Crystallography Open Database

Information card for entry 4307214

Preview

Coordinates	4307214.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H32 Cl N5 Zn
Calculated formula	C22 H32 Cl N5 Zn
Title of publication	Aluminum and Zinc Complexes Based on an Amino-Bis(pyrazolyl) Ligand: Synthesis, Structures, and Use in MMA and Lactide Polymerization
Authors of publication	Bing Lian; Christophe M. Thomas; Osvaldo L. Casagrande; Christian W. Lehmann; Thierry Roisnel; Jean-François Carpentier
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	328 - 340
a	8.675 ± 0.002 Å
b	21.637 ± 0.005 Å
c	12.645 ± 0.003 Å
α	90°
β	106.436 ± 0.012°
γ	90°
Cell volume	2276.5 ± 0.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0298
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.0716
Weighted residual factors for all reflections included in the refinement	0.0736
Goodness-of-fit parameter for all reflections included in the refinement	1.045
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179110 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/72.	4307214.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4307214.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4307214.cif
1194	2010-06-06	cif/4/ Adding data from Inorg-Chem-2007_01-13/ processing directory.	4307214.cif