#------------------------------------------------------------------------------
#$Date: 2008-01-14 00:15:36 +0200 (Mon, 14 Jan 2008) $
#$Revision: 14 $
#$URL: file:///home/coder/svn-repositories/cod/cif/9/9004546.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_9004546
_chemical_name 'Masuyite'
loop_
_publ_author_name
'Burns P C'
'Hanchar J M'
_journal_name_full "The Canadian Mineralogist"
_journal_volume 37
_journal_year 1999
_journal_page_first 1483
_journal_page_last 1491
_publ_section_title
;
 The structure of masuyite, Pb[(UO2)3O3(OH)2](H2O)3,
 and its relationship to protasite
;
_chemical_formula_sum 'U3 Pb1.05 O14 H5'
_cell_length_a 12.241
_cell_length_b 7.008
_cell_length_c 6.983
_cell_angle_alpha 90
_cell_angle_beta 90.402
_cell_angle_gamma 90
_cell_volume 599.021
_symmetry_space_group_name_H-M 'P 1 n 1'
loop_
_symmetry_equiv_pos_as_xyz
  'x,y,z'
  '1/2+x,-y,1/2+z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_Uiso_or_equiv
U1   0.99880   0.01850   0.00240   1.00000   0.01600
U2   0.17970   0.01800   0.54190   1.00000   0.01640
U3   0.88020   0.01220   0.48360   1.00000   0.01800
Pb1   0.02540   0.49600   0.66250   0.93000   0.03280
Pb2   0.85300   0.50900   0.19200   0.12000   0.04150
O1   0.99400   0.28300   0.02900   1.00000   0.04160
O2   0.00800   0.76700   0.95700   1.00000   0.03770
O3   0.19600   0.27000   0.49600   1.00000   0.03420
O4   0.16200   0.76300   0.61000   1.00000   0.03600
O5   0.86800   0.27100   0.45100   1.00000   0.03160
O6   0.89500   0.75600   0.53600   1.00000   0.03610
O7   0.01800   0.08600   0.68100   1.00000   0.03700
O8   0.04100   0.97400   0.30200   1.00000   0.06480
O9   0.84700   0.98400   0.17400   1.00000   0.01010
O-H10   0.19400   0.05300   0.92400   1.00000   0.03290
O-H11   0.81200   0.06500   0.78700   1.00000   0.04030
Wat12   0.80200   0.48500   0.83200   1.00000   0.05360
Wat13   0.19000   0.48200   0.93800   1.00000   0.01600
Wat14   0.06100   0.52500   0.29600   1.00000   0.02040