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Information card for entry 4308374
Preview
| Coordinates | 4308374.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H57 N2 S2 Si4 V |
|---|---|
| Calculated formula | C30 H48 N2 S2 Si4 V |
| Title of publication | Synthesis of a Vanadium(III) Tris(arylthiolato) Complex and Its Reactions with Azide and Azo Compounds: Formation of a Sulfenamide Complex via Cleavage of an Azo NN Bond |
| Authors of publication | Komuro, Takashi; Matsuo, Tsukasa; Kawaguchi, Hiroyuki; Tatsumi, Kazuyuki |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2005 |
| Journal volume | 44 |
| Journal issue | 2 |
| Pages of publication | 175 - 177 |
| a | 9.338 ± 0.004 Å |
| b | 19.654 ± 0.007 Å |
| c | 21.4 ± 0.009 Å |
| α | 90° |
| β | 106.141 ± 0.006° |
| γ | 90° |
| Cell volume | 3773 ± 3 Å3 |
| Cell temperature | 173.1 K |
| Number of distinct elements | 6 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for significantly intense reflections | 0.082 |
| Weighted residual factors for all reflections included in the refinement | 0.245 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.001 |
| Diffraction radiation wavelength | 0.7107 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 210259 (current) | 2018-08-31 | cif/4/30/ Updating bibliography in entries 4300938-4300941, 4308373-4308376. Marking entries 4300938-4300941 as duplicates of entries 4308373-4308376. |
4308374.cif |
| 176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4308374.cif |
| 120081 | 2014-07-12 | Adding DOIs to range 4/30 structures. | 4308374.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4308374.cif |
| 32063 | 2012-01-26 | cif/4 Correction of volume and publication year for files coming from a couple of issues of Inorg. Chem. The mistake was made when fetching bibliography for these entries and detected just now. I have checked that all other Inorg. Chem. files are correct. |
4308374.cif |
| 1526 | 2010-09-26 | cif/4/ Adding new CIFs from Inorg. Chem. 2005 deposited via Web deposition site to the COD test database (and transferede to the main COD database after renaming). |
4308374.cif |
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