Crystallography Open Database

Information card for entry 7707447

Preview

Coordinates	7707447.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C219 H124 Cl3 N12 O62 Rh3 Zr6
Calculated formula	C217 H124 Cl0.9996 N12 O59.9668 Rh3.0003 Zr6
Title of publication	Immobilization of Rh(I) precursor in a porphyrin metal-organic framework - turning on the catalytic activity.
Authors of publication	Szczepkowska, Anna M.; Janeta, Mateusz; Siczek, Miłosz; Tylus, Włodzimierz; Trzeciak, Anna M.; Bury, Wojciech
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	26
Pages of publication	9051 - 9058
a	25.388 ± 0.003 Å
b	25.388 ± 0.003 Å
c	25.388 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	16364 ± 3 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	221
Hermann-Mauguin space group symbol	P m -3 m
Hall space group symbol	-P 4 2 3
Residual factor for all reflections	0.1155
Residual factor for significantly intense reflections	0.0901
Weighted residual factors for significantly intense reflections	0.2518
Weighted residual factors for all reflections included in the refinement	0.3109
Goodness-of-fit parameter for all reflections included in the refinement	1.234
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
268762 (current)	2021-09-06	cif/ Updating files of 7707445, 7707446, 7707447 Original log message: Adding full bibliography for 7707445--7707447.cif.	7707447.cif
265353	2021-05-20	cif/ Adding structures of 7707445, 7707446, 7707447 via cif-deposit CGI script.	7707447.cif