Crystallography Open Database

Information card for entry 4064703

Preview

Coordinates	4064703.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C128 H168 K2 Nd2 O10
Calculated formula	C128 H118 K2 Nd2 O10
Title of publication	Synthesis and Structural Diversity of Heterobimetallic Lanthanide‒Potassium Complexes and Catalytic Activity for Amidation of Aldehydes with Amines
Authors of publication	Xu, Bin; Huang, Lingling; Yang, Zijian; Yao, Yingming; Zhang, Yong; Shen, Qi
Journal of publication	Organometallics
Year of publication	2011
Journal volume	30
Journal issue	13
Pages of publication	3588
a	13.7855 ± 0.0007 Å
b	15.4725 ± 0.0011 Å
c	15.9167 ± 0.0009 Å
α	75.615 ± 0.005°
β	68.163 ± 0.005°
γ	77.512 ± 0.006°
Cell volume	3023.5 ± 0.3 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0426
Residual factor for significantly intense reflections	0.0391
Weighted residual factors for significantly intense reflections	0.1009
Weighted residual factors for all reflections included in the refinement	0.1036
Goodness-of-fit parameter for all reflections included in the refinement	1.129
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178541 (current)	2016-03-21	cif/4/06/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/06/47.	4064703.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4064703.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4064703.cif
33010	2012-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4064702, 4064703, 4064704, 4064705 via cif-deposit CGI script.	4064703.cif