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Information card for entry 2241943
Preview
| Coordinates | 2241943.cif |
|---|---|
| Structure factors | 2241943.hkl |
| Original IUCr paper | HTML |
| Chemical name | Tetrakis[μ~3~-4-methyl-<i>N</i>-(2-oxidophenyl)salicylideneiminato]tetrakis[methanolnickel(II)] methanol 0.8-solvate |
|---|---|
| Formula | C60.8 H63.2 N4 Ni4 O12.8 |
| Calculated formula | C60.8 H63.2 N4 Ni4 O12.8 |
| Title of publication | A tetranuclear cubane-like nickel(II) complex with a tridentate salicylideneimine Schiff base ligand: tetrakis[μ~3~-4-methyl-<i>N</i>-(2-oxidophenyl)salicylideneiminato]tetrakis[methanolnickel(II)] methanol 0.8-solvate |
| Authors of publication | Pavlović, Gordana; Majer, Mihael; Cindrić, Marina |
| Journal of publication | Acta Crystallographica Section E |
| Year of publication | 2016 |
| Journal volume | 72 |
| Journal issue | 12 |
| Pages of publication | 1776 - 1779 |
| a | 22.581 ± 0.0005 Å |
| b | 13.7701 ± 0.0003 Å |
| c | 18.5242 ± 0.0004 Å |
| α | 90° |
| β | 92.125 ± 0.002° |
| γ | 90° |
| Cell volume | 5756 ± 0.2 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1432 |
| Residual factor for significantly intense reflections | 0.0675 |
| Weighted residual factors for significantly intense reflections | 0.1092 |
| Weighted residual factors for all reflections included in the refinement | 0.1301 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.994 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | Yes |
| Revision | Date | Message | Files |
|---|---|---|---|
| 188381 (current) | 2016-11-11 | cif/ hkl/ Adding structures of 2241943 via cif-deposit CGI script. |
2241943.cif 2241943.hkl |
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