Crystallography Open Database

Information card for entry 7026988

Preview

Coordinates	7026988.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C57 H71 Cl2 F6 N10 O14 P Ru
Calculated formula	C57 H59 Cl1.7 F6 N10 O12.8 P Ru
Title of publication	Stepwise synthetic strategy for the preparation of trinuclear complexes of bis(terpyridyl) bridging ligands containing aza-crown macrocyclic spacer groups
Authors of publication	Bushell, Karen L.; Couchman, Samantha M.; Jeffery, John C.; Rees, Leigh H.; Ward, Michael D.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1998
Journal issue	20
Pages of publication	3397
a	8.357 ± 0.004 Å
b	17.697 ± 0.005 Å
c	22.442 ± 0.008 Å
α	76.16 ± 0.03°
β	87.85 ± 0.02°
γ	81.87 ± 0.02°
Cell volume	3190 ± 2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1476
Residual factor for significantly intense reflections	0.1044
Weighted residual factors for significantly intense reflections	0.282
Weighted residual factors for all reflections included in the refinement	0.3185
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179975 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/69.	7026988.cif
94902	2014-01-28	cif/ Adding structures of 7026988, 7026989 via cif-deposit CGI script.	7026988.cif