Crystallography Open Database

Information card for entry 4307213

Preview

Coordinates	4307213.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H48 N7.5 O0 Zn3
Calculated formula	C20 H37 N5 O Zn2
Title of publication	Aluminum and Zinc Complexes Based on an Amino-Bis(pyrazolyl) Ligand: Synthesis, Structures, and Use in MMA and Lactide Polymerization
Authors of publication	Bing Lian; Christophe M. Thomas; Osvaldo L. Casagrande; Christian W. Lehmann; Thierry Roisnel; Jean-François Carpentier
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	328 - 340
a	8.739 ± 0.005 Å
b	9.505 ± 0.005 Å
c	14.631 ± 0.005 Å
α	83.137 ± 0.005°
β	81.479 ± 0.005°
γ	77.207 ± 0.005°
Cell volume	1167.3 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0616
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.109
Weighted residual factors for all reflections included in the refinement	0.1187
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4307213.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4307213.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4307213.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4307213.cif