Crystallography Open Database

Information card for entry 8104551

Preview

Coordinates	8104551.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H36 Cl N4 Na Ni2 O8
Calculated formula	C24 H36 Cl N4 Na Ni2 O8
Title of publication	Redetermination of the crystal structure of bis[N,N′-ethylenebis(acetylacetoniminato)nickel(II)] sodium perchlorate, C24H36ClN4NaNi2O8
Authors of publication	Dey, Lucky; Rabi, Saswata; Begum, Zinnat A.; Takase, Tsugiko; Rahman, Ismail M.M.; Tiekink, Edward R.T.; Roy, Tapashi Ghosh
Journal of publication	Zeitschrift für Kristallographie - New Crystal Structures
Year of publication	2021
Journal volume	236
Journal issue	6
Pages of publication	1147 - 1150
a	19.5909 ± 0.0011 Å
b	10.8023 ± 0.0006 Å
c	14.5722 ± 0.0008 Å
α	90°
β	112.032 ± 0.001°
γ	90°
Cell volume	2858.7 ± 0.3 Å³
Cell temperature	93 ± 2 K
Ambient diffraction temperature	93 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0269
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.0695
Weighted residual factors for all reflections included in the refinement	0.0701
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
272871 (current)	2022-02-09	cif/ Adding structures of 8104551 via cif-deposit CGI script.	8104551.cif