Crystallography Open Database

Information card for entry 7026989

Preview

Coordinates	7026989.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C74.22 H77.6 F16.17 N12 O5.81 P2.7 Ru
Calculated formula	C74.256 H67 F16.116 N12 O5.814 P2.686 Ru
Title of publication	Stepwise synthetic strategy for the preparation of trinuclear complexes of bis(terpyridyl) bridging ligands containing aza-crown macrocyclic spacer groups
Authors of publication	Bushell, Karen L.; Couchman, Samantha M.; Jeffery, John C.; Rees, Leigh H.; Ward, Michael D.
Journal of publication	Journal of the Chemical Society, Dalton Transactions
Year of publication	1998
Journal issue	20
Pages of publication	3397
a	11.417 ± 0.004 Å
b	18.318 ± 0.009 Å
c	20.444 ± 0.009 Å
α	76.4 ± 0.03°
β	88.87 ± 0.05°
γ	81.32 ± 0.04°
Cell volume	4108 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.239
Residual factor for significantly intense reflections	0.1329
Weighted residual factors for significantly intense reflections	0.3461
Weighted residual factors for all reflections included in the refinement	0.429
Goodness-of-fit parameter for all reflections included in the refinement	1.021
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7026989.cif
94902	2014-01-28	cif/ Adding structures of 7026988, 7026989 via cif-deposit CGI script.	7026989.cif