Crystallography Open Database

Information card for entry 7133343

Preview

Coordinates	7133343.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C50 H90 N4 Si4 Yb
Calculated formula	C50 H90 N4 Si4 Yb
Title of publication	Yb/Si frustrated Lewis pairs with a labile naphthalenyl bridge.
Authors of publication	Xu, Cheng; Zhao, Sixuan; Zhang, Heng; Peng, Qian; Chen, Yaofeng
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	64
Pages of publication	8411 - 8414
a	18.0881 ± 0.0004 Å
b	22.6537 ± 0.0004 Å
c	26.9902 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	11059.6 ± 0.4 Å³
Cell temperature	173 ± 0.2 K
Ambient diffraction temperature	173 ± 0.2 K
Number of distinct elements	5
Space group number	61
Hermann-Mauguin space group symbol	P b c a
Hall space group symbol	-P 2ac 2ab
Residual factor for all reflections	0.0933
Residual factor for significantly intense reflections	0.0544
Weighted residual factors for significantly intense reflections	0.0958
Weighted residual factors for all reflections included in the refinement	0.108
Goodness-of-fit parameter for all reflections included in the refinement	1.063
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
294423 (current)	2024-09-06	cif/ Updating files of 7133340, 7133341, 7133342, 7133343, 7133344 Original log message: Adding full bibliography for 7133340--7133344.cif.	7133343.cif
293413	2024-07-16	cif/ Adding structures of 7133340, 7133341, 7133342, 7133343, 7133344 via cif-deposit CGI script.	7133343.cif