Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7708960
Preview
| Coordinates | 7708960.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C51.8 H73.2 Mg N3 O Si |
|---|---|
| Calculated formula | C50 H69 Mg N3 O Si |
| Title of publication | Isocyanate deoxygenation by a molecular magnesium silanide. |
| Authors of publication | Okokhere-Edeghoghon, Bibian; Neale, Samuel E.; Hill, Michael S.; Mahon, Mary F.; McMullin, Claire L. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2021 |
| Journal volume | 51 |
| Journal issue | 1 |
| Pages of publication | 136 - 144 |
| a | 13.7088 ± 0.0001 Å |
| b | 17.6095 ± 0.0001 Å |
| c | 21.7081 ± 0.0002 Å |
| α | 90° |
| β | 106.096 ± 0.001° |
| γ | 90° |
| Cell volume | 5035.01 ± 0.07 Å3 |
| Cell temperature | 150 ± 0.1 K |
| Ambient diffraction temperature | 150 ± 0.1 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0524 |
| Residual factor for significantly intense reflections | 0.0449 |
| Weighted residual factors for significantly intense reflections | 0.1168 |
| Weighted residual factors for all reflections included in the refinement | 0.1221 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.037 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 272661 (current) | 2022-02-04 | cif/ Updating files of 7708958, 7708959, 7708960 Original log message: Adding full bibliography for 7708958--7708960.cif. |
7708960.cif |
| 270923 | 2021-11-30 | cif/ Adding structures of 7708958, 7708959, 7708960 via cif-deposit CGI script. |
7708960.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.