Crystallography Open Database

Information card for entry 7700525

Preview

Coordinates	7700525.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H74 B N5 O Si
Calculated formula	C52 H74 B N5 O Si
Title of publication	Synthesis and reactivity of boryl substituted silaimines.
Authors of publication	Yuvaraj, K.; Jones, Cameron
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	31
Pages of publication	11961 - 11965
a	19.7295 ± 0.0015 Å
b	12.4632 ± 0.0009 Å
c	19.9618 ± 0.0015 Å
α	90°
β	96.766 ± 0.004°
γ	90°
Cell volume	4874.3 ± 0.6 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.241
Residual factor for significantly intense reflections	0.1066
Weighted residual factors for significantly intense reflections	0.249
Weighted residual factors for all reflections included in the refinement	0.3216
Goodness-of-fit parameter for all reflections included in the refinement	1.028
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
224362 (current)	2019-11-08	cif/ Updating files of 7700519, 7700520, 7700521, 7700522, 7700523, 7700524, 7700525, 7700526 Original log message: Adding full bibliography for 7700519--7700526.cif.	7700525.cif
216991	2019-07-13	cif/ Adding structures of 7700519, 7700520, 7700521, 7700522, 7700523, 7700524, 7700525, 7700526 via cif-deposit CGI script.	7700525.cif