Crystallography Open Database

Information card for entry 4306623

Preview

Coordinates	4306623.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H18 Cr Ga N O5
Calculated formula	C14 H18 Cr Ga N O5
SMILES	[Ga]([Cr](C#[O])(C#[O])(C#[O])(C#[O])C#[O])N1C(CCCC1(C)C)(C)C
Title of publication	2,2,6,6-Tetramethylpiperidinogallium as a Terminal and Bridging Ligand in Homo- and Heteroleptic Chromium, Nickel, and Cobalt Complexes
Authors of publication	Annekathrin Seifert; Gerald Linti
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11398 - 11404
a	11.048 ± 0.002 Å
b	12.432 ± 0.003 Å
c	12.797 ± 0.003 Å
α	90°
β	95.78 ± 0.03°
γ	90°
Cell volume	1748.7 ± 0.7 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0615
Residual factor for significantly intense reflections	0.0436
Weighted residual factors for significantly intense reflections	0.1003
Weighted residual factors for all reflections included in the refinement	0.1085
Goodness-of-fit parameter for all reflections included in the refinement	0.92
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179104 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/66.	4306623.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306623.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306623.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306623.cif