Crystallography Open Database

Information card for entry 1564891

Preview

Coordinates	1564891.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C67 H58 B Cl2 F29 N P Pd
Calculated formula	C67 H58 B Cl2 F29 N P Pd
Title of publication	Highly efficient vinylic addition polymerization of 5-vinyl-2-norbornene using benzylic palladium complexes as precatalysts
Authors of publication	Pérez-Ortega, Ignacio; Albéniz, Ana C.
Journal of publication	Polymer Chemistry
Year of publication	2021
Journal volume	12
Journal issue	41
Pages of publication	5963 - 5969
a	13.4173 ± 0.0007 Å
b	15.6707 ± 0.0007 Å
c	18.5278 ± 0.0008 Å
α	84.761 ± 0.004°
β	70.245 ± 0.004°
γ	89.96 ± 0.004°
Cell volume	3649.1 ± 0.3 Å³
Cell temperature	298 K
Ambient diffraction temperature	298 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.091
Residual factor for significantly intense reflections	0.0506
Weighted residual factors for significantly intense reflections	0.1067
Weighted residual factors for all reflections included in the refinement	0.1345
Goodness-of-fit parameter for all reflections included in the refinement	1.013
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
270516 (current)	2021-11-06	cif/ Updating files of 1564891, 1564892 Original log message: Adding full bibliography for 1564891--1564892.cif.	1564891.cif
269873	2021-10-09	cif/ Adding structures of 1564891, 1564892 via cif-deposit CGI script.	1564891.cif