Crystallography Open Database

Information card for entry 4107538

Preview

Coordinates	4107538.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H86 Co14 Cs4 O83
Calculated formula	C48 H32 Co14 Cs4 O83
Title of publication	Reversible Single-Crystal-to-Single-Crystal Cross-Linking of a Ribbon of Cobalt Citrate Cubanes To Form a 2D Net
Authors of publication	Javier Campo; Larry R. Falvello; Isabel Mayoral; Fernando Palacio; Tatiana Soler; Milagros Tomás
Journal of publication	Journal of the American Chemical Society
Year of publication	2008
Journal volume	130
Pages of publication	2932 - 2933
a	11.405 ± 0.0005 Å
b	13.0515 ± 0.0009 Å
c	18.4855 ± 0.0009 Å
α	101.734 ± 0.005°
β	95.682 ± 0.004°
γ	115.79 ± 0.005°
Cell volume	2370.3 ± 0.3 Å³
Cell temperature	303 ± 1 K
Ambient diffraction temperature	303 ± 1 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1377
Residual factor for significantly intense reflections	0.086
Weighted residual factors for significantly intense reflections	0.1944
Weighted residual factors for all reflections included in the refinement	0.2174
Goodness-of-fit parameter for all reflections included in the refinement	1.095
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
178821 (current)	2016-03-21	cif/4/10/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/10/75.	4107538.cif
120076	2014-07-11	Adding DOIs to range 4/10 structures.	4107538.cif
55224	2012-05-04	cif/ Adding structures of 4107538 via cif-deposit CGI script.	4107538.cif