Crystallography Open Database

Information card for entry 4306624

Preview

Coordinates	4306624.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H54 Cr2 Ga3 N3 O6
Calculated formula	C33 H54 Cr2 Ga3 N3 O6
Title of publication	2,2,6,6-Tetramethylpiperidinogallium as a Terminal and Bridging Ligand in Homo- and Heteroleptic Chromium, Nickel, and Cobalt Complexes
Authors of publication	Annekathrin Seifert; Gerald Linti
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	11398 - 11404
a	10.554 ± 0.002 Å
b	39.15 ± 0.008 Å
c	10.15 ± 0.002 Å
α	90°
β	103.09 ± 0.03°
γ	90°
Cell volume	4084.9 ± 1.5 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0509
Residual factor for significantly intense reflections	0.0362
Weighted residual factors for significantly intense reflections	0.0888
Weighted residual factors for all reflections included in the refinement	0.0938
Goodness-of-fit parameter for all reflections included in the refinement	0.891
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179104 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/66.	4306624.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4306624.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4306624.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4306624.cif