Crystallography Open Database

Information card for entry 7018910

Preview

Coordinates	7018910.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tetrakis-trimethylphosphine-rhodium(i) bis-trifluoromethyl-pyrazolate
Formula	C17 H37 F6 N2 P4 Rh
Calculated formula	C17 H37 F6 N2 P4 Rh
Title of publication	Rhodium pyrazolate complexes as potential CVD precursors.
Authors of publication	Rivers, Joseph H.; Depue Anderson, Lauren J.; Starr, Cotton M. N.; Jones, Richard A.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2012
Journal volume	41
Journal issue	17
Pages of publication	5401 - 5408
a	9.2999 ± 0.0004 Å
b	16.5877 ± 0.0009 Å
c	9.4383 ± 0.0004 Å
α	90°
β	111.392 ± 0.003°
γ	90°
Cell volume	1355.68 ± 0.11 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.1572
Residual factor for significantly intense reflections	0.0663
Weighted residual factors for significantly intense reflections	0.1138
Weighted residual factors for all reflections included in the refinement	0.1524
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179893 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/89.	7018910.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7018910.cif
55991	2012-05-08	cif/ Adding structures of 7018906, 7018907, 7018908, 7018909, 7018910 via cif-deposit CGI script.	7018910.cif