Crystallography Open Database

Information card for entry 7700526

Preview

Coordinates	7700526.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H79 B N5 Si
Calculated formula	C55 H79 B N5 Si
Title of publication	Synthesis and reactivity of boryl substituted silaimines.
Authors of publication	Yuvaraj, K.; Jones, Cameron
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2019
Journal volume	48
Journal issue	31
Pages of publication	11961 - 11965
a	12.776 ± 0.003 Å
b	20.405 ± 0.004 Å
c	21.92 ± 0.004 Å
α	114.35 ± 0.03°
β	91.65 ± 0.03°
γ	93.08 ± 0.03°
Cell volume	5190 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0702
Residual factor for significantly intense reflections	0.0612
Weighted residual factors for significantly intense reflections	0.1633
Weighted residual factors for all reflections included in the refinement	0.1724
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.7109 Å
Diffraction radiation type	Synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
224362 (current)	2019-11-08	cif/ Updating files of 7700519, 7700520, 7700521, 7700522, 7700523, 7700524, 7700525, 7700526 Original log message: Adding full bibliography for 7700519--7700526.cif.	7700526.cif
216991	2019-07-13	cif/ Adding structures of 7700519, 7700520, 7700521, 7700522, 7700523, 7700524, 7700525, 7700526 via cif-deposit CGI script.	7700526.cif