Crystallography Open Database

Information card for entry 7707446

Preview

Coordinates	7707446.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56.3 H36.3 Cl0.9 N4 O12 Rh2
Calculated formula	C56.3 H36.3 Cl0.9 N4 O12 Rh2
Title of publication	Immobilization of Rh(I) precursor in a porphyrin metal-organic framework - turning on the catalytic activity.
Authors of publication	Szczepkowska, Anna M.; Janeta, Mateusz; Siczek, Miłosz; Tylus, Włodzimierz; Trzeciak, Anna M.; Bury, Wojciech
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	26
Pages of publication	9051 - 9058
a	10.301 ± 0.002 Å
b	29.369 ± 0.006 Å
c	10.68 ± 0.002 Å
α	90°
β	104.88 ± 0.02°
γ	90°
Cell volume	3122.7 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.2728
Residual factor for significantly intense reflections	0.1312
Weighted residual factors for significantly intense reflections	0.3121
Weighted residual factors for all reflections included in the refinement	0.4174
Goodness-of-fit parameter for all reflections included in the refinement	1.004
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268762 (current)	2021-09-06	cif/ Updating files of 7707445, 7707446, 7707447 Original log message: Adding full bibliography for 7707445--7707447.cif.	7707446.cif
265353	2021-05-20	cif/ Adding structures of 7707445, 7707446, 7707447 via cif-deposit CGI script.	7707446.cif