Crystallography Open Database

Information card for entry 4107537

Preview

Coordinates	4107537.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H58 Co7 Cs2 O49
Calculated formula	C24 H16 Co7 Cs2 O49
Title of publication	Reversible Single-Crystal-to-Single-Crystal Cross-Linking of a Ribbon of Cobalt Citrate Cubanes To Form a 2D Net
Authors of publication	Javier Campo; Larry R. Falvello; Isabel Mayoral; Fernando Palacio; Tatiana Soler; Milagros Tomás
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	2932 - 2933
a	11.5021 ± 0.0005 Å
b	13.2108 ± 0.0009 Å
c	20.0315 ± 0.0013 Å
α	99.997 ± 0.005°
β	91.157 ± 0.004°
γ	114.8 ± 0.005°
Cell volume	2706.4 ± 0.3 Å³
Cell temperature	278 ± 1 K
Ambient diffraction temperature	278 ± 1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.122
Residual factor for significantly intense reflections	0.0584
Weighted residual factors for significantly intense reflections	0.1456
Weighted residual factors for all reflections included in the refinement	0.1576
Goodness-of-fit parameter for all reflections included in the refinement	0.973
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
178821 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/75.	4107537.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4107537.cif
55223	2012-05-04	cif/ Adding structures of 4107537 via cif-deposit CGI script.	4107537.cif