Crystallography Open Database

Information card for entry 7133342

Preview

Coordinates	7133342.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H83 N5 Si4 Yb
Calculated formula	C46 H83 N5 Si4 Yb
Title of publication	Yb/Si frustrated Lewis pairs with a labile naphthalenyl bridge.
Authors of publication	Xu, Cheng; Zhao, Sixuan; Zhang, Heng; Peng, Qian; Chen, Yaofeng
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	64
Pages of publication	8411 - 8414
a	13.2397 ± 0.0004 Å
b	22.4875 ± 0.0008 Å
c	18.0354 ± 0.0005 Å
α	90°
β	105.208 ± 0.002°
γ	90°
Cell volume	5181.6 ± 0.3 Å³
Cell temperature	181.99 K
Ambient diffraction temperature	181.99 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1025
Residual factor for significantly intense reflections	0.0674
Weighted residual factors for significantly intense reflections	0.1511
Weighted residual factors for all reflections included in the refinement	0.1713
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
294423 (current)	2024-09-06	cif/ Updating files of 7133340, 7133341, 7133342, 7133343, 7133344 Original log message: Adding full bibliography for 7133340--7133344.cif.	7133342.cif
293413	2024-07-16	cif/ Adding structures of 7133340, 7133341, 7133342, 7133343, 7133344 via cif-deposit CGI script.	7133342.cif