186.37 11.76 0 0 -12 200.06 12.93 0 0 12 185.14 10.99 0 0 12 186.79 11.21 0 0 -13 2.65 1.68 0 0 13 1.51 0.70 0 0 13 1.13 0.92 0 0 13 1.87 1.09 0 0 -13 1.10 0.99 0 0 -13 -0.35 0.94 0 0 -13 0.44 1.34 0 0 -14 396.86 24.18 0 0 14 419.72 21.58 0 0 14 411.98 22.03 0 0 14 415.25 21.73 0 0 -14 444.21 25.13 0 0 -14 391.50 26.20 0 0 15 0.24 0.66 0 0 -15 -0.72 3.39 0 0 -15 2.69 1.92 0 0 -15 3.13 3.05 0 0 -15 0.60 1.61 0 0 -15 -0.46 0.88 0 0 15 0.76 0.84 0 0 16 2.50 1.46 0 0 -16 0.73 3.11 0 0 -16 3.27 3.83 0 0 16 2.11 1.19 0 0 -16 1.52 1.68 0 0 16 2.03 1.74 0 0 16 1.72 1.47 0 0 -16 0.67 1.58 0 0 -17 8.25 3.80 0 0 17 0.60 1.22 0 0 -17 0.83 3.17 0 0 17 0.85 1.02 0 0 -17 5.06 3.05 0 0 -17 2.72 3.88 0 0 17 -0.44 1.88 0 0 17 0.87 1.04 0 0 17 5.34 2.15 0 0 17 0.41 1.10 0 0 17 4.06 2.06 0 0 17 2.40 1.61 0 0 17 0.37 1.51 0 0 -18 305.94 24.02 0 0 18 255.80 15.89 0 0 -18 227.07 22.61 0 0 -18 220.78 23.32 0 0 -18 243.99 19.50 0 0 18 249.79 15.53 0 0 18 227.26 15.25 0 0 18 226.07 17.53 0 0 18 279.78 18.27 0 0 18 235.20 17.11 0 0 18 229.97 16.91 0 0 18 269.07 16.67 0 0 18 252.60 17.46 0 0 18 260.20 17.20 0 0 -19 0.85 2.31 0 0 -19 1.14 4.36 0 0 -19 -2.97 4.44 0 0 19 1.88 1.34 0 0 -19 0.62 1.68 0 0 -19 -1.06 4.32 0 0 19 -0.46 1.53 0 0 19 0.31 1.33 0 0 19 2.96 2.21 0 0 19 0.44 2.41 0 0 19 2.20 1.88 0 0 19 1.09 1.20 0 0 19 0.41 1.46 0 0 -20 1461.47 65.42 0 0 -20 727.86 59.76 0 0 -20 744.20 58.81 0 0 20 1109.07 50.52 0 0 20 1025.31 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844.57 41.75 0 -5 8 981.64 43.50 0 5 -8 1302.04 49.56 0 -5 8 997.41 43.25 0 5 8 1038.09 43.58 0 5 -8 700.22 45.09 0 5 8 904.82 43.17 0 -5 8 1086.86 42.87 0 -5 -8 862.73 42.49 0 -5 8 1154.54 46.36 0 -5 -8 822.86 42.18 0 5 -9 3.48 1.36 0 -5 9 5.92 1.76 0 -5 9 2.17 1.27 0 -5 9 3.89 1.59 0 -5 9 2.96 1.12 0 -5 -9 3.48 1.89 0 5 -9 7.29 1.69 0 5 -9 7.22 2.88 0 -5 9 4.48 1.38 0 -5 9 1.68 1.04 0 5 -9 1.81 1.94 0 5 9 4.34 1.56 0 -5 -9 2.82 1.28 0 -5 9 3.33 1.88 0 5 -9 6.41 2.11 0 -5 -9 2.15 1.13 0 5 -10 577.71 29.29 0 -5 10 720.52 30.60 0 -5 10 671.44 28.15 0 -5 -10 384.99 28.76 0 5 -10 789.82 35.63 0 -5 -10 583.70 28.59 0 5 -10 589.22 28.75 0 -5 10 670.21 30.31 0 -5 10 664.13 29.35 0 -5 10 646.22 28.43 0 5 10 635.61 29.20 0 5 10 691.86 30.40 0 5 -10 661.64 31.99 0 -5 -10 472.65 27.90 0 -5 10 747.01 32.11 0 -5 -10 541.55 29.75 0 -5 11 193.58 11.64 0 5 -11 147.68 10.87 0 5 -11 161.90 11.97 0 -5 11 159.76 10.39 0 5 -11 160.04 10.59 0 -5 11 144.64 9.43 0 5 -11 182.35 14.49 0 -5 -11 158.15 10.26 0 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24.20 0 -6 11 372.59 21.00 0 6 11 425.19 22.11 0 6 11 376.53 23.27 0 6 11 344.39 22.32 0 6 -11 403.85 23.03 0 -6 11 407.42 22.16 0 6 -11 384.61 23.62 0 6 -12 94.01 10.33 0 6 -12 115.27 11.34 0 6 12 84.49 9.44 0 6 -12 90.49 9.58 0 -6 12 118.78 10.02 0 -6 -12 78.76 8.55 0 -6 -12 64.54 7.98 0 6 -12 98.73 10.31 0 -6 12 121.08 9.53 0 -6 12 112.55 8.56 0 -6 12 105.52 7.82 0 -6 12 100.24 8.35 0 -6 -12 96.31 8.03 0 -6 12 100.96 9.02 0 -6 12 108.10 8.77 0 -6 12 104.32 9.32 0 6 12 92.38 9.53 0 6 12 105.03 10.53 0 6 12 89.50 9.16 0 6 12 119.88 10.11 0 6 12 100.84 10.14 0 6 12 111.27 10.86 0 6 12 101.66 9.32 0 6 12 154.87 12.91 0 6 12 116.31 11.21 0 -6 12 120.84 9.59 0 6 12 99.66 10.54 0 6 12 117.94 9.95 0 6 12 108.55 9.28 0 6 12 105.58 10.51 0 6 -12 101.53 11.00 0 -6 12 99.13 9.33 0 6 -12 122.45 11.25 0 6 -13 43.80 7.14 0 6 13 33.31 5.82 0 6 -13 55.79 7.50 0 6 -13 54.56 7.97 0 -6 -13 34.04 5.77 0 -6 -13 40.63 5.98 0 -6 13 54.96 6.69 0 6 -13 50.38 7.71 0 -6 13 53.33 5.81 0 -6 13 48.39 5.54 0 -6 13 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350.73 19.03 0 6 -21 294.48 21.66 0 6 -21 335.37 22.33 0 6 -22 22.63 4.30 0 -6 22 19.49 3.46 0 6 -22 23.21 4.14 0 -6 22 22.77 3.76 0 -6 -22 32.06 5.94 0 -6 22 27.56 4.18 0 6 22 21.55 3.99 0 6 22 17.24 3.95 0 -6 22 23.69 3.61 0 6 22 23.45 4.15 0 6 -22 14.70 3.99 0 6 -22 28.07 5.21 0 -6 23 573.80 27.62 0 6 -23 530.72 30.05 0 -6 23 615.87 28.02 0 6 23 511.47 27.83 0 6 23 579.71 28.08 0 -6 23 652.46 28.56 0 6 -23 479.84 28.48 0 6 -23 576.32 30.01 0 -6 24 21.74 3.20 0 6 24 21.55 3.17 0 6 -24 23.72 3.43 0 6 -24 23.65 3.77 0 -6 24 26.72 3.31 0 6 -24 23.66 3.93 0 -6 25 113.42 7.05 0 6 25 93.20 6.32 0 6 -25 98.50 7.32 0 -7 0 1.19 1.21 0 -7 0 1.51 1.62 0 7 0 0.38 1.04 0 7 0 0.55 1.06 0 -7 0 1.00 1.27 0 -7 0 1.64 2.77 0 -7 0 2.44 1.98 0 -7 1 1067.00 49.25 0 -7 1 959.63 45.77 0 7 -1 1071.73 47.53 0 -7 1 947.18 45.27 0 -7 -1 1255.97 51.64 0 -7 -1 1073.23 48.47 0 7 1 996.93 47.06 0 7 -1 1091.19 50.44 0 7 -1 898.56 46.55 0 -7 -1 1215.02 49.29 0 -7 -1 1143.01 51.99 0 -7 1 853.87 50.12 0 -7 1 1282.15 54.90 0 -7 -1 1024.27 52.93 0 -7 2 306.34 18.74 0 -7 2 285.88 16.52 0 7 -2 323.85 15.72 0 -7 2 296.39 16.29 0 7 -2 316.23 17.92 0 -7 2 297.49 17.40 0 -7 -2 375.46 21.53 0 -7 -2 355.72 19.45 0 7 -2 266.46 16.93 0 7 -2 289.14 19.67 0 7 2 301.31 17.54 0 -7 2 176.98 17.95 0 -7 2 299.99 21.93 0 -7 -2 366.23 19.04 0 -7 -2 369.16 21.70 0 -7 2 406.82 23.29 0 -7 -2 303.71 21.89 0 -7 3 40.75 4.67 0 7 -3 46.77 4.60 0 -7 3 46.86 5.78 0 -7 3 44.13 4.67 0 -7 3 43.36 5.03 0 -7 -3 56.77 7.65 0 -7 -3 51.39 6.42 0 7 3 48.37 5.45 0 7 -3 44.15 6.53 0 7 3 37.29 5.40 0 -7 -3 45.39 5.53 0 -7 3 17.45 5.06 0 -7 -3 48.95 6.91 0 -7 3 45.08 7.27 0 -7 -3 33.18 6.47 0 7 -4 360.71 17.62 0 -7 4 318.47 17.10 0 -7 4 305.73 18.25 0 -7 4 303.22 16.57 0 -7 4 302.46 17.37 0 -7 -4 376.10 22.70 0 -7 4 294.88 16.99 0 -7 -4 361.23 20.64 0 7 -4 279.99 19.91 0 7 4 305.36 18.62 0 7 4 339.02 17.97 0 -7 -4 233.16 19.41 0 -7 -4 367.15 20.90 0 -7 -4 333.80 18.29 0 -7 4 298.22 19.92 0 -7 5 444.87 23.63 0 7 -5 603.06 26.10 0 -7 5 433.18 24.65 0 -7 5 464.35 23.49 0 -7 5 485.93 24.39 0 -7 -5 567.54 28.65 0 -7 5 443.06 23.55 0 -7 -5 468.01 28.64 0 7 -5 380.19 26.49 0 7 5 473.22 25.26 0 7 5 436.55 24.03 0 -7 -5 455.19 24.58 0 -7 -5 553.36 27.74 0 -7 5 516.61 26.94 0 -7 5 278.41 24.75 0 7 -5 456.79 24.23 0 7 -6 79.15 7.78 0 -7 6 62.12 6.27 0 -7 6 59.79 5.97 0 -7 6 59.21 6.30 0 -7 6 63.74 6.09 0 -7 -6 70.39 8.78 0 7 6 65.32 6.90 0 7 -6 41.92 7.23 0 7 6 56.81 6.24 0 -7 6 57.34 6.79 0 -7 -6 57.03 7.25 0 -7 -6 54.37 6.24 0 -7 6 52.38 7.56 0 7 -6 58.71 6.44 0 -7 7 986.18 43.47 0 -7 -7 783.56 42.44 0 7 -7 898.08 43.64 0 -7 -7 914.89 45.10 0 -7 7 934.60 46.41 0 -7 7 898.87 42.43 0 -7 7 902.22 42.69 0 -7 7 940.46 42.97 0 -7 7 961.42 42.38 0 7 7 929.55 45.83 0 -7 -7 1120.82 49.99 0 7 7 1114.80 50.65 0 7 7 895.66 43.04 0 7 7 899.58 43.49 0 7 7 909.43 43.56 0 7 7 1012.22 47.79 0 7 -7 728.96 46.01 0 7 -7 936.36 45.15 0 7 7 796.39 45.01 0 7 -7 908.40 44.19 0 -7 8 176.29 11.47 0 -7 -8 166.24 13.20 0 7 -8 144.47 12.01 0 -7 -8 126.17 11.14 0 -7 8 178.22 13.84 0 -7 8 185.95 13.75 0 -7 8 159.76 11.55 0 -7 8 165.37 11.77 0 7 -8 134.54 12.41 0 7 8 201.52 16.38 0 7 8 196.60 13.70 0 -7 -8 177.44 15.60 0 -7 8 164.71 12.23 0 -7 8 159.10 10.97 0 7 8 158.33 13.56 0 7 8 192.11 15.27 0 7 8 151.37 11.60 0 7 8 158.82 12.06 0 7 8 175.60 13.08 0 7 8 175.73 12.35 0 7 -8 138.84 14.26 0 7 -8 155.35 12.63 0 7 -8 156.99 13.18 0 7 8 154.03 13.40 0 7 -9 18.12 4.22 0 7 -9 16.40 3.96 0 7 9 13.10 3.68 0 7 -9 17.71 4.01 0 -7 9 14.87 2.88 0 -7 9 19.59 4.29 0 -7 -9 12.40 3.52 0 7 -9 13.58 3.49 0 -7 -9 19.96 3.82 0 -7 9 20.50 3.84 0 -7 9 18.36 3.58 0 -7 9 19.55 3.60 0 -7 9 16.52 3.16 0 -7 9 17.82 3.89 0 7 9 20.49 4.21 0 7 9 19.11 5.07 0 -7 -9 12.05 4.05 0 7 9 19.32 4.04 0 7 9 17.85 3.99 0 -7 9 26.47 4.40 0 -7 9 16.64 3.04 0 7 9 14.39 3.96 0 7 9 13.66 3.23 0 7 -9 11.63 4.28 0 7 9 18.66 3.82 0 7 9 18.30 3.72 0 7 9 12.75 4.19 0 7 9 19.99 4.12 0 -7 9 19.79 4.28 0 7 -9 20.46 3.87 0 7 10 108.09 11.81 0 7 -10 154.94 13.28 0 7 -10 132.56 10.98 0 7 -10 136.54 12.36 0 7 -10 137.11 12.11 0 -7 10 168.33 12.87 0 -7 -10 104.28 10.21 0 -7 10 168.89 12.07 0 -7 10 148.59 10.34 0 -7 10 144.95 10.85 0 -7 10 140.53 11.47 0 -7 10 149.70 10.14 0 7 10 140.26 11.89 0 7 10 158.75 12.36 0 -7 10 132.37 11.04 0 7 10 129.65 11.62 0 7 10 147.10 11.86 0 7 10 147.09 13.06 0 7 10 156.57 12.86 0 7 10 138.00 11.08 0 7 10 151.33 12.60 0 7 10 116.56 10.21 0 7 10 155.29 13.98 0 7 10 138.86 11.50 0 -7 10 142.18 11.79 0 7 -10 134.53 11.48 0 7 11 282.06 22.79 0 7 -11 388.31 22.96 0 7 -11 408.30 25.52 0 -7 11 446.48 24.40 0 -7 -11 274.60 21.27 0 -7 11 476.71 24.11 0 -7 11 427.49 22.55 0 -7 -11 337.37 20.83 0 -7 11 422.92 21.58 0 -7 11 407.94 23.09 0 7 11 515.38 25.45 0 -7 11 395.78 23.01 0 7 11 408.92 23.73 0 7 11 440.92 24.50 0 7 11 426.03 25.70 0 7 11 431.53 25.21 0 7 11 400.68 24.43 0 7 11 394.73 24.45 0 7 11 425.92 26.48 0 7 -11 399.57 23.98 0 -7 11 442.18 24.08 0 7 -12 34.72 6.42 0 7 12 21.28 4.95 0 7 -12 34.17 5.56 0 -7 -12 19.50 4.21 0 -7 12 39.13 5.91 0 -7 12 37.00 5.51 0 -7 12 34.92 4.44 0 -7 12 32.71 4.81 0 -7 12 30.56 5.01 0 7 12 42.79 7.20 0 7 12 45.92 6.25 0 7 12 45.88 7.15 0 7 12 37.39 6.27 0 -7 12 26.88 4.69 0 7 12 44.17 6.22 0 7 12 40.47 6.17 0 7 12 38.08 6.36 0 7 12 32.56 5.85 0 -7 12 35.93 5.50 0 7 -12 43.33 6.57 0 7 -13 582.10 33.88 0 7 -13 583.31 31.73 0 7 -13 450.28 31.78 0 -7 13 556.69 28.44 0 -7 13 570.57 29.39 0 -7 13 537.11 29.75 0 7 -13 565.06 33.20 0 -7 13 625.74 31.59 0 -7 -13 364.15 28.44 0 7 13 735.60 35.96 0 7 13 614.42 31.57 0 7 13 595.14 33.27 0 -7 13 639.57 31.26 0 7 13 604.57 32.62 0 7 13 548.27 32.27 0 7 13 590.16 33.19 0 7 13 554.80 30.67 0 7 13 595.63 30.87 0 7 13 637.65 31.79 0 7 -13 574.50 32.70 0 -7 13 620.92 31.22 0 -7 13 699.92 32.83 0 7 -14 4.59 2.70 0 7 -14 4.69 2.38 0 7 -14 10.20 3.82 0 -7 14 6.83 2.12 0 -7 14 5.29 2.07 0 -7 14 3.17 1.80 0 -7 -14 0.43 1.17 0 -7 14 9.83 2.97 0 7 -14 6.95 3.14 0 7 14 7.92 2.74 0 7 14 9.20 3.88 0 7 14 5.35 2.62 0 -7 14 0.37 1.83 0 7 14 5.70 2.82 0 7 14 4.95 2.77 0 7 14 4.97 2.51 0 7 14 6.70 2.45 0 7 14 7.46 2.56 0 7 -14 9.10 3.48 0 -7 14 8.58 2.93 0 -7 14 7.59 2.58 0 7 -15 113.64 12.71 0 7 -15 92.42 11.24 0 7 -15 113.75 11.47 0 -7 15 104.28 9.64 0 -7 15 115.78 9.47 0 -7 15 109.59 9.19 0 7 15 112.46 10.21 0 7 15 159.31 13.59 0 7 15 120.46 11.98 0 7 15 95.42 11.18 0 7 15 127.98 12.19 0 7 15 128.41 11.16 0 -7 15 127.01 10.66 0 7 -15 116.66 12.27 0 -7 15 125.46 10.86 0 7 -16 86.00 10.80 0 7 -16 97.91 10.59 0 -7 16 80.74 7.62 0 -7 16 82.86 8.13 0 -7 16 77.29 7.55 0 7 16 92.54 10.19 0 7 16 77.01 9.76 0 7 16 84.12 9.77 0 7 16 75.15 9.49 0 7 16 86.56 9.00 0 -7 16 74.52 8.15 0 7 -16 93.05 10.96 0 -7 16 90.53 8.89 0 7 -17 7.14 3.10 0 7 -17 8.90 3.86 0 -7 17 3.53 1.76 0 -7 17 5.57 2.23 0 -7 17 9.35 2.44 0 7 17 6.42 3.17 0 7 17 9.50 3.53 0 7 17 7.07 3.01 0 7 17 6.78 3.16 0 7 17 6.69 2.73 0 -7 17 10.50 2.87 0 7 -17 6.44 2.98 0 -7 17 3.57 2.06 0 7 -18 173.68 15.32 0 7 -18 175.08 16.55 0 -7 18 206.38 13.29 0 -7 18 208.43 14.22 0 -7 18 206.27 13.01 0 7 18 206.70 16.51 0 7 18 218.44 15.86 0 7 18 201.69 15.33 0 7 18 217.43 15.91 0 7 18 217.90 14.67 0 -7 18 192.84 13.74 0 7 -18 201.73 16.96 0 -7 18 177.03 13.42 0 7 -18 219.21 18.00 0 7 -19 359.40 25.58 0 -7 19 438.12 22.96 0 -7 19 424.95 22.93 0 7 -19 409.68 26.37 0 -7 19 438.31 23.24 0 -7 19 400.00 21.26 0 -7 19 430.08 23.55 0 7 19 414.58 24.25 0 7 19 410.45 24.05 0 7 19 444.35 23.36 0 7 19 410.20 24.26 0 7 -19 381.79 24.88 0 7 -19 338.02 25.37 0 7 -20 2.59 1.94 0 7 -20 2.05 2.20 0 7 -20 3.11 2.17 0 -7 20 3.28 1.67 0 -7 20 2.51 1.76 0 7 20 4.15 2.10 0 7 20 2.89 1.84 0 7 20 2.88 2.13 0 7 20 4.24 1.80 0 -7 20 3.22 1.64 0 -7 20 2.77 1.46 0 7 -20 2.97 2.13 0 7 -20 3.89 2.38 0 7 -21 244.07 16.31 0 7 -21 186.88 15.73 0 7 -21 255.78 16.72 0 -7 21 257.39 14.75 0 -7 21 258.99 15.04 0 7 21 250.05 15.42 0 7 21 216.63 14.34 0 -7 21 265.24 14.48 0 7 21 215.14 13.46 0 7 21 242.05 15.30 0 -7 21 236.85 14.35 0 7 -21 238.07 16.98 0 7 -21 211.53 15.81 0 7 -22 126.17 10.16 0 7 -22 110.99 10.16 0 7 -22 140.53 10.64 0 -7 22 145.62 9.45 0 7 22 125.47 9.56 0 -7 22 138.46 9.51 0 7 22 122.10 9.37 0 7 -22 129.42 10.89 0 7 -22 123.23 9.87 0 -7 22 135.32 9.24 0 -7 23 22.13 3.09 0 7 -23 15.98 2.61 0 7 23 23.66 3.38 0 -7 23 26.18 3.41 0 7 23 23.96 3.33 0 7 -23 18.21 3.21 0 7 -23 22.51 3.47 0 -7 24 17.24 2.37 0 -7 24 15.92 2.43 0 7 24 18.42 2.51 0 7 24 16.39 2.31 0 7 -24 19.68 2.59 0 8 0 832.25 38.28 0 8 0 811.92 38.45 0 -8 0 827.13 38.27 0 8 0 748.02 36.87 0 8 0 609.39 40.07 0 -8 0 914.20 41.32 0 -8 0 695.11 34.98 0 8 0 706.09 36.92 0 8 0 776.70 40.12 0 8 0 701.40 39.22 0 -8 0 611.20 40.80 0 -8 0 921.83 43.36 0 8 1 1.31 2.53 0 8 1 7.84 2.53 0 8 -1 9.68 2.89 0 8 -1 7.26 2.48 0 8 -1 7.07 2.64 0 8 1 8.73 2.57 0 8 1 8.41 2.59 0 -8 -1 10.02 2.28 0 -8 1 8.37 2.22 0 -8 -1 10.26 2.97 0 8 1 7.58 3.44 0 -8 1 12.69 3.37 0 8 -1 7.40 3.29 0 8 1 8.48 2.52 0 -8 -1 10.55 3.42 0 8 -1 8.61 2.50 0 8 1 9.89 3.43 0 8 1 7.60 2.54 0 8 -1 3.93 2.23 0 -8 -1 6.95 3.33 0 -8 -1 11.62 3.31 0 -8 1 7.25 4.18 0 -8 1 3.96 3.24 0 -8 -2 231.30 18.36 0 -8 2 88.25 13.17 0 -8 -2 221.37 15.33 0 -8 2 207.87 18.14 0 -8 2 186.69 11.99 0 -8 2 194.00 13.09 0 8 -2 208.41 14.15 0 -8 -2 195.47 12.12 0 -8 2 213.56 12.88 0 8 2 222.86 14.53 0 8 -2 206.61 14.65 0 8 2 183.58 17.23 0 8 2 211.55 13.94 0 -8 2 204.51 13.69 0 -8 -2 239.14 15.66 0 8 2 176.21 14.45 0 -8 -2 281.40 18.81 0 -8 2 198.25 14.85 0 8 -2 109.72 13.52 0 8 -2 203.71 16.12 0 8 2 204.07 15.24 0 8 2 194.73 13.78 0 8 2 198.25 16.02 0 8 2 214.58 14.24 0 8 -2 223.52 15.31 0 8 2 129.16 15.27 0 8 -2 213.55 14.65 0 8 3 9.57 2.67 0 8 -3 7.52 2.79 0 8 3 3.03 2.48 0 8 3 9.78 2.81 0 8 -3 6.47 2.12 0 8 3 6.37 2.27 0 8 -3 7.17 2.54 0 -8 3 1.93 2.48 0 -8 -3 7.65 2.74 0 -8 3 7.68 3.85 0 -8 -3 8.88 3.51 0 -8 3 7.37 2.26 0 8 -3 3.95 2.03 0 -8 3 6.20 1.92 0 -8 3 7.93 2.18 0 -8 -3 17.29 4.72 0 8 3 4.45 2.35 0 -8 3 8.04 2.62 0 8 3 8.86 2.66 0 -8 3 7.91 2.28 0 8 3 10.15 4.00 0 -8 -3 8.03 2.85 0 8 3 4.69 2.25 0 8 3 6.82 3.27 0 8 -3 2.71 1.96 0 8 3 10.52 3.02 0 8 3 9.34 2.66 0 8 -3 5.66 2.15 0 -8 3 7.21 3.37 0 8 4 69.91 7.22 0 8 -4 65.95 7.94 0 8 -4 59.88 7.32 0 8 4 53.34 6.54 0 8 4 28.72 7.07 0 8 -4 62.38 6.92 0 -8 4 31.60 7.05 0 -8 -4 58.72 7.25 0 -8 4 63.88 8.61 0 -8 -4 70.85 9.31 0 -8 4 63.69 6.67 0 -8 4 53.06 5.73 0 -8 4 56.21 6.07 0 8 4 67.12 7.25 0 8 -4 54.38 7.41 0 8 4 75.43 10.69 0 8 4 40.11 6.71 0 -8 4 58.07 7.14 0 -8 4 64.05 6.63 0 -8 -4 79.17 9.05 0 -8 -4 66.79 9.72 0 8 4 59.54 6.87 0 8 4 59.54 6.77 0 8 4 56.63 8.26 0 8 -4 45.24 7.67 0 8 4 62.16 7.29 0 8 4 59.14 7.41 0 8 -4 60.96 6.80 0 -8 4 68.35 8.96 0 8 -5 117.94 10.29 0 8 -5 108.75 10.93 0 8 -5 113.09 10.75 0 8 5 125.71 10.34 0 8 5 116.69 10.04 0 -8 -5 112.77 10.43 0 -8 -5 128.43 12.60 0 -8 5 135.15 11.96 0 -8 5 99.79 11.85 0 -8 5 121.19 9.94 0 -8 5 113.30 9.05 0 -8 5 117.10 9.67 0 -8 5 115.32 9.42 0 8 5 106.90 9.75 0 8 -5 118.95 11.16 0 -8 -5 153.92 13.46 0 8 5 106.93 13.03 0 -8 5 130.90 10.89 0 -8 5 111.83 9.42 0 8 5 130.59 10.68 0 8 5 116.31 11.54 0 8 5 119.68 12.37 0 8 -5 89.90 11.36 0 8 5 135.14 11.05 0 8 5 106.72 10.29 0 8 5 114.03 9.95 0 -8 5 159.80 13.27 0 8 -5 121.91 10.42 0 8 6 374.48 22.09 0 8 -6 339.44 23.64 0 8 6 266.38 23.68 0 8 -6 425.00 23.72 0 8 -6 428.36 24.68 0 8 6 393.05 22.55 0 -8 -6 376.99 23.03 0 -8 -6 429.03 26.20 0 -8 6 395.18 26.06 0 -8 6 463.85 24.44 0 -8 6 427.64 22.96 0 -8 6 374.07 21.33 0 -8 6 384.08 21.92 0 8 -6 461.09 22.93 0 8 -6 416.67 24.81 0 8 6 408.45 22.80 0 -8 6 390.84 23.14 0 -8 6 373.83 21.58 0 8 6 399.85 23.07 0 -8 -6 498.12 28.57 0 8 6 394.37 24.91 0 8 6 427.76 28.53 0 8 -6 348.01 25.97 0 8 6 395.40 22.74 0 8 6 363.40 22.99 0 8 6 421.45 23.60 0 8 6 389.53 26.03 0 -8 6 419.97 25.22 0 8 -6 389.13 23.14 0 8 -7 116.12 10.77 0 8 -7 113.96 11.30 0 8 7 117.23 10.20 0 8 -7 105.85 11.35 0 8 7 106.63 11.86 0 -8 7 156.07 13.67 0 -8 -7 98.87 10.02 0 -8 -7 120.60 12.11 0 -8 7 138.27 10.88 0 -8 7 137.63 10.93 0 8 -7 150.31 11.49 0 -8 7 130.03 10.33 0 8 -7 106.04 11.15 0 8 7 125.83 10.46 0 8 7 116.66 10.77 0 -8 -7 150.45 14.69 0 8 7 147.50 12.12 0 8 7 102.61 11.41 0 8 7 134.65 14.28 0 -8 7 133.13 10.07 0 8 7 130.03 13.25 0 8 7 144.83 11.52 0 8 7 107.40 10.37 0 8 -7 105.44 12.87 0 8 7 138.29 11.15 0 8 7 114.22 10.26 0 -8 7 159.14 12.81 0 -8 8 495.62 24.68 0 -8 8 510.99 28.78 0 -8 -8 356.99 24.31 0 -8 -8 418.37 27.13 0 -8 8 533.35 27.63 0 -8 8 454.89 24.92 0 -8 8 446.56 24.81 0 -8 8 485.68 24.71 0 8 -8 549.36 27.27 0 8 8 443.46 24.81 0 -8 8 449.14 26.32 0 8 -8 446.36 27.44 0 8 8 455.97 27.85 0 8 8 531.58 27.56 0 -8 -8 494.94 31.25 0 8 8 569.62 32.44 0 -8 8 434.07 23.95 0 -8 8 480.16 26.11 0 8 8 462.27 25.91 0 8 8 492.89 29.72 0 8 8 480.28 25.98 0 8 8 434.45 25.08 0 8 8 474.81 26.03 0 8 -8 381.77 28.64 0 8 -8 484.80 26.85 0 8 -8 396.74 26.33 0 8 -8 312.60 25.13 0 8 8 334.00 26.16 0 -8 -9 19.26 4.24 0 -8 9 38.84 6.49 0 -8 -9 34.53 6.14 0 -8 9 34.61 5.69 0 8 -9 34.80 5.14 0 8 -9 43.45 6.35 0 -8 9 35.00 4.88 0 -8 9 39.03 5.46 0 8 9 35.96 5.23 0 -8 9 35.43 5.66 0 8 9 33.20 5.62 0 8 9 31.34 6.12 0 -8 -9 27.68 6.65 0 -8 9 35.33 4.79 0 8 9 36.05 7.30 0 -8 9 45.44 6.13 0 8 9 40.66 6.06 0 8 9 33.01 5.23 0 8 9 41.44 7.49 0 8 9 36.44 5.72 0 8 9 48.05 6.45 0 8 9 31.90 5.17 0 8 -9 21.70 5.08 0 8 -9 30.84 5.63 0 8 9 18.70 5.05 0 8 -9 40.28 6.73 0 8 -10 5.29 2.68 0 8 -10 7.04 3.11 0 8 -10 4.90 2.30 0 -8 -10 0.40 0.77 0 -8 -10 1.51 2.46 0 -8 10 1.82 2.04 0 -8 10 2.72 1.75 0 -8 10 4.54 2.01 0 8 -10 7.49 2.84 0 -8 10 4.57 1.85 0 -8 10 4.84 2.26 0 8 10 4.85 2.53 0 -8 10 1.60 1.54 0 8 10 3.19 1.85 0 8 10 9.69 3.91 0 8 10 3.08 2.15 0 8 10 8.53 2.77 0 8 10 6.16 2.61 0 8 10 4.86 2.40 0 8 10 1.79 2.15 0 8 10 1.94 1.58 0 8 -10 4.54 1.99 0 -8 10 6.08 2.52 0 8 -11 193.99 16.55 0 8 -11 190.70 16.09 0 -8 11 236.90 16.42 0 -8 -11 137.62 13.15 0 -8 -11 179.92 15.62 0 -8 11 213.50 14.99 0 8 -11 236.91 17.12 0 -8 11 207.77 14.24 0 -8 11 209.26 13.44 0 -8 11 191.82 14.45 0 8 11 218.89 15.46 0 -8 11 200.85 14.85 0 8 11 236.06 16.17 0 8 11 210.08 15.95 0 8 11 209.04 16.79 0 8 11 194.71 14.48 0 8 11 199.71 14.90 0 8 11 192.11 16.91 0 -8 11 197.58 14.71 0 8 -11 186.62 14.49 0 -8 -12 688.82 46.04 0 -8 -12 705.77 47.51 0 -8 12 1101.04 49.71 0 -8 12 1114.86 48.93 0 8 -12 951.06 48.56 0 -8 12 1079.93 47.73 0 8 -12 1285.11 53.31 0 -8 12 1025.25 45.91 0 -8 12 1071.84 47.60 0 -8 12 1000.30 47.93 0 -8 12 1022.87 48.62 0 8 12 1072.66 49.01 0 8 12 1117.38 49.89 0 8 12 976.02 50.76 0 8 12 1089.28 50.75 0 8 12 1083.93 49.27 0 8 12 947.31 47.75 0 8 12 1028.98 52.25 0 8 -12 891.76 50.48 0 8 -12 952.77 47.54 0 8 -13 2.35 2.12 0 8 -13 5.59 2.24 0 8 -13 3.68 2.47 0 -8 13 5.59 1.76 0 8 13 2.50 2.04 0 8 13 2.66 2.40 0 8 13 5.48 2.43 0 8 13 5.93 3.32 0 -8 13 7.57 2.67 0 -8 13 2.18 1.97 0 8 -13 4.18 2.19 0 8 13 4.76 2.35 0 -8 13 5.92 2.19 0 -8 13 5.87 2.59 0 -8 14 258.59 16.02 0 -8 14 251.70 16.48 0 8 -14 258.36 19.02 0 8 14 249.39 18.51 0 8 14 255.90 18.93 0 8 14 247.28 17.05 0 8 14 238.92 16.55 0 8 14 286.47 20.26 0 -8 14 301.64 18.33 0 8 -14 257.64 18.41 0 8 -14 253.23 20.04 0 -8 14 252.83 16.73 0 8 -14 235.98 17.00 0 8 -14 193.82 17.85 0 8 -15 56.54 8.50 0 8 -15 36.59 6.82 0 8 -15 53.76 7.10 0 -8 15 54.28 6.44 0 -8 15 61.94 6.44 0 8 -15 49.49 7.68 0 8 15 62.51 8.30 0 8 15 54.28 7.76 0 8 15 60.62 8.50 0 8 15 49.49 6.45 0 8 15 66.36 7.63 0 -8 15 48.59 6.33 0 8 -15 58.45 8.77 0 -8 15 61.97 7.28 0 8 -15 56.05 7.85 0 8 -16 2.36 2.12 0 8 -16 2.51 1.79 0 8 -16 5.05 2.56 0 -8 16 5.47 2.27 0 -8 16 3.63 1.82 0 8 16 2.96 2.22 0 8 16 4.21 2.46 0 8 16 3.87 2.10 0 -8 16 3.74 2.01 0 -8 16 4.00 2.21 0 8 -16 6.05 3.07 0 8 -16 4.47 2.61 0 8 -17 22.83 5.42 0 8 -17 29.90 5.15 0 8 -17 38.34 6.36 0 -8 17 26.07 4.24 0 -8 17 29.06 4.09 0 8 17 22.90 4.89 0 8 17 28.24 5.52 0 8 17 30.22 4.89 0 -8 17 31.50 4.79 0 -8 17 30.12 4.74 0 8 -17 31.78 6.41 0 8 -17 32.04 5.99 0 8 -18 246.66 19.09 0 8 -18 237.37 16.86 0 8 -18 275.45 18.52 0 -8 18 287.72 16.24 0 -8 18 262.72 14.98 0 8 18 245.59 17.14 0 8 18 248.21 17.41 0 8 18 263.49 17.73 0 8 18 277.05 16.78 0 -8 18 285.02 16.56 0 8 -18 241.11 18.87 0 -8 18 255.47 15.93 0 8 -18 270.69 18.67 0 8 -19 4.44 1.97 0 8 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184.30 14.34 0 9 1 215.50 14.84 0 9 -1 193.75 14.53 0 9 -1 205.31 15.28 0 -9 1 98.32 14.61 0 -9 -1 135.56 16.40 0 -9 1 180.13 18.45 0 -9 -1 200.22 20.24 0 -9 -1 191.35 13.16 0 -9 1 184.34 13.06 0 -9 1 172.51 12.12 0 -9 -1 180.16 12.06 0 9 -1 203.41 15.02 0 -9 -1 213.75 15.27 0 9 -1 213.09 14.64 0 -9 -1 251.53 18.44 0 9 -1 116.88 14.26 0 -9 1 212.65 16.33 0 9 1 160.78 16.76 0 9 1 215.36 14.73 0 9 -1 188.76 16.27 0 9 -1 196.67 13.12 0 9 -2 438.48 24.82 0 9 -2 411.09 23.02 0 9 2 400.89 23.61 0 9 -2 386.50 24.59 0 -9 2 211.49 24.21 0 -9 -2 386.46 30.49 0 -9 -2 337.14 27.57 0 -9 2 457.32 29.42 0 -9 2 428.77 23.03 0 -9 -2 397.59 22.35 0 -9 2 391.09 22.32 0 -9 2 394.30 21.70 0 9 -2 423.17 24.91 0 9 2 441.63 24.49 0 9 -2 262.01 23.73 0 -9 -2 460.75 25.79 0 9 2 385.20 28.41 0 -9 2 426.79 23.72 0 -9 -2 555.45 30.53 0 -9 2 423.75 25.54 0 9 -2 428.41 23.87 0 9 2 476.78 24.85 0 9 2 397.31 25.48 0 9 -2 394.73 26.72 0 9 2 371.90 26.01 0 9 -2 414.19 22.65 0 9 3 0.78 1.05 0 9 -3 1.39 1.77 0 9 -3 2.18 1.56 0 9 -3 0.49 1.14 0 9 3 0.80 1.21 0 9 3 0.41 1.11 0 -9 -3 1.51 3.07 0 -9 -3 3.57 2.18 0 -9 3 2.23 3.02 0 -9 3 -0.63 2.82 0 -9 3 1.07 1.02 0 -9 -3 3.94 1.88 0 -9 3 3.10 1.68 0 -9 3 0.66 1.10 0 -9 3 0.60 0.99 0 9 3 0.76 2.06 0 9 -3 1.16 1.57 0 -9 3 -0.36 1.20 0 -9 -3 0.69 2.63 0 -9 -3 -0.51 1.68 0 9 3 0.41 1.90 0 9 3 1.22 2.34 0 9 3 0.82 1.23 0 9 3 0.44 1.77 0 9 3 -0.50 1.90 0 9 -3 1.04 1.15 0 9 4 412.44 24.31 0 9 4 441.85 24.35 0 9 -4 418.51 24.08 0 9 -4 374.97 25.18 0 -9 4 490.59 28.20 0 -9 -4 415.78 25.83 0 -9 4 364.66 27.80 0 -9 -4 369.82 28.40 0 9 -4 506.31 26.31 0 -9 4 406.36 23.36 0 -9 -4 406.82 22.98 0 -9 4 395.15 22.46 0 -9 4 414.18 23.24 0 9 -4 403.53 25.38 0 9 4 417.99 24.29 0 -9 -4 512.95 28.54 0 -9 4 410.46 23.53 0 -9 4 431.62 25.43 0 9 4 432.37 30.11 0 9 4 382.43 25.82 0 9 4 440.52 24.88 0 9 -4 349.18 26.93 0 9 4 384.87 23.86 0 9 4 452.37 25.30 0 9 4 358.12 24.60 0 9 4 408.92 27.59 0 9 -4 383.41 23.28 0 -9 4 497.99 27.33 0 9 5 296.24 19.14 0 9 -5 278.30 20.80 0 9 -5 311.94 19.78 0 9 -5 307.44 21.01 0 -9 -5 314.13 24.13 0 -9 5 329.77 24.22 0 -9 5 397.07 22.82 0 -9 -5 307.63 20.99 0 9 -5 307.52 20.33 0 -9 5 304.57 19.13 0 -9 5 295.10 18.31 0 -9 5 296.82 18.69 0 9 -5 302.94 21.07 0 9 5 327.80 20.04 0 9 -5 314.89 22.10 0 -9 -5 404.75 24.98 0 9 5 360.70 21.04 0 -9 5 312.65 20.42 0 9 5 331.70 25.40 0 9 5 283.46 21.17 0 -9 5 302.34 18.87 0 9 5 323.14 20.47 0 9 5 293.10 20.48 0 9 -5 241.84 21.96 0 9 5 305.72 22.95 0 9 5 297.22 19.64 0 -9 5 419.92 23.16 0 9 -5 295.26 19.36 0 9 6 22.06 4.33 0 9 6 23.74 4.36 0 9 -6 18.53 4.56 0 9 -6 19.33 4.84 0 9 -6 21.63 4.43 0 9 -6 24.70 5.28 0 -9 -6 21.17 4.63 0 -9 6 33.34 5.50 0 -9 6 29.54 6.42 0 -9 -6 25.00 6.07 0 -9 6 19.71 4.04 0 -9 6 27.81 4.62 0 -9 6 24.62 4.21 0 -9 6 24.89 4.28 0 -9 6 20.26 4.51 0 9 6 22.09 6.18 0 9 6 19.78 5.02 0 -9 6 21.76 4.10 0 -9 -6 32.03 6.86 0 9 6 20.12 4.35 0 9 6 26.49 4.78 0 9 -6 22.02 6.15 0 9 6 25.02 6.27 0 9 6 18.78 4.53 0 9 6 28.94 5.15 0 -9 6 33.93 5.76 0 9 -6 23.05 4.56 0 9 7 400.07 23.27 0 9 -7 395.25 24.52 0 9 -7 422.98 26.32 0 -9 -7 353.27 24.04 0 -9 7 500.63 28.70 0 -9 7 483.60 24.79 0 -9 -7 423.08 28.15 0 -9 7 440.79 24.38 0 -9 7 406.14 23.11 0 -9 7 417.62 23.38 0 9 -7 390.31 25.91 0 9 7 417.27 23.94 0 9 7 418.12 29.46 0 9 7 379.05 25.95 0 -9 7 431.17 23.44 0 9 7 442.50 25.91 0 -9 -7 506.18 30.97 0 9 7 380.95 23.79 0 9 7 398.33 24.62 0 9 7 379.94 27.30 0 9 -7 299.61 26.40 0 9 7 433.01 25.05 0 9 -7 407.58 24.82 0 -9 7 483.28 25.95 0 9 -8 451.51 27.60 0 9 -8 475.90 29.13 0 -9 -8 440.45 27.10 0 -9 -8 442.78 30.01 0 -9 8 614.05 31.59 0 -9 8 521.11 27.45 0 -9 8 464.34 25.61 0 -9 8 476.97 26.29 0 9 -8 449.49 28.83 0 -9 8 532.96 28.81 0 9 8 455.00 26.13 0 -9 -8 553.39 34.20 0 -9 8 455.43 25.47 0 9 8 514.92 33.02 0 9 8 478.48 29.57 0 9 8 544.21 29.12 0 9 8 524.14 28.13 0 9 8 431.61 26.80 0 9 8 459.81 26.75 0 9 -8 319.23 28.62 0 9 8 456.18 30.38 0 9 -8 461.05 27.73 0 -9 8 554.18 28.36 0 -9 9 51.51 7.53 0 -9 -9 36.49 6.00 0 9 -9 41.81 6.73 0 -9 9 47.87 6.61 0 -9 9 47.15 5.75 0 -9 9 39.39 5.52 0 -9 9 40.96 5.01 0 -9 9 46.19 6.68 0 9 -9 38.78 6.80 0 -9 9 35.87 5.24 0 9 9 35.33 6.67 0 9 9 43.18 6.45 0 9 9 48.81 7.01 0 9 9 37.83 7.58 0 -9 9 32.08 5.67 0 9 9 42.67 7.96 0 9 9 29.10 5.41 0 9 -9 31.61 7.28 0 9 9 30.66 5.79 0 9 9 44.76 6.47 0 9 9 36.47 5.79 0 9 -9 32.17 6.25 0 9 -9 37.82 6.31 0 9 -10 208.78 16.53 0 -9 10 203.26 14.82 0 -9 10 218.41 14.78 0 -9 10 209.15 13.94 0 9 -10 163.95 15.63 0 -9 10 211.06 15.47 0 9 10 199.24 15.59 0 9 10 243.74 16.39 0 9 10 210.95 18.65 0 9 10 180.83 16.18 0 9 10 201.32 17.65 0 9 10 194.36 14.35 0 9 10 226.81 15.85 0 9 -10 202.39 17.03 0 9 -10 195.60 16.00 0 9 -11 48.35 7.41 0 -9 11 45.23 6.17 0 -9 11 43.60 5.81 0 -9 11 40.24 5.27 0 -9 11 40.37 5.95 0 9 11 38.93 6.24 0 9 11 42.07 7.28 0 9 11 48.56 8.26 0 9 11 36.61 5.85 0 9 11 39.48 7.35 0 9 11 31.90 5.26 0 9 11 48.24 6.71 0 9 -11 42.29 6.82 0 9 -11 31.41 6.20 0 9 -11 46.38 7.54 0 -9 12 189.05 13.94 0 -9 12 231.50 16.23 0 9 -12 183.51 15.95 0 -9 12 204.13 13.02 0 -9 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40.58 0 -9 16 737.17 35.98 0 -9 16 895.88 37.85 0 9 -17 7.10 2.82 0 9 -17 10.59 3.12 0 -9 17 11.45 2.33 0 -9 17 9.04 2.11 0 9 17 11.97 3.17 0 9 17 3.92 2.58 0 9 17 10.61 2.81 0 -9 17 10.87 2.66 0 9 -17 9.58 3.33 0 -9 17 10.62 2.57 0 9 -18 137.58 12.16 0 9 -18 179.11 12.47 0 -9 18 133.07 9.10 0 9 18 149.63 11.12 0 9 18 156.58 11.57 0 9 -18 144.35 12.40 0 -9 18 137.89 9.78 0 9 -18 136.47 10.84 0 -9 18 158.95 10.41 0 9 18 139.99 10.22 0 -9 18 135.32 10.26 0 9 -19 88.73 8.79 0 -9 19 95.13 7.48 0 9 -19 103.65 8.67 0 9 19 79.91 7.53 0 9 19 78.64 7.39 0 9 19 86.86 7.04 0 9 19 88.53 7.83 0 9 -19 87.06 8.64 0 -9 19 109.66 7.51 0 -9 19 87.29 6.92 0 9 -19 90.91 7.87 0 9 -20 70.07 6.76 0 9 -20 68.65 6.01 0 -9 20 64.98 5.35 0 9 20 64.33 5.86 0 9 20 44.35 5.00 0 -9 20 67.86 5.68 0 9 20 60.24 5.10 0 -9 20 75.81 5.55 0 9 20 69.45 6.17 0 9 -20 70.63 6.95 0 -9 21 75.25 4.98 0 9 21 53.21 4.48 0 9 21 68.42 5.04 0 -9 21 56.34 4.25 0 9 -21 56.83 4.93 0 -10 0 43.83 8.87 0 -10 0 13.83 6.38 0 -10 0 37.97 5.43 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118.10 10.55 0 10 -6 109.61 10.64 0 10 6 101.56 13.47 0 10 -6 93.34 12.24 0 10 6 103.63 12.67 0 10 6 125.43 11.36 0 10 -6 101.14 10.03 0 -10 6 119.48 10.61 0 10 -7 96.67 9.88 0 10 -7 97.21 10.85 0 -10 7 101.32 9.50 0 -10 7 96.77 8.83 0 -10 7 106.16 10.83 0 10 -7 102.21 11.30 0 10 7 87.93 9.17 0 10 7 98.54 10.47 0 10 7 99.28 11.27 0 10 7 93.24 12.59 0 10 -7 88.95 11.76 0 10 7 109.32 10.45 0 10 7 92.59 9.83 0 10 7 83.51 11.23 0 10 -7 103.49 10.10 0 -10 7 104.32 9.60 0 10 -8 129.08 13.12 0 10 -8 127.17 12.08 0 -10 8 164.67 12.52 0 -10 8 158.58 11.67 0 -10 8 149.39 10.76 0 -10 8 155.84 13.17 0 10 -8 142.15 13.67 0 10 8 155.21 15.92 0 10 8 139.74 13.80 0 10 8 167.65 13.39 0 10 8 167.98 13.75 0 10 8 127.76 14.25 0 10 8 170.82 13.33 0 10 8 149.54 12.42 0 10 -8 130.62 14.41 0 -10 8 149.73 11.81 0 10 -8 151.66 12.83 0 10 -9 545.05 32.80 0 10 -9 523.76 31.06 0 -10 9 590.67 30.50 0 -10 9 542.04 28.74 0 -10 9 568.87 27.87 0 -10 9 574.76 29.75 0 10 -9 503.34 32.02 0 -10 9 660.34 32.07 0 10 9 478.45 31.57 0 10 9 639.74 31.70 0 10 9 620.14 32.25 0 10 9 563.50 35.21 0 10 -9 475.95 32.68 0 10 9 527.55 29.76 0 10 9 593.51 31.15 0 10 9 554.63 34.09 0 10 -9 555.67 31.52 0 -10 9 572.68 29.57 0 -10 10 59.56 6.78 0 10 -10 53.37 7.51 0 -10 10 58.09 6.30 0 -10 10 57.23 6.59 0 -10 10 60.82 7.27 0 10 -10 50.46 7.68 0 10 10 61.34 7.74 0 10 10 53.72 6.88 0 10 10 58.66 9.23 0 10 10 50.84 7.79 0 10 10 49.27 6.38 0 10 10 52.50 6.98 0 10 10 57.35 8.54 0 10 -10 60.23 7.85 0 10 -10 52.45 7.98 0 -10 11 509.48 26.80 0 -10 11 554.95 30.01 0 10 -11 512.96 29.82 0 -10 11 530.57 26.30 0 -10 11 545.40 28.06 0 -10 11 562.52 27.77 0 10 -11 408.66 28.07 0 10 11 455.93 29.11 0 10 11 568.50 28.10 0 10 11 516.53 28.73 0 10 11 526.44 32.03 0 10 11 518.03 28.33 0 10 11 476.78 30.37 0 10 -11 486.55 29.17 0 10 -11 436.19 29.42 0 -10 12 123.14 10.61 0 -10 12 94.08 8.25 0 10 -12 91.67 10.00 0 -10 12 93.18 7.63 0 10 12 78.96 9.39 0 10 12 91.76 9.23 0 10 12 100.21 11.18 0 10 -12 95.63 10.10 0 10 -12 91.42 10.55 0 10 12 57.50 8.78 0 10 12 101.22 9.39 0 -10 12 91.50 8.16 0 -10 12 95.47 8.74 0 -10 13 45.75 5.50 0 -10 13 38.04 4.84 0 -10 13 32.40 4.59 0 -10 13 39.30 5.67 0 10 -13 37.70 6.34 0 10 13 31.69 5.65 0 10 13 35.60 5.31 0 10 13 43.65 7.11 0 10 13 41.95 5.68 0 10 13 41.88 6.72 0 10 -13 36.68 6.15 0 10 -13 26.57 5.50 0 -10 14 8.45 2.16 0 -10 14 7.28 2.19 0 -10 14 7.91 2.62 0 -10 14 4.94 1.81 0 10 14 5.16 2.59 0 10 14 5.45 2.14 0 10 14 6.54 3.02 0 10 14 6.90 2.45 0 10 -14 5.92 2.63 0 10 -14 6.30 2.74 0 -10 15 252.31 13.75 0 -10 15 241.62 14.30 0 -10 15 274.07 15.48 0 -10 15 239.86 13.99 0 10 15 246.72 15.06 0 10 15 205.78 15.55 0 10 15 228.77 15.64 0 10 -15 222.48 16.54 0 10 -15 189.49 15.19 0 10 16 12.83 3.33 0 10 16 16.54 3.47 0 10 -16 12.74 2.94 0 -10 16 19.31 3.29 0 -10 16 15.68 2.72 0 10 -16 22.92 4.40 0 10 17 167.54 11.54 0 10 17 174.00 12.09 0 -10 17 139.26 10.51 0 10 -17 207.73 12.90 0 10 -17 158.56 12.53 0 -10 17 172.00 10.39 0 -10 17 213.50 11.60 0 -10 18 33.24 4.01 0 10 18 44.61 4.39 0 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2.49 1.31 1 2 -15 2.55 2.19 1 2 -15 3.83 3.74 1 2 -14 641.64 44.40 -1 -2 14 729.87 34.02 -1 2 14 757.87 33.24 1 -2 -14 713.49 34.58 1 -2 -14 825.74 38.34 -1 2 14 764.68 33.66 1 2 -14 760.80 42.88 1 2 -14 732.72 45.53 1 -2 -14 676.06 34.58 1 2 -14 665.38 37.37 -1 -2 13 75.68 6.45 1 2 -13 65.41 11.58 1 2 -13 64.36 9.80 1 -2 -13 61.07 6.34 -1 2 13 70.56 6.20 1 2 -13 62.35 10.77 1 2 -13 70.90 8.24 1 -2 -13 73.42 6.71 -1 2 13 69.94 5.94 1 -2 -13 73.05 7.87 1 -2 -13 73.82 6.66 1 2 -12 996.55 62.83 -1 -2 12 1352.02 54.92 -1 -2 12 1179.68 52.52 1 2 -12 1121.48 57.46 1 -2 -12 1344.38 55.07 1 -2 -12 1182.79 54.90 -1 2 12 1324.43 54.68 1 2 -12 1226.35 62.06 1 2 -12 1031.09 62.83 -1 2 12 1391.61 54.43 1 -2 -12 1350.41 57.84 1 -2 -12 1237.37 54.93 -1 -2 11 208.18 12.24 -1 2 11 261.80 13.40 -1 -2 11 219.47 11.22 1 -2 -11 236.82 12.62 1 -2 -11 208.43 12.45 1 2 -11 228.54 17.55 1 2 -11 202.88 14.46 -1 2 11 244.44 12.39 1 -2 -11 206.77 12.46 -1 2 11 214.71 12.49 1 -2 -11 233.45 14.28 -1 -2 10 149.21 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12.88 2.25 7 12 -7 16.92 3.05 -7 12 7 15.69 2.71 7 12 -7 13.65 2.98 7 12 -7 10.67 2.73 -7 -12 6 97.80 7.11 -7 -12 6 98.74 6.71 7 12 -6 93.99 8.39 -7 -12 6 98.90 6.94 -7 12 6 96.47 7.47 -7 12 6 75.83 7.24 -7 12 6 75.16 6.61 7 12 -6 87.00 8.23 7 12 -6 79.85 7.70 -7 -12 5 185.09 10.55 7 12 -5 165.94 12.31 -7 -12 5 185.80 11.24 -7 -12 5 167.65 10.51 -7 12 5 158.39 11.53 7 12 -5 168.33 11.54 -7 12 5 182.22 11.50 -7 12 5 162.08 10.97 7 12 -5 137.41 11.14 7 12 -4 1.67 1.50 7 12 -4 1.45 1.36 -7 -12 4 3.08 1.26 -7 -12 4 3.23 1.45 -7 -12 4 2.76 1.63 -7 12 4 2.43 1.60 7 12 -4 4.31 1.77 -7 12 4 2.71 1.42 -7 12 4 2.10 1.47 -7 -12 4 2.64 1.49 7 12 -3 211.84 13.56 -7 -12 3 207.28 11.99 7 -12 -3 186.96 11.93 -7 -12 3 219.92 12.58 -7 -12 3 210.90 13.33 -7 12 3 203.86 13.80 7 12 -3 208.92 14.22 -7 12 3 193.18 13.31 -7 -12 3 200.30 12.50 7 -12 -2 9.35 2.16 -7 -12 2 9.64 2.10 7 -12 -2 10.09 2.19 -7 -12 2 9.54 1.99 -7 -12 2 13.25 2.69 -7 -12 2 7.71 2.53 7 12 -2 9.95 2.83 -7 12 2 8.36 2.49 7 12 -2 6.74 2.36 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2.20 1.60 -8 6 -10 3.36 2.16 8 6 10 2.48 2.03 8 6 11 138.13 12.26 -8 -6 -11 87.57 9.48 -8 -6 -11 92.41 9.49 8 -6 11 131.89 11.39 -8 -6 -11 85.42 9.78 8 -6 11 119.89 9.50 8 -6 11 104.82 9.77 8 6 11 130.92 9.63 8 6 11 115.62 9.81 -8 -6 -11 91.01 11.32 8 -6 11 110.29 10.67 -8 6 -11 118.34 13.86 8 -6 11 121.50 10.59 8 -6 11 123.92 9.85 -8 -6 -11 98.31 10.90 -8 -6 -11 108.43 12.31 -8 -6 -11 95.55 10.80 8 6 11 122.84 12.81 8 -6 11 109.54 10.60 -8 6 -11 124.66 10.21 8 6 11 131.02 13.81 8 6 11 98.84 9.52 8 6 11 124.66 10.51 8 6 11 108.08 11.08 -8 6 -11 114.84 11.57 8 -6 11 131.32 11.97 -8 6 -11 106.98 9.41 8 6 12 25.45 5.24 -8 -6 -12 18.33 4.17 -8 -6 -12 16.71 3.84 8 -6 12 29.46 5.08 -8 -6 -12 24.60 4.94 8 -6 12 26.50 3.98 8 -6 12 25.93 4.44 8 6 12 23.10 3.90 -8 -6 -12 23.65 5.10 -8 6 -12 29.87 7.02 8 -6 12 24.76 4.20 -8 -6 -12 24.77 5.62 -8 -6 -12 12.39 4.42 -8 -6 -12 18.77 4.43 8 -6 12 21.99 4.58 8 6 12 30.35 6.19 -8 6 -12 22.60 4.28 8 -6 12 24.23 4.70 8 6 12 24.57 6.17 8 6 12 20.07 4.82 8 6 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3.74 -8 -7 6 18.98 5.86 -8 -7 6 15.86 5.41 -8 7 6 16.47 4.15 -8 7 6 18.04 4.68 -8 7 6 18.09 4.27 -8 7 6 20.22 4.29 -8 7 6 18.58 5.69 -8 7 6 16.01 4.59 -8 7 6 18.23 4.30 -8 7 6 19.38 5.23 -8 7 6 18.49 4.67 8 7 -6 16.48 4.66 8 -7 -6 18.59 4.22 -8 -7 6 22.10 5.72 8 7 -6 16.90 4.07 -8 -7 6 26.15 6.09 -8 7 5 319.63 19.26 -8 7 5 332.93 20.58 8 7 -5 268.58 20.21 -8 7 5 320.83 22.83 8 7 -5 311.59 21.45 -8 7 5 222.68 18.00 -8 7 5 290.86 22.07 8 -7 -5 306.60 19.10 -8 -7 5 288.86 20.68 8 -7 -5 335.27 21.33 -8 -7 5 283.37 17.37 -8 -7 5 300.66 18.10 -8 -7 5 314.49 17.10 8 7 -5 345.02 21.24 -8 -7 5 303.82 18.58 -8 -7 5 293.70 17.99 -8 -7 5 317.56 25.71 8 7 -5 277.28 20.72 -8 7 5 325.11 24.90 -8 7 5 300.88 19.60 -8 7 5 287.67 21.23 -8 7 5 316.88 20.01 -8 7 5 334.95 20.85 -8 7 5 346.76 23.70 8 -7 -5 341.97 20.83 -8 7 5 312.91 20.83 -8 7 5 280.39 20.96 8 7 -5 266.51 21.43 8 7 -5 293.87 19.52 -8 -7 5 354.23 24.66 8 7 -4 355.00 24.53 -8 7 4 433.01 23.68 8 7 -4 404.36 25.25 -8 7 4 437.59 24.89 -8 7 4 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2.48 8 7 0 6.89 2.39 -8 -7 0 10.06 2.77 -8 -7 0 6.80 2.27 -8 -7 0 10.23 2.86 -8 -7 0 3.10 3.64 -8 -7 0 7.49 4.13 -8 7 0 7.64 3.35 -8 7 0 9.48 2.87 -8 7 0 5.82 2.28 -8 7 0 4.64 2.85 8 7 0 5.49 3.08 8 7 0 10.25 2.92 -8 7 0 7.15 2.50 8 7 0 3.05 2.36 8 7 0 8.11 2.79 -8 7 -1 140.09 11.14 8 7 1 140.82 12.24 8 7 1 136.05 11.28 8 7 1 144.92 14.26 -8 7 -1 87.60 12.01 -8 -7 -1 120.12 12.78 8 -7 1 175.02 13.99 -8 -7 -1 121.65 14.76 -8 -7 -1 166.37 12.62 8 -7 1 154.66 12.16 -8 -7 -1 148.62 11.27 8 7 1 154.10 11.86 -8 -7 -1 133.13 11.09 -8 -7 -1 142.13 11.35 -8 -7 -1 172.29 16.88 8 7 1 151.57 12.39 -8 7 -1 160.16 15.80 -8 7 -1 131.81 11.08 -8 7 -1 154.23 14.77 -8 7 -1 142.59 12.23 -8 -7 -1 163.95 15.47 -8 7 -1 151.93 11.68 8 7 2 29.84 6.32 -8 7 -2 20.75 4.28 8 7 2 26.77 4.85 -8 7 -2 23.72 4.21 -8 7 -2 21.57 4.70 -8 7 -2 17.75 5.04 8 -7 2 22.94 4.41 8 -7 2 27.98 5.57 -8 -7 -2 28.17 5.84 -8 -7 -2 23.54 6.50 -8 -7 -2 30.64 5.29 8 -7 2 28.80 4.98 -8 -7 -2 29.99 4.81 -8 -7 -2 23.22 4.34 -8 -7 -2 29.71 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8 7 2.96 1.98 -8 8 7 1.37 2.62 -8 8 7 0.94 1.42 -8 8 7 -0.49 1.76 -8 8 7 4.45 2.92 8 8 -7 -0.48 1.96 -8 8 6 382.78 25.89 8 8 -6 339.50 23.70 8 8 -6 363.33 24.62 8 -8 -6 371.17 22.13 -8 -8 6 409.29 24.29 8 -8 -6 357.37 23.23 -8 -8 6 364.17 20.90 -8 -8 6 370.24 20.39 8 8 -6 394.62 24.12 -8 -8 6 361.63 21.38 -8 -8 6 374.84 21.05 8 8 -6 328.09 23.95 -8 -8 6 498.95 29.93 -8 -8 6 365.09 26.05 -8 8 6 348.21 24.34 -8 8 6 337.77 26.16 -8 8 6 361.47 22.60 -8 8 6 389.03 23.19 -8 8 6 460.56 26.70 8 -8 -6 403.56 24.00 -8 8 6 354.08 23.23 -8 8 6 236.14 21.94 8 8 -6 306.54 24.58 8 8 -6 336.55 22.32 -8 8 5 143.39 11.69 -8 8 5 138.66 14.35 8 8 -5 114.14 12.33 -8 8 5 134.93 12.10 8 8 -5 147.17 13.70 8 -8 -5 161.97 12.43 -8 -8 5 135.48 13.20 -8 -8 5 156.89 16.45 8 -8 -5 143.52 13.15 -8 -8 5 147.05 11.25 -8 -8 5 155.38 11.01 8 8 -5 149.10 13.11 -8 -8 5 124.32 9.65 -8 -8 5 137.14 11.38 -8 -8 5 131.80 10.74 8 8 -5 130.85 13.24 -8 -8 5 137.74 14.90 -8 -8 5 178.49 17.80 -8 8 5 133.44 13.51 -8 8 5 117.17 14.68 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471.41 26.52 -8 10 -3 427.79 25.43 -8 -10 -4 271.04 17.62 8 -10 4 178.79 13.74 -8 -10 -4 242.65 16.05 -8 -10 -4 210.49 14.87 8 -10 4 189.98 13.18 8 -10 4 189.56 14.13 -8 -10 -4 214.02 15.14 -8 -10 -4 215.67 14.30 8 10 4 219.16 14.70 -8 -10 -4 103.42 14.23 -8 10 -4 214.16 15.09 -8 10 -4 172.14 13.70 -8 10 -4 219.41 18.60 8 10 4 205.91 14.82 8 10 4 197.51 14.71 -8 10 -4 196.15 14.64 8 10 4 168.33 17.02 -8 10 -4 179.19 16.52 -8 10 -4 222.44 14.17 8 10 5 1.95 1.97 -8 10 -5 6.33 2.23 8 10 5 3.45 2.27 8 10 5 2.40 1.74 8 -10 5 2.92 1.72 -8 -10 -5 6.54 2.81 -8 -10 -5 3.10 2.17 8 -10 5 2.25 1.61 -8 -10 -5 8.15 2.79 -8 -10 -5 2.25 1.83 -8 -10 -5 3.13 2.94 -8 10 -5 3.96 2.22 -8 10 -5 1.86 1.67 -8 10 -5 2.69 2.74 8 10 5 5.19 2.65 8 -10 5 0.64 1.43 -8 10 -6 229.41 14.59 8 10 6 194.89 17.71 8 10 6 227.21 15.23 8 -10 6 230.47 15.31 -8 -10 -6 284.32 19.03 8 -10 6 243.79 15.78 -8 -10 -6 299.85 18.55 -8 -10 -6 242.11 16.88 8 -10 6 228.32 15.34 -8 -10 -6 258.16 17.24 -8 -10 -6 279.98 17.02 -8 -10 -6 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10 -4 -5 27.23 4.41 -10 4 5 17.05 4.08 10 4 -5 17.38 4.01 10 4 -5 20.33 3.68 -10 -4 5 14.77 4.27 -10 -4 5 17.93 3.25 10 4 -5 16.22 3.86 10 4 -5 39.06 5.40 10 4 -5 42.13 5.99 -10 -4 5 22.06 3.98 -10 -4 5 18.86 3.42 -10 -4 5 20.62 3.40 10 4 -5 23.43 4.47 -10 -4 5 9.26 4.49 -10 4 5 20.24 4.20 -10 4 5 33.30 6.55 -10 4 5 15.15 4.01 -10 4 5 24.09 4.42 10 -4 -5 18.71 4.05 -10 4 5 14.60 3.69 10 4 -5 18.70 4.13 -10 -4 5 18.84 5.69 10 4 -4 2.57 1.64 10 4 -4 1.33 1.60 -10 4 4 2.68 1.70 10 4 -4 3.91 1.61 -10 4 4 3.02 1.94 10 4 -4 7.14 2.61 10 -4 -4 4.43 1.87 -10 -4 4 1.05 2.47 10 4 -4 5.56 2.28 -10 -4 4 2.96 1.46 10 4 -4 2.40 1.88 10 4 -4 3.48 1.70 -10 -4 4 2.78 1.46 10 4 -4 5.06 2.11 -10 -4 4 3.53 1.84 -10 -4 4 2.91 1.63 -10 -4 4 -0.72 2.59 -10 4 4 1.43 1.38 -10 4 4 -0.47 1.80 10 -4 -4 3.00 1.83 -10 -4 4 3.79 3.09 -10 4 3 64.09 6.94 10 4 -3 67.07 7.86 -10 4 3 60.38 7.64 10 -4 -3 78.49 7.40 10 4 -3 54.80 5.76 -10 -4 3 45.61 7.70 10 4 -3 73.94 7.96 -10 -4 3 62.40 6.35 10 4 -3 71.18 7.44 10 -4 -3 77.45 7.86 -10 -4 3 60.61 6.47 -10 -4 3 65.49 6.86 -10 -4 3 67.52 6.14 10 4 -3 81.20 8.24 -10 -4 3 65.63 5.68 -10 -4 3 67.05 6.38 -10 4 2 677.46 36.62 10 4 -2 707.34 38.42 10 -4 -2 831.76 37.71 -10 -4 2 695.65 40.01 10 4 -2 816.31 38.91 -10 -4 2 729.77 36.36 10 4 -2 818.20 38.01 10 4 -2 793.66 38.79 -10 -4 2 763.62 35.72 -10 -4 2 803.56 37.35 -10 -4 2 815.27 37.61 -10 -4 2 742.30 34.93 -10 -4 2 761.63 36.23 -10 4 1 5.20 1.99 10 4 -1 2.40 1.72 10 -4 -1 4.07 1.90 -10 -4 1 1.95 2.64 10 4 -1 9.10 2.75 10 -4 -1 3.01 1.64 10 4 -1 2.26 1.52 -10 -4 1 1.97 1.16 -10 -4 1 3.02 1.57 -10 -4 1 3.46 1.76 -10 -4 1 3.53 1.57 -10 4 0 1790.18 83.94 10 4 0 1759.88 85.83 -10 4 0 1688.21 86.42 10 -4 0 2076.67 85.50 -10 -4 0 2222.62 89.32 -10 -4 0 1943.36 84.67 10 -4 0 1934.21 84.40 10 4 0 2103.28 85.53 -10 -4 0 1902.10 82.15 10 -4 0 1957.96 86.06 -10 -4 0 2005.46 84.01 -10 -4 0 1981.93 85.37 -10 -4 0 2118.96 85.55 -10 -4 0 1958.25 83.19 -10 4 -1 52.06 5.87 -10 4 -1 51.59 7.16 -10 -4 -1 66.53 7.83 -10 -4 -1 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565.96 29.95 -10 -4 -6 546.87 28.75 10 4 6 530.52 31.92 -10 4 -6 603.35 29.92 -10 4 -6 547.84 37.31 10 4 6 558.95 32.27 10 4 6 578.32 31.33 10 -4 6 633.95 30.53 -10 4 -6 541.55 30.17 -10 4 -6 567.55 30.14 -10 -4 -6 551.16 29.06 -10 4 -6 584.28 29.33 10 4 6 530.17 29.21 10 4 7 3.91 1.69 -10 -4 -7 4.01 2.04 -10 4 -7 3.34 1.76 -10 -4 -7 4.88 2.28 -10 -4 -7 3.85 2.03 -10 -4 -7 2.57 1.93 -10 -4 -7 4.62 2.21 -10 -4 -7 4.90 2.22 10 -4 7 4.51 1.83 -10 -4 -7 5.31 2.40 10 -4 7 7.07 2.45 -10 -4 -7 3.03 1.60 -10 -4 -7 10.59 2.68 -10 4 -7 5.33 2.46 10 4 7 4.92 1.95 10 -4 7 8.41 2.61 -10 -4 -7 6.44 2.04 10 -4 7 1.78 1.71 -10 -4 -7 5.95 2.28 10 -4 7 5.07 1.95 10 4 7 5.12 2.78 -10 4 -7 3.71 1.84 10 4 7 5.27 2.34 10 4 7 2.09 1.88 -10 4 -7 5.03 2.23 10 4 7 3.21 1.69 -10 4 -7 5.55 2.30 -10 -4 -7 5.58 2.02 -10 4 -7 5.10 1.99 -10 -4 -8 24.07 4.44 10 4 8 29.02 5.58 -10 -4 -8 17.22 3.91 -10 -4 -8 29.97 5.16 -10 -4 -8 22.24 4.58 10 4 8 25.06 4.18 -10 -4 -8 21.00 4.54 -10 -4 -8 21.73 4.55 -10 -4 -8 22.70 4.55 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4 15 63.90 7.17 10 -4 15 59.77 6.78 10 4 16 131.23 10.60 -10 4 -16 108.76 11.23 -10 -4 -16 163.58 21.99 -10 -4 -16 109.96 13.97 -10 -4 -16 106.56 13.52 10 4 16 109.22 9.64 10 -4 16 115.33 11.13 10 -4 16 114.17 10.07 -10 4 -16 107.89 10.82 10 -4 16 99.91 11.23 10 -4 16 118.75 11.17 10 4 16 144.34 13.17 10 4 16 110.42 9.14 10 4 16 94.03 10.53 -10 4 -16 97.24 10.93 -10 4 -16 122.84 9.88 -10 -4 -16 93.45 9.79 -10 4 -16 109.34 10.77 10 4 16 100.07 8.95 10 -4 16 104.51 8.76 -10 4 -17 0.50 1.66 -10 -4 -17 1.47 5.64 -10 -4 -17 2.42 2.68 -10 -4 -17 2.83 3.61 10 4 17 3.03 1.65 -10 -4 -17 5.29 3.40 10 -4 17 4.91 2.49 10 4 17 5.05 2.74 10 -4 17 3.06 1.85 -10 4 -17 2.27 2.04 10 -4 17 3.40 2.23 10 4 17 2.90 1.38 10 4 17 5.10 2.93 10 4 17 2.33 1.90 -10 -4 -17 0.88 2.06 10 -4 17 2.10 1.88 -10 4 -17 1.05 1.89 -10 4 -17 0.32 1.81 -10 4 -17 1.35 1.62 -10 4 -18 363.27 24.19 -10 -4 -18 439.33 39.65 -10 -4 -18 345.46 29.77 -10 -4 -18 377.52 28.62 10 4 18 398.58 21.94 10 4 18 480.14 25.70 10 -4 18 403.96 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21 16.29 3.52 -10 4 -21 11.27 3.39 -10 -4 -21 11.01 3.53 -10 4 -21 9.67 2.99 -10 -4 -22 41.90 7.05 -10 4 -22 64.80 6.96 -10 4 -22 67.58 7.11 10 4 22 58.18 6.39 10 4 22 71.62 6.05 10 -4 22 70.36 6.16 -10 4 -22 78.91 7.42 10 -4 22 56.44 6.12 10 -4 22 59.72 5.19 10 4 22 56.70 5.77 -10 -4 -22 64.31 10.09 10 -4 23 4.90 1.56 -10 -4 -23 4.39 2.23 -10 4 -23 6.22 2.08 10 4 23 4.06 1.59 10 4 23 3.97 1.29 -10 -4 -23 5.45 3.69 10 -4 24 232.20 12.72 -10 -4 -24 431.63 24.63 -10 5 23 7.78 1.46 -10 -5 23 7.43 1.43 10 5 -23 10.54 1.83 10 5 -23 9.63 1.96 -10 -5 22 293.08 14.75 -10 5 22 261.16 14.58 10 5 -22 265.07 15.17 -10 5 22 274.56 14.58 -10 5 22 289.05 14.79 -10 -5 21 104.65 7.56 -10 5 21 110.85 8.00 -10 5 21 106.50 7.83 -10 5 21 96.69 7.62 10 5 -21 98.46 8.45 10 5 -20 1.75 1.71 -10 -5 20 0.53 0.84 -10 -5 20 1.05 0.95 -10 -5 20 2.10 1.41 -10 5 20 0.53 0.95 -10 5 20 1.58 1.38 -10 5 20 1.33 1.25 10 5 -20 0.73 0.98 10 5 -19 253.60 17.02 10 5 -19 196.24 13.67 10 5 -19 209.38 13.41 -10 -5 19 188.10 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102.62 11.88 -10 5 0 99.34 8.66 10 5 0 92.52 9.68 10 5 0 81.28 8.94 10 5 1 22.46 5.32 10 5 1 29.63 5.16 -10 5 -1 35.16 5.40 -10 5 -1 28.19 4.28 -10 5 -1 33.41 6.14 -10 -5 -1 16.88 4.07 -10 -5 -1 33.41 6.48 10 -5 1 31.66 4.95 -10 -5 -1 39.97 5.43 -10 -5 -1 25.56 3.73 -10 -5 -1 40.74 5.67 -10 -5 -1 34.87 4.79 10 5 1 33.28 5.37 10 -5 1 33.82 5.19 -10 -5 -1 28.64 4.16 -10 -5 -1 53.65 9.10 -10 5 -1 27.37 4.76 10 5 1 35.73 5.51 -10 -5 -1 42.76 7.48 -10 5 -1 28.95 6.69 -10 5 -1 28.47 4.42 10 -5 1 40.17 5.75 -10 5 -1 32.56 6.30 -10 5 -1 29.63 4.56 10 5 1 32.18 5.77 -10 5 -2 1002.71 49.47 10 5 2 982.60 52.24 10 5 2 1017.66 49.99 -10 -5 -2 1315.65 53.38 -10 5 -2 849.32 51.01 10 -5 2 1053.46 49.41 -10 -5 -2 863.13 48.16 -10 -5 -2 1186.99 53.37 -10 -5 -2 1099.89 49.65 10 -5 2 1063.43 49.40 -10 -5 -2 1052.12 49.69 -10 -5 -2 1217.84 51.50 -10 -5 -2 1038.00 48.64 10 -5 2 1058.70 49.75 -10 -5 -2 1054.62 47.95 -10 -5 -2 1029.07 48.95 -10 -5 -2 1423.43 59.67 10 5 2 986.61 49.32 -10 5 -2 1076.69 49.48 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1303.62 61.08 -10 6 11 1158.91 59.62 10 6 -11 1133.58 58.72 10 6 -11 1281.49 62.28 10 6 -11 1257.27 63.68 -10 6 11 1149.39 57.98 -10 6 10 24.65 5.03 10 6 -10 28.54 5.39 10 6 -10 20.89 5.16 10 6 -10 28.77 6.29 -10 6 10 23.30 4.75 10 6 -10 23.96 5.26 -10 -6 10 29.16 4.12 10 6 -10 28.76 5.54 -10 -6 10 21.38 4.44 -10 -6 10 34.60 6.12 10 6 -10 38.92 6.95 -10 6 10 28.69 5.70 -10 6 10 16.00 4.66 -10 6 10 28.89 5.37 -10 6 10 33.15 5.99 -10 6 10 26.56 5.62 -10 6 10 32.14 5.84 10 -6 -10 32.90 5.72 -10 6 10 22.12 4.74 -10 -6 10 36.13 5.74 -10 -6 10 32.40 6.06 10 6 -10 30.74 6.36 10 6 -9 957.41 51.58 10 6 -9 984.25 52.21 -10 6 9 887.47 49.86 -10 6 9 825.22 50.18 10 6 -9 874.73 50.85 -10 -6 9 1016.42 47.68 -10 -6 9 1107.44 50.54 -10 -6 9 968.29 47.92 -10 -6 9 1221.76 53.77 10 6 -9 997.21 53.42 -10 -6 9 1368.89 58.96 -10 6 9 1013.75 52.38 -10 6 9 1098.68 51.81 -10 6 9 1081.80 51.22 -10 6 9 1216.57 53.50 -10 6 9 1209.15 54.06 -10 6 9 980.79 50.15 -10 6 9 985.00 51.48 10 -6 -9 1130.91 52.27 -10 -6 9 1262.62 52.93 -10 -6 9 1267.89 55.19 10 6 -8 84.17 9.87 10 6 -8 87.68 10.32 10 6 -8 94.84 11.55 -10 6 8 81.70 9.35 -10 6 8 82.21 10.21 10 -6 -8 98.49 9.51 -10 -6 8 91.36 8.25 -10 -6 8 104.17 9.61 -10 -6 8 88.65 8.44 -10 -6 8 89.50 7.86 -10 6 8 95.79 9.56 -10 -6 8 116.92 11.80 10 6 -8 88.05 10.89 -10 -6 8 124.95 14.15 -10 6 8 114.80 10.54 -10 6 8 121.28 11.45 -10 6 8 124.43 11.95 -10 6 8 87.23 9.98 10 6 -8 86.93 10.68 -10 6 8 100.56 10.01 -10 6 8 96.00 10.10 10 -6 -8 108.74 10.76 -10 -6 8 108.10 10.87 -10 -6 8 121.25 12.62 -10 6 7 13.73 3.52 10 6 -7 10.64 3.48 10 6 -7 8.69 3.44 10 6 -7 5.35 2.93 -10 6 7 11.25 3.28 -10 6 7 7.13 3.17 10 -6 -7 12.15 3.19 -10 -6 7 10.73 4.29 -10 -6 7 7.90 2.36 -10 -6 7 12.24 3.30 -10 -6 7 7.64 2.49 -10 -6 7 12.26 2.80 -10 -6 7 10.80 5.02 -10 -6 7 13.33 4.59 -10 6 7 12.38 3.60 -10 6 7 9.95 3.57 -10 6 7 10.93 3.26 10 -6 -7 9.79 3.18 -10 6 7 6.30 2.61 -10 6 7 12.09 3.61 10 6 -7 4.77 2.71 -10 -6 7 6.37 3.24 -10 -6 7 10.86 4.43 10 6 -6 8.50 3.28 10 6 -6 11.71 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6 4 5.61 2.44 10 6 -4 6.74 2.90 10 6 -4 3.07 2.09 -10 6 4 3.61 1.97 -10 6 4 2.34 2.25 10 -6 -4 5.67 2.24 -10 -6 4 5.11 3.43 -10 -6 4 5.25 2.04 -10 -6 4 5.60 1.89 10 6 -4 7.25 3.01 -10 -6 4 7.90 2.60 -10 -6 4 3.34 1.76 -10 -6 4 6.80 2.38 -10 -6 4 9.83 5.42 -10 -6 4 1.25 2.68 -10 6 4 7.35 3.05 -10 6 4 6.32 3.11 -10 6 4 5.05 2.49 -10 6 4 3.96 2.31 -10 6 4 6.77 2.54 10 -6 -4 8.94 2.97 -10 6 4 5.83 2.87 10 6 -4 1.23 1.88 -10 -6 4 10.71 5.18 -10 6 3 683.15 33.89 10 6 -3 698.90 36.92 10 6 -3 549.57 34.08 10 6 -3 591.41 34.40 -10 6 3 488.03 31.52 -10 6 3 525.30 35.15 10 -6 -3 677.47 33.52 -10 -6 3 521.08 37.37 -10 -6 3 636.84 32.32 -10 -6 3 704.56 33.51 10 6 -3 708.07 35.80 -10 -6 3 662.41 31.33 -10 -6 3 731.17 34.04 -10 -6 3 635.80 31.82 -10 -6 3 469.06 38.31 -10 6 3 741.90 35.16 -10 6 3 859.47 38.64 -10 6 3 687.81 37.33 -10 6 3 687.72 33.79 -10 6 3 575.38 33.02 10 -6 -3 635.42 34.15 -10 6 3 628.19 35.28 10 6 -3 547.50 35.80 -10 -6 3 549.61 38.12 10 6 -2 28.68 5.54 -10 6 2 30.43 5.22 10 6 -2 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9 5 163.42 14.27 -10 9 5 178.35 13.34 -10 9 5 184.72 14.21 -10 9 5 146.09 13.08 10 9 -5 142.91 13.65 10 9 -5 149.71 13.85 -10 9 5 159.38 14.55 -10 -9 4 388.07 22.23 -10 -9 4 389.51 20.89 -10 -9 4 393.61 22.89 -10 -9 4 393.90 21.87 -10 -9 4 400.34 22.22 -10 9 4 390.27 25.67 -10 9 4 414.39 23.72 -10 9 4 448.49 24.61 -10 9 4 478.44 25.99 -10 9 4 371.27 24.44 10 9 -4 341.57 24.50 -10 9 4 404.96 26.70 10 9 -4 374.85 24.72 -10 9 3 3.64 2.73 -10 -9 3 2.71 1.78 -10 -9 3 3.99 1.82 -10 -9 3 4.98 1.75 -10 -9 3 2.15 1.76 10 -9 -3 4.12 1.97 -10 -9 3 4.27 3.73 -10 9 3 4.12 2.50 -10 9 3 4.48 2.63 -10 9 3 6.63 2.59 -10 9 3 3.71 2.52 -10 9 3 0.50 2.26 -10 9 3 4.50 1.99 10 9 -3 4.19 2.46 10 9 -3 2.37 1.82 -10 -9 2 178.88 12.98 -10 -9 2 170.36 11.73 -10 -9 2 179.50 13.19 10 -9 -2 142.31 12.29 -10 -9 2 183.22 12.61 10 9 -2 163.07 14.42 -10 -9 2 169.58 17.54 -10 9 2 173.26 15.46 -10 9 2 185.43 13.62 -10 9 2 194.80 14.31 -10 9 2 219.50 15.67 10 9 -2 146.46 14.94 -10 9 2 169.76 12.75 10 9 -2 148.94 13.98 -10 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356.17 20.15 -10 -10 -9 197.33 20.98 10 -10 9 397.11 21.16 10 -10 9 367.07 21.04 10 10 9 372.86 21.68 -10 10 -9 380.20 20.84 -10 10 -9 377.12 22.05 -10 -10 -10 38.19 5.60 -10 -10 -10 38.51 5.71 10 -10 10 24.42 3.58 -10 -10 -10 13.91 4.45 10 -10 10 23.80 3.60 10 10 10 32.31 4.27 -10 10 -10 26.07 4.00 -10 10 -10 26.88 4.32 10 -10 10 28.22 4.14 10 10 10 29.51 4.43 -10 10 -10 27.68 3.98 -10 10 -10 30.43 4.64 -10 -10 -11 336.77 18.44 -10 -10 -11 303.74 18.32 -10 10 -11 211.22 13.10 -10 10 -11 211.59 13.81 10 -10 11 204.57 12.48 -10 -10 -11 123.75 13.84 10 -10 11 225.82 12.88 10 -10 11 225.17 13.37 10 10 11 252.88 14.39 -10 10 -11 209.81 12.95 10 10 11 191.49 14.60 -10 10 -11 212.82 14.08 -10 10 -12 88.59 7.06 -10 10 -12 89.34 7.78 10 -10 12 82.43 6.48 10 -10 12 102.05 6.86 10 -10 12 84.67 6.93 10 10 12 98.34 7.71 10 10 12 73.78 7.66 -10 10 -12 89.84 7.90 -10 10 -12 94.18 7.14 -10 10 -13 35.94 4.03 -10 10 -13 39.79 4.61 10 -10 13 41.06 3.97 -10 -10 -13 26.28 5.34 10 -10 13 39.40 3.72 10 10 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11 3 16 582.96 33.04 -11 3 -16 589.25 33.79 -11 3 -16 731.02 33.07 -11 -3 -16 553.85 32.44 11 3 16 609.52 30.86 11 -3 16 609.99 30.49 -11 -3 -17 246.38 18.97 11 3 17 212.51 14.69 11 -3 17 219.56 16.47 11 3 17 289.11 19.12 11 -3 17 226.49 15.52 -11 3 -17 264.03 17.79 -11 -3 -17 199.21 15.36 -11 -3 -17 223.72 28.49 11 -3 17 228.90 17.50 11 3 17 250.11 18.32 11 3 17 201.87 15.89 11 3 17 172.07 16.20 -11 3 -17 207.75 16.85 -11 3 -17 261.45 16.26 -11 -3 -17 196.71 16.01 11 3 17 207.14 13.70 11 3 18 40.32 5.52 -11 -3 -18 41.05 10.54 11 -3 18 48.05 6.85 11 3 18 58.13 7.66 -11 3 -18 53.51 7.46 -11 -3 -18 34.32 5.77 -11 -3 -18 20.33 10.64 11 -3 18 40.89 6.78 11 3 18 47.16 7.12 11 3 18 34.69 5.86 11 3 18 37.61 6.64 -11 3 -18 34.09 6.38 -11 3 -18 55.11 6.65 -11 3 -18 39.67 6.40 -11 -3 -18 31.98 6.02 11 3 19 272.19 16.96 11 -3 19 264.15 16.36 11 -3 19 291.07 18.67 11 3 19 354.53 20.28 11 -3 19 267.64 17.34 -11 3 -19 330.55 20.52 -11 -3 -19 271.93 18.83 -11 -3 -19 240.89 31.70 11 3 19 319.89 19.74 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56.49 7.11 -11 6 -1 64.76 9.52 11 -6 1 70.35 8.32 -11 -6 -1 70.86 10.83 -11 6 -1 64.23 7.24 11 6 1 58.02 8.27 11 6 2 3.58 2.10 -11 6 -2 3.98 2.16 11 6 2 9.54 3.85 -11 6 -2 1.78 1.90 11 6 2 2.37 2.13 -11 6 -2 0.67 1.56 11 -6 2 1.63 1.46 -11 -6 -2 -0.67 2.56 11 -6 2 1.54 1.65 -11 -6 -2 0.87 1.56 -11 -6 -2 1.99 1.34 11 -6 2 4.36 2.37 -11 -6 -2 3.31 1.74 -11 -6 -2 3.19 2.09 -11 -6 -2 9.00 2.92 -11 -6 -2 4.75 2.50 11 -6 2 2.10 1.89 -11 6 -2 2.91 2.39 -11 -6 -2 0.83 3.37 -11 -6 -2 2.05 3.06 -11 6 -2 3.10 3.15 -11 6 -2 2.08 1.56 11 -6 2 0.90 1.62 -11 6 -2 2.76 2.29 11 6 2 2.99 2.29 -11 6 -2 3.19 1.92 11 6 2 1.08 1.94 11 6 3 25.88 4.88 11 6 3 23.53 5.67 -11 -6 -3 29.75 5.94 -11 6 -3 18.01 4.20 11 6 3 19.69 4.46 11 -6 3 38.59 5.79 -11 6 -3 18.72 5.22 -11 -6 -3 26.21 5.88 -11 -6 -3 31.16 5.51 -11 -6 -3 26.51 4.35 11 -6 3 31.10 5.67 11 -6 3 24.48 4.50 -11 -6 -3 27.76 5.01 -11 -6 -3 29.91 5.11 -11 -6 -3 29.07 5.57 11 -6 3 23.11 4.65 -11 -6 -3 27.36 4.60 -11 6 -3 25.66 4.92 -11 -6 -3 37.16 8.29 -11 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11 -6 5 7.19 2.60 -11 -6 -5 5.73 2.81 -11 6 -5 3.15 1.94 11 6 5 7.71 3.17 -11 -6 -5 6.29 3.64 -11 6 -5 5.28 2.01 11 -6 5 5.61 2.42 -11 6 -5 9.73 4.49 11 6 5 2.74 2.36 -11 6 -5 4.79 2.22 11 6 5 2.72 2.22 -11 6 -5 4.88 2.23 -11 6 -6 520.35 31.14 11 6 6 580.43 34.97 11 6 6 572.13 31.11 -11 -6 -6 649.04 32.83 -11 -6 -6 457.92 30.60 -11 6 -6 413.59 32.26 11 -6 6 616.10 31.87 -11 -6 -6 494.68 29.61 -11 -6 -6 570.76 33.23 -11 -6 -6 635.05 32.16 11 -6 6 602.23 32.58 -11 -6 -6 700.64 34.54 -11 -6 -6 630.09 34.88 -11 -6 -6 565.73 33.99 -11 -6 -6 669.67 33.28 -11 -6 -6 660.62 34.04 11 6 6 616.11 30.39 11 6 6 554.52 33.66 -11 6 -6 604.08 31.21 -11 6 -6 509.87 29.09 -11 6 -6 671.04 42.02 11 6 6 603.48 33.68 11 -6 6 587.40 31.45 -11 6 -6 578.69 30.15 -11 -6 -6 717.18 35.76 11 6 6 516.00 32.73 11 6 7 18.77 5.16 11 6 7 24.43 4.41 -11 -6 -7 23.79 4.80 -11 6 -7 21.38 4.58 -11 -6 -7 26.31 5.07 -11 -6 -7 16.80 3.63 -11 6 -7 18.83 5.10 11 -6 7 23.33 4.55 11 -6 7 18.94 4.63 -11 -6 -7 14.63 4.18 11 6 7 22.44 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107.50 13.60 11 -6 14 98.86 9.62 11 6 14 115.63 11.90 11 -6 14 112.84 9.73 11 6 14 119.89 12.83 11 -6 14 93.31 9.68 11 -6 14 96.64 9.81 11 6 14 97.88 9.01 -11 6 -14 116.84 11.05 -11 -6 -14 80.37 8.36 -11 6 -14 103.50 9.44 11 6 15 35.05 5.53 -11 -6 -15 25.77 5.17 -11 -6 -15 32.77 8.60 11 6 15 28.31 4.34 -11 -6 -15 48.81 9.42 11 -6 15 27.75 4.84 11 6 15 41.43 6.80 11 -6 15 32.97 4.89 11 6 15 39.20 7.16 11 -6 15 27.62 5.04 11 6 15 33.41 4.86 -11 6 -15 34.62 5.86 -11 -6 -15 25.97 4.39 -11 6 -15 29.81 4.87 11 -6 15 35.47 4.60 11 6 16 90.05 8.52 -11 -6 -16 96.25 10.21 -11 -6 -16 110.53 15.78 -11 -6 -16 90.21 13.33 -11 -6 -16 82.64 12.73 11 6 16 105.17 8.36 -11 -6 -16 133.23 20.56 11 -6 16 88.37 8.62 11 6 16 108.06 10.71 11 -6 16 101.07 8.40 11 6 16 122.74 11.89 11 -6 16 89.16 8.75 11 6 16 95.64 8.07 11 -6 16 80.22 8.63 -11 -6 -16 71.07 7.88 -11 6 -16 86.97 9.51 -11 6 -16 96.56 8.90 -11 -6 -17 2.90 2.54 -11 -6 -17 5.52 4.32 -11 -6 -17 3.25 4.15 11 6 17 3.65 1.55 -11 -6 -17 7.83 8.22 11 -6 17 3.15 1.71 11 -6 17 2.49 1.39 11 6 17 3.78 2.56 11 6 17 3.29 1.53 11 -6 17 4.85 1.99 -11 6 -17 3.40 2.16 -11 6 -17 1.29 1.45 -11 -6 -18 500.94 27.98 -11 -6 -18 525.83 35.38 11 -6 18 366.09 21.62 -11 -6 -18 622.93 50.34 11 6 18 571.22 27.44 -11 6 -18 441.06 25.18 -11 6 -18 458.81 23.60 11 -6 18 381.78 22.77 11 -6 18 413.73 22.68 11 -6 18 420.14 21.47 11 -6 19 1.41 1.11 11 6 19 0.60 1.35 11 -6 19 0.21 0.86 11 6 19 1.75 1.89 -11 6 -19 0.36 1.45 -11 6 -19 0.26 1.17 11 -6 19 -0.52 1.45 -11 -6 -19 -0.54 2.06 -11 6 -20 277.40 14.43 -11 6 -20 283.67 16.12 11 6 20 194.17 13.50 11 -6 20 242.76 13.50 11 -6 20 219.83 12.91 11 -6 20 211.62 13.35 -11 -6 -20 355.40 22.60 11 6 20 346.23 16.63 11 -6 21 2.27 0.94 -11 -6 -21 3.49 4.09 -11 6 -21 2.35 1.25 11 6 21 1.61 1.25 -11 7 19 39.88 3.59 -11 7 19 41.01 3.99 11 7 -19 50.44 4.68 11 7 -19 42.01 3.94 -11 -7 19 40.89 3.93 -11 7 18 247.04 13.91 -11 7 18 248.50 14.44 -11 -7 18 237.30 14.26 11 7 -18 341.37 16.62 11 7 -18 307.51 15.88 11 7 -17 12.28 3.25 -11 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59.42 5.70 -11 9 12 59.58 5.97 -11 -9 12 71.89 5.89 -11 -9 11 1.39 1.26 -11 -9 11 1.92 1.22 -11 9 11 0.25 0.96 -11 9 11 0.83 1.29 -11 9 11 1.52 1.33 11 9 -11 1.40 1.42 -11 -9 10 30.70 4.29 -11 -9 10 24.40 3.81 11 9 -10 33.02 5.36 -11 9 10 24.92 4.43 -11 9 10 34.46 4.53 -11 9 10 30.02 4.35 -11 9 10 32.48 4.66 11 9 -10 32.41 4.61 11 9 -10 34.47 5.72 -11 -9 9 179.24 12.15 -11 -9 9 159.86 11.27 11 9 -9 180.52 14.02 -11 9 9 164.19 11.89 -11 9 9 159.92 11.62 -11 9 9 184.31 12.65 11 9 -9 159.75 12.41 -11 9 9 153.06 11.70 11 9 -9 161.93 13.84 11 9 -8 5.13 2.61 11 9 -8 6.80 2.49 11 9 -8 6.69 2.90 -11 9 8 3.27 1.72 -11 -9 8 6.23 1.90 -11 -9 8 7.95 2.25 -11 -9 8 5.53 2.09 -11 9 8 5.38 2.11 -11 9 8 4.81 2.38 -11 9 8 6.68 2.35 -11 9 8 6.20 2.31 -11 -9 8 5.49 2.51 -11 9 7 440.23 25.87 11 9 -7 447.35 26.44 11 9 -7 403.43 26.31 -11 -9 7 423.83 22.84 -11 -9 7 452.30 24.01 11 9 -7 434.95 26.95 -11 9 7 396.53 25.40 -11 9 7 499.91 25.38 -11 9 7 451.24 24.91 -11 9 7 500.68 25.95 -11 -9 7 512.11 26.37 11 9 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73.91 8.86 -11 -9 3 83.58 10.15 -11 -9 3 84.66 9.22 -11 9 2 4.06 1.95 11 9 -2 2.96 2.22 11 9 -2 2.71 2.08 11 9 -2 3.48 2.43 11 9 -2 2.92 2.26 -11 -9 2 4.68 2.08 11 -9 -2 3.57 1.65 -11 -9 2 4.56 1.80 -11 -9 2 2.36 1.43 11 -9 -2 2.26 1.54 -11 -9 2 2.75 3.49 -11 -9 2 2.26 3.16 -11 9 2 5.89 2.50 -11 9 2 6.37 3.06 -11 9 2 5.37 2.28 -11 9 2 7.79 2.87 -11 -9 2 1.74 2.94 -11 -9 2 0.93 2.74 -11 9 1 301.80 18.07 11 9 -1 276.37 20.73 11 9 -1 263.62 19.30 -11 9 1 225.71 19.71 11 9 -1 293.78 18.52 11 9 -1 301.76 17.91 11 -9 -1 222.93 16.36 -11 -9 1 283.91 16.67 11 -9 -1 271.34 18.00 -11 -9 1 297.66 17.54 -11 -9 1 300.00 23.32 11 9 -1 280.59 19.57 -11 -9 1 232.32 19.68 -11 9 1 264.26 20.07 -11 9 1 301.85 18.19 -11 9 1 316.39 19.15 -11 9 1 329.57 20.08 -11 -9 1 312.24 20.65 -11 9 0 20.32 4.05 11 9 0 18.97 5.26 11 9 0 21.31 4.71 -11 9 0 24.44 5.69 -11 -9 0 28.90 4.85 11 9 0 18.84 3.86 11 -9 0 26.50 4.41 -11 -9 0 26.52 4.16 11 -9 0 22.14 4.44 -11 -9 0 25.07 3.63 -11 -9 0 28.48 4.57 -11 -9 0 18.62 6.04 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12 4 12 808.02 42.73 -12 4 -12 785.26 39.30 12 -4 12 723.30 39.76 12 4 12 657.55 40.69 12 -4 12 703.71 38.22 -12 4 -12 731.90 39.11 -12 4 -12 870.89 37.93 -12 -4 -12 707.89 37.50 -12 4 -12 717.48 37.96 12 4 12 769.51 39.51 12 -4 13 8.78 2.43 12 4 13 14.39 4.16 -12 -4 -13 10.52 3.48 -12 -4 -13 11.57 6.22 -12 -4 -13 4.68 3.68 -12 -4 -13 9.77 5.30 12 4 13 11.87 3.17 12 4 13 7.99 2.68 -12 -4 -13 7.00 4.48 12 -4 13 13.63 3.57 12 4 13 9.08 3.86 -12 4 -13 7.14 2.98 12 -4 13 8.61 3.16 12 4 13 9.08 4.03 12 -4 13 7.65 3.07 -12 4 -13 3.34 2.17 -12 4 -13 5.77 2.23 12 4 13 10.56 3.22 -12 -4 -13 7.21 2.73 -12 4 -13 10.85 3.63 12 -4 13 9.13 2.99 12 4 14 408.32 23.07 -12 -4 -14 338.64 22.77 -12 -4 -14 396.69 33.16 -12 -4 -14 349.73 27.97 -12 -4 -14 328.79 26.72 12 4 14 327.77 19.97 12 -4 14 300.90 20.62 12 4 14 339.75 23.69 12 -4 14 336.79 21.29 -12 4 -14 371.94 22.33 12 -4 14 343.17 22.52 12 -4 14 323.25 21.43 12 4 14 333.14 23.62 12 4 14 264.16 18.36 -12 4 -14 315.15 21.75 -12 4 -14 378.20 20.50 -12 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2.86 2.22 -12 -4 -17 1.16 2.35 -12 -4 -18 633.84 34.15 12 4 18 509.15 26.47 -12 -4 -18 482.23 45.90 12 -4 18 515.82 27.62 -12 4 -18 640.03 30.68 12 -4 18 569.27 28.94 12 -4 18 446.39 27.33 -12 4 -18 429.82 28.50 -12 -4 -18 517.18 29.53 -12 4 -18 535.26 28.98 -12 -4 -19 10.95 4.38 12 4 19 10.33 2.50 12 -4 19 10.82 2.47 -12 -4 -19 16.91 10.80 12 4 19 8.44 3.59 12 -4 19 11.73 2.84 12 4 19 7.55 2.66 12 -4 19 9.45 2.57 12 -4 19 13.61 3.15 12 -4 19 10.24 2.79 -12 4 -19 10.30 3.21 -12 -4 -19 14.85 3.95 -12 4 -19 11.42 3.34 -12 -4 -20 205.27 15.44 12 4 20 199.02 13.47 12 -4 20 157.79 11.33 12 -4 20 202.64 11.86 -12 -4 -20 246.86 19.57 12 4 20 208.72 12.61 12 -4 20 188.15 11.42 12 -4 21 3.44 1.44 -12 -4 -21 8.17 3.32 12 4 21 4.84 1.72 -12 4 -21 5.98 2.01 -12 -4 -21 4.61 4.04 12 -4 21 5.49 1.64 12 4 22 5.27 1.43 -12 -4 -22 13.57 6.37 12 5 -21 207.12 10.75 -12 5 21 172.93 9.44 -12 5 21 157.81 8.84 -12 -5 21 132.35 8.69 -12 -5 21 189.55 9.66 12 5 -21 230.76 11.37 12 5 -20 3.45 1.49 -12 5 20 2.32 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5 1.36 2.03 -12 5 5 2.22 2.00 -12 5 5 1.14 2.04 -12 5 5 0.55 1.49 12 -5 -5 2.81 1.90 12 5 -5 -0.63 2.41 -12 5 5 1.54 1.81 -12 -5 5 2.30 3.11 -12 5 5 2.39 1.87 -12 -5 4 467.93 33.35 12 5 -4 567.38 32.79 12 5 -4 492.05 31.63 -12 5 4 460.57 28.96 -12 5 4 530.31 32.41 12 -5 -4 637.54 31.27 -12 -5 4 480.98 33.32 -12 -5 4 574.07 29.28 12 -5 -4 531.26 29.84 12 5 -4 568.38 30.48 12 5 -4 577.05 32.56 -12 -5 4 629.72 31.01 -12 -5 4 557.23 29.68 -12 -5 4 525.73 37.58 -12 5 4 624.62 32.17 -12 -5 4 574.98 32.52 -12 5 4 639.16 34.70 -12 5 4 534.49 32.72 -12 5 4 615.67 31.76 12 5 -4 553.25 34.17 12 -5 -4 591.66 31.76 -12 -5 4 467.15 31.73 -12 5 4 598.20 30.75 -12 -5 4 523.89 36.01 -12 -5 3 55.36 9.56 12 5 -3 76.69 9.61 12 5 -3 59.85 8.43 12 5 -3 58.45 8.29 -12 5 3 59.28 7.24 -12 5 3 62.66 8.69 12 -5 -3 78.40 8.29 -12 -5 3 53.78 9.23 -12 -5 3 62.76 7.06 12 -5 -3 56.06 7.22 -12 -5 3 67.48 7.13 12 5 -3 81.58 9.42 -12 -5 3 70.11 7.81 -12 -5 3 52.02 6.81 -12 -5 3 54.15 10.74 -12 5 3 76.19 8.71 -12 -5 3 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32.65 -12 -5 -8 719.02 36.03 -12 -5 -8 777.36 36.06 -12 -5 -8 718.55 35.60 12 5 8 623.01 32.77 12 -5 8 588.49 33.31 12 -5 8 627.96 32.42 12 -5 8 591.00 32.85 -12 -5 -8 599.83 35.08 -12 -5 -8 511.58 34.04 12 -5 8 631.27 33.27 12 -5 8 682.24 35.75 -12 -5 -8 571.57 33.53 -12 -5 -8 510.14 31.43 12 5 8 662.86 36.60 12 -5 8 657.27 34.58 12 -5 8 600.83 33.63 12 5 8 613.23 34.51 -12 -5 -8 606.36 32.57 -12 5 -8 598.74 33.62 -12 5 -8 657.00 32.85 12 5 9 46.28 7.71 -12 5 -9 28.45 5.22 -12 -5 -9 35.02 6.00 12 -5 9 30.85 5.26 12 -5 9 28.62 4.38 -12 -5 -9 41.88 7.25 -12 -5 -9 41.51 7.06 -12 -5 -9 42.81 7.13 -12 -5 -9 38.94 6.82 12 5 9 37.07 5.35 12 5 9 30.32 4.97 12 -5 9 33.45 5.64 12 -5 9 34.54 5.13 12 -5 9 28.97 4.94 12 5 9 36.30 6.87 12 -5 9 37.48 6.16 12 -5 9 36.59 6.13 -12 5 -9 35.76 6.03 -12 5 -9 32.02 5.18 -12 -5 -9 25.19 4.63 12 5 9 20.28 4.95 12 5 10 414.19 25.79 -12 -5 -10 381.82 23.16 -12 5 -10 321.02 21.63 12 -5 10 342.08 21.43 12 -5 10 337.63 19.40 -12 -5 -10 437.77 27.04 -12 -5 -10 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13.15 3.48 -12 5 -12 10.96 3.08 12 -5 13 48.81 5.42 12 5 13 55.05 7.69 -12 -5 -13 56.51 7.61 -12 -5 -13 72.74 12.86 12 -5 13 48.53 5.58 -12 -5 -13 71.74 11.14 -12 -5 -13 61.59 10.20 12 5 13 54.18 6.34 12 5 13 43.02 5.88 12 5 13 47.87 7.86 12 -5 13 42.60 6.23 12 -5 13 51.36 7.33 12 5 13 34.93 5.57 12 -5 13 40.39 6.16 -12 5 -13 54.89 7.50 -12 -5 -13 38.50 5.76 -12 5 -13 52.05 6.68 12 5 13 45.23 6.77 12 5 14 216.71 15.70 -12 -5 -14 203.84 16.00 -12 -5 -14 295.37 27.41 -12 -5 -14 252.19 22.45 -12 -5 -14 206.76 20.18 -12 -5 -14 212.44 20.38 12 5 14 179.89 13.22 12 -5 14 189.46 14.27 12 5 14 192.48 16.42 12 -5 14 207.85 14.85 12 -5 14 203.93 15.44 12 -5 14 197.39 14.71 12 5 14 169.70 13.05 -12 5 -14 202.86 15.69 -12 -5 -14 163.93 13.50 -12 5 -14 210.72 14.80 12 5 14 189.77 14.28 12 -5 14 198.92 13.88 12 5 15 1.18 1.60 -12 -5 -15 2.52 2.16 -12 -5 -15 1.96 3.99 12 5 15 2.20 1.41 -12 -5 -15 2.54 5.44 12 -5 15 2.26 1.69 12 5 15 2.10 2.25 12 -5 15 1.08 1.47 12 -5 15 2.12 1.73 12 5 15 -0.59 1.39 12 -5 15 2.80 1.88 -12 5 -15 0.94 1.80 -12 -5 -15 1.15 1.28 -12 5 -15 1.15 1.64 12 -5 15 0.59 1.26 12 5 16 210.84 13.95 -12 -5 -16 204.65 16.27 -12 -5 -16 220.54 23.29 12 5 16 190.98 12.97 12 -5 16 186.60 13.70 12 5 16 207.54 16.03 12 -5 16 184.71 13.29 12 5 16 225.99 17.71 12 -5 16 176.73 13.77 12 5 16 178.97 12.13 -12 5 -16 192.26 15.19 -12 -5 -16 185.04 14.12 -12 5 -16 207.22 14.51 -12 -5 -17 106.31 11.07 12 5 17 67.94 6.78 -12 -5 -17 78.30 14.67 -12 -5 -17 77.14 17.18 12 -5 17 64.45 7.07 12 5 17 88.79 9.23 12 -5 17 65.45 6.75 12 5 17 81.09 9.86 12 -5 17 67.77 7.54 -12 5 -17 71.40 8.54 -12 -5 -17 75.76 8.38 -12 5 -17 83.95 8.23 12 5 18 6.09 1.91 -12 -5 -18 5.24 5.61 12 -5 18 5.78 1.83 -12 -5 -18 10.64 9.91 12 5 18 6.04 3.31 12 -5 18 4.63 1.88 -12 5 -18 5.43 2.78 -12 -5 -18 3.25 2.07 -12 5 -18 7.78 2.60 -12 -5 -18 9.79 4.13 12 -5 18 5.98 2.23 -12 -5 -19 273.13 19.79 12 -5 19 231.95 12.66 12 5 19 218.36 13.64 12 -5 19 210.81 11.78 12 5 19 277.44 15.83 12 -5 19 169.88 11.80 12 -5 19 221.22 12.82 -12 5 -19 226.14 14.81 -12 -5 -19 253.89 16.32 -12 5 -19 244.81 14.19 -12 -5 -20 220.28 15.93 -12 5 -20 248.98 13.68 12 5 20 259.84 14.39 12 5 20 194.82 12.43 12 -5 20 204.59 11.66 12 -5 20 133.63 10.73 12 -5 20 198.19 11.67 -12 5 -20 172.21 12.40 -12 -5 -20 259.93 20.70 -12 5 -21 83.79 6.23 12 5 21 73.77 5.96 12 5 21 33.08 3.98 12 -5 21 47.66 3.97 -12 -5 -21 67.36 12.25 -12 6 20 54.84 4.13 -12 6 20 57.11 4.37 -12 -6 20 46.87 3.88 -12 -6 20 44.47 3.86 12 6 -20 64.05 4.97 12 6 -19 212.60 12.35 -12 -6 19 192.24 10.41 -12 -6 19 149.34 9.27 -12 -6 19 182.46 10.39 12 6 -19 237.78 12.46 12 6 -19 166.29 10.44 -12 6 19 184.70 10.46 -12 6 19 169.93 10.40 -12 -6 18 19.61 2.92 -12 -6 18 17.31 2.65 -12 6 18 14.49 2.61 -12 6 18 12.66 2.33 -12 -6 18 19.52 3.05 12 6 -18 20.13 3.59 12 6 -18 19.93 3.42 -12 -6 17 549.22 25.38 -12 -6 17 554.73 25.45 -12 -6 17 500.17 24.89 -12 6 17 428.03 24.43 -12 6 17 496.01 25.47 -12 6 17 469.90 24.77 -12 -6 17 511.96 25.42 12 6 -17 618.28 28.54 12 6 -17 580.82 28.06 12 6 -16 2.11 1.81 -12 -6 16 0.51 1.09 -12 -6 16 1.26 1.24 -12 -6 16 2.24 1.39 -12 -6 16 1.57 1.14 -12 6 16 1.97 1.43 -12 6 16 0.51 0.98 -12 6 16 1.81 1.36 -12 -6 16 1.84 1.56 12 6 -16 3.08 2.02 12 6 -16 0.81 1.66 -12 -6 15 122.55 9.43 12 6 -15 136.63 12.18 -12 -6 15 130.46 9.73 -12 6 15 121.66 9.58 -12 6 15 109.16 9.56 -12 6 15 117.09 9.95 -12 -6 15 126.85 9.82 12 6 -15 118.52 9.56 -12 -6 15 124.61 9.56 -12 6 15 109.53 9.36 12 6 -15 157.73 12.42 12 6 -15 139.96 12.27 12 6 -14 4.53 2.82 -12 -6 14 4.06 2.12 -12 -6 14 6.01 2.36 -12 -6 14 5.46 2.10 -12 6 14 5.08 2.15 -12 6 14 3.44 1.93 -12 6 14 4.82 2.00 -12 6 14 5.69 2.18 12 6 -14 6.25 2.45 12 6 -14 5.39 2.44 12 6 -14 5.19 2.73 -12 -6 13 177.70 12.99 -12 -6 13 168.57 11.15 12 6 -13 193.02 15.70 -12 -6 13 167.86 12.45 -12 -6 13 170.64 13.18 -12 -6 13 187.75 13.00 12 6 -13 173.87 13.90 -12 6 13 165.79 12.65 -12 6 13 177.66 13.25 -12 6 13 187.28 13.71 -12 6 13 149.91 11.84 -12 6 13 177.37 13.24 12 6 -13 191.54 14.90 12 6 -13 189.42 15.92 -12 -6 12 1.17 1.67 -12 -6 12 1.31 1.33 12 6 -12 1.64 1.82 -12 -6 12 1.73 1.33 -12 -6 12 0.85 1.81 -12 -6 12 1.79 1.81 -12 6 12 5.20 2.20 -12 6 12 0.84 1.50 -12 6 12 0.78 1.30 -12 6 12 2.83 1.82 -12 6 12 3.76 2.02 12 6 -12 2.92 1.86 12 6 -12 0.96 1.59 12 6 -12 1.18 2.65 -12 -6 11 542.73 27.79 -12 -6 11 579.80 30.92 12 6 -11 571.77 32.75 -12 -6 11 506.56 28.53 -12 -6 11 604.13 31.92 -12 -6 11 608.29 30.30 12 6 -11 600.36 32.72 -12 6 11 511.09 29.21 -12 6 11 498.79 28.47 -12 6 11 563.29 30.14 -12 6 11 540.83 30.37 -12 6 11 551.51 30.50 -12 6 11 467.80 27.98 12 6 -11 516.79 29.62 12 6 -11 579.69 31.52 -12 -6 10 17.28 4.40 -12 -6 10 14.62 3.42 12 6 -10 13.87 4.16 -12 -6 10 14.01 3.40 -12 -6 10 14.37 3.90 -12 6 10 12.01 3.51 -12 6 10 17.43 4.21 -12 6 10 17.08 4.01 -12 6 10 13.63 4.02 -12 6 10 14.07 3.50 -12 6 10 14.69 3.59 12 6 -10 17.93 4.77 12 6 -10 18.07 4.30 12 6 -10 11.27 3.47 -12 -6 9 402.49 22.67 -12 -6 9 441.18 26.04 12 6 -9 362.49 24.63 -12 -6 9 361.65 22.06 -12 -6 9 428.98 24.30 12 6 -9 390.62 25.88 -12 6 9 314.37 23.09 -12 6 9 360.64 22.36 -12 6 9 351.74 22.69 -12 6 9 421.61 24.10 -12 6 9 375.80 23.83 -12 6 9 390.71 24.57 12 6 -9 368.77 24.10 12 6 -9 361.85 23.38 12 6 -9 396.19 26.48 -12 -6 8 21.32 4.59 -12 -6 8 23.97 5.87 -12 -6 8 15.69 3.74 -12 -6 8 20.54 6.34 -12 -6 8 24.20 5.14 -12 6 8 21.27 4.26 -12 6 8 26.58 4.92 -12 6 8 20.97 4.82 -12 6 8 14.83 4.06 -12 6 8 14.31 4.43 -12 6 8 20.15 4.29 12 6 -8 16.03 4.54 12 6 -8 17.44 4.53 12 6 -8 14.24 4.50 12 6 -7 18.56 4.99 12 6 -7 19.15 4.80 12 6 -7 26.75 6.10 -12 -6 7 21.81 3.87 -12 -6 7 14.68 3.63 -12 -6 7 25.47 7.28 -12 -6 7 19.29 5.20 -12 6 7 15.79 3.91 -12 6 7 23.88 4.89 -12 6 7 19.40 4.73 -12 6 7 14.37 4.21 -12 6 7 16.41 3.88 -12 -6 7 18.69 4.54 -12 -6 7 19.28 5.69 -12 6 6 49.44 7.10 12 6 -6 46.89 7.59 12 6 -6 64.57 9.13 -12 -6 6 49.11 6.20 -12 -6 6 60.51 7.23 12 6 -6 64.55 9.28 -12 6 6 59.16 7.48 -12 -6 6 76.92 11.95 -12 -6 6 65.51 8.80 -12 6 6 74.65 9.09 -12 6 6 50.54 7.87 -12 6 6 61.25 7.78 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250.81 23.02 -12 6 0 318.61 19.20 12 6 0 284.05 20.61 12 6 1 715.23 39.50 12 6 1 623.28 35.86 -12 6 -1 623.73 35.10 -12 6 -1 490.72 36.23 -12 -6 -1 517.53 37.43 12 -6 1 661.75 34.68 -12 -6 -1 713.85 35.39 -12 -6 -1 638.86 31.47 -12 -6 -1 716.08 34.30 -12 -6 -1 744.59 36.46 12 -6 1 633.00 35.03 -12 -6 -1 672.06 32.87 -12 -6 -1 530.95 40.32 -12 6 -1 773.15 36.38 12 6 1 606.97 35.34 -12 6 -1 673.37 40.15 -12 6 -1 693.43 33.65 -12 6 -1 591.04 34.06 -12 6 -1 697.18 39.15 12 -6 1 675.61 35.66 -12 -6 -1 611.03 39.66 -12 6 -1 707.41 34.63 12 6 1 607.41 36.03 -12 -6 -2 5.28 2.98 12 6 2 2.62 2.81 12 6 2 5.67 2.65 -12 6 -2 6.90 2.79 12 6 2 5.02 2.81 -12 6 -2 4.10 2.78 12 -6 2 2.55 1.83 -12 -6 -2 2.06 2.64 12 -6 2 3.70 2.09 -12 -6 -2 5.82 2.65 -12 -6 -2 5.44 2.06 12 -6 2 3.57 2.50 -12 -6 -2 5.83 2.42 -12 -6 -2 5.39 2.45 -12 -6 -2 2.34 1.76 -12 -6 -2 5.41 2.58 12 -6 2 3.59 2.28 -12 -6 -2 3.30 2.02 -12 6 -2 6.53 2.71 -12 -6 -2 6.21 4.66 -12 -6 -2 5.10 4.07 -12 6 -2 4.18 2.47 -12 6 -2 4.77 2.12 12 -6 2 2.33 2.10 -12 6 -2 5.56 3.13 12 6 2 1.27 1.92 -12 6 -2 3.42 2.00 12 6 2 4.93 2.68 12 6 3 365.17 26.54 12 6 3 364.35 23.96 -12 -6 -3 407.76 26.23 -12 6 -3 338.95 23.13 -12 -6 -3 436.58 25.06 -12 -6 -3 393.28 21.33 12 -6 3 370.77 24.38 -12 -6 -3 405.15 21.89 -12 -6 -3 412.64 23.81 -12 -6 -3 435.59 25.81 -12 -6 -3 416.55 25.09 12 -6 3 378.48 23.64 -12 -6 -3 410.52 22.94 -12 -6 -3 432.69 24.64 -12 6 -3 274.93 24.59 12 -6 3 382.84 23.57 -12 -6 -3 318.04 25.43 -12 -6 -3 402.63 30.03 -12 6 -3 467.20 24.89 12 6 3 383.14 23.71 -12 6 -3 457.03 30.03 12 6 3 338.09 25.36 12 -6 3 392.39 24.13 -12 -6 -3 376.59 27.20 -12 6 -3 421.06 23.27 12 6 3 321.70 24.24 12 6 4 61.96 7.93 -12 -6 -4 66.13 8.92 12 6 4 56.27 9.14 -12 6 -4 47.68 7.03 -12 -6 -4 71.99 8.82 -12 -6 -4 57.18 6.50 12 -6 4 61.56 8.07 -12 -6 -4 60.45 6.88 -12 -6 -4 74.46 9.23 -12 -6 -4 49.94 7.63 12 -6 4 61.89 7.67 -12 -6 -4 76.08 8.03 -12 -6 -4 65.27 8.12 12 -6 4 63.43 7.82 -12 6 -4 34.26 7.39 -12 -6 -4 49.89 8.42 -12 -6 -4 61.13 10.51 12 6 4 68.78 7.97 -12 6 -4 62.58 7.68 12 -6 4 60.16 7.18 12 6 4 57.06 8.78 12 -6 4 61.03 7.76 -12 -6 -4 57.20 9.03 -12 6 -4 55.67 6.88 12 6 4 53.39 8.21 12 6 5 -0.66 1.55 -12 -6 -5 5.00 2.79 -12 6 -5 3.13 2.10 12 6 5 2.21 1.47 12 6 5 3.45 1.95 -12 -6 -5 1.55 1.71 -12 -6 -5 1.78 1.53 -12 -6 -5 1.66 1.62 -12 -6 -5 3.01 2.17 12 -6 5 1.93 1.73 -12 -6 -5 0.85 1.53 -12 -6 -5 3.40 2.28 -12 -6 -5 2.84 2.31 -12 -6 -5 3.26 2.08 12 -6 5 6.45 2.73 12 -6 5 3.98 2.34 -12 -6 -5 2.36 2.39 -12 6 -5 2.92 1.96 -12 -6 -5 0.78 3.52 12 6 5 4.20 2.66 -12 -6 -5 5.56 3.92 12 -6 5 0.40 1.22 12 6 5 0.58 2.08 12 6 5 2.78 2.26 -12 6 -5 3.32 1.80 -12 6 -6 8.08 2.80 12 6 6 7.21 3.45 -12 -6 -6 4.83 2.54 -12 6 -6 5.35 2.64 12 6 6 6.25 2.53 -12 -6 -6 8.74 3.13 -12 -6 -6 4.61 2.51 -12 -6 -6 10.56 3.61 -12 -6 -6 10.68 3.62 -12 -6 -6 6.71 2.74 -12 -6 -6 5.57 2.37 -12 -6 -6 7.44 2.70 12 -6 6 3.78 2.49 -12 6 -6 5.76 2.38 -12 -6 -6 7.57 4.36 -12 -6 -6 7.08 3.40 12 6 6 7.68 3.16 12 -6 6 8.36 2.90 12 6 6 4.96 2.80 -12 6 -6 4.81 2.20 -12 6 -7 494.27 29.91 12 6 7 587.02 35.08 12 6 7 553.33 30.37 -12 -6 -7 590.53 32.42 -12 6 -7 537.03 31.19 -12 -6 -7 690.20 32.60 -12 -6 -7 537.23 32.74 -12 -6 -7 651.90 32.51 12 6 7 539.34 29.02 12 -6 7 538.80 31.52 -12 -6 -7 643.65 32.70 -12 -6 -7 573.96 33.28 -12 -6 -7 677.30 34.18 12 6 7 553.83 33.39 -12 6 -7 556.86 30.79 12 -6 7 519.65 30.78 -12 6 -7 613.00 30.77 -12 -6 -7 637.97 34.71 12 6 7 461.28 31.67 -12 -6 -8 3.63 2.22 12 6 8 5.64 2.25 -12 6 -8 4.46 2.19 -12 6 -8 4.39 2.24 -12 -6 -8 8.21 3.21 -12 -6 -8 7.42 3.02 12 -6 8 5.17 2.30 12 6 8 7.33 2.34 -12 -6 -8 7.99 3.25 12 6 8 5.19 2.43 12 -6 8 9.00 3.18 -12 -6 -8 8.95 3.40 12 -6 8 4.50 2.00 12 -6 8 8.27 2.57 -12 -6 -8 5.47 2.97 12 6 8 6.94 3.14 12 6 8 6.85 3.20 12 -6 8 8.44 2.89 -12 6 -8 3.65 2.32 -12 6 -8 3.28 2.17 12 6 9 455.01 24.99 -12 -6 -9 515.45 28.13 -12 6 -9 437.87 28.36 -12 6 -9 432.35 26.93 -12 -6 -9 621.89 31.09 -12 -6 -9 599.34 31.40 -12 -6 -9 599.93 31.06 12 6 9 446.18 25.02 12 6 9 436.63 26.09 12 -6 9 451.27 26.04 12 -6 9 477.41 27.18 12 -6 9 468.12 25.33 12 -6 9 422.31 25.40 12 6 9 458.59 29.54 12 -6 9 492.80 28.00 12 6 9 509.54 30.66 12 -6 9 449.34 27.27 -12 6 -9 470.47 27.70 -12 6 -9 474.90 26.24 12 6 9 423.60 27.97 -12 -6 -9 524.02 29.86 12 6 10 1.18 2.40 -12 -6 -10 0.88 1.34 -12 6 -10 -0.45 1.22 12 -6 10 1.42 1.44 -12 -6 -10 4.11 2.64 -12 -6 -10 1.15 2.46 12 6 10 0.64 0.96 12 6 10 2.26 1.61 -12 -6 -10 3.01 2.82 -12 -6 -10 0.64 2.11 12 -6 10 1.21 1.44 12 -6 10 0.59 0.89 12 -6 10 1.45 1.55 12 6 10 0.59 2.10 12 -6 10 -0.44 1.89 12 6 10 -0.60 1.98 12 -6 10 0.45 1.38 -12 6 -10 3.65 2.23 -12 -6 -10 -0.72 1.75 12 6 10 0.99 1.77 -12 6 -10 -0.37 1.64 -12 -6 -11 98.48 10.01 12 6 11 103.94 11.38 -12 6 -11 88.16 9.71 -12 -6 -11 121.08 13.10 12 -6 11 91.30 8.61 -12 -6 -11 132.79 13.74 -12 -6 -11 121.22 13.04 12 6 11 99.30 8.77 12 6 11 91.71 8.89 12 -6 11 89.12 7.86 -12 -6 -11 108.84 12.77 12 -6 11 84.45 8.73 12 6 11 93.66 11.20 12 6 11 90.31 11.31 12 -6 11 100.52 10.23 12 6 11 95.11 9.56 -12 -6 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26.96 4.71 -12 7 11 30.42 5.09 12 7 -11 29.33 4.97 12 7 -11 26.81 5.29 -12 -7 10 108.52 9.58 -12 -7 10 139.43 11.38 12 7 -10 106.42 11.41 -12 7 10 110.02 10.09 -12 7 10 112.99 9.82 -12 7 10 107.67 9.74 -12 7 10 133.22 11.08 -12 -7 10 125.79 10.00 -12 -7 10 133.59 11.19 12 7 -10 112.79 11.49 12 7 -10 117.04 10.89 -12 7 10 100.27 9.66 -12 -7 9 167.26 12.58 -12 -7 9 197.09 14.43 12 7 -9 169.42 15.02 -12 7 9 173.28 13.05 -12 7 9 177.45 13.43 -12 7 9 166.98 12.66 -12 7 9 160.51 13.13 -12 -7 9 195.49 13.55 -12 -7 9 192.93 14.68 12 7 -9 159.05 14.05 -12 7 9 144.46 12.87 12 7 -9 174.49 14.33 12 7 -9 167.10 15.43 -12 -7 8 2.05 2.29 -12 -7 8 0.99 2.43 12 7 -8 4.26 2.40 -12 -7 8 2.16 1.69 -12 -7 8 -0.92 2.70 -12 7 8 1.21 1.55 -12 7 8 1.25 1.69 -12 7 8 0.35 1.27 -12 7 8 0.39 1.29 12 7 -8 -0.57 1.72 12 7 -8 1.51 1.80 -12 7 8 0.93 1.67 12 7 -8 0.59 1.60 12 7 -7 379.41 24.88 12 7 -7 349.58 25.04 -12 7 7 364.90 24.25 -12 -7 7 360.58 21.02 -12 -7 7 387.54 22.49 -12 -7 7 447.75 25.59 12 7 -7 361.14 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516.19 30.47 12 -7 11 509.94 28.71 12 7 11 488.40 28.21 -12 7 -11 529.94 27.45 -12 -7 -11 512.04 30.49 -12 7 -12 0.36 1.46 12 7 12 0.98 1.87 -12 -7 -12 2.74 1.91 -12 7 -12 0.42 1.70 12 -7 12 2.08 1.56 -12 -7 -12 0.67 2.71 -12 -7 -12 -0.65 3.74 -12 -7 -12 4.09 3.20 -12 -7 -12 2.12 2.71 12 7 12 2.46 2.41 -12 7 -12 -0.83 1.68 -12 7 -12 2.17 1.62 12 7 12 0.36 1.30 12 -7 12 3.46 2.14 12 -7 12 1.25 1.20 12 7 12 2.53 2.56 12 -7 12 3.51 1.96 -12 -7 -12 -0.50 2.14 -12 7 -13 274.44 19.16 12 7 13 356.24 21.98 -12 -7 -13 324.67 20.70 -12 7 -13 325.75 20.82 12 -7 13 346.36 19.51 12 7 13 269.74 20.72 12 -7 13 320.68 19.50 -12 -7 -13 514.26 30.00 -12 -7 -13 458.30 28.79 12 7 13 331.89 21.94 12 -7 13 335.22 20.41 12 7 13 348.34 20.15 -12 7 -13 337.87 21.19 -12 7 -13 391.74 20.14 -12 -7 -13 367.50 23.12 12 7 14 69.29 7.74 -12 -7 -14 53.58 7.08 -12 7 -14 57.07 6.80 12 7 14 57.52 7.63 12 -7 14 62.50 6.41 12 -7 14 57.74 6.25 -12 -7 -14 92.13 12.71 12 7 14 69.88 8.39 12 -7 14 64.68 6.98 12 -7 14 57.36 6.03 12 7 14 65.71 6.71 -12 7 -14 57.42 7.29 -12 -7 -14 74.02 9.17 12 -7 14 54.32 5.70 -12 7 -15 1.59 1.62 12 7 15 1.60 1.50 -12 -7 -15 3.95 2.21 12 -7 15 2.05 1.30 -12 -7 -15 0.51 2.29 12 7 15 5.21 2.55 12 -7 15 1.75 1.13 -12 -7 -15 3.50 3.14 -12 -7 -15 3.53 4.15 -12 -7 -15 3.66 5.11 12 7 15 3.23 2.26 12 -7 15 3.90 1.82 12 7 15 1.30 1.27 12 -7 15 1.92 1.26 -12 7 -15 1.49 1.68 -12 7 -16 114.13 9.46 -12 -7 -16 125.98 11.16 12 7 16 101.12 9.54 12 -7 16 112.93 8.23 12 -7 16 112.84 8.38 12 7 16 131.70 10.66 12 -7 16 95.06 7.84 12 7 16 124.01 8.56 -12 -7 -16 135.15 12.96 -12 7 -16 127.02 10.46 -12 -7 -17 228.74 17.65 12 -7 17 173.69 10.49 -12 -7 -17 275.27 23.71 12 7 17 162.04 11.85 12 -7 17 180.62 10.21 12 7 17 178.02 10.16 12 -7 17 127.43 9.35 -12 7 -17 181.88 11.97 -12 -7 -17 188.75 14.37 12 7 17 210.71 13.07 12 -7 18 1.02 0.79 -12 -7 -18 5.72 6.00 -12 -7 -18 6.79 4.41 12 -7 18 0.71 0.72 -12 7 -18 3.04 1.49 12 7 18 4.38 1.86 -12 7 -19 235.39 13.03 -12 -8 17 4.05 1.08 12 8 -17 3.85 1.21 -12 -8 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20.21 12 8 -6 301.87 21.14 12 8 -6 262.08 20.59 -12 -8 6 273.89 17.59 -12 -8 6 301.95 18.72 12 8 -6 311.57 21.88 -12 -8 6 394.49 22.67 -12 -8 6 449.01 26.39 -12 8 6 268.68 20.15 -12 8 6 324.78 19.77 -12 8 6 336.88 20.18 -12 8 6 339.19 21.40 -12 -8 6 365.30 21.73 -12 -8 6 391.20 22.36 12 8 -5 44.80 7.12 -12 8 5 37.86 6.64 12 8 -5 37.09 6.55 -12 -8 5 33.63 4.88 -12 -8 5 49.60 6.04 12 8 -5 43.92 7.18 -12 -8 5 64.41 9.87 -12 -8 5 49.28 7.45 -12 8 5 37.94 6.55 -12 8 5 43.26 6.14 -12 8 5 54.14 7.46 -12 8 5 42.76 6.04 -12 -8 5 54.71 7.85 -12 -8 5 50.79 7.60 -12 8 4 2.21 1.58 -12 8 4 3.35 2.27 12 8 -4 2.10 2.13 12 8 -4 1.97 1.89 -12 -8 4 4.19 1.95 12 -8 -4 0.83 1.37 -12 -8 4 0.89 1.07 -12 -8 4 6.66 2.33 -12 -8 4 5.90 4.36 -12 -8 4 2.67 2.70 -12 8 4 3.23 2.05 -12 8 4 0.53 1.43 -12 8 4 0.50 2.01 -12 -8 4 5.42 3.20 -12 -8 4 4.42 3.26 -12 8 3 29.86 4.93 12 8 -3 30.52 6.02 -12 8 3 29.92 6.17 12 8 -3 23.25 5.35 12 8 -3 25.56 5.15 -12 -8 3 25.73 4.52 12 -8 -3 30.85 5.29 -12 -8 3 32.59 4.79 -12 -8 3 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252.79 22.21 -12 8 0 351.18 24.64 -12 8 0 366.28 21.23 -12 8 0 387.45 22.70 -12 8 0 371.49 24.54 -12 8 0 364.86 24.55 -12 -8 0 285.83 24.05 12 8 1 14.65 4.69 -12 8 -1 11.12 3.52 12 8 1 17.47 4.20 -12 8 -1 19.90 4.37 12 8 1 17.44 4.42 -12 8 -1 15.68 4.89 -12 -8 -1 17.28 4.00 12 -8 1 18.24 4.13 -12 -8 -1 18.74 3.42 -12 -8 -1 19.16 3.96 12 -8 1 18.03 4.25 -12 -8 -1 12.66 5.64 -12 8 -1 16.95 3.89 -12 8 -1 19.36 5.03 -12 8 -1 14.79 3.44 -12 8 -1 12.69 4.38 -12 -8 -1 14.13 5.19 12 8 2 29.14 6.41 -12 8 -2 18.57 4.40 12 8 2 29.85 5.59 -12 8 -2 27.89 4.95 -12 8 -2 24.27 5.85 -12 -8 -2 33.35 5.54 12 8 2 25.23 4.80 12 -8 2 19.38 4.33 -12 -8 -2 34.76 5.27 12 -8 2 25.65 5.11 -12 -8 -2 27.15 4.26 -12 -8 -2 24.71 6.87 12 8 2 31.25 5.44 -12 8 -2 24.61 4.83 -12 8 -2 24.22 4.42 -12 8 -2 36.26 7.13 -12 -8 -2 19.88 6.18 12 8 3 0.84 1.27 -12 8 -3 1.30 2.16 -12 8 -3 0.77 1.81 12 8 3 1.95 2.49 -12 8 -3 -0.44 1.33 12 8 3 2.77 1.98 -12 -8 -3 1.37 1.75 -12 -8 -3 2.15 1.46 12 8 3 1.21 1.55 12 -8 3 1.70 1.63 -12 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3.01 12 8 6 607.69 37.71 12 8 6 720.51 35.01 -12 8 -6 583.34 36.79 -12 8 -6 630.75 33.84 -12 8 -6 670.28 35.28 -12 -8 -6 786.59 38.48 -12 -8 -6 726.48 34.06 12 8 6 653.12 34.12 12 -8 6 692.22 35.29 -12 -8 -6 746.32 34.70 12 -8 6 699.78 35.42 12 -8 6 683.32 34.55 -12 -8 -6 796.69 36.35 -12 -8 -6 809.85 38.11 -12 -8 -6 510.78 37.59 -12 8 -6 622.67 32.77 -12 8 -6 637.81 34.35 12 -8 6 628.03 33.66 12 8 6 612.19 34.87 -12 -8 -6 505.17 35.32 -12 8 -7 16.53 4.48 12 -8 7 20.81 4.24 -12 -8 -7 21.97 5.03 -12 -8 -7 26.55 4.84 -12 -8 -7 25.60 4.72 12 8 7 21.23 4.25 -12 -8 -7 27.92 5.57 12 -8 7 18.49 4.05 12 -8 7 20.27 4.00 -12 -8 -7 32.94 5.49 12 -8 7 22.13 3.78 -12 -8 -7 14.55 5.29 -12 -8 -7 16.25 4.83 -12 8 -7 19.59 3.71 12 8 7 16.64 4.05 12 -8 7 21.80 4.29 -12 8 -7 23.56 4.45 12 8 7 24.18 5.74 12 8 7 24.80 4.34 -12 8 -7 20.06 4.32 -12 8 -8 244.96 17.00 12 8 8 272.96 16.78 12 8 8 277.41 20.68 -12 8 -8 220.83 18.14 -12 8 -8 262.49 18.15 -12 -8 -8 353.12 19.33 -12 -8 -8 367.98 20.51 -12 -8 -8 367.55 20.24 12 8 8 305.33 18.00 12 -8 8 281.68 17.95 -12 -8 -8 364.39 22.20 12 -8 8 278.23 18.07 12 -8 8 277.87 17.21 -12 -8 -8 382.59 21.68 12 -8 8 262.50 16.16 -12 -8 -8 236.81 20.89 12 8 8 216.11 17.93 12 -8 8 294.78 18.34 -12 8 -8 249.90 16.26 12 -8 8 247.24 17.17 12 8 8 280.78 18.57 -12 -8 -8 227.95 18.78 -12 8 -9 152.07 12.21 -12 8 -9 168.68 13.32 12 -8 9 169.14 12.62 12 -8 9 182.39 11.94 -12 -8 -9 225.48 15.73 -12 -8 -9 216.43 14.80 -12 -8 -9 222.59 15.44 12 8 9 184.99 12.85 12 -8 9 166.36 11.95 -12 -8 -9 238.54 16.75 12 -8 9 164.94 11.61 -12 -8 -9 145.09 15.37 12 8 9 124.26 12.69 12 -8 9 179.73 13.07 -12 8 -9 152.94 11.43 12 -8 9 162.54 12.65 12 8 9 168.31 13.19 -12 -8 -9 137.54 13.60 -12 8 -10 108.95 9.42 -12 8 -10 96.42 9.60 -12 -8 -10 146.85 12.22 -12 -8 -10 152.11 13.01 -12 -8 -10 138.40 12.29 12 8 10 105.73 9.07 12 -8 10 103.42 9.02 12 -8 10 101.44 8.38 12 -8 10 92.72 8.06 -12 -8 -10 85.09 11.41 12 8 10 74.54 9.26 -12 8 -10 94.26 8.16 12 -8 10 100.03 9.18 12 8 10 118.48 10.15 -12 -8 -10 81.76 9.89 12 -8 11 1.76 1.25 -12 -8 -11 1.06 2.27 -12 -8 -11 1.97 2.58 -12 -8 -11 2.20 2.68 -12 -8 -11 2.97 2.79 12 -8 11 0.48 0.85 12 8 11 2.61 1.89 -12 8 -11 1.26 1.08 -12 8 -11 0.65 1.25 12 8 11 1.42 1.70 -12 8 -11 0.38 2.30 12 -8 11 1.00 1.42 12 -8 11 1.81 1.27 -12 -8 -11 3.19 2.99 12 8 11 1.76 1.97 -12 -8 -11 3.32 2.41 12 8 12 403.38 24.05 -12 8 -12 361.42 21.50 -12 8 -12 429.40 23.35 12 -8 12 350.22 20.24 -12 -8 -12 411.30 27.30 12 8 12 270.73 21.51 12 -8 12 438.36 22.05 -12 -8 -12 605.00 29.74 -12 -8 -12 674.56 31.93 -12 -8 -12 622.11 30.64 12 8 12 319.15 21.64 12 -8 12 404.73 22.10 -12 -8 -12 352.64 23.72 12 -8 13 7.27 1.97 -12 -8 -13 5.16 3.72 12 -8 13 9.64 2.38 -12 -8 -13 5.57 2.97 -12 -8 -13 14.73 5.07 -12 -8 -13 12.05 4.63 -12 -8 -13 15.78 5.20 12 8 13 8.04 2.59 12 -8 13 7.47 2.19 12 8 13 10.73 2.71 12 8 13 7.51 2.81 -12 8 -13 9.59 2.63 12 8 14 95.73 8.67 12 -8 14 91.92 7.24 -12 -8 -14 98.51 12.31 12 -8 14 105.86 7.82 12 8 14 75.70 7.96 12 -8 14 102.23 8.19 12 8 14 119.36 8.63 -12 -8 -14 96.57 10.40 12 8 15 23.90 3.82 12 -8 15 21.20 2.95 -12 -8 -15 25.47 6.85 12 -8 15 28.61 3.41 -12 -8 -15 24.69 5.38 12 -8 15 24.06 3.49 12 8 15 31.18 3.91 12 8 15 22.13 3.55 12 8 16 94.56 7.50 12 -8 16 84.47 6.25 -12 -8 -16 122.82 14.91 12 -8 16 104.12 6.61 12 8 16 120.14 7.41 -12 -8 -16 121.10 12.00 -12 8 -17 -0.19 0.70 12 -8 17 0.56 0.60 12 9 -15 108.33 7.29 -12 9 14 1.01 0.71 -12 9 14 1.80 0.90 12 9 -14 1.77 1.08 -12 -9 13 59.92 4.05 -12 9 13 55.94 4.47 12 9 -13 53.37 4.50 -12 9 13 59.84 4.78 12 9 -13 66.22 6.21 -12 9 12 292.29 16.20 -12 9 12 305.21 16.64 -12 -9 12 318.78 15.75 -12 -9 11 1.23 0.98 -12 -9 11 1.79 1.01 -12 9 11 1.69 1.18 -12 9 11 0.91 1.11 -12 9 11 0.59 0.93 12 9 -11 1.04 1.25 12 9 -11 1.75 1.31 -12 -9 10 314.59 16.15 -12 -9 10 285.73 15.92 12 9 -10 316.70 18.51 -12 9 10 248.19 15.58 -12 9 10 300.95 16.84 12 9 -10 300.91 16.63 12 9 -10 321.40 19.20 -12 -9 9 53.70 5.57 -12 -9 9 50.89 5.36 -12 -9 9 56.20 5.44 -12 -9 9 59.15 6.26 12 9 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2.49 13 -6 2 9.91 3.55 -13 -6 -2 8.38 2.62 -13 -6 -2 13.02 3.48 13 -6 2 6.94 2.97 -13 6 -2 13.37 3.93 -13 -6 -2 3.65 4.30 -13 6 -2 7.62 3.06 -13 -6 -2 9.82 4.48 -13 6 -2 9.79 3.12 13 6 2 8.63 3.75 13 6 2 15.96 4.11 -13 -6 -2 9.81 3.82 13 6 2 10.47 4.36 -13 6 -2 8.29 3.20 13 6 2 10.32 3.65 13 6 3 1.82 1.75 -13 6 -3 2.14 1.84 -13 -6 -3 2.33 2.62 13 6 3 1.98 2.37 -13 6 -3 1.82 1.85 13 6 3 1.49 1.35 -13 -6 -3 4.70 2.47 -13 -6 -3 0.31 1.12 13 -6 3 2.04 1.83 -13 -6 -3 4.09 2.20 -13 -6 -3 5.29 2.39 13 -6 3 2.26 1.84 -13 6 -3 2.64 2.15 -13 -6 -3 3.53 3.78 -13 -6 -3 2.16 2.76 -13 6 -3 3.33 2.40 13 -6 3 7.54 2.46 -13 6 -3 3.13 1.76 13 6 3 2.73 2.22 -13 6 -4 185.08 14.64 13 6 4 212.61 18.24 13 6 4 187.52 15.30 -13 -6 -4 207.96 17.15 -13 6 -4 163.97 14.40 -13 -6 -4 220.63 14.37 -13 -6 -4 224.04 16.53 -13 -6 -4 200.35 13.54 13 -6 4 189.36 15.80 -13 -6 -4 218.04 16.12 13 -6 4 197.51 15.21 -13 -6 -4 222.41 15.25 -13 -6 -4 177.16 19.03 13 6 4 208.01 15.16 -13 6 -4 222.93 15.83 -13 6 -4 161.80 13.94 13 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5 996.55 44.06 -14 -6 5 1134.92 53.55 -14 6 5 901.07 44.21 -14 6 5 910.02 43.70 14 6 -5 829.16 44.97 14 6 -5 782.84 44.42 -14 -6 5 901.83 43.42 -14 -6 5 955.29 48.79 14 -6 -4 11.08 3.37 -14 -6 4 12.71 3.27 14 -6 -4 9.57 3.46 -14 -6 4 21.43 6.80 -14 -6 4 15.23 4.04 -14 6 4 8.61 3.12 -14 6 4 7.19 2.90 -14 6 4 12.25 3.76 14 6 -4 15.63 4.40 14 6 -4 12.82 3.95 -14 -6 4 11.26 4.88 -14 -6 4 8.68 3.42 14 -6 -3 276.81 19.32 -14 -6 3 316.53 19.06 14 -6 -3 307.36 20.57 14 6 -3 281.73 20.83 -14 6 3 266.04 18.67 -14 -6 3 332.82 20.34 -14 -6 3 338.36 26.39 -14 6 3 321.38 20.55 -14 6 3 286.84 19.19 14 6 -3 279.60 20.59 14 6 -3 288.33 20.23 -14 -6 3 270.80 19.92 -14 6 3 263.29 17.90 -14 -6 3 267.68 22.90 14 -6 -2 62.56 8.02 14 -6 -2 62.52 8.30 -14 -6 2 43.88 9.96 -14 6 2 62.08 7.83 -14 -6 2 77.09 8.85 14 6 -2 54.36 8.10 -14 6 2 80.65 9.14 -14 6 2 66.40 8.00 14 6 -2 76.97 9.84 14 6 -2 51.76 8.05 14 6 -2 65.70 8.34 -14 6 2 65.10 7.54 -14 -6 2 62.33 10.37 14 -6 -1 60.83 7.83 14 -6 -1 54.51 7.70 -14 -6 1 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35.12 5.39 -14 -6 -5 25.07 4.99 14 6 5 17.24 4.56 -14 6 -6 16.92 4.02 14 6 6 18.37 5.15 -14 -6 -6 17.72 4.71 -14 6 -6 19.49 4.34 14 6 6 23.66 4.57 -14 -6 -6 19.86 4.01 -14 -6 -6 26.82 4.72 14 6 6 18.16 3.60 14 6 6 28.63 5.12 14 -6 6 21.01 4.58 14 -6 6 27.38 4.82 14 -6 6 21.38 4.54 14 6 6 21.25 4.51 -14 6 -6 28.82 5.10 14 -6 6 22.18 4.42 -14 -6 -6 24.44 6.00 -14 6 -6 21.06 4.30 14 -6 6 26.10 4.59 -14 -6 -6 16.31 4.40 -14 6 -6 22.13 4.42 14 6 6 13.99 4.35 -14 6 -7 378.96 22.91 14 6 7 397.48 26.52 14 6 7 392.25 22.59 -14 -6 -7 378.81 24.49 -14 6 -7 373.77 23.21 14 -6 7 387.95 23.31 14 -6 7 400.16 21.83 -14 -6 -7 436.12 23.57 -14 -6 -7 460.94 24.62 14 6 7 357.97 21.13 14 6 7 345.62 22.61 14 -6 7 396.33 24.01 14 -6 7 366.04 22.28 -14 -6 -7 343.63 27.43 14 6 7 412.41 24.33 -14 6 -7 450.51 24.26 14 -6 7 399.83 23.38 14 -6 7 387.87 22.51 -14 -6 -7 315.76 21.92 -14 -6 -7 364.36 25.63 -14 6 -7 429.38 23.22 14 6 7 357.23 24.31 -14 6 -8 21.98 4.50 14 6 8 21.22 5.44 -14 -6 -8 14.48 4.16 -14 6 -8 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115.26 9.10 -14 6 -14 36.15 4.93 14 -6 14 25.84 3.77 14 6 14 26.05 4.77 -14 -6 -14 39.75 8.96 -14 -6 -14 38.47 6.93 14 6 14 25.16 4.69 -14 6 -14 45.23 5.59 14 6 14 23.86 3.77 -14 6 -14 33.35 4.92 14 6 14 29.92 4.96 -14 -6 -14 38.96 6.29 -14 -6 -15 428.39 25.73 -14 6 -15 409.12 20.03 14 6 15 361.11 20.22 -14 -6 -15 428.69 30.15 14 6 15 290.34 19.48 14 -6 15 347.82 18.70 14 6 15 278.88 17.22 -14 6 -15 319.92 19.30 14 6 15 365.71 19.50 -14 -6 -15 406.15 23.90 -14 6 -16 2.25 1.52 14 6 16 2.20 1.71 -14 -6 -16 2.00 5.24 14 6 16 3.30 1.91 -14 -6 -16 0.63 2.97 14 -6 16 1.75 1.22 -14 6 -16 2.45 1.61 -14 -6 -16 3.63 2.98 -14 -6 -17 84.63 11.97 -14 6 -17 52.87 4.90 14 6 17 44.72 4.76 -14 -6 -17 81.30 16.05 14 6 17 41.08 4.79 -14 6 -17 57.16 5.37 -14 -6 -17 74.54 9.84 14 -6 17 45.34 4.47 -14 -6 -18 13.25 7.67 -14 7 16 83.35 5.80 -14 7 16 88.11 5.72 14 7 -15 271.10 13.63 -14 7 15 185.03 11.45 -14 7 15 220.84 12.04 -14 -7 15 217.76 11.62 -14 -7 15 235.37 11.69 -14 7 15 220.31 11.97 14 7 -15 294.94 14.79 14 7 -14 7.47 2.14 -14 -7 14 11.58 2.16 -14 -7 14 9.79 1.90 -14 7 14 6.83 1.73 -14 7 14 6.58 1.68 -14 7 14 8.52 1.93 14 7 -14 9.53 1.96 14 7 -14 12.62 2.94 -14 -7 13 291.59 16.01 -14 -7 13 299.20 16.25 14 7 -13 350.65 17.59 -14 -7 13 312.89 15.90 -14 7 13 269.78 15.75 -14 7 13 280.44 16.06 -14 7 13 307.71 16.52 -14 -7 13 278.39 15.64 14 7 -13 361.44 18.24 -14 -7 12 172.26 11.11 -14 -7 12 187.11 11.83 14 7 -12 204.16 13.03 -14 -7 12 187.40 11.14 -14 7 12 158.52 10.92 -14 7 12 162.22 11.12 -14 7 12 166.63 11.39 -14 -7 12 179.88 11.25 14 7 -12 178.10 12.40 14 7 -11 3.50 1.62 -14 -7 11 1.04 1.27 -14 -7 11 2.18 1.31 14 -7 -11 1.29 1.11 -14 -7 11 0.88 1.31 -14 -7 11 1.87 1.49 -14 7 11 2.62 1.42 -14 7 11 1.04 1.27 -14 7 11 1.70 1.67 14 7 -11 2.51 1.76 14 7 -11 1.79 1.20 14 7 -11 3.28 2.08 -14 -7 10 95.98 8.32 -14 -7 10 87.23 7.55 14 -7 -10 75.08 7.48 -14 -7 10 109.41 9.22 14 7 -10 99.26 9.53 -14 -7 10 99.08 7.90 -14 7 10 83.45 7.70 -14 7 10 79.23 7.45 -14 7 10 78.27 6.65 -14 7 10 92.35 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7 6 106.04 9.19 -14 7 6 94.08 9.75 14 7 -6 96.28 10.13 14 7 -6 93.64 10.14 -14 7 6 80.58 9.19 -14 -7 5 47.08 6.30 -14 -7 5 59.57 8.19 -14 -7 5 46.37 5.75 14 -7 -5 30.52 5.12 -14 7 5 35.54 5.02 -14 -7 5 47.30 6.48 -14 -7 5 54.57 9.02 -14 7 5 42.89 6.18 -14 7 5 39.50 5.05 -14 7 5 47.22 5.97 -14 7 5 36.84 6.14 14 7 -5 46.52 6.96 -14 7 5 41.22 6.48 14 7 -5 41.80 6.61 -14 -7 4 29.14 5.36 -14 -7 4 30.23 6.46 -14 -7 4 26.38 4.45 14 -7 -4 20.45 4.28 -14 -7 4 33.15 7.47 -14 7 4 24.79 4.22 -14 -7 4 31.70 5.26 -14 7 4 30.34 5.12 -14 7 4 28.03 4.61 -14 7 4 28.74 5.64 14 7 -4 23.35 5.10 14 7 -4 19.22 4.63 -14 -7 3 75.32 9.11 -14 -7 3 94.28 11.41 14 -7 -3 64.17 7.76 -14 7 3 59.93 7.12 -14 -7 3 84.28 8.99 14 7 -3 65.46 8.68 -14 -7 3 110.42 13.49 -14 7 3 81.04 8.51 -14 7 3 72.13 9.15 -14 7 3 91.83 8.88 14 7 -3 82.28 9.58 14 7 -3 74.62 8.67 14 -7 -2 62.07 8.07 14 -7 -2 49.18 6.75 -14 -7 2 50.75 9.99 -14 7 2 53.75 6.72 -14 -7 2 79.76 8.81 14 7 -2 60.61 8.20 -14 7 2 60.49 7.39 -14 7 2 72.63 8.01 14 7 -2 79.68 9.23 14 7 -2 74.14 9.00 14 7 -2 57.52 7.38 -14 -7 2 45.60 7.69 -14 -7 2 59.64 9.50 14 -7 -1 376.44 24.24 14 -7 -1 340.28 22.33 -14 -7 1 380.45 29.02 -14 7 1 381.18 22.51 14 7 -1 394.85 24.95 -14 -7 1 388.07 23.98 -14 7 1 425.70 23.88 -14 7 1 414.31 23.60 14 7 -1 428.38 26.01 -14 -7 1 387.90 27.22 14 -7 0 10.41 3.42 14 -7 0 9.31 3.09 -14 -7 0 7.33 4.83 -14 -7 0 8.34 3.63 -14 7 0 8.13 2.86 -14 7 0 19.03 4.11 14 7 0 10.16 3.43 -14 7 0 11.21 3.41 14 7 0 21.05 5.05 14 7 0 13.04 3.98 -14 -7 0 9.48 4.32 -14 7 0 9.39 2.72 14 -7 1 137.95 12.71 14 -7 1 162.24 13.54 14 -7 1 137.05 11.74 -14 -7 -1 111.56 15.00 14 7 1 151.79 13.09 -14 7 -1 175.75 12.76 -14 -7 -1 143.13 12.99 -14 7 -1 163.00 12.69 14 7 1 175.75 15.48 14 7 1 126.23 12.57 -14 7 -1 177.96 12.09 -14 -7 -1 110.73 13.78 14 -7 2 114.24 10.96 14 -7 2 112.86 10.97 -14 -7 -2 83.30 12.64 14 7 2 105.97 10.39 -14 7 -2 119.38 10.27 -14 -7 -2 70.35 9.32 -14 7 -2 117.30 10.32 14 7 2 115.28 12.42 14 7 2 106.22 10.79 -14 7 -2 122.27 9.74 -14 -7 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11.82 -14 7 -10 178.70 12.90 -14 -7 -10 141.71 12.52 14 7 10 148.48 12.65 14 -7 10 192.85 13.03 14 -7 10 175.64 11.79 -14 -7 -10 234.94 15.95 -14 7 -10 159.39 12.52 14 -7 10 186.42 12.74 -14 -7 -10 164.74 14.62 -14 7 -10 196.89 12.57 -14 7 -11 172.19 12.32 14 7 11 185.03 14.46 -14 -7 -11 144.54 12.42 14 7 11 174.13 12.08 14 -7 11 167.84 12.00 14 7 11 175.02 12.50 -14 -7 -11 168.47 14.53 14 7 11 134.39 11.90 14 -7 11 177.84 12.23 -14 7 -12 8.22 2.57 14 7 12 9.29 3.07 -14 -7 -12 8.60 2.84 -14 -7 -12 6.91 4.50 14 7 12 4.54 2.14 14 -7 12 9.70 2.49 -14 -7 -12 10.57 3.81 -14 -7 -12 15.01 4.37 14 -7 12 11.64 2.74 14 7 12 8.85 2.64 14 -7 12 7.90 2.24 -14 -7 -13 123.09 11.98 14 -7 13 113.66 8.07 14 7 13 100.46 8.15 -14 7 -13 93.80 8.62 -14 -7 -13 130.28 14.65 14 7 13 78.53 8.34 14 7 13 115.64 8.67 -14 7 -13 126.17 9.40 14 7 13 125.65 10.15 -14 -7 -13 98.85 9.74 -14 -7 -14 132.02 12.98 14 -7 14 136.10 8.19 14 7 14 107.42 8.33 -14 7 -14 99.18 8.78 -14 -7 -14 154.65 16.32 14 7 14 95.52 8.91 14 -7 14 145.25 9.19 14 7 14 124.42 8.72 14 7 14 136.01 9.97 -14 7 -14 162.52 10.43 -14 -7 -14 122.42 10.89 -14 7 -15 6.39 2.09 -14 -7 -15 6.95 4.86 14 -7 15 6.15 1.62 -14 -7 -15 6.97 3.86 14 7 15 6.78 1.81 -14 7 -15 8.74 2.25 14 7 15 5.67 1.71 -14 -7 -16 113.38 12.96 -14 -7 -16 104.66 16.21 -14 7 -16 94.70 6.35 -14 8 14 207.09 11.72 -14 8 14 249.48 12.20 -14 8 13 30.36 3.30 -14 8 13 26.26 3.04 -14 -8 13 34.85 3.23 14 8 -13 31.15 3.30 -14 8 12 77.21 6.08 -14 -8 12 96.79 6.38 14 8 -12 92.19 7.07 -14 -8 12 83.20 5.87 -14 8 12 83.07 6.38 14 8 -12 89.89 7.73 -14 -8 11 4.09 1.47 -14 -8 11 5.82 1.65 -14 8 11 3.28 1.35 -14 -8 11 4.19 1.31 14 8 -11 4.76 1.84 14 8 -11 5.79 2.11 -14 -8 10 124.67 8.68 -14 -8 10 135.52 9.23 14 8 -10 147.32 10.80 -14 -8 10 145.15 9.22 -14 8 10 125.51 8.98 -14 -8 10 122.21 8.43 14 8 -10 126.04 9.11 14 8 -10 146.93 11.11 14 8 -9 12.52 3.15 14 8 -9 9.67 2.46 14 8 -9 12.03 3.24 14 -8 -9 6.98 1.97 -14 -8 9 12.43 2.39 -14 -8 9 12.96 2.82 -14 -8 9 10.59 2.42 -14 8 9 9.45 2.29 -14 8 9 9.98 2.57 -14 8 9 8.37 1.90 -14 -8 9 13.11 2.57 14 8 -8 546.32 26.76 14 8 -8 514.61 27.19 -14 8 8 424.46 24.48 14 -8 -8 442.61 24.64 -14 -8 8 444.14 23.82 -14 -8 8 573.03 26.65 14 8 -8 549.24 27.84 -14 -8 8 550.71 25.33 -14 8 8 439.34 23.23 -14 8 8 460.34 24.71 -14 8 8 533.38 25.98 -14 -8 8 478.94 23.60 -14 -8 8 527.82 25.11 14 8 -7 8.48 2.82 14 8 -7 11.45 3.05 14 8 -7 7.57 2.64 -14 8 7 10.43 2.73 14 -8 -7 9.87 2.52 -14 -8 7 10.15 2.31 -14 -8 7 11.44 2.74 -14 8 7 7.53 2.27 -14 8 7 9.03 2.69 -14 8 7 11.16 2.33 -14 -8 7 9.68 2.64 -14 -8 7 9.26 2.40 14 8 -6 110.76 10.12 -14 8 6 98.37 9.42 14 8 -6 92.22 9.41 14 -8 -6 90.34 8.63 -14 -8 6 109.48 8.47 14 8 -6 110.28 10.54 -14 -8 6 133.85 9.78 -14 8 6 110.56 9.13 -14 8 6 100.69 7.93 -14 8 6 118.08 9.82 -14 -8 6 118.42 8.94 -14 -8 6 124.22 9.89 14 8 -5 16.37 4.04 14 8 -5 15.84 3.63 -14 8 5 15.74 3.70 14 -8 -5 8.91 2.64 -14 -8 5 16.00 2.98 -14 8 5 17.75 3.48 -14 -8 5 15.32 3.29 -14 -8 5 17.55 3.78 -14 8 5 21.58 4.17 -14 8 5 13.52 2.68 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425.04 22.40 -15 6 -12 508.38 24.02 15 6 12 360.95 21.56 -15 6 -12 418.47 22.65 15 6 12 447.21 24.65 -15 -6 -12 385.68 24.49 -15 6 -13 7.77 2.33 15 -6 13 6.26 1.89 -15 6 -13 2.90 1.83 15 6 13 5.53 2.02 -15 6 -13 8.05 2.53 -15 -6 -13 8.19 3.70 -15 -6 -13 9.20 4.98 15 6 13 3.52 1.85 15 -6 13 4.75 1.90 15 6 13 2.96 1.68 -15 6 -13 3.83 1.84 15 6 13 6.65 2.43 -15 -6 -13 6.32 3.07 -15 -6 -14 97.96 11.09 -15 6 -14 116.83 8.20 15 -6 14 69.92 5.82 15 6 14 61.78 6.04 -15 6 -14 50.87 5.96 -15 -6 -14 82.86 12.44 15 6 14 57.11 6.53 15 6 14 68.04 5.95 15 -6 14 72.19 6.77 -15 6 -14 98.90 7.86 15 6 14 95.77 7.95 -15 -6 -14 91.93 9.92 -15 6 -15 13.03 2.66 -15 6 -15 2.98 1.58 15 -6 15 7.45 2.06 -15 6 -15 14.34 2.84 15 6 15 5.36 1.61 -15 -6 -15 11.98 4.12 -15 -6 -15 10.50 6.34 15 6 15 8.60 2.29 -15 -6 -15 13.26 4.85 -15 -6 -16 160.38 16.05 15 6 16 65.61 5.36 15 -6 16 78.21 5.37 -15 6 -16 124.92 7.20 15 7 -15 141.83 8.59 -15 7 14 8.68 1.53 -15 7 14 9.75 1.64 -15 -7 14 9.06 1.55 -15 7 14 9.83 1.69 15 7 -14 13.46 2.54 -15 7 13 207.90 10.95 -15 7 13 158.29 10.00 -15 -7 13 163.02 9.75 -15 7 13 187.48 10.47 15 7 -13 229.09 11.51 -15 -7 13 189.23 9.81 -15 -7 13 207.69 10.78 -15 -7 12 253.20 13.72 -15 -7 12 293.28 14.61 15 7 -12 282.30 15.30 -15 -7 12 262.10 13.32 -15 7 12 224.18 13.47 -15 7 12 238.12 13.69 -15 7 12 268.19 14.37 15 7 -12 285.62 16.30 -15 -7 11 18.39 2.94 -15 -7 11 18.22 2.84 -15 -7 11 22.63 3.45 -15 -7 11 18.86 2.71 -15 7 11 16.20 2.79 -15 7 11 14.75 2.63 -15 7 11 19.13 3.16 15 7 -11 15.96 3.26 15 7 -11 18.63 2.79 15 7 -11 16.03 3.44 -15 -7 10 165.56 10.80 -15 -7 10 155.64 10.17 -15 -7 10 171.85 11.39 15 7 -10 172.46 12.28 -15 -7 10 159.14 9.85 -15 7 10 158.34 10.45 -15 7 10 151.49 10.24 -15 7 10 158.35 10.90 15 7 -10 150.91 10.64 15 7 -10 160.67 12.18 -15 -7 9 97.68 8.04 -15 -7 9 73.45 6.69 15 -7 -9 80.69 7.30 -15 -7 9 98.09 8.50 15 7 -9 95.19 8.96 -15 -7 9 86.35 6.84 -15 7 9 83.47 7.23 -15 7 9 86.31 7.19 -15 7 9 88.41 7.79 15 7 -9 87.17 7.94 15 7 -9 87.52 8.70 -15 7 8 5.73 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26.06 -15 7 4 485.59 27.39 -15 -7 4 514.21 25.74 -15 -7 4 557.44 29.54 15 7 -3 101.53 10.17 15 -7 -3 101.99 9.89 15 -7 -3 81.52 8.50 -15 7 3 75.57 7.58 -15 -7 3 105.01 8.91 15 7 -3 101.34 10.24 -15 -7 3 140.30 13.89 -15 7 3 103.47 9.16 -15 7 3 88.77 9.56 -15 -7 3 83.21 8.39 -15 -7 3 111.47 11.21 15 7 -2 25.00 5.02 15 7 -2 27.27 5.39 15 7 -2 25.49 5.14 15 -7 -2 22.39 4.65 15 -7 -2 20.25 4.21 -15 -7 2 34.13 7.18 -15 -7 2 26.99 4.51 -15 7 2 23.18 4.11 -15 7 2 29.52 4.83 -15 7 2 20.56 4.87 -15 -7 2 25.92 4.79 -15 -7 2 23.61 5.67 15 -7 -1 175.79 14.24 15 -7 -1 168.04 13.03 -15 7 1 167.91 12.55 15 7 -1 190.47 14.83 -15 -7 1 205.51 13.76 -15 -7 1 225.25 19.00 -15 7 1 193.15 13.68 15 7 -1 232.82 15.99 -15 -7 1 160.61 13.44 -15 -7 1 200.82 16.62 15 -7 0 251.14 17.43 15 -7 0 245.27 17.27 15 -7 0 202.64 15.26 -15 -7 0 253.25 21.18 -15 7 0 246.01 15.68 15 7 0 231.54 16.93 -15 -7 0 269.69 16.60 15 -7 0 241.95 14.54 -15 7 0 266.46 16.68 15 7 0 301.53 19.31 15 7 0 225.56 17.14 -15 -7 0 249.79 19.37 15 -7 1 17.39 4.07 15 -7 1 15.27 3.82 -15 7 -1 20.29 3.84 -15 -7 -1 21.85 6.37 15 -7 1 17.13 3.20 -15 -7 -1 12.27 3.85 -15 7 -1 17.67 3.66 15 7 1 14.41 3.71 15 7 1 17.89 4.61 15 7 1 14.22 4.00 -15 -7 -1 10.45 4.42 15 -7 2 300.33 19.69 -15 7 -2 316.44 18.75 -15 -7 -2 232.48 21.58 15 7 2 315.05 19.31 -15 7 -2 326.46 18.59 -15 -7 -2 290.88 18.56 15 -7 2 317.60 17.70 15 7 2 353.69 22.15 15 7 2 293.51 19.65 -15 -7 -2 222.96 19.89 15 7 3 2.44 1.99 15 -7 3 1.23 1.36 -15 7 -3 2.40 1.80 -15 -7 -3 0.70 3.44 15 -7 3 1.46 1.37 -15 7 -3 1.98 1.84 15 7 3 2.11 1.72 15 7 3 1.57 1.74 15 7 3 2.88 2.01 -15 7 -3 0.54 1.80 -15 -7 -3 -0.57 3.11 15 -7 4 4.01 1.92 15 -7 4 6.74 2.52 -15 -7 -4 2.77 3.64 15 -7 4 5.09 1.95 -15 7 -4 6.92 2.41 -15 7 -4 5.05 2.33 -15 -7 -4 2.82 3.06 -15 7 -4 2.12 2.04 -15 7 -4 3.88 2.14 15 7 4 7.40 3.28 15 7 4 8.15 2.79 -15 7 -5 117.02 9.75 15 7 5 104.17 11.20 15 7 5 115.34 9.79 -15 7 -5 81.31 10.07 15 -7 5 111.13 9.96 15 -7 5 105.89 9.38 15 -7 5 107.04 8.86 -15 -7 -5 56.79 10.10 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241.46 13.71 15 7 10 231.32 13.71 -15 7 -10 218.83 13.46 -15 -7 -10 170.78 15.02 15 -7 10 217.88 13.32 -15 7 -10 213.64 13.63 -15 -7 -10 146.94 12.88 15 -7 10 229.11 12.38 -15 -7 -11 63.78 8.46 15 -7 11 64.76 6.10 -15 7 -11 69.23 6.60 -15 -7 -11 56.10 9.45 15 -7 11 69.24 6.42 15 7 11 63.36 6.47 -15 7 -11 71.68 6.84 15 7 11 85.29 8.51 -15 -7 -11 50.86 6.56 15 -7 12 12.39 2.42 -15 -7 -12 11.25 3.90 -15 7 -12 10.66 2.53 -15 -7 -12 7.96 4.34 15 -7 12 16.83 2.94 15 7 12 9.89 2.52 -15 7 -12 15.72 3.07 -15 -7 -12 11.71 3.10 15 7 12 20.63 3.91 -15 -7 -13 20.82 5.24 15 -7 13 17.04 2.49 -15 7 -13 20.87 3.26 -15 -7 -13 18.26 6.42 15 -7 13 18.73 2.90 15 7 13 15.58 2.72 -15 7 -13 19.78 3.32 15 7 13 18.42 3.51 -15 -7 -14 282.98 18.75 -15 7 -14 162.53 10.16 -15 -7 -14 305.03 22.87 -15 7 -14 301.70 12.79 15 7 14 148.65 9.94 15 7 14 162.21 9.40 15 -7 14 106.37 8.74 -15 8 12 32.56 3.04 15 8 -12 32.26 3.59 15 8 -11 296.20 14.45 -15 8 11 214.27 12.06 -15 -8 11 219.15 11.53 15 8 -11 308.35 14.10 -15 -8 11 222.36 11.82 -15 8 10 4.34 1.32 -15 -8 10 4.02 1.35 -15 -8 10 5.49 1.32 -15 -8 10 5.42 1.32 15 8 -10 6.96 1.95 15 8 -10 5.18 1.34 15 8 -10 4.52 1.78 -15 8 9 100.61 7.18 -15 -8 9 106.13 7.48 15 8 -9 106.59 8.48 -15 -8 9 95.89 6.69 -15 -8 9 89.30 6.62 15 8 -9 112.20 7.76 15 8 -9 103.71 8.33 -15 -8 8 48.52 4.65 -15 8 8 46.79 4.81 -15 -8 8 50.97 5.25 15 8 -8 57.81 6.24 -15 -8 8 43.13 4.34 -15 8 8 44.39 4.97 15 8 -8 55.99 5.61 15 8 -8 47.04 5.50 -15 -8 7 55.42 5.42 -15 -8 7 69.23 6.48 15 8 -7 57.33 6.54 -15 -8 7 53.80 5.09 -15 8 7 58.99 5.56 -15 8 7 62.31 6.06 15 8 -7 60.02 6.32 15 8 -7 54.26 6.10 15 8 -6 17.62 3.56 15 8 -6 19.75 3.63 15 -8 -6 16.68 3.12 -15 -8 6 24.30 3.39 -15 8 6 16.63 3.26 -15 8 6 26.38 3.74 -15 8 6 23.75 3.76 -15 -8 6 26.24 3.86 15 8 -5 311.37 18.69 -15 8 5 264.57 17.62 15 -8 -5 260.11 16.94 -15 -8 5 342.54 17.08 -15 8 5 308.03 17.28 -15 8 5 340.81 18.34 -15 -8 5 320.69 17.85 15 8 -4 8.84 2.84 15 8 -4 10.34 2.87 -15 8 4 10.78 2.88 15 -8 -4 7.84 2.35 15 -8 -4 5.58 2.04 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5.26 1.93 -21 2 -1 3.17 1.32 -21 2 -2 20.13 3.23 -21 2 -2 13.93 2.52 21 -2 2 19.54 2.75 -21 -2 -2 20.95 3.40 21 2 2 22.26 2.70 21 -2 2 19.80 2.46 -21 2 -3 1.04 1.23 -21 2 -3 0.89 1.11 21 -2 3 0.79 0.77 21 2 3 1.24 0.90 -21 -2 -3 0.25 1.31 -21 2 -4 360.53 18.16 -21 2 -4 397.09 18.05 21 -2 4 387.55 17.29 21 2 5 2.66 1.18 -21 2 -5 4.03 1.39 21 2 6 97.00 5.77 21 -2 6 12.61 2.65 21 3 -5 4.41 1.17 21 -3 -5 3.50 1.06 -21 3 4 250.20 12.87 21 3 -4 262.10 13.19 -21 3 3 71.14 5.14 -21 -3 3 57.63 4.76 21 -3 -3 66.02 4.85 -21 3 2 29.33 3.15 21 -3 -2 28.05 3.02 -21 -3 2 22.90 2.93 21 3 -2 25.40 3.01 21 -3 -2 19.78 2.64 21 -3 -1 97.10 5.98 -21 3 1 91.07 5.90 -21 3 1 60.76 5.11 -21 3 1 51.48 4.84 -21 -3 1 67.19 5.55 21 3 -1 87.95 5.89 21 -3 -1 70.25 5.22 -21 3 0 111.53 7.00 -21 3 0 109.15 6.94 -21 -3 0 116.10 7.58 21 3 0 119.04 7.11 21 -3 0 104.02 6.55 -21 3 -1 6.00 1.50 -21 -3 -1 2.75 1.17 -21 3 -1 3.58 1.37 -21 3 -1 2.26 1.25 21 3 1 4.56 1.22 -21 -3 -1 4.38 1.62 -21 3 -2 113.11 7.14 -21 -3 -2 108.01 7.59 -21 3 -3 34.81 3.60 21 -3 3 39.64 3.45 -21 -3 -3 36.48 4.13 -21 3 -4 0.60 0.79 -21 -3 -4 0.78 1.03 -21 3 -5 75.02 5.50 TITL exp_1546 4,4'-dimetylo-2,2'-bpy [W(CN)8] in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 17.322103 10.989259 22.604200 90.0000 90.1583 90.0000 ZERR 8.00 0.000095 0.000060 0.000126 0.0000 0.0005 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N W UNIT 160.00 96.00 80.00 8.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 79531 _shelx_fab_file ; 0 0 2 -18.90 0.00 0 0 4 -29.98 0.00 0 0 6 19.42 0.00 0 0 8 7.86 0.00 0 0 10 -5.94 0.00 0 0 12 -7.28 0.00 0 0 14 9.12 0.00 0 0 16 -2.13 0.00 0 0 18 -3.48 0.00 0 0 20 4.65 0.00 0 0 22 -3.69 0.00 0 0 24 0.85 0.00 0 0 26 1.94 0.00 0 0 28 -1.80 0.00 0 1 1 26.65 0.00 0 1 2 15.09 0.00 0 1 3 -38.72 0.00 0 1 4 -0.01 0.00 0 1 5 2.91 0.00 0 1 6 -15.82 0.00 0 1 7 14.39 0.00 0 1 8 8.13 0.00 0 1 9 -0.61 0.00 0 1 10 4.13 0.00 0 1 11 -8.50 0.00 0 1 12 -5.29 0.00 0 1 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0.00 5 1 28 0.06 0.00 6 1 28 -0.27 0.00 -6 2 28 1.26 0.00 -5 2 28 -1.03 0.00 -4 2 28 0.76 0.00 -3 2 28 0.22 0.00 4 2 28 -0.02 0.00 5 2 28 -0.87 0.00 6 2 28 -0.12 0.00 -5 3 28 0.47 0.00 -4 3 28 -0.50 0.00 -3 3 28 -0.22 0.00 -2 3 28 0.87 0.00 -1 3 28 -0.19 0.00 0 3 28 1.57 0.00 1 3 28 0.40 0.00 2 3 28 0.41 0.00 3 3 28 -0.03 0.00 4 3 28 -1.18 0.00 5 3 28 -0.25 0.00 -3 4 28 0.15 0.00 -2 4 28 -0.11 0.00 -1 4 28 1.38 0.00 0 4 28 0.73 0.00 1 4 28 0.88 0.00 2 4 28 0.21 0.00 3 4 28 -0.85 0.00 -3 0 29 1.47 0.00 -1 0 29 0.30 0.00 1 0 29 -0.78 0.00 3 0 29 -0.54 0.00 -4 1 29 1.37 0.00 -3 1 29 -0.44 0.00 -2 1 29 0.84 0.00 -1 1 29 0.11 0.00 0 1 29 -0.41 0.00 1 1 29 0.51 0.00 2 1 29 -0.58 0.00 3 1 29 0.46 0.00 -3 2 29 0.86 0.00 -2 2 29 -0.31 0.00 -1 2 29 -0.11 0.00 0 2 29 0.58 0.00 1 2 29 -0.31 0.00 2 2 29 1.05 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 110917) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.090 0.026 0.839 39 14 ' ' 2 0.910 -0.026 0.161 40 14 ' ' 3 0.590 0.474 0.339 39 14 ' ' 4 0.410 0.526 0.661 40 14 ' ' _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL exp_15464,4'-dimetylo-2,2'-bpy[w(cn)8]_a.res in P2(1)/n CELL 17.3221 10.9893 22.6042 90.00 90.16 90.00 SPGR P21/n # Solvent Accessible Volume = 155 # Electrons Found in S.A.V. = 55 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.898 0.940 0.147 ! 9.51 eA-3 C102 0.423 0.420 0.703 ! 5.82 eA-3 Q103 0.294 0.371 0.373 ! 0.93 eA-3 Q104 0.242 0.858 0.229 ! 0.92 eA-3 Q105 0.940 0.580 0.360 ! 0.89 eA-3 Q106 0.306 0.856 0.023 ! 0.88 eA-3 Q107 0.632 0.605 0.609 ! 0.87 eA-3 Q108 0.810 0.246 0.984 ! 0.82 eA-3 Q109 0.754 0.134 0.827 ! 0.82 eA-3 Q110 0.072 0.887 0.127 ! 0.81 eA-3 Q111 0.563 0.099 0.869 ! 0.81 eA-3 Q112 0.171 0.879 0.086 ! 0.77 eA-3 Q113 0.060 0.530 0.198 ! 0.77 eA-3 Q114 0.406 0.968 0.522 ! 0.76 eA-3 Q115 0.766 0.346 0.617 ! 0.75 eA-3 Q116 0.265 0.348 0.358 ! 0.74 eA-3 Q117 0.130 0.391 0.390 ! 0.72 eA-3 Q118 0.742 0.997 0.915 ! 0.71 eA-3 Q119 0.506 0.390 0.143 ! 0.71 eA-3 Q120 0.422 0.511 0.961 ! 0.69 eA-3 Q121 0.784 0.019 0.991 ! 0.69 eA-3 Q122 0.665 0.812 0.483 ! 0.69 eA-3 Q123 0.575 0.717 0.008 ! 0.68 eA-3 Q124 0.542 0.098 0.446 ! 0.68 eA-3 Q125 0.540 0.558 0.077 ! 0.67 eA-3 Q126 0.572 0.450 0.390 ! 0.67 eA-3 Q127 0.263 0.810 0.027 ! 0.66 eA-3 Q128 0.480 0.795 0.530 ! 0.66 eA-3 Q129 0.943 0.434 0.124 ! 0.66 eA-3 Q130 0.241 0.357 0.164 ! 0.66 eA-3 Q131 0.323 0.263 0.838 ! 0.65 eA-3 Q132 0.133 0.281 0.530 ! 0.65 eA-3 Q133 0.249 0.918 0.023 ! 0.64 eA-3 Q134 0.728 0.331 0.895 ! 0.64 eA-3 Q135 0.234 0.560 0.397 ! 0.64 eA-3 Q136 0.399 0.796 0.447 ! 0.63 eA-3 Q137 0.223 0.397 0.483 ! 0.62 eA-3 Q138 0.278 0.581 0.118 ! 0.62 eA-3 Q139 0.738 0.046 0.400 ! 0.61 eA-3 Q140 0.041 0.598 0.141 ! 0.61 eA-3 Q141 0.042 0.247 0.024 ! 0.61 eA-3 Q142 0.385 0.470 0.668 ! 0.60 eA-3 Q143 0.374 0.191 0.796 ! 0.60 eA-3 Q144 0.980 0.529 0.109 ! 0.60 eA-3 Q145 0.960 0.183 0.444 ! 0.59 eA-3 Q146 0.335 0.827 0.006 ! 0.59 eA-3 Q147 0.744 0.814 0.369 ! 0.59 eA-3 Q148 0.076 0.050 0.279 ! 0.59 eA-3 Q149 0.530 0.075 0.710 ! 0.58 eA-3 Q150 0.970 0.374 0.171 ! 0.57 eA-3 Q151 0.279 0.624 0.834 ! 0.57 eA-3 Q152 0.710 0.106 0.016 ! 0.56 eA-3 Q153 0.497 0.487 0.866 ! 0.56 eA-3 Q154 0.180 0.936 0.101 ! 0.56 eA-3 Q155 0.545 0.425 0.826 ! 0.55 eA-3 Q156 0.807 0.951 0.040 ! 0.55 eA-3 Q157 0.250 0.478 0.454 ! 0.55 eA-3 Q158 0.313 0.804 0.772 ! 0.55 eA-3 Q159 0.516 0.659 0.802 ! 0.54 eA-3 Q160 0.747 0.585 0.641 ! 0.54 eA-3 Q161 0.214 0.987 0.647 ! 0.54 eA-3 Q162 0.910 0.830 0.780 ! 0.54 eA-3 Q163 0.618 0.910 0.737 ! 0.53 eA-3 Q164 0.532 0.653 0.436 ! 0.53 eA-3 Q165 0.115 0.875 0.474 ! 0.52 eA-3 Q166 0.086 0.469 0.625 ! 0.52 eA-3 Q167 0.433 0.627 0.577 ! 0.52 eA-3 Q168 0.894 0.878 0.078 ! 0.51 eA-3 Q169 0.490 0.077 0.259 ! 0.50 eA-3 Q170 0.190 0.049 0.098 ! 0.50 eA-3 ) ; _shelx_fab_checksum 66700 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W1 W 0.24327(2) 0.36915(2) 0.42220(2) 0.00733(5) Uani 1 1 d . . . . . N9 N 0.26274(12) 0.1832(2) 0.62959(9) 0.0173(4) Uani 1 1 d . . . . . H9N H 0.288479 0.148661 0.600580 0.021 Uiso 1 1 calc R U . . . N18 N 0.42553(12) 0.4002(2) 0.38059(9) 0.0149(4) Uani 1 1 d . . . . . N25 N 0.08173(11) 0.01958(19) 0.54273(9) 0.0134(4) Uani 1 1 d . . . . . H25N H 0.083390 0.095834 0.554548 0.016 Uiso 1 1 calc R U . . . N31 N 0.01534(13) 0.1059(2) 0.63774(10) 0.0159(4) Uani 1 1 d . . . . . N34 N 0.40375(12) 0.9656(2) 0.52155(10) 0.0166(4) Uani 1 1 d . . . . . N45 N 0.44911(13) 1.0652(2) 0.62201(10) 0.0182(4) Uani 1 1 d . . . . . N48 N 0.12510(12) 0.2802(2) 0.52967(9) 0.0187(4) Uani 1 1 d . . . . . N50 N 0.06359(13) 0.4011(2) 0.37347(10) 0.0183(4) Uani 1 1 d . . . . . N52 N 0.22436(13) 0.0807(2) 0.38172(9) 0.0157(4) Uani 1 1 d . . . . . N54 N 0.25176(13) 0.36064(18) 0.27590(10) 0.0153(4) Uani 1 1 d . . . . . N56 N 0.23159(13) 0.6587(2) 0.38273(10) 0.0166(4) Uani 1 1 d . . . . . N15 N 0.25910(12) -0.0520(2) 0.60307(10) 0.0187(4) Uani 1 1 d . . . . . N58 N 0.33893(13) 0.1925(2) 0.51572(9) 0.0192(4) Uani 1 1 d . . . . . C57 C 0.23439(13) 0.5583(2) 0.39684(10) 0.0116(4) Uani 1 1 d . . . . . C61 C 0.28197(14) 0.4822(2) 0.49558(10) 0.0132(5) Uani 1 1 d . . . . . N60 N 0.30628(14) 0.5372(2) 0.53487(10) 0.0226(5) Uani 1 1 d . . . . . C53 C 0.22841(13) 0.1824(2) 0.39492(10) 0.0110(4) Uani 1 1 d . . . . . C19 C 0.36227(14) 0.3919(2) 0.39620(11) 0.0110(4) Uani 1 1 d . . . . . C51 C 0.12579(14) 0.3902(2) 0.39113(11) 0.0119(4) Uani 1 1 d . . . . . C28 C -0.07329(14) -0.0354(2) 0.71618(11) 0.0161(5) Uani 1 1 d . . . . . C49 C 0.16459(13) 0.3173(2) 0.49277(10) 0.0134(5) Uani 1 1 d . . . . . C27 C -0.04066(14) -0.0865(2) 0.66563(11) 0.0142(5) Uani 1 1 d . . . . . H27 H -0.048219 -0.170167 0.656664 0.017 Uiso 1 1 calc R U . . . C55 C 0.24947(14) 0.36472(19) 0.32646(10) 0.0097(5) Uani 1 1 d . . . . . C35 C 0.45553(14) 0.9013(2) 0.55331(11) 0.0149(5) Uani 1 1 d . . . . . C20 C 0.04082(13) -0.0616(2) 0.57505(11) 0.0141(5) Uani 1 1 d . . . . . C59 C 0.30806(13) 0.2538(2) 0.48159(10) 0.0130(5) Uani 1 1 d . . . . . C43 C 0.52948(16) 1.0746(2) 0.70870(12) 0.0202(5) Uani 1 1 d . . . . . H43 H 0.544368 1.118275 0.743159 0.024 Uiso 1 1 calc R U . . . C40 C 0.48216(14) 0.9572(2) 0.60950(11) 0.0149(5) Uani 1 1 d . . . . . C26 C 0.00308(13) -0.0131(2) 0.62861(10) 0.0131(5) Uani 1 1 d . . . . . C21 C 0.03811(14) -0.1814(2) 0.55594(11) 0.0144(5) Uani 1 1 d . . . . . H21 H 0.009344 -0.239398 0.577907 0.017 Uiso 1 1 calc R U . . . C42 C 0.56316(14) 0.9625(2) 0.69593(11) 0.0156(5) Uani 1 1 d . . . . . C39 C 0.37488(14) 0.9272(3) 0.46978(11) 0.0190(5) Uani 1 1 d . . . . . H39 H 0.337481 0.974993 0.449570 0.023 Uiso 1 1 calc R U . . . C41 C 0.53865(14) 0.9037(2) 0.64447(11) 0.0150(5) Uani 1 1 d . . . . . H41 H 0.560443 0.827634 0.633511 0.018 Uiso 1 1 calc R U . . . C10 C 0.21705(14) -0.0191(2) 0.65056(11) 0.0173(5) Uani 1 1 d . . . . . C5 C 0.17940(14) 0.1670(3) 0.71104(11) 0.0181(5) Uani 1 1 d . . . . . H5 H 0.149600 0.118559 0.737247 0.022 Uiso 1 1 calc R U . . . C36 C 0.48167(14) 0.7923(2) 0.53030(11) 0.0163(5) Uani 1 1 d . . . . . H36 H 0.517992 0.745185 0.551998 0.020 Uiso 1 1 calc R U . . . C6 C 0.18283(14) 0.2927(3) 0.71927(11) 0.0185(5) Uani 1 1 d . . . . . C11 C 0.17417(15) -0.1007(3) 0.68401(12) 0.0196(5) Uani 1 1 d . . . . . H11 H 0.145542 -0.073004 0.717164 0.023 Uiso 1 1 calc R U . . . C37 C 0.45532(15) 0.7508(2) 0.47574(12) 0.0183(5) Uani 1 1 d . . . . . C23 C 0.11805(16) -0.1302(2) 0.47349(12) 0.0179(6) Uani 1 1 d . . . . . H23 H 0.144754 -0.152146 0.438420 0.022 Uiso 1 1 calc R U . . . C29 C -0.06039(15) 0.0880(2) 0.72640(11) 0.0185(5) Uani 1 1 d . . . . . H29 H -0.081010 0.126249 0.760573 0.022 Uiso 1 1 calc R U . . . C4 C 0.21909(15) 0.1120(2) 0.66492(11) 0.0165(5) Uani 1 1 d . . . . . C46 C 0.62310(15) 0.9076(3) 0.73569(12) 0.0196(5) Uani 1 1 d . . . . . H46A H 0.668167 0.961387 0.737549 0.029 Uiso 1 1 calc R U . . . H46B H 0.638649 0.828133 0.720055 0.029 Uiso 1 1 calc R U . . . H46C H 0.601699 0.897333 0.775464 0.029 Uiso 1 1 calc R U . . . C8 C 0.26871(15) 0.3040(3) 0.63661(12) 0.0203(5) Uani 1 1 d . . . . . H8 H 0.299931 0.350254 0.610443 0.024 Uiso 1 1 calc R U . . . C44 C 0.47407(18) 1.1219(2) 0.67074(13) 0.0211(6) Uani 1 1 d . . . . . H44 H 0.452609 1.199192 0.679909 0.025 Uiso 1 1 calc R U . . . C22 C 0.07697(14) -0.2183(2) 0.50489(11) 0.0165(5) Uani 1 1 d . . . . . C13 C 0.21756(16) -0.2582(3) 0.62023(13) 0.0222(5) Uani 1 1 d . . . . . H13 H 0.219681 -0.341184 0.608555 0.027 Uiso 1 1 calc R U . . . C7 C 0.22980(18) 0.3607(2) 0.68151(14) 0.0210(6) Uani 1 1 d . . . . . H7 H 0.234740 0.446057 0.686973 0.025 Uiso 1 1 calc R U . . . C38 C 0.39918(15) 0.8191(3) 0.44586(12) 0.0195(5) Uani 1 1 d . . . . . H38 H 0.378173 0.790849 0.409499 0.023 Uiso 1 1 calc R U . . . C12 C 0.17347(15) -0.2237(3) 0.66854(12) 0.0203(5) Uani 1 1 d . . . . . C24 C 0.11998(14) -0.0118(2) 0.49316(11) 0.0170(5) Uani 1 1 d . . . . . H24 H 0.148258 0.047779 0.471841 0.020 Uiso 1 1 calc R U . . . C30 C -0.01686(16) 0.1549(3) 0.68593(12) 0.0188(5) Uani 1 1 d . . . . . H30 H -0.009750 0.239350 0.692956 0.023 Uiso 1 1 calc R U . . . C32 C -0.12153(18) -0.1108(3) 0.75787(13) 0.0233(6) Uani 1 1 d . . . . . H32A H -0.175131 -0.082418 0.756645 0.035 Uiso 1 1 calc R U . . . H32B H -0.101299 -0.102664 0.798206 0.035 Uiso 1 1 calc R U . . . H32C H -0.119472 -0.196454 0.745829 0.035 Uiso 1 1 calc R U . . . C16 C 0.12633(16) -0.3129(3) 0.70295(13) 0.0261(6) Uani 1 1 d . . . . . H16A H 0.150602 -0.326997 0.741562 0.039 Uiso 1 1 calc R U . . . H16B H 0.123268 -0.389869 0.681178 0.039 Uiso 1 1 calc R U . . . H16C H 0.074224 -0.280290 0.708675 0.039 Uiso 1 1 calc R U . . . C33 C 0.07443(17) -0.3481(3) 0.48569(13) 0.0228(6) Uani 1 1 d . . . . . H33A H 0.119632 -0.391138 0.501360 0.034 Uiso 1 1 calc R U . . . H33B H 0.074696 -0.352133 0.442384 0.034 Uiso 1 1 calc R U . . . H33C H 0.027295 -0.386384 0.500727 0.034 Uiso 1 1 calc R U . . . C47 C 0.4873(2) 0.6368(2) 0.44954(14) 0.0283(7) Uani 1 1 d . . . . . H47A H 0.539163 0.622135 0.465378 0.042 Uiso 1 1 calc R U . . . H47B H 0.489914 0.645199 0.406433 0.042 Uiso 1 1 calc R U . . . H47C H 0.453681 0.568101 0.459615 0.042 Uiso 1 1 calc R U . . . C17 C 0.13474(17) 0.3509(3) 0.76607(13) 0.0233(6) Uani 1 1 d . . . . . H17A H 0.084649 0.374218 0.749313 0.035 Uiso 1 1 calc R U . . . H17B H 0.161168 0.423465 0.781108 0.035 Uiso 1 1 calc R U . . . H17C H 0.126823 0.293160 0.798544 0.035 Uiso 1 1 calc R U . . . C14 C 0.25870(15) -0.1705(3) 0.58894(13) 0.0214(5) Uani 1 1 d . . . . . H14 H 0.288083 -0.196072 0.555759 0.026 Uiso 1 1 calc R U . . . O1 O 0.23961(12) 0.36532(16) 0.16281(9) 0.0166(4) Uani 1 1 d . . . . . O2 O 0.06225(13) 0.4217(2) 0.63762(10) 0.0292(5) Uani 1 1 d . . . . . H2B H 0.027(2) 0.476(4) 0.6308(16) 0.032(10) Uiso 1 1 d . . . . . H2A H 0.075(3) 0.386(4) 0.609(2) 0.061(16) Uiso 1 1 d . . . . . H34N H 0.3917(18) 1.032(3) 0.5346(14) 0.014(7) Uiso 1 1 d . . . . . H1A H 0.253(3) 0.364(4) 0.202(3) 0.064(16) Uiso 1 1 d . . . . . H1B H 0.257(3) 0.432(6) 0.148(3) 0.085(19) Uiso 1 1 d . . . . . H1C H 0.254(2) 0.290(3) 0.1446(15) 0.025(9) Uiso 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W1 0.00801(7) 0.00733(7) 0.00667(7) 0.00056(3) 0.00167(4) 0.00072(3) N9 0.0170(10) 0.0217(11) 0.0132(10) 0.0014(8) 0.0020(8) 0.0009(9) N18 0.0147(10) 0.0162(10) 0.0138(10) -0.0010(8) -0.0013(8) 0.0001(8) N25 0.0115(9) 0.0161(10) 0.0125(9) -0.0006(8) 0.0024(7) -0.0006(8) N31 0.0162(10) 0.0169(10) 0.0145(10) -0.0011(8) 0.0034(8) -0.0026(8) N34 0.0137(10) 0.0174(11) 0.0188(10) 0.0024(9) 0.0030(8) 0.0033(8) N45 0.0202(11) 0.0163(10) 0.0181(10) 0.0014(8) 0.0048(8) 0.0039(8) N48 0.0175(10) 0.0241(11) 0.0145(10) 0.0000(9) 0.0036(8) -0.0027(9) N50 0.0159(11) 0.0181(10) 0.0208(11) 0.0025(9) 0.0012(9) 0.0005(9) N52 0.0208(11) 0.0147(11) 0.0117(10) -0.0005(8) 0.0029(8) 0.0003(8) N54 0.0157(11) 0.0152(11) 0.0149(11) 0.0006(7) 0.0011(9) 0.0001(7) N56 0.0195(11) 0.0140(10) 0.0163(11) 0.0007(9) 0.0023(8) 0.0006(9) N15 0.0173(10) 0.0204(11) 0.0184(11) 0.0035(9) 0.0001(8) 0.0009(9) N58 0.0203(11) 0.0223(11) 0.0152(10) 0.0037(9) 0.0022(8) 0.0065(9) C57 0.0119(10) 0.0121(11) 0.0108(11) 0.0016(9) 0.0030(8) 0.0006(9) C61 0.0137(11) 0.0138(11) 0.0120(11) -0.0004(9) 0.0015(9) -0.0004(9) N60 0.0246(12) 0.0228(12) 0.0205(11) -0.0035(9) 0.0002(9) -0.0029(9) C53 0.0116(10) 0.0138(12) 0.0076(10) 0.0006(8) 0.0030(8) -0.0001(9) C19 0.0116(11) 0.0108(10) 0.0105(11) -0.0002(9) 0.0010(9) 0.0012(9) C51 0.0106(11) 0.0115(10) 0.0137(11) 0.0021(9) 0.0012(9) 0.0000(9) C28 0.0157(11) 0.0189(12) 0.0136(11) 0.0010(9) 0.0020(9) 0.0019(9) C49 0.0126(11) 0.0173(12) 0.0102(10) -0.0010(9) 0.0027(9) -0.0004(9) C27 0.0135(11) 0.0145(12) 0.0146(11) -0.0018(9) 0.0012(9) 0.0011(9) C55 0.0116(11) 0.0117(11) 0.0058(11) 0.0002(7) 0.0029(9) 0.0007(8) C35 0.0120(11) 0.0154(11) 0.0172(12) 0.0031(10) 0.0026(9) -0.0007(10) C20 0.0096(10) 0.0194(12) 0.0132(11) 0.0012(9) -0.0004(9) 0.0011(9) C59 0.0129(11) 0.0142(11) 0.0119(11) -0.0011(9) 0.0028(9) 0.0015(9) C43 0.0252(13) 0.0164(12) 0.0190(12) -0.0019(10) 0.0032(10) -0.0024(10) C40 0.0144(11) 0.0136(11) 0.0166(11) 0.0007(9) 0.0046(9) -0.0015(9) C26 0.0100(10) 0.0184(12) 0.0108(11) -0.0020(9) -0.0010(8) 0.0008(9) C21 0.0120(11) 0.0174(12) 0.0137(11) -0.0018(9) 0.0015(9) 0.0014(9) C42 0.0155(11) 0.0150(12) 0.0162(11) 0.0004(9) 0.0041(9) -0.0044(9) C39 0.0137(11) 0.0260(14) 0.0174(12) 0.0066(10) 0.0009(9) 0.0017(10) C41 0.0129(11) 0.0140(11) 0.0180(12) -0.0001(10) 0.0027(9) -0.0015(9) C10 0.0115(11) 0.0228(13) 0.0177(12) 0.0009(10) -0.0036(9) 0.0013(10) C5 0.0115(11) 0.0264(13) 0.0164(12) 0.0036(11) -0.0012(9) 0.0011(10) C36 0.0148(11) 0.0145(12) 0.0195(12) 0.0019(10) -0.0021(9) 0.0006(9) C6 0.0131(11) 0.0275(13) 0.0147(11) 0.0007(10) -0.0045(9) 0.0030(10) C11 0.0139(12) 0.0242(13) 0.0205(13) 0.0038(11) -0.0021(10) -0.0016(11) C37 0.0173(12) 0.0165(12) 0.0210(12) 0.0008(10) -0.0009(10) -0.0030(10) C23 0.0147(12) 0.0260(15) 0.0131(12) -0.0027(9) 0.0031(10) 0.0027(9) C29 0.0209(13) 0.0202(13) 0.0145(12) -0.0046(10) 0.0053(10) 0.0011(10) C4 0.0136(12) 0.0230(13) 0.0129(12) 0.0043(10) -0.0020(9) 0.0018(10) C46 0.0199(12) 0.0195(13) 0.0193(12) -0.0019(10) -0.0028(10) -0.0033(10) C8 0.0212(13) 0.0225(13) 0.0171(12) 0.0042(10) 0.0013(10) 0.0004(10) C44 0.0274(15) 0.0148(13) 0.0212(14) -0.0014(9) 0.0056(11) 0.0039(10) C22 0.0101(10) 0.0241(13) 0.0155(12) -0.0019(10) -0.0001(9) 0.0022(9) C13 0.0210(13) 0.0198(13) 0.0257(14) 0.0003(11) -0.0048(11) -0.0007(10) C7 0.0225(14) 0.0175(13) 0.0228(15) 0.0006(10) -0.0022(12) 0.0038(10) C38 0.0161(12) 0.0259(14) 0.0166(12) 0.0038(10) -0.0023(9) -0.0032(10) C12 0.0151(12) 0.0249(14) 0.0209(13) 0.0039(10) -0.0061(10) -0.0015(10) C24 0.0136(11) 0.0250(13) 0.0123(11) 0.0040(10) 0.0020(9) -0.0003(10) C30 0.0220(13) 0.0165(11) 0.0181(13) -0.0055(10) 0.0040(10) -0.0019(10) C32 0.0309(15) 0.0195(12) 0.0197(13) -0.0002(11) 0.0114(12) -0.0006(11) C16 0.0217(13) 0.0259(15) 0.0306(15) 0.0059(12) -0.0022(11) -0.0048(11) C33 0.0211(13) 0.0231(13) 0.0243(14) -0.0082(11) 0.0068(11) 0.0020(11) C47 0.0402(18) 0.0218(15) 0.0228(15) -0.0064(10) -0.0077(13) 0.0041(12) C17 0.0188(13) 0.0308(14) 0.0202(14) -0.0024(11) 0.0001(11) 0.0040(11) C14 0.0211(13) 0.0236(14) 0.0194(12) -0.0011(11) -0.0004(10) 0.0012(11) O1 0.0247(11) 0.0120(10) 0.0132(9) 0.0015(6) 0.0006(8) 0.0002(7) O2 0.0313(11) 0.0331(12) 0.0230(11) -0.0083(9) -0.0098(9) 0.0164(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -5.4734 5.5774 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C53 W1 C59 71.38(9) . . ? C53 W1 C19 98.38(9) . . ? C59 W1 C19 75.07(9) . . ? C53 W1 C57 146.13(9) . . ? C59 W1 C57 140.00(9) . . ? C19 W1 C57 83.31(9) . . ? C53 W1 C51 84.11(9) . . ? C59 W1 C51 138.73(9) . . ? C19 W1 C51 142.84(9) . . ? C57 W1 C51 75.22(9) . . ? C53 W1 C55 72.51(8) . . ? C59 W1 C55 125.49(9) . . ? C19 W1 C55 71.39(9) . . ? C57 W1 C55 76.14(8) . . ? C51 W1 C55 74.18(9) . . ? C53 W1 C61 142.83(9) . . ? C59 W1 C61 72.71(9) . . ? C19 W1 C61 81.32(9) . . ? C57 W1 C61 71.02(9) . . ? C51 W1 C61 118.28(9) . . ? C55 W1 C61 139.25(9) . . ? C53 W1 C49 83.44(9) . . ? C59 W1 C49 73.50(9) . . ? C19 W1 C49 146.08(9) . . ? C57 W1 C49 113.70(9) . . ? C51 W1 C49 71.07(9) . . ? C55 W1 C49 139.33(9) . . ? C61 W1 C49 77.49(9) . . ? C8 N9 C4 123.1(2) . . ? C8 N9 H9N 118.4 . . ? C4 N9 H9N 118.4 . . ? C24 N25 C20 122.6(2) . . ? C24 N25 H25N 118.7 . . ? C20 N25 H25N 118.7 . . ? C30 N31 C26 116.8(2) . . ? C39 N34 C35 123.2(2) . . ? C39 N34 H34N 120(2) . . ? C35 N34 H34N 117(2) . . ? C44 N45 C40 116.6(2) . . ? C14 N15 C10 116.6(2) . . ? N56 C57 W1 178.2(2) . . ? N60 C61 W1 175.7(2) . . ? N52 C53 W1 176.2(2) . . ? N18 C19 W1 177.1(2) . . ? N50 C51 W1 178.7(2) . . ? C29 C28 C27 117.6(2) . . ? C29 C28 C32 121.3(2) . . ? C27 C28 C32 121.1(2) . . ? N48 C49 W1 174.4(2) . . ? C26 C27 C28 118.8(2) . . ? C26 C27 H27 120.6 . . ? C28 C27 H27 120.6 . . ? N54 C55 W1 178.7(2) . . ? N34 C35 C36 118.2(2) . . ? N34 C35 C40 116.4(2) . . ? C36 C35 C40 125.4(2) . . ? N25 C20 C21 118.3(2) . . ? N25 C20 C26 115.9(2) . . ? C21 C20 C26 125.7(2) . . ? N58 C59 W1 175.8(2) . . ? C44 C43 C42 119.5(2) . . ? C44 C43 H43 120.2 . . ? C42 C43 H43 120.2 . . ? N45 C40 C41 123.6(2) . . ? N45 C40 C35 114.4(2) . . ? C41 C40 C35 122.0(2) . . ? N31 C26 C27 124.1(2) . . ? N31 C26 C20 114.1(2) . . ? C27 C26 C20 121.8(2) . . ? C20 C21 C22 121.1(2) . . ? C20 C21 H21 119.4 . . ? C22 C21 H21 119.4 . . ? C43 C42 C41 117.1(2) . . ? C43 C42 C46 121.4(2) . . ? C41 C42 C46 121.5(2) . . ? N34 C39 C38 120.2(2) . . ? N34 C39 H39 119.9 . . ? C38 C39 H39 119.9 . . ? C40 C41 C42 119.4(2) . . ? C40 C41 H41 120.3 . . ? C42 C41 H41 120.3 . . ? N15 C10 C11 123.4(3) . . ? N15 C10 C4 115.1(2) . . ? C11 C10 C4 121.5(2) . . ? C4 C5 C6 120.7(2) . . ? C4 C5 H5 119.7 . . ? C6 C5 H5 119.7 . . ? C35 C36 C37 120.7(2) . . ? C35 C36 H36 119.7 . . ? C37 C36 H36 119.7 . . ? C5 C6 C7 118.2(2) . . ? C5 C6 C17 119.7(2) . . ? C7 C6 C17 122.1(3) . . ? C10 C11 C12 119.5(3) . . ? C10 C11 H11 120.2 . . ? C12 C11 H11 120.2 . . ? C36 C37 C38 118.6(2) . . ? C36 C37 C47 120.4(2) . . ? C38 C37 C47 121.1(3) . . ? C24 C23 C22 120.2(2) . . ? C24 C23 H23 119.9 . . ? C22 C23 H23 119.9 . . ? C28 C29 C30 119.3(2) . . ? C28 C29 H29 120.3 . . ? C30 C29 H29 120.3 . . ? N9 C4 C5 118.1(2) . . ? N9 C4 C10 116.6(2) . . ? C5 C4 C10 125.3(2) . . ? C42 C46 H46A 109.5 . . ? C42 C46 H46B 109.5 . . ? H46A C46 H46B 109.5 . . ? C42 C46 H46C 109.5 . . ? H46A C46 H46C 109.5 . . ? H46B C46 H46C 109.5 . . ? N9 C8 C7 120.0(2) . . ? N9 C8 H8 120.0 . . ? C7 C8 H8 120.0 . . ? N45 C44 C43 123.8(2) . . ? N45 C44 H44 118.1 . . ? C43 C44 H44 118.1 . . ? C23 C22 C21 117.8(2) . . ? C23 C22 C33 122.0(2) . . ? C21 C22 C33 120.2(2) . . ? C12 C13 C14 119.6(3) . . ? C12 C13 H13 120.2 . . ? C14 C13 H13 120.2 . . ? C8 C7 C6 119.9(3) . . ? C8 C7 H7 120.1 . . ? C6 C7 H7 120.1 . . ? C39 C38 C37 119.1(2) . . ? C39 C38 H38 120.4 . . ? C37 C38 H38 120.4 . . ? C13 C12 C11 117.2(2) . . ? C13 C12 C16 122.2(3) . . ? C11 C12 C16 120.6(3) . . ? N25 C24 C23 120.0(2) . . ? N25 C24 H24 120.0 . . ? C23 C24 H24 120.0 . . ? N31 C30 C29 123.3(3) . . ? N31 C30 H30 118.3 . . ? C29 C30 H30 118.3 . . ? C28 C32 H32A 109.5 . . ? C28 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C28 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C12 C16 H16A 109.5 . . ? C12 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C12 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C22 C33 H33A 109.5 . . ? C22 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C22 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C37 C47 H47A 109.5 . . ? C37 C47 H47B 109.5 . . ? H47A C47 H47B 109.5 . . ? C37 C47 H47C 109.5 . . ? H47A C47 H47C 109.5 . . ? H47B C47 H47C 109.5 . . ? C6 C17 H17A 109.5 . . ? C6 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C6 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N15 C14 C13 123.6(3) . . ? N15 C14 H14 118.2 . . ? C13 C14 H14 118.2 . . ? H1A O1 H1B 108(5) . . ? H1A O1 H1C 109(3) . . ? H1B O1 H1C 119(5) . . ? H2B O2 H2A 113(4) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag W1 C53 2.158(2) . ? W1 C59 2.159(2) . ? W1 C19 2.160(2) . ? W1 C57 2.162(2) . ? W1 C51 2.163(2) . ? W1 C55 2.168(2) . ? W1 C61 2.177(2) . ? W1 C49 2.177(2) . ? N9 C8 1.341(4) . ? N9 C4 1.351(3) . ? N9 H9N 0.8800 . ? N18 C19 1.156(3) . ? N25 C24 1.348(3) . ? N25 C20 1.355(3) . ? N25 H25N 0.8800 . ? N31 C30 1.338(3) . ? N31 C26 1.341(3) . ? N34 C39 1.339(4) . ? N34 C35 1.347(3) . ? N34 H34N 0.82(3) . ? N45 C44 1.337(4) . ? N45 C40 1.347(3) . ? N48 C49 1.154(3) . ? N50 C51 1.154(3) . ? N52 C53 1.158(4) . ? N54 C55 1.145(3) . ? N56 C57 1.149(3) . ? N15 C14 1.341(4) . ? N15 C10 1.348(3) . ? N58 C59 1.155(3) . ? C61 N60 1.153(3) . ? C28 C29 1.393(4) . ? C28 C27 1.394(3) . ? C28 C32 1.509(4) . ? C27 C26 1.389(3) . ? C27 H27 0.9500 . ? C35 C36 1.383(4) . ? C35 C40 1.483(4) . ? C20 C21 1.386(4) . ? C20 C26 1.477(3) . ? C43 C44 1.387(4) . ? C43 C42 1.393(4) . ? C43 H43 0.9500 . ? C40 C41 1.387(4) . ? C21 C22 1.397(3) . ? C21 H21 0.9500 . ? C42 C41 1.396(4) . ? C42 C46 1.498(4) . ? C39 C38 1.372(4) . ? C39 H39 0.9500 . ? C41 H41 0.9500 . ? C10 C11 1.389(4) . ? C10 C4 1.477(4) . ? C5 C4 1.389(4) . ? C5 C6 1.395(4) . ? C5 H5 0.9500 . ? C36 C37 1.390(4) . ? C36 H36 0.9500 . ? C6 C7 1.397(4) . ? C6 C17 1.492(4) . ? C11 C12 1.396(4) . ? C11 H11 0.9500 . ? C37 C38 1.400(4) . ? C37 C47 1.493(4) . ? C23 C24 1.375(4) . ? C23 C22 1.396(4) . ? C23 H23 0.9500 . ? C29 C30 1.396(4) . ? C29 H29 0.9500 . ? C46 H46A 0.9800 . ? C46 H46B 0.9800 . ? C46 H46C 0.9800 . ? C8 C7 1.370(4) . ? C8 H8 0.9500 . ? C44 H44 0.9500 . ? C22 C33 1.492(4) . ? C13 C12 1.387(4) . ? C13 C14 1.393(4) . ? C13 H13 0.9500 . ? C7 H7 0.9500 . ? C38 H38 0.9500 . ? C12 C16 1.495(4) . ? C24 H24 0.9500 . ? C30 H30 0.9500 . ? C32 H32A 0.9800 . ? C32 H32B 0.9800 . ? C32 H32C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C33 H33A 0.9800 . ? C33 H33B 0.9800 . ? C33 H33C 0.9800 . ? C47 H47A 0.9800 . ? C47 H47B 0.9800 . ? C47 H47C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? C14 H14 0.9500 . ? O1 H1A 0.92(6) . ? O1 H1B 0.86(6) . ? O1 H1C 0.96(4) . ? O2 H2B 0.87(4) . ? O2 H2A 0.78(6) . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N9 H9N N58 0.88 2.16 2.898(3) 140.5 . yes N25 H25N N48 0.88 2.22 2.976(3) 143.2 . yes C27 H27 N50 0.95 2.64 3.590(3) 176.7 3_556 yes C21 H21 N50 0.95 2.44 3.391(3) 174.7 3_556 yes C41 H41 N18 0.95 2.54 3.444(3) 160.0 3_666 yes C36 H36 N18 0.95 2.41 3.331(3) 162.4 3_666 yes C8 H8 N60 0.95 2.67 3.505(4) 146.4 . yes C13 H13 N60 0.95 2.61 3.340(4) 133.7 1_545 yes C24 H24 N52 0.95 2.46 3.267(3) 143.2 . yes O2 H2B N50 0.87(4) 2.07(4) 2.933(3) 172(3) 3_566 yes O2 H2A N48 0.78(6) 2.32(6) 3.094(3) 174(5) . yes N34 H34N N58 0.82(3) 2.03(3) 2.738(3) 145(3) 1_565 yes O1 H1A N54 0.92(6) 1.66(6) 2.565(3) 165(5) . yes O1 H1B N52 0.86(6) 1.80(6) 2.648(3) 170(6) 2 yes O1 H1C N56 0.96(4) 1.58(4) 2.543(3) 173(3) 2_545 yes