Crystallography Open Database

Information card for entry 7133344

Preview

Coordinates	7133344.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34.06 H68.23 N4 O0.06 S2 Si4 Yb
Calculated formula	C34 H68 N4 S2 Si4 Yb
Title of publication	Yb/Si frustrated Lewis pairs with a labile naphthalenyl bridge.
Authors of publication	Xu, Cheng; Zhao, Sixuan; Zhang, Heng; Peng, Qian; Chen, Yaofeng
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2024
Journal volume	60
Journal issue	64
Pages of publication	8411 - 8414
a	15.4962 ± 0.0003 Å
b	17.7037 ± 0.0003 Å
c	19.308 ± 0.0003 Å
α	78.382 ± 0.001°
β	69.436 ± 0.001°
γ	69.691 ± 0.002°
Cell volume	4632.04 ± 0.15 Å³
Cell temperature	173 ± 0.1 K
Ambient diffraction temperature	173 ± 0.1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0499
Residual factor for significantly intense reflections	0.0337
Weighted residual factors for significantly intense reflections	0.0793
Weighted residual factors for all reflections included in the refinement	0.0844
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
294423 (current)	2024-09-06	cif/ Updating files of 7133340, 7133341, 7133342, 7133343, 7133344 Original log message: Adding full bibliography for 7133340--7133344.cif.	7133344.cif
293413	2024-07-16	cif/ Adding structures of 7133340, 7133341, 7133342, 7133343, 7133344 via cif-deposit CGI script.	7133344.cif