Crystallography Open Database

Information card for entry 7707952

Preview

Coordinates	7707952.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	Ce(Ph-PDB)3
Chemical name	Ce(BH3Ph2BH3)3
Formula	C72 H96 B12 Ce2 P6
Calculated formula	C72 H96 B12 Ce2 P6
Title of publication	Mechanochemical synthesis and structural analysis of trivalent lanthanide and uranium diphenylphosphinodiboranates.
Authors of publication	Fetrow, Taylor V.; Daly, Scott R.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2021
Journal volume	50
Journal issue	33
Pages of publication	11472 - 11484
a	11.4324 ± 0.0011 Å
b	12.7542 ± 0.0013 Å
c	28.438 ± 0.003 Å
α	94.057 ± 0.005°
β	94.695 ± 0.005°
γ	107.346 ± 0.005°
Cell volume	3924.9 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100.15 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0538
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.0659
Weighted residual factors for all reflections included in the refinement	0.0704
Goodness-of-fit parameter for all reflections included in the refinement	1.038
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
268752 (current)	2021-09-06	cif/ Updating files of 7707952, 7707953, 7707954, 7707955, 7707956, 7707957, 7707958 Original log message: Adding full bibliography for 7707952--7707958.cif.	7707952.cif
267955	2021-08-05	cif/ Adding structures of 7707952, 7707953, 7707954, 7707955, 7707956, 7707957, 7707958 via cif-deposit CGI script.	7707952.cif