Crystallography Open Database

Information card for entry 7045415

Preview

Coordinates	7045415.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39 H98 Mo24 N6 Ni4 O134 P16 Pb2
Calculated formula	C39 H16 Mo24 N6 Ni4 O134 P16 Pb2
Title of publication	Influence of Pb element on the catalytic properties of {P<sub>4</sub>Mo<sub>6</sub>}-polyoxometalate for redox reactions.
Authors of publication	Han, Zhangang; Xin, Xing; Zheng, Ran; Yu, Haitao
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	10
Pages of publication	3356 - 3365
a	22.1924 ± 0.0008 Å
b	21.7343 ± 0.0007 Å
c	16.5637 ± 0.0007 Å
α	90°
β	96.612 ± 0.003°
γ	90°
Cell volume	7936.1 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0489
Residual factor for significantly intense reflections	0.0422
Weighted residual factors for significantly intense reflections	0.1072
Weighted residual factors for all reflections included in the refinement	0.112
Goodness-of-fit parameter for all reflections included in the refinement	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229248 (current)	2019-11-17	cif/ Updating files of 7045414, 7045415, 7045416, 7045417 Original log message: Adding full bibliography for 7045414--7045417.cif.	7045415.cif
205770	2018-01-27	cif/ Adding structures of 7045414, 7045415, 7045416, 7045417 via cif-deposit CGI script.	7045415.cif