Crystallography Open Database

Information card for entry 4064702

Preview

Coordinates	4064702.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C132 H200 K2 La2 O18
Calculated formula	C132 H184 K2 La2 O18
Title of publication	Synthesis and Structural Diversity of Heterobimetallic Lanthanide‒Potassium Complexes and Catalytic Activity for Amidation of Aldehydes with Amines
Authors of publication	Xu, Bin; Huang, Lingling; Yang, Zijian; Yao, Yingming; Zhang, Yong; Shen, Qi
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	13
Pages of publication	3588
a	23.8228 ± 0.0019 Å
b	24.848 ± 0.002 Å
c	24.213 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	14333 ± 2 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	20
Hermann-Mauguin space group symbol	C 2 2 21
Hall space group symbol	C 2c 2
Residual factor for all reflections	0.0998
Residual factor for significantly intense reflections	0.087
Weighted residual factors for significantly intense reflections	0.2233
Weighted residual factors for all reflections included in the refinement	0.2312
Goodness-of-fit parameter for all reflections included in the refinement	1.169
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178541 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/47.	4064702.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064702.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064702.cif
33010	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064702, 4064703, 4064704, 4064705 via cif-deposit CGI script.	4064702.cif