Crystallography Open Database

Information card for entry 7045414

Preview

Coordinates	7045414.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C65 H130 Mn4 Mo24 N10 O136 P16 Pb2
Calculated formula	C65 H72 Mn4 Mo24 N10 O136 P16 Pb2
Title of publication	Influence of Pb element on the catalytic properties of {P<sub>4</sub>Mo<sub>6</sub>}-polyoxometalate for redox reactions.
Authors of publication	Han, Zhangang; Xin, Xing; Zheng, Ran; Yu, Haitao
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	10
Pages of publication	3356 - 3365
a	13.248 ± 0.004 Å
b	13.889 ± 0.004 Å
c	23.386 ± 0.006 Å
α	93.433 ± 0.004°
β	98.979 ± 0.004°
γ	99.678 ± 0.004°
Cell volume	4173 ± 2 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0302
Residual factor for significantly intense reflections	0.0296
Weighted residual factors for significantly intense reflections	0.086
Weighted residual factors for all reflections included in the refinement	0.0868
Goodness-of-fit parameter for all reflections included in the refinement	1.023
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229248 (current)	2019-11-17	cif/ Updating files of 7045414, 7045415, 7045416, 7045417 Original log message: Adding full bibliography for 7045414--7045417.cif.	7045414.cif
205770	2018-01-27	cif/ Adding structures of 7045414, 7045415, 7045416, 7045417 via cif-deposit CGI script.	7045414.cif