Crystallography Open Database

Information card for entry 1564892

Preview

Coordinates	1564892.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H44 B F9 N P Pd
Calculated formula	C34 H44 B F9 N P Pd
Title of publication	Highly efficient vinylic addition polymerization of 5-vinyl-2-norbornene using benzylic palladium complexes as precatalysts
Authors of publication	Pérez-Ortega, Ignacio; Albéniz, Ana C.
Journal of publication	Polymer Chemistry
Year of publication	2021
Journal volume	12
Journal issue	41
Pages of publication	5963 - 5969
a	10.3004 ± 0.0006 Å
b	13.2588 ± 0.0007 Å
c	16.2684 ± 0.0014 Å
α	109.041 ± 0.006°
β	91.911 ± 0.006°
γ	107.037 ± 0.005°
Cell volume	1987.5 ± 0.3 Å³
Cell temperature	298 K
Ambient diffraction temperature	298 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0965
Residual factor for significantly intense reflections	0.0547
Weighted residual factors for significantly intense reflections	0.098
Weighted residual factors for all reflections included in the refinement	0.1218
Goodness-of-fit parameter for all reflections included in the refinement	1.005
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
270516 (current)	2021-11-06	cif/ Updating files of 1564891, 1564892 Original log message: Adding full bibliography for 1564891--1564892.cif.	1564892.cif
269873	2021-10-09	cif/ Adding structures of 1564891, 1564892 via cif-deposit CGI script.	1564892.cif